#------------------------------------------------------------------------------ #$Date: 2019-01-12 02:26:57 +0200 (Sat, 12 Jan 2019) $ #$Revision: 213013 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/55/04/1550462.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1550462 _cell_angle_alpha 90.000 _cell_angle_beta 92.999 _cell_angle_gamma 90.000 _cell_length_a 13.7016 _cell_length_b 11.3485 _cell_length_c 28.5385 _exptl_crystal_F_000 1920.00 _reflns_d_resolution_high 0.7488 _cod_data_source_file sj4200Isup2.hkl _cod_data_source_block I _shelx_title ' LJYNo1-m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 331.16 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7042.38 7654.89 103.30 o 4 0 0 568.60 538.91 43.11 o 6 0 0 4889.22 5221.95 146.86 o 8 0 0 1.69 -9.66 18.02 o 10 0 0 361.11 430.75 66.66 o 12 0 0 176.14 263.21 62.10 o 14 0 0 40.44 10.21 38.28 o 16 0 0 11.72 27.63 90.94 o 18 0 0 4.08 -49.50 81.73 o 1 1 0 413.48 428.56 16.65 o 2 1 0 5720.47 5720.84 88.78 o 3 1 0 10486.99 10518.48 279.59 o 4 1 0 2194.46 1976.82 52.97 o 5 1 0 2042.43 1824.06 69.26 o 6 1 0 7705.66 7985.47 153.61 o 7 1 0 4023.03 4149.99 100.84 o 8 1 0 586.73 674.13 46.84 o 9 1 0 5937.49 6365.01 141.57 o 10 1 0 3382.89 3421.51 111.21 o 11 1 0 467.84 557.57 57.61 o 12 1 0 730.48 718.61 61.47 o 13 1 0 21.84 39.16 26.41 o 14 1 0 183.36 266.13 53.08 o 15 1 0 33.75 7.40 39.26 o 16 1 0 104.72 150.71 89.36 o 17 1 0 0.14 -35.68 64.30 o 18 1 0 89.15 96.69 117.41 o 0 2 0 2662.34 2441.51 109.36 o 1 2 0 6112.48 6074.79 89.80 o 2 2 0 679.94 693.44 31.23 o 3 2 0 2553.58 2590.96 65.44 o 4 2 0 1495.53 1285.09 52.12 o 5 2 0 1226.04 979.07 42.73 o 6 2 0 3407.67 3324.03 100.30 o 7 2 0 10.77 15.16 13.77 o 8 2 0 893.40 906.77 52.52 o 9 2 0 119.02 107.59 25.94 o 10 2 0 1829.30 1857.44 82.81 o 11 2 0 1666.92 1839.79 87.39 o 12 2 0 608.75 683.52 69.47 o 13 2 0 25.15 -8.66 27.38 o 14 2 0 43.85 28.90 34.56 o 15 2 0 0.76 -2.73 39.14 o 16 2 0 32.89 29.73 44.21 o 17 2 0 5.09 -72.52 90.94 o 18 2 0 0.24 18.42 132.38 o 1 3 0 4757.93 4503.47 177.27 o 2 3 0 3394.60 3468.67 82.77 o 3 3 0 15840.72 16369.66 204.10 o 4 3 0 302.06 332.70 28.65 o 5 3 0 2183.36 2387.78 77.68 o 6 3 0 7916.98 7754.46 279.64 o 7 3 0 202.87 230.16 32.97 o 8 3 0 912.07 877.61 57.74 o 9 3 0 96.94 87.48 27.83 o 10 3 0 111.01 99.58 29.69 o 11 3 0 131.12 181.72 48.74 o 12 3 0 185.24 113.66 43.65 o 13 3 0 952.51 944.65 94.94 o 14 3 0 48.75 12.58 36.95 o 15 3 0 168.03 211.43 62.62 o 16 3 0 58.10 111.26 54.94 o 17 3 0 5.27 49.50 88.64 o 0 4 0 548.88 402.89 67.92 o 1 4 0 381.06 367.59 39.74 o 2 4 0 1092.25 1044.46 53.95 o 3 4 0 6395.99 7116.63 206.98 o 4 4 0 759.49 847.21 49.64 o 5 4 0 2203.37 2660.69 85.05 o 6 4 0 940.70 1063.89 57.43 o 7 4 0 700.30 659.91 46.91 o 8 4 0 169.60 131.39 28.20 o 9 4 0 161.68 155.97 33.12 o 10 4 0 27.72 17.20 30.28 o 11 4 0 357.58 304.19 64.22 o 12 4 0 132.39 84.52 44.61 o 13 4 0 231.21 196.16 56.87 o 14 4 0 34.87 34.98 41.99 o 15 4 0 282.89 279.50 73.43 o 16 4 0 191.72 266.84 82.55 o 17 4 0 33.08 88.00 61.48 o 1 5 0 1804.07 1954.93 92.98 o 2 5 0 192.51 220.05 34.54 o 3 5 0 539.89 516.25 44.79 o 4 5 0 6667.00 7448.83 154.24 o 5 5 0 380.23 417.27 43.35 o 6 5 0 443.30 449.95 45.87 o 7 5 0 1082.38 1110.13 66.48 o 8 5 0 18.50 10.71 24.86 o 9 5 0 11.16 21.28 29.98 o 10 5 0 479.85 506.45 75.35 o 11 5 0 1900.47 2003.44 132.44 o 12 5 0 981.72 789.57 91.30 o 13 5 0 206.19 157.45 55.88 o 14 5 0 47.70 99.87 50.78 o 15 5 0 6.02 24.84 69.84 o 16 5 0 6.48 27.97 73.34 o 17 5 0 59.69 121.99 70.43 o 0 6 0 118.92 117.24 43.93 o 1 6 0 135.52 103.73 33.90 o 2 6 0 300.40 332.93 43.58 o 3 6 0 6353.93 6653.25 161.55 o 4 6 0 1168.36 1007.65 64.16 o 5 6 0 1167.07 1076.30 70.86 o 6 6 0 2595.84 3129.30 211.22 o 7 6 0 110.90 173.71 64.87 o 8 6 0 118.69 166.30 53.35 o 9 6 0 393.76 522.88 87.47 o 10 6 0 70.98 46.52 40.60 o 11 6 0 68.44 67.05 48.11 o 12 6 0 24.54 -16.77 37.65 o 13 6 0 126.70 81.04 53.89 o 14 6 0 49.17 14.84 61.08 o 15 6 0 2.17 63.59 68.27 o 16 6 0 85.19 56.35 77.99 o 1 7 0 15.13 17.38 20.08 o 2 7 0 859.87 831.56 81.17 o 3 7 0 99.39 100.41 31.71 o 4 7 0 2492.26 2482.89 109.34 o 5 7 0 3.07 26.33 24.12 o 6 7 0 209.49 167.03 63.55 o 7 7 0 112.18 121.06 62.17 o 8 7 0 608.23 712.50 119.97 o 9 7 0 132.47 91.99 47.47 o 10 7 0 642.53 765.55 106.64 o 11 7 0 986.03 1031.66 119.26 o 12 7 0 100.68 90.45 51.42 o 13 7 0 83.44 90.75 73.13 o 14 7 0 94.66 51.28 74.39 o 15 7 0 83.68 236.56 98.02 o 16 7 0 29.30 23.80 69.94 o 0 8 0 4559.11 4561.58 216.08 o 1 8 0 633.75 584.56 60.51 o 2 8 0 622.62 585.54 54.34 o 3 8 0 33.60 60.61 26.57 o 4 8 0 32.10 24.63 22.69 o 5 8 0 635.26 652.59 102.09 o 6 8 0 186.90 195.66 73.86 o 7 8 0 59.69 66.55 56.70 o 8 8 0 12.34 80.85 61.72 o 9 8 0 300.00 289.22 79.56 o 10 8 0 143.77 146.01 60.44 o 11 8 0 193.47 221.94 70.46 o 12 8 0 60.02 52.43 70.40 o 13 8 0 88.83 194.31 90.89 o 14 8 0 40.73 6.56 65.43 o 15 8 0 40.53 133.40 151.37 o 1 9 0 1009.50 959.45 80.19 o 2 9 0 83.12 102.25 34.71 o 3 9 0 322.63 350.09 52.57 o 4 9 0 90.99 109.41 59.15 o 5 9 0 390.93 497.98 113.31 o 6 9 0 92.02 97.97 56.54 o 7 9 0 415.75 450.58 113.18 o 8 9 0 215.05 264.62 92.25 o 9 9 0 61.96 99.98 51.91 o 10 9 0 0.59 2.64 43.43 o 11 9 0 140.30 241.70 94.16 o 12 9 0 1.86 25.40 106.48 o 13 9 0 2.51 2.50 65.34 o 14 9 0 6.11 -55.88 55.88 o 0 10 0 128.09 135.71 66.03 o 1 10 0 111.11 141.35 40.15 o 2 10 0 57.44 53.25 32.83 o 3 10 0 201.64 176.61 73.82 o 4 10 0 103.00 69.72 49.82 o 5 10 0 130.03 260.63 83.07 o 6 10 0 306.96 324.57 101.22 o 7 10 0 594.84 634.67 123.61 o 8 10 0 158.36 253.21 92.91 o 9 10 0 51.79 64.71 55.12 o 10 10 0 468.08 681.62 159.94 o 11 10 0 22.58 38.49 66.69 o 12 10 0 14.99 -55.53 55.53 o 13 10 0 0.20 17.98 74.66 o 1 11 0 1.27 -14.99 31.68 o 2 11 0 1200.57 1450.01 160.50 o 3 11 0 0.37 -15.75 43.20 o 4 11 0 81.64 116.66 61.13 o 5 11 0 214.70 244.05 87.91 o 6 11 0 515.97 811.20 133.37 o 7 11 0 1.06 23.58 53.10 o 8 11 0 265.86 394.33 110.26 o 9 11 0 2.71 -21.75 57.17 o 10 11 0 74.38 36.53 66.19 o 11 11 0 178.64 122.07 135.26 o 12 11 0 7.00 12.11 75.23 o 0 12 0 7.14 -37.99 77.12 o 1 12 0 282.05 209.71 83.25 o 2 12 0 41.61 117.49 62.89 o 3 12 0 388.75 627.34 136.32 o 4 12 0 57.29 91.73 65.92 o 5 12 0 271.18 372.35 119.72 o 6 12 0 188.09 264.81 99.41 o 7 12 0 52.75 116.82 83.54 o 8 12 0 236.50 -73.67 73.67 o 9 12 0 0.10 48.17 71.95 o 10 12 0 109.75 -4.73 68.27 o 11 12 0 121.01 149.22 105.33 o 1 13 0 276.69 400.59 164.61 o 2 13 0 45.78 110.74 78.15 o 3 13 0 41.74 6.09 64.46 o 4 13 0 3.39 2.33 57.77 o 5 13 0 255.96 287.56 100.89 o 6 13 0 27.64 17.58 68.49 o 7 13 0 109.71 187.63 122.02 o 8 13 0 7.88 115.11 124.32 o 9 13 0 57.69 20.65 85.36 o 0 14 0 103.26 222.17 125.47 o 1 14 0 83.34 127.24 81.35 o 2 14 0 120.17 117.41 110.51 o 3 14 0 74.65 151.40 86.55 o 4 14 0 68.55 97.58 76.16 o 5 14 0 211.42 319.21 108.66 o 6 14 0 16.18 86.33 142.74 o 1 15 0 66.56 100.96 94.38 o 2 15 0 62.32 47.09 84.23 o -17 0 1 145.08 171.52 131.23 o -15 0 1 3.79 -58.71 58.71 o -13 0 1 893.49 992.21 104.86 o -11 0 1 53.67 49.02 37.75 o -9 0 1 521.32 449.66 58.50 o -7 0 1 65.63 45.13 27.51 o -5 0 1 19578.67 22181.15 270.16 o -3 0 1 308.97 216.33 27.60 o -1 0 1 9354.83 7399.37 138.13 o 1 0 1 3235.88 1056.96 1051.69 o 3 0 1 27338.48 29115.26 362.24 o 5 0 1 12168.45 12773.41 210.55 o 7 0 1 7939.07 8369.97 203.21 o 9 0 1 5.75 -17.96 21.32 o 11 0 1 877.63 1002.79 96.91 o 13 0 1 352.72 387.81 81.52 o 15 0 1 283.31 388.22 112.47 o 17 0 1 24.37 145.04 116.26 o -18 1 1 18.84 -40.26 64.57 o -17 1 1 2.43 -39.62 67.79 o -16 1 1 22.26 149.73 81.44 o -15 1 1 0.54 44.95 47.26 o -14 1 1 115.65 28.60 40.88 o -13 1 1 241.25 349.20 59.11 o -12 1 1 335.56 377.96 53.11 o -11 1 1 87.63 95.05 31.77 o -10 1 1 610.38 583.27 50.68 o -9 1 1 1041.91 1041.78 59.62 o -8 1 1 3943.75 3932.51 104.10 o -7 1 1 132.59 127.64 23.59 o -6 1 1 1.42 7.31 11.42 o -5 1 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241.13 58.97 o -9 5 1 738.66 655.55 78.75 o -8 5 1 1177.73 1068.96 87.39 o -7 5 1 6.85 -6.71 24.23 o -6 5 1 3413.01 3390.98 157.64 o -5 5 1 444.00 446.85 38.15 o -4 5 1 6960.49 7355.77 155.06 o -3 5 1 992.47 908.68 55.59 o -2 5 1 3968.99 4178.82 157.75 o -1 5 1 529.76 461.60 47.27 o 0 5 1 1376.33 1528.42 80.79 o 1 5 1 87.38 66.61 26.23 o 2 5 1 738.51 606.37 48.50 o 3 5 1 1470.93 1381.38 70.34 o 4 5 1 2251.20 2311.18 98.47 o 5 5 1 4222.35 4701.85 138.69 o 6 5 1 10.59 -9.29 16.97 o 7 5 1 201.85 248.33 37.52 o 8 5 1 1.17 -7.87 17.66 o 9 5 1 35.87 63.19 33.25 o 10 5 1 237.59 181.12 49.76 o 11 5 1 335.85 335.52 70.17 o 12 5 1 130.83 75.13 39.59 o 13 5 1 168.60 146.27 54.38 o 14 5 1 0.02 44.58 49.38 o 15 5 1 37.74 112.84 62.63 o 16 5 1 204.61 211.63 79.48 o 17 5 1 3.62 64.61 65.04 o -16 6 1 34.69 74.36 58.95 o -15 6 1 73.52 133.86 67.30 o -14 6 1 89.96 109.60 57.14 o -13 6 1 86.13 76.51 47.19 o -12 6 1 69.13 98.79 47.82 o -11 6 1 176.22 237.36 60.99 o -10 6 1 32.69 42.18 36.13 o -9 6 1 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