#------------------------------------------------------------------------------ #$Date: 2025-02-07 03:14:43 +0200 (Fri, 07 Feb 2025) $ #$Revision: 297626 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/38/1573862.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573862 loop_ _publ_author_name 'Meher, Niranjan' 'Khatun, Mst Nasima' 'Parui, Retwik' 'Iyer, Parameswar K.' _publ_section_title ; Non-Conjugated Alkyl Chains Engineering to Tune Condensed State Photophysical and Supramolecular Assembly Properties ; _journal_name_full Nanoscale _journal_paper_doi 10.1039/D5NR00163C _journal_year 2025 _chemical_formula_sum 'C16 H15 N O2' _chemical_formula_weight 253.29 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2016/6 _audit_update_record ; 2024-07-30 deposited with the CCDC. 2025-02-06 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 4.7154(10) _cell_length_b 12.531(3) _cell_length_c 22.215(4) _cell_measurement_reflns_used 4650 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 19.59 _cell_measurement_theta_min 2.45 _cell_volume 1312.7(5) _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0876 _diffrn_reflns_av_unetI/netI 0.0409 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 5 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 42762 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 24.990 _diffrn_reflns_theta_max 24.990 _diffrn_reflns_theta_min 1.833 _exptl_absorpt_coefficient_mu 0.085 _exptl_crystal_colour Colourless _exptl_crystal_density_diffrn 1.282 _exptl_crystal_description Block _exptl_crystal_F_000 536 _refine_diff_density_max 0.118 _refine_diff_density_min -0.149 _refine_diff_density_rms 0.034 _refine_ls_abs_structure_details ; Flack x determined using 594 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -2.1(10) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 173 _refine_ls_number_reflns 2319 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.045 _refine_ls_R_factor_all 0.0647 _refine_ls_R_factor_gt 0.0471 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0500P)^2^+0.2779P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1090 _refine_ls_wR_factor_ref 0.1213 _reflns_Friedel_coverage 0.666 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 1.000 _reflns_number_gt 1805 _reflns_number_total 2319 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d5nr00163c2.cif _cod_data_source_block NC-4_0m_a _cod_database_code 1573862 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL NC-4_0m_a.res in P2(1)2(1)2(1) NC-4_0m_a.res created by SHELXL-2016/6 at 15:52:15 on 05-Jul-2019 CELL 0.71073 4.7154 12.5315 22.2151 90.000 90.000 90.000 ZERR 4.000 0.0010 0.0025 0.0043 0.000 0.000 0.000 LATT -1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H N O UNIT 64 60 4 8 OMIT -3 50 REM Old TITL NC-4_0m in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.167, Rweak 0.038, Alpha 0.005, Orientation as input REM Flack x= -1.937 ( 1.145 ) from Parsons' quotients REM Formula found by SHELXT: C16 N O2 L.S. 20 ACTA BOND $H FMAP 2 PLAN 4 TEMP 23.000 WGHT 0.050000 0.277900 FVAR 0.73891 O001 4 0.628260 0.522001 0.476614 11.00000 0.08814 0.07449 = 0.05835 0.00381 -0.01547 0.00885 N002 3 0.304709 0.500479 0.402702 11.00000 0.05484 0.04056 = 0.05388 0.00214 0.00561 -0.00065 O003 4 -0.013942 0.476614 0.328091 11.00000 0.08060 0.05710 = 0.09749 -0.00476 -0.02275 -0.01145 C004 1 0.515544 0.557679 0.431399 11.00000 0.05107 0.05239 = 0.04713 -0.00718 0.00244 0.00724 C005 1 0.595298 0.661373 0.405726 11.00000 0.05081 0.04369 = 0.05304 -0.01015 0.00506 0.00125 C006 1 0.263964 0.633625 0.322727 11.00000 0.05619 0.04683 = 0.04705 -0.00104 0.00312 0.00914 C007 1 0.469310 0.696595 0.351521 11.00000 0.05278 0.04086 = 0.05251 -0.00312 0.01462 0.00596 C008 1 0.171134 0.531791 0.349549 11.00000 0.05222 0.04116 = 0.06516 -0.00689 0.00162 0.00259 C009 1 0.215488 0.398189 0.429249 11.00000 0.06697 0.04563 = 0.07243 0.00881 0.01331 0.00048 AFIX 23 H00A 2 0.011928 0.390494 0.424690 11.00000 -1.20000 H00B 2 0.257837 0.398692 0.471977 11.00000 -1.20000 AFIX 0 C00A 1 0.360978 0.303877 0.400364 11.00000 0.06330 0.04423 = 0.07289 0.00246 0.00526 0.00109 AFIX 23 H00C 2 0.563228 0.308469 0.407904 11.00000 -1.20000 H00D 2 0.332181 0.306844 0.357162 11.00000 -1.20000 AFIX 0 C00B 1 0.547976 0.796167 0.326835 11.00000 0.06915 0.04274 = 0.07756 0.00188 0.02433 0.00648 C00C 1 0.142553 0.667749 0.269649 11.00000 0.07619 0.07082 = 0.05892 0.00048 -0.00594 0.01511 AFIX 43 H00E 2 0.008788 0.625455 0.250228 11.00000 -1.20000 AFIX 0 C00D 1 0.792504 0.724405 0.433794 11.00000 0.06643 0.06809 = 0.06990 -0.02045 0.00449 -0.00825 AFIX 43 H00F 2 0.876107 0.701156 0.469370 11.00000 -1.20000 AFIX 0 C00E 1 0.416381 0.827971 0.272318 11.00000 0.09369 0.06050 = 0.08598 0.02555 0.03062 0.01752 AFIX 43 H00G 2 0.466050 0.892911 0.255012 11.00000 -1.20000 AFIX 0 C00F 1 0.251771 0.198222 0.423844 11.00000 0.07894 0.04958 = 0.09075 0.00900 0.00926 -0.00594 AFIX 23 H00H 2 0.289163 0.194144 0.466719 11.00000 -1.20000 H00I 2 0.047865 0.195617 0.418266 11.00000 -1.20000 AFIX 0 C00G 1 0.752044 0.857461 0.357619 11.00000 0.07979 0.04431 = 0.11437 -0.00833 0.03171 -0.01007 AFIX 43 H00J 2 0.807585 0.923013 0.341928 11.00000 -1.20000 AFIX 0 C00H 1 0.221328 0.766321 0.245072 11.00000 0.09727 0.08868 = 0.06808 0.02538 0.00631 0.02836 AFIX 43 H00K 2 0.137716 0.789433 0.209469 11.00000 -1.20000 AFIX 0 C00I 1 0.868920 0.822369 0.409825 11.00000 0.07341 0.06824 = 0.10559 -0.03328 0.01372 -0.01845 AFIX 43 H00L 2 1.001588 0.864480 0.429706 11.00000 -1.20000 AFIX 0 C00J 1 0.382726 0.102729 0.393538 11.00000 0.11924 0.04775 = 0.11586 -0.00156 0.00925 -0.00139 AFIX 137 H00M 2 0.342773 0.105086 0.351185 11.00000 -1.50000 H00N 2 0.304679 0.038613 0.410417 11.00000 -1.50000 H00O 2 0.584230 0.103596 0.399686 11.00000 -1.50000 AFIX 0 HKLF 4 REM NC-4_0m_a.res in P2(1)2(1)2(1) REM R1 = 0.0471 for 1805 Fo > 4sig(Fo) and 0.0647 for all 2319 data REM 173 parameters refined using 0 restraints END WGHT 0.0432 0.2947 REM Highest difference peak 0.118, deepest hole -0.149, 1-sigma level 0.034 Q1 1 -0.3460 0.4852 0.3151 11.00000 0.05 0.12 Q2 1 0.6615 0.4737 0.4038 11.00000 0.05 0.11 Q3 1 1.1085 0.5757 0.4752 11.00000 0.05 0.11 Q4 1 -0.0774 0.3640 0.3444 11.00000 0.05 0.10 ; _shelx_res_checksum 30313 _shelx_hkl_file ; -1 0 0 3.40 1.10 -1 0 0 0.00 0.80 1 0 0 -0.80 0.80 1 0 0 0.30 1.00 1 0 0 -0.80 0.70 1 0 0 11.50 2.00 1 0 0 -0.70 0.80 1 0 0 0.40 0.60 1 0 0 0.20 0.80 1 0 0 -0.30 0.60 -1 0 0 0.00 0.80 2 0 0 233.78 33.90 -2 0 0 274.27 33.60 2 0 0 263.87 34.10 2 0 0 272.37 34.20 2 0 0 276.47 34.00 2 0 0 241.68 33.30 -2 0 0 268.87 33.80 2 0 0 231.78 33.50 2 0 0 272.27 34.10 -2 0 0 278.47 34.10 -2 0 0 250.37 33.80 2 0 0 265.17 34.30 -3 0 0 0.10 2.50 -3 0 0 -3.20 1.80 3 0 0 -3.40 2.00 3 0 0 1.00 1.50 3 0 0 1.00 1.60 3 0 0 4.80 3.10 3 0 0 3.30 2.60 3 0 0 1.30 2.40 -3 0 0 -2.70 2.00 3 0 0 2.20 3.20 -3 0 0 -3.20 1.70 -4 0 0 19.10 6.20 4 0 0 17.00 6.20 4 0 0 32.70 7.70 -4 0 0 16.00 4.90 -4 0 0 21.80 5.80 4 0 0 23.70 6.90 -4 0 0 31.60 6.30 -4 0 0 21.60 6.10 4 0 0 34.20 7.80 4 0 0 13.80 6.50 -5 0 0 -6.00 3.60 5 0 0 -7.50 4.10 5 0 0 -3.60 5.80 5 0 0 3.40 5.00 -5 0 0 5.10 4.40 -5 0 0 -0.50 3.80 -5 0 0 0.60 4.70 5 0 0 -10.90 5.00 5 0 0 4.20 5.00 6 0 0 -6.60 5.70 6 0 0 -7.00 5.80 -6 0 0 -5.10 4.90 -6 0 0 1.40 5.30 6 0 0 -6.80 6.90 6 0 0 -1.20 8.20 0 -1 0 0.40 0.40 0 -1 0 1.60 0.30 0 -1 0 1.30 0.50 0 1 0 0.90 0.30 0 1 0 0.40 0.30 0 1 0 2.00 0.50 -1 -1 0 946.61 117.09 1 -1 0 998.70 117.19 1 -1 0 971.30 117.29 1 -1 0 1033.70 117.19 1 -1 0 1007.40 117.39 1 -1 0 1018.00 117.29 1 -1 0 928.41 117.09 -1 -1 0 954.70 117.19 -1 -1 0 865.71 117.19 -1 1 0 886.41 117.09 1 1 0 860.91 117.29 1 1 0 891.41 117.09 1 1 0 909.61 117.19 -1 1 0 885.11 117.09 1 1 0 804.12 117.39 1 1 0 788.32 117.09 -1 1 0 936.71 117.09 1 1 0 811.12 116.89 1 1 0 888.01 117.19 1 1 0 998.60 117.39 -1 1 0 962.70 117.09 2 -1 0 132.79 16.80 2 -1 0 115.29 16.60 -2 -1 0 120.39 16.50 2 -1 0 117.19 16.20 2 -1 0 110.69 15.90 2 -1 0 134.29 16.60 2 -1 0 134.29 16.70 -2 -1 0 121.69 16.40 2 -1 0 129.79 16.50 -2 -1 0 134.99 16.20 2 1 0 106.19 16.40 2 1 0 121.29 16.60 -2 1 0 116.99 16.30 2 1 0 103.09 16.60 2 1 0 134.89 16.90 2 1 0 134.79 16.60 2 1 0 108.29 15.80 2 1 0 130.89 16.50 -2 1 0 112.39 16.20 -2 1 0 124.99 16.30 -2 1 0 113.19 16.40 2 1 0 124.09 17.10 -2 1 0 125.09 15.90 -3 -1 0 309.67 40.70 -3 -1 0 312.57 40.40 -3 -1 0 309.57 40.40 -3 -1 0 350.56 40.20 3 -1 0 298.87 39.70 3 -1 0 288.27 40.80 3 -1 0 288.67 40.00 3 -1 0 360.86 41.20 3 -1 0 308.67 40.60 3 -1 0 314.77 41.10 3 -1 0 362.06 40.90 3 1 0 317.57 41.50 3 1 0 307.47 40.80 3 1 0 283.07 40.60 3 1 0 311.77 41.10 3 1 0 303.67 40.70 -3 1 0 295.47 39.70 -3 1 0 290.47 40.30 -3 1 0 304.37 40.30 3 1 0 301.57 41.10 -3 1 0 293.87 40.20 -3 1 0 313.97 40.60 3 1 0 272.57 39.60 -4 -1 0 -1.70 3.20 4 -1 0 7.70 5.00 -4 -1 0 2.00 2.90 4 -1 0 -2.20 3.50 4 -1 0 4.50 4.40 4 -1 0 3.00 4.40 -4 -1 0 5.40 3.60 -4 -1 0 2.10 3.00 4 -1 0 7.00 4.70 4 1 0 4.00 3.70 4 1 0 -0.60 3.00 -4 1 0 2.50 2.90 4 1 0 2.50 3.70 -4 1 0 3.30 3.50 -4 1 0 -1.50 3.00 4 1 0 4.60 4.00 4 1 0 1.10 4.70 -4 1 0 5.50 3.50 5 -1 0 9.40 6.10 -5 -1 0 -2.90 4.00 -5 -1 0 0.60 3.70 -5 -1 0 0.70 4.70 5 -1 0 -8.60 4.60 -5 -1 0 6.40 4.30 5 -1 0 -2.30 5.80 5 -1 0 -3.30 5.40 5 -1 0 -2.10 5.70 -5 1 0 -1.70 3.40 5 1 0 5.90 5.50 5 1 0 -5.30 5.60 5 1 0 -11.80 4.20 5 1 0 -4.30 4.80 -5 1 0 4.90 4.30 5 1 0 1.00 5.20 -5 1 0 -3.50 3.60 -5 1 0 4.70 5.00 -6 -1 0 7.20 5.70 6 -1 0 13.00 8.40 6 -1 0 -12.70 6.20 -6 -1 0 -2.00 4.60 6 -1 0 5.30 7.40 6 -1 0 6.40 8.50 -6 1 0 4.20 5.90 6 1 0 14.20 8.20 -6 1 0 11.10 5.40 6 1 0 22.70 8.50 -6 1 0 -4.30 5.60 6 1 0 -5.70 6.50 6 1 0 -4.80 7.00 0 -2 0 701.63 88.59 0 2 0 732.13 88.59 0 2 0 656.13 88.39 1 -2 0 484.85 60.39 -1 -2 0 519.65 60.69 -1 -2 0 458.45 60.49 -1 -2 0 485.95 60.19 1 -2 0 481.65 60.49 1 -2 0 480.05 60.69 1 -2 0 516.65 60.49 1 -2 0 494.85 60.39 1 -2 0 474.85 60.49 -1 -2 0 447.86 60.39 1 2 0 523.05 60.89 -1 2 0 478.25 60.29 1 2 0 479.95 60.59 1 2 0 483.65 60.59 1 2 0 454.25 60.39 1 2 0 482.25 60.19 1 2 0 430.06 60.59 1 2 0 402.46 60.69 1 2 0 432.66 60.39 -1 2 0 479.35 60.39 1 2 0 491.75 60.59 -1 2 0 474.05 60.39 -1 2 0 448.96 60.29 -1 2 0 437.06 60.29 2 -2 0 84.49 11.70 -2 -2 0 90.09 10.80 -2 -2 0 73.69 11.40 -2 -2 0 81.09 11.70 -2 -2 0 73.89 10.80 2 -2 0 83.99 12.40 2 -2 0 96.39 11.60 2 -2 0 85.69 11.50 2 -2 0 90.29 11.40 2 -2 0 99.49 11.80 2 -2 0 81.19 11.10 -2 -2 0 82.49 11.20 2 2 0 71.79 11.90 2 2 0 90.69 12.50 -2 2 0 65.69 11.10 2 2 0 88.99 12.80 -2 2 0 79.49 10.80 2 2 0 100.39 13.30 2 2 0 67.79 12.30 2 2 0 83.39 11.70 -2 2 0 72.99 11.20 2 2 0 73.89 10.70 2 2 0 77.59 11.90 2 2 0 76.79 10.90 -2 2 0 86.29 11.50 2 2 0 79.09 11.40 -2 2 0 85.39 11.20 -3 -2 0 13.00 4.10 -3 -2 0 13.80 3.80 3 -2 0 15.50 4.90 3 -2 0 9.40 3.40 3 -2 0 7.60 3.80 3 -2 0 8.30 3.30 -3 -2 0 5.00 3.40 3 -2 0 5.00 2.40 3 -2 0 6.60 3.70 3 -2 0 20.00 5.20 -3 2 0 10.90 3.70 3 2 0 7.40 3.50 -3 2 0 5.50 2.60 3 2 0 20.60 5.30 3 2 0 8.80 4.30 -3 2 0 11.80 3.60 -3 2 0 10.20 3.60 3 2 0 12.90 3.90 3 2 0 9.10 3.90 -3 2 0 12.80 3.50 3 2 0 5.20 2.10 3 2 0 9.60 4.10 3 2 0 9.50 3.90 4 -2 0 -2.60 3.00 4 -2 0 5.60 4.50 -4 -2 0 -2.60 3.00 4 -2 0 8.80 5.20 4 -2 0 -3.60 3.30 -4 -2 0 -1.80 3.20 -4 -2 0 4.80 3.40 4 -2 0 -1.50 4.10 -4 -2 0 -1.40 2.70 4 2 0 2.80 5.20 -4 2 0 -1.10 2.30 4 2 0 -5.70 4.10 4 2 0 0.60 3.70 4 2 0 9.80 5.30 -4 2 0 2.80 3.00 -4 2 0 6.70 4.20 4 2 0 -1.20 4.20 4 2 0 -0.20 3.40 -4 2 0 5.90 3.30 4 2 0 -1.70 4.10 -5 -2 0 5.70 4.00 5 -2 0 0.00 5.60 -5 -2 0 0.70 4.40 5 -2 0 1.20 6.10 5 -2 0 -4.10 4.90 -5 -2 0 -0.70 4.30 5 -2 0 2.40 5.90 5 -2 0 -1.50 5.30 -5 -2 0 0.10 3.90 5 2 0 -2.20 4.80 -5 2 0 -3.50 3.80 -5 2 0 0.60 3.70 5 2 0 0.30 7.20 5 2 0 0.10 5.20 -5 2 0 6.90 4.20 -5 2 0 -0.30 4.30 5 2 0 1.00 6.00 5 2 0 0.90 5.00 -5 2 0 -3.30 3.10 -6 -2 0 7.40 5.90 6 -2 0 6.70 6.90 6 -2 0 11.10 7.20 -6 -2 0 7.70 6.50 6 -2 0 12.40 9.80 6 -2 0 15.20 9.10 6 2 0 11.60 7.70 -6 2 0 6.90 5.40 -6 2 0 15.70 5.80 -6 2 0 9.30 7.00 6 2 0 -11.20 7.10 6 2 0 -7.10 8.10 6 2 0 7.60 7.30 0 -3 0 0.00 0.60 0 -3 0 1.20 0.90 0 -3 0 0.80 0.80 0 3 0 0.00 0.60 0 3 0 -0.50 0.70 0 3 0 0.40 0.90 0 3 0 0.60 0.70 0 3 0 1.10 0.60 1 -3 0 56.39 8.50 1 -3 0 54.69 8.10 1 -3 0 49.50 8.60 1 -3 0 64.99 8.30 1 -3 0 66.79 8.20 1 -3 0 74.79 8.40 -1 -3 0 63.89 8.40 -1 -3 0 63.39 8.10 1 -3 0 64.99 8.60 -1 -3 0 51.89 8.30 -1 3 0 62.59 8.20 1 3 0 66.79 8.90 -1 3 0 59.69 8.10 1 3 0 53.49 8.40 -1 3 0 62.39 8.10 1 3 0 53.89 8.40 1 3 0 60.79 8.60 -1 3 0 57.59 8.30 1 3 0 58.09 9.30 1 3 0 56.39 8.20 1 3 0 58.49 8.30 -1 3 0 62.29 8.20 -2 -3 0 67.79 10.00 2 -3 0 73.39 11.90 -2 -3 0 78.09 11.10 2 -3 0 64.49 10.10 2 -3 0 76.19 11.20 -2 -3 0 86.09 10.40 2 -3 0 91.29 12.20 2 -3 0 83.79 11.00 -2 -3 0 73.59 10.70 2 -3 0 80.59 11.70 2 -3 0 85.99 11.80 2 -3 0 63.69 11.10 -2 -3 0 87.59 11.10 -2 3 0 90.09 11.00 2 3 0 84.89 12.10 2 3 0 65.89 11.50 2 3 0 81.89 10.90 -2 3 0 82.19 10.10 2 3 0 73.09 11.60 2 3 0 71.19 10.00 2 3 0 68.69 11.10 -2 3 0 85.29 10.60 2 3 0 88.99 12.80 -2 3 0 71.09 10.60 2 3 0 64.89 12.10 2 3 0 76.49 12.10 -2 3 0 71.59 10.50 -2 3 0 70.79 10.60 3 -3 0 42.70 7.40 -3 -3 0 40.30 7.00 3 -3 0 52.09 8.20 -3 -3 0 27.80 6.70 3 -3 0 46.20 7.60 3 -3 0 33.80 7.50 3 -3 0 39.60 6.60 -3 -3 0 36.80 7.40 3 -3 0 37.10 7.10 3 -3 0 22.00 6.50 3 3 0 24.30 6.30 3 3 0 53.19 8.00 3 3 0 27.70 6.90 3 3 0 52.79 9.30 -3 3 0 30.90 6.20 3 3 0 29.90 6.50 3 3 0 39.70 7.70 -3 3 0 31.80 6.60 3 3 0 22.90 7.50 -3 3 0 32.80 6.20 -3 3 0 36.20 5.60 -3 3 0 37.00 6.60 -3 3 0 30.40 6.50 3 3 0 28.50 6.90 -4 -3 0 -1.30 3.20 -4 -3 0 -1.00 3.00 4 -3 0 4.50 5.00 -4 -3 0 7.30 3.70 4 -3 0 0.70 4.70 4 -3 0 3.70 3.20 -4 -3 0 0.20 3.00 4 -3 0 1.70 4.20 4 -3 0 -1.00 4.30 4 -3 0 3.10 4.20 -4 3 0 2.50 3.60 4 3 0 -1.80 4.50 4 3 0 0.10 3.70 4 3 0 -1.10 3.90 -4 3 0 -2.00 3.70 -4 3 0 2.30 3.10 4 3 0 4.20 3.70 4 3 0 1.70 4.60 -4 3 0 3.40 3.00 -4 3 0 3.00 3.40 4 3 0 2.60 4.30 4 3 0 6.20 5.00 5 -3 0 4.00 5.90 5 -3 0 -1.70 4.70 -5 -3 0 3.80 4.10 -5 -3 0 -6.10 4.00 5 -3 0 -3.90 6.20 -5 -3 0 4.30 4.40 5 -3 0 1.50 6.90 5 -3 0 -4.60 4.60 -5 -3 0 1.00 4.30 5 3 0 -8.30 5.30 -5 3 0 7.90 4.60 5 3 0 -1.30 5.20 -5 3 0 -4.60 3.80 5 3 0 1.70 6.30 -5 3 0 -0.70 3.50 5 3 0 10.20 6.10 -5 3 0 -3.60 3.80 5 3 0 -3.20 4.90 -5 3 0 -3.60 3.70 6 -3 0 6.00 7.40 6 -3 0 0.90 6.60 -6 -3 0 -10.80 4.40 6 -3 0 0.40 7.50 -6 -3 0 3.20 5.80 6 -3 0 2.50 7.80 -6 3 0 3.30 5.80 6 3 0 4.00 6.20 6 3 0 -9.30 6.00 6 3 0 1.20 7.00 -6 3 0 4.10 5.40 0 -4 0 225.98 27.40 0 -4 0 218.88 27.40 0 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3.80 -2 4 0 14.20 3.10 2 4 0 3.30 3.30 -2 4 0 20.10 2.90 -2 4 0 18.10 3.30 -2 4 0 16.30 3.50 -2 4 0 14.10 3.20 -3 -4 0 -0.10 2.60 3 -4 0 0.10 2.60 3 -4 0 0.10 2.40 3 -4 0 -1.80 2.30 3 -4 0 1.40 3.30 -3 -4 0 1.20 2.80 3 -4 0 -3.00 2.50 -3 -4 0 -0.10 2.40 -3 -4 0 -1.50 1.90 3 -4 0 1.70 2.80 3 -4 0 -0.70 2.30 3 4 0 2.60 3.30 3 4 0 2.40 2.80 3 4 0 -1.50 2.40 -3 4 0 0.60 2.50 -3 4 0 2.00 2.40 -3 4 0 2.30 2.40 -3 4 0 1.30 2.00 -3 4 0 2.40 2.50 3 4 0 -1.60 2.50 3 4 0 4.50 3.60 3 4 0 2.10 2.90 3 4 0 -1.90 2.30 3 4 0 -1.70 3.30 4 -4 0 -1.30 4.00 4 -4 0 1.20 4.30 -4 -4 0 5.10 3.80 4 -4 0 4.10 4.50 -4 -4 0 -2.80 3.30 4 -4 0 1.20 4.90 4 -4 0 0.00 4.10 -4 -4 0 6.00 4.00 4 -4 0 3.90 4.00 4 4 0 -0.30 3.10 4 4 0 2.10 5.40 -4 4 0 -0.90 2.80 -4 4 0 -4.10 2.70 4 4 0 -5.60 3.50 4 4 0 0.00 3.60 4 4 0 4.00 4.80 -4 4 0 -1.10 3.10 4 4 0 2.70 4.00 -4 4 0 -1.10 3.10 -4 4 0 1.40 3.10 4 4 0 0.80 4.70 5 -4 0 4.70 6.50 -5 -4 0 2.10 4.60 -5 -4 0 0.30 4.40 5 -4 0 -3.20 6.00 -5 -4 0 1.30 3.80 -5 -4 0 0.90 4.60 5 -4 0 -1.00 6.20 5 -4 0 16.60 6.90 5 -4 0 -7.00 5.00 5 4 0 10.30 6.70 -5 4 0 2.20 4.40 -5 4 0 2.40 4.80 5 4 0 -3.00 5.10 5 4 0 5.20 6.80 5 4 0 13.20 8.90 -5 4 0 4.00 5.10 5 4 0 -0.90 5.30 5 4 0 4.90 6.00 -5 4 0 7.50 5.50 -5 4 0 -3.60 3.80 6 -4 0 21.10 9.20 -6 -4 0 18.20 6.90 6 -4 0 9.80 8.70 6 -4 0 8.90 9.40 -6 -4 0 12.10 6.80 6 4 0 8.90 8.20 6 4 0 8.40 8.90 -6 4 0 14.30 7.20 -6 4 0 7.50 5.80 6 4 0 10.70 7.40 0 -5 0 -0.40 1.30 0 -5 0 -0.80 1.00 0 -5 0 -2.20 0.90 0 5 0 2.60 0.80 0 5 0 1.90 1.70 0 5 0 2.80 0.80 0 5 0 -0.50 1.00 0 5 0 -0.80 1.00 1 -5 0 71.89 11.60 1 -5 0 83.19 12.10 1 -5 0 85.19 12.50 -1 -5 0 90.19 11.80 1 -5 0 87.09 11.90 -1 -5 0 75.59 11.70 1 -5 0 75.79 11.40 -1 -5 0 91.99 11.60 -1 -5 0 92.09 11.60 1 5 0 86.49 12.80 -1 5 0 103.49 11.60 1 5 0 87.19 11.40 -1 5 0 81.79 11.60 -1 5 0 87.09 11.40 1 5 0 87.79 11.70 1 5 0 72.89 11.80 -1 5 0 90.89 11.50 1 5 0 86.99 13.10 1 5 0 82.79 11.80 1 5 0 83.19 13.00 -1 5 0 89.89 11.60 -1 5 0 78.89 11.30 -2 -5 0 66.19 8.80 -2 -5 0 56.79 10.30 -2 -5 0 61.79 8.90 2 -5 0 62.79 10.80 2 -5 0 68.99 10.20 2 -5 0 82.99 10.70 -2 -5 0 80.39 10.80 2 -5 0 59.49 10.60 -2 -5 0 64.49 10.50 2 -5 0 60.99 9.80 2 -5 0 75.39 10.60 2 -5 0 66.89 9.20 -2 -5 0 83.49 10.40 2 5 0 74.69 10.90 2 5 0 69.79 10.60 2 5 0 64.49 10.90 -2 5 0 64.49 8.90 -2 5 0 69.99 9.90 2 5 0 45.50 9.10 -2 5 0 70.99 10.10 2 5 0 66.09 11.00 2 5 0 42.10 9.30 2 5 0 51.39 10.60 -2 5 0 67.89 9.70 2 5 0 80.59 12.00 -2 5 0 70.79 9.20 -2 5 0 62.69 9.20 3 -5 0 139.39 18.80 -3 -5 0 134.09 17.90 3 -5 0 125.39 20.10 -3 -5 0 133.99 18.90 -3 -5 0 131.09 18.40 3 -5 0 171.68 20.80 3 -5 0 139.69 18.50 -3 -5 0 139.49 18.90 3 -5 0 136.29 18.60 3 5 0 126.19 21.10 3 5 0 102.09 19.10 3 5 0 127.09 20.30 3 5 0 93.29 20.00 -3 5 0 137.89 18.00 -3 5 0 155.58 18.80 -3 5 0 121.49 18.10 3 5 0 122.09 20.20 3 5 0 112.89 20.00 3 5 0 100.09 18.40 -3 5 0 126.49 18.30 -3 5 0 151.78 18.30 -4 -5 0 7.00 4.70 4 -5 0 5.20 5.40 4 -5 0 -0.80 4.10 4 -5 0 9.60 5.00 -4 -5 0 1.90 3.50 4 -5 0 5.80 4.40 -4 -5 0 -4.90 2.60 4 -5 0 -2.70 4.40 4 -5 0 11.40 5.00 -4 5 0 0.40 3.80 -4 5 0 6.00 3.80 -4 5 0 5.00 3.80 -4 5 0 4.80 3.00 4 5 0 -0.40 4.10 4 5 0 -4.10 3.60 4 5 0 -2.70 4.00 4 5 0 -0.10 4.40 4 5 0 -5.40 4.70 -4 5 0 3.10 3.60 4 5 0 -5.60 4.50 -5 -5 0 13.50 5.00 -5 -5 0 14.80 5.80 -5 -5 0 -5.40 4.70 5 -5 0 -0.10 5.70 5 -5 0 7.30 6.40 5 -5 0 -1.80 6.60 -5 -5 0 14.60 5.80 5 -5 0 12.90 7.50 5 5 0 2.10 7.60 -5 5 0 4.60 4.70 5 5 0 0.00 6.70 5 5 0 1.70 5.70 5 5 0 4.90 5.50 5 5 0 19.70 8.40 -5 5 0 4.40 4.20 5 5 0 0.20 5.30 -5 5 0 18.00 6.10 -5 5 0 8.30 5.40 -5 5 0 11.70 4.60 0 -6 0 2108.19 257.47 0 -6 0 2074.39 257.27 0 -6 0 1946.51 257.27 0 6 0 2064.39 256.87 0 6 0 2122.39 257.37 0 6 0 1808.82 257.27 0 6 0 2149.08 257.47 0 6 0 1878.01 257.07 0 6 0 2050.69 256.87 -1 -6 0 5.70 2.60 -1 -6 0 6.50 2.30 -1 -6 0 3.90 2.00 1 -6 0 3.90 2.40 1 -6 0 16.00 3.80 1 -6 0 8.70 2.90 -1 -6 0 6.30 2.40 1 -6 0 6.60 1.90 1 -6 0 3.70 2.20 -1 6 0 8.40 1.90 1 6 0 7.30 2.50 1 6 0 4.20 2.80 1 6 0 4.50 1.70 -1 6 0 5.40 2.20 -1 6 0 5.20 2.30 -1 6 0 7.80 1.90 1 6 0 9.10 2.30 -1 6 0 9.70 2.40 1 6 0 5.50 2.70 -1 6 0 8.90 2.20 -1 6 0 2.80 1.50 1 6 0 5.30 3.00 1 6 0 6.80 2.50 2 -6 0 5.50 3.00 2 -6 0 2.50 2.20 -2 -6 0 0.30 2.40 -2 -6 0 9.00 2.30 -2 -6 0 8.10 2.40 2 -6 0 8.10 2.80 2 -6 0 5.30 2.70 -2 -6 0 2.90 2.80 2 -6 0 9.80 2.90 2 -6 0 9.70 3.60 2 -6 0 4.50 2.50 -2 -6 0 0.50 2.20 -2 6 0 5.60 2.40 2 6 0 6.90 3.40 -2 6 0 14.20 3.20 2 6 0 2.70 2.50 2 6 0 9.30 4.10 -2 6 0 6.00 2.20 -2 6 0 14.10 2.80 2 6 0 6.50 3.20 2 6 0 4.00 2.30 2 6 0 1.40 2.50 2 6 0 4.90 3.10 -2 6 0 6.40 2.50 -2 6 0 9.90 2.50 -3 -6 0 174.58 23.80 3 -6 0 174.08 24.40 3 -6 0 180.68 24.40 3 -6 0 199.58 27.00 -3 -6 0 165.38 24.20 3 -6 0 173.58 24.90 -3 -6 0 156.98 24.40 -3 -6 0 202.18 25.10 3 -6 0 160.68 24.20 -3 6 0 196.08 24.40 3 6 0 173.78 25.50 -3 6 0 197.48 24.20 -3 6 0 177.68 23.70 -3 6 0 168.98 23.80 3 6 0 158.18 24.40 3 6 0 171.48 26.50 3 6 0 186.48 25.10 3 6 0 173.28 26.60 -3 6 0 174.18 23.90 3 6 0 143.09 26.50 -4 -6 0 23.70 6.40 -4 -6 0 25.60 6.20 4 -6 0 38.10 7.80 4 -6 0 27.20 7.80 4 -6 0 10.80 6.10 4 -6 0 14.60 7.10 -4 -6 0 23.40 7.60 4 -6 0 31.10 8.50 4 -6 0 32.50 7.30 -4 6 0 24.30 6.20 4 6 0 10.20 5.90 -4 6 0 29.10 6.10 4 6 0 19.80 7.40 4 6 0 10.10 5.40 -4 6 0 18.20 6.20 4 6 0 19.40 7.10 4 6 0 12.50 6.90 -4 6 0 19.10 5.70 -4 6 0 31.10 6.80 4 6 0 20.40 8.40 4 6 0 22.90 8.20 5 -6 0 -2.60 6.60 -5 -6 0 -4.00 4.70 -5 -6 0 0.70 4.30 5 -6 0 -9.30 6.80 5 -6 0 -3.60 5.70 5 -6 0 -2.90 6.20 -5 -6 0 -1.20 4.80 -5 -6 0 1.50 4.70 -5 6 0 -3.20 4.70 5 6 0 3.00 5.00 -5 6 0 1.40 4.80 -5 6 0 -1.90 4.90 5 6 0 2.10 7.10 5 6 0 6.30 7.10 5 6 0 -0.60 8.10 5 6 0 -6.80 5.30 -5 6 0 4.00 4.60 5 6 0 -3.20 5.40 0 -7 0 6.50 3.30 0 -7 0 12.70 3.50 0 -7 0 2.40 2.20 0 -7 0 21.50 4.20 0 7 0 16.40 3.40 0 7 0 5.00 2.00 0 7 0 5.40 1.70 0 7 0 5.90 2.60 0 7 0 8.10 2.90 -1 -7 0 379.16 48.50 -1 -7 0 400.76 48.30 -1 -7 0 385.06 48.30 1 -7 0 389.36 48.70 1 -7 0 331.17 47.70 1 -7 0 350.46 48.40 -1 -7 0 396.96 48.50 1 -7 0 394.66 49.00 1 -7 0 357.36 48.30 1 7 0 385.86 49.10 -1 7 0 358.76 48.00 -1 7 0 330.47 47.60 -1 7 0 432.06 48.40 -1 7 0 389.56 47.90 1 7 0 345.27 48.20 1 7 0 372.26 48.40 -1 7 0 389.86 48.40 1 7 0 377.76 48.60 -1 7 0 405.16 47.80 1 7 0 326.17 47.70 1 7 0 418.66 49.30 -1 7 0 368.36 48.30 1 7 0 350.76 48.70 -2 -7 0 45.70 10.00 2 -7 0 59.79 10.10 2 -7 0 52.69 10.40 -2 -7 0 47.50 9.10 2 -7 0 76.09 10.60 2 -7 0 80.79 12.00 2 -7 0 77.99 11.50 -2 -7 0 50.49 9.10 2 -7 0 81.49 10.50 -2 -7 0 66.19 10.60 -2 -7 0 59.49 10.40 2 7 0 79.39 12.70 -2 7 0 74.29 10.10 2 7 0 74.09 12.20 2 7 0 82.89 11.40 2 7 0 74.49 11.60 -2 7 0 66.79 9.90 -2 7 0 55.59 9.10 -2 7 0 56.49 9.70 2 7 0 61.49 11.00 -2 7 0 74.59 9.90 2 7 0 44.50 9.20 2 7 0 64.49 11.20 3 -7 0 340.37 40.20 -3 -7 0 277.07 39.00 -3 -7 0 269.97 39.30 3 -7 0 352.86 39.50 -3 -7 0 290.77 39.60 -3 -7 0 262.37 38.50 3 -7 0 333.27 39.40 3 -7 0 322.47 39.90 3 7 0 254.07 39.50 -3 7 0 328.17 38.70 -3 7 0 300.17 38.80 -3 7 0 300.67 38.60 -3 7 0 289.17 38.90 3 7 0 276.37 39.80 -3 7 0 308.47 38.80 3 7 0 248.68 39.50 3 7 0 284.27 40.60 3 7 0 224.68 39.70 4 -7 0 4.00 5.70 4 -7 0 12.70 6.30 4 -7 0 12.50 6.20 -4 -7 0 10.70 5.50 4 -7 0 4.80 5.80 4 -7 0 15.30 5.90 -4 -7 0 1.00 5.10 -4 -7 0 13.90 5.20 4 -7 0 -2.00 4.20 4 7 0 0.30 5.20 -4 7 0 11.70 4.80 4 7 0 7.30 5.20 -4 7 0 20.70 5.20 -4 7 0 2.90 4.20 4 7 0 -3.10 4.70 4 7 0 4.90 5.50 4 7 0 26.20 8.20 -4 7 0 23.90 5.80 4 7 0 1.10 5.50 4 7 0 7.20 4.60 -4 7 0 19.40 5.50 -5 -7 0 -0.70 4.60 5 -7 0 -17.80 6.10 -5 -7 0 7.30 5.90 5 -7 0 -5.20 5.30 5 -7 0 5.80 7.40 5 -7 0 8.70 6.80 5 7 0 1.60 5.70 5 7 0 -0.90 4.90 -5 7 0 2.70 4.60 -5 7 0 8.90 5.20 5 7 0 6.00 10.10 5 7 0 4.10 6.30 -5 7 0 -0.50 4.40 5 7 0 4.60 5.50 -5 7 0 -0.60 5.10 0 -8 0 41.90 6.70 0 -8 0 25.70 5.40 0 -8 0 28.60 6.00 0 -8 0 19.80 5.30 0 8 0 28.20 5.80 0 8 0 31.90 5.20 0 8 0 37.50 6.70 0 8 0 32.60 5.50 0 8 0 36.80 6.00 0 8 0 21.00 5.70 1 -8 0 58.39 11.30 -1 -8 0 62.89 11.00 -1 -8 0 77.69 11.70 -1 -8 0 81.09 11.20 1 -8 0 70.29 11.30 1 -8 0 67.39 10.90 1 -8 0 73.89 11.70 -1 -8 0 63.79 10.80 -1 8 0 75.59 9.80 1 8 0 59.69 11.40 -1 8 0 67.79 9.50 1 8 0 83.59 12.50 -1 8 0 78.79 10.50 -1 8 0 82.69 11.40 -1 8 0 78.09 10.80 1 8 0 65.89 10.70 1 8 0 54.69 10.90 -1 8 0 56.99 9.40 -1 8 0 85.79 11.50 1 8 0 74.59 12.30 1 8 0 67.69 11.00 -2 -8 0 183.98 24.60 2 -8 0 168.18 24.30 2 -8 0 181.18 24.10 2 -8 0 178.38 24.80 2 -8 0 179.48 25.30 -2 -8 0 169.78 23.90 2 -8 0 181.28 25.00 -2 -8 0 180.38 24.60 2 8 0 188.08 25.90 2 8 0 176.88 24.70 2 8 0 174.38 24.90 -2 8 0 198.98 24.10 2 8 0 159.28 24.80 -2 8 0 150.78 23.60 -2 8 0 206.78 24.30 -2 8 0 178.28 23.70 2 8 0 194.98 25.60 -2 8 0 192.78 24.40 -2 8 0 187.58 24.40 2 8 0 159.38 26.80 -3 -8 0 10.00 4.20 3 -8 0 5.50 5.00 3 -8 0 14.70 6.30 -3 -8 0 7.20 3.90 -3 -8 0 -0.20 3.60 3 -8 0 4.00 4.50 3 -8 0 4.80 3.80 -3 -8 0 0.70 4.50 3 -8 0 11.80 4.60 3 8 0 5.80 5.80 3 8 0 7.20 5.10 3 8 0 4.40 5.10 3 8 0 9.80 5.50 3 8 0 7.70 5.40 -3 8 0 10.90 4.00 3 8 0 2.70 4.50 -3 8 0 8.70 3.70 -3 8 0 25.70 5.70 -3 8 0 8.50 3.40 -3 8 0 6.70 3.50 4 -8 0 0.70 5.30 -4 -8 0 0.60 3.90 -4 -8 0 -3.80 3.80 -4 -8 0 7.00 4.70 4 -8 0 16.70 6.50 4 -8 0 23.50 8.00 4 -8 0 -4.40 4.30 4 -8 0 14.50 6.50 4 -8 0 13.20 6.30 4 8 0 10.20 6.20 4 8 0 11.60 7.40 -4 8 0 7.00 4.90 4 8 0 6.00 6.10 4 8 0 6.10 6.30 -4 8 0 4.00 4.50 4 8 0 9.80 5.70 -4 8 0 6.60 4.40 4 8 0 13.80 7.80 -4 8 0 7.50 4.80 5 -8 0 2.00 6.80 -5 -8 0 4.40 5.20 -5 -8 0 -5.60 5.30 5 -8 0 4.10 7.90 5 -8 0 -0.80 6.00 -5 8 0 -5.30 5.20 5 8 0 10.40 7.30 -5 8 0 0.60 4.90 5 8 0 4.30 6.20 5 8 0 7.30 6.30 -5 8 0 -1.30 4.70 0 -9 0 1.00 2.40 0 -9 0 -0.80 2.30 0 -9 0 2.80 2.40 0 -9 0 3.60 2.40 0 9 0 2.50 1.70 0 9 0 0.70 2.00 0 9 0 4.50 2.00 0 9 0 5.70 3.10 0 9 0 -1.20 2.20 0 9 0 -1.60 2.30 -1 -9 0 -1.10 2.90 1 -9 0 2.70 2.80 1 -9 0 3.10 2.80 -1 -9 0 4.30 2.60 1 -9 0 6.20 3.40 -1 -9 0 -1.40 2.20 -1 -9 0 5.00 2.80 1 9 0 1.90 2.60 -1 9 0 2.80 2.80 1 9 0 1.20 2.50 1 9 0 1.00 3.40 -1 9 0 4.10 2.40 1 9 0 7.80 4.10 -1 9 0 3.50 1.90 -1 9 0 -2.60 2.50 1 9 0 2.70 2.30 -1 9 0 0.70 1.60 -1 9 0 9.90 3.70 1 9 0 4.10 4.10 -2 -9 0 31.20 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22.80 7.60 5 -2 -3 17.40 7.20 -5 -2 3 27.90 6.70 5 2 -3 10.30 6.50 -5 2 3 23.00 7.10 -5 2 3 12.90 5.10 5 2 -3 13.90 7.50 5 2 -3 22.30 8.00 -5 2 3 18.40 6.50 5 2 -3 7.30 7.60 5 2 -3 15.80 6.60 -5 2 3 9.20 5.50 -4 -2 3 3.90 3.20 4 -2 -3 13.30 5.80 4 -2 -3 3.90 4.00 4 -2 -3 3.50 4.50 4 -2 -3 4.50 4.70 -4 -2 3 8.10 4.10 -4 -2 3 8.50 4.20 4 -2 -3 4.40 4.60 -4 -2 3 3.30 3.90 4 2 -3 7.60 4.90 -4 2 3 4.10 3.80 -4 2 3 3.60 3.10 -4 2 3 5.70 3.40 4 2 -3 2.00 4.30 4 2 -3 6.60 4.50 -4 2 3 5.20 3.60 4 2 -3 4.90 4.20 4 2 -3 6.40 4.50 -4 2 3 15.70 4.60 3 -2 -3 16.10 3.90 -3 -2 3 29.10 5.40 -3 -2 3 13.30 4.00 -3 -2 3 7.50 3.80 3 -2 -3 13.20 3.40 3 -2 -3 14.00 4.30 3 -2 -3 7.90 4.20 3 -2 -3 15.80 4.90 3 -2 -3 15.20 4.60 3 -2 -3 15.00 4.50 -3 2 3 17.60 4.50 3 2 -3 19.80 5.80 -3 2 3 24.20 4.10 3 2 -3 19.90 5.10 3 2 -3 27.40 6.00 -3 2 3 12.10 3.70 3 2 -3 12.60 4.40 3 2 -3 16.20 4.60 3 2 -3 9.30 4.10 3 2 -3 12.30 5.00 -3 2 3 23.70 5.00 -2 -2 3 244.98 38.50 -2 -2 3 277.97 37.80 2 -2 -3 309.27 38.70 -2 -2 3 280.77 38.30 2 -2 -3 339.97 38.60 2 -2 -3 293.67 38.10 2 -2 -3 285.77 38.80 2 -2 -3 288.67 38.30 -2 -2 3 273.77 38.50 2 -2 -3 292.77 38.60 2 -2 -3 327.37 38.70 2 2 -3 284.47 38.70 -2 2 3 320.27 38.10 -2 2 3 301.17 38.30 2 2 -3 280.27 38.60 2 2 -3 285.97 38.50 2 2 -3 322.57 38.80 2 2 -3 308.07 38.90 -2 2 3 295.77 38.40 -2 2 3 289.87 38.50 2 2 -3 287.97 39.00 2 2 -3 330.07 39.30 -1 -2 3 1907.71 227.78 1 -2 -3 1738.33 227.58 -1 -2 3 1610.74 227.68 1 -2 -3 1653.23 227.48 1 -2 -3 1817.92 227.88 -1 -2 3 1772.12 227.18 1 -2 -3 1739.53 227.58 1 -2 -3 1898.51 227.68 -1 -2 3 1909.91 227.68 -1 -2 3 1768.82 227.48 1 -2 -3 1765.02 227.68 -1 2 3 1573.94 227.38 -1 2 3 1660.43 227.58 1 2 -3 1792.12 227.68 -1 2 3 1840.32 227.58 1 2 -3 1846.92 227.98 1 2 -3 1728.23 227.18 -1 2 3 1664.03 227.48 1 2 -3 1984.80 227.88 1 2 -3 1939.21 228.08 1 2 -3 1829.82 227.78 1 2 -3 1869.81 227.68 1 2 -3 1941.61 227.88 0 -2 3 212.68 27.40 0 -2 3 216.68 27.40 0 -2 -3 217.58 27.40 0 -2 -3 202.28 27.40 0 -2 -3 218.38 27.40 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5.80 -3 -3 4 11.20 3.90 3 -3 -4 8.60 4.10 3 -3 -4 5.90 3.50 -3 -3 4 10.40 3.60 -3 -3 4 14.80 3.90 3 -3 -4 2.20 3.10 3 -3 -4 10.50 3.70 3 -3 -4 7.50 4.10 3 -3 -4 6.80 2.60 3 -3 -4 9.30 3.40 3 3 -4 10.50 5.00 3 3 -4 8.70 3.90 -3 3 4 7.60 3.20 -3 3 4 13.00 3.60 -3 3 4 9.90 3.60 -3 3 4 8.20 2.90 3 3 -4 0.90 2.90 3 3 -4 7.00 4.00 3 3 -4 13.50 4.80 -3 3 4 9.20 3.20 3 3 -4 11.80 4.50 3 3 -4 8.00 3.50 2 -3 -4 215.28 29.80 2 -3 -4 246.38 30.60 2 -3 -4 229.18 30.60 -2 -3 4 243.68 31.00 -2 -3 4 196.38 30.50 2 -3 -4 228.68 30.60 2 -3 -4 226.68 31.00 2 -3 -4 251.77 30.90 -2 -3 4 222.28 30.00 2 -3 -4 238.68 30.70 -2 -3 4 248.48 30.60 2 -3 -4 215.78 30.30 2 3 -4 221.68 30.90 -2 3 4 235.28 30.60 2 3 -4 264.87 31.50 -2 3 4 245.58 30.60 -2 3 4 231.78 30.40 2 3 -4 245.68 31.30 -2 3 4 240.88 30.20 2 3 -4 234.28 30.80 2 3 -4 216.98 30.50 2 3 -4 233.48 31.00 2 3 -4 233.48 30.80 -2 3 4 235.48 30.40 -1 -3 4 466.15 57.29 -1 -3 4 439.66 57.39 -1 -3 4 446.36 56.89 1 -3 -4 435.26 57.49 -1 -3 4 412.66 57.29 -1 -3 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6.10 3.00 0 8 -4 3.30 1.40 0 8 -4 2.20 1.70 0 8 4 5.70 3.20 0 8 4 5.10 1.80 0 8 -4 7.70 3.20 0 8 -4 6.50 2.60 0 8 4 -0.20 2.70 0 8 4 -1.10 1.70 1 -8 4 -0.30 2.30 1 -8 4 6.40 2.90 1 -8 4 7.10 2.90 1 -8 4 5.90 2.40 -1 -8 -4 4.60 3.10 -1 -8 -4 -0.80 2.20 1 -8 4 6.40 2.20 1 -8 4 2.10 2.80 -1 -8 -4 6.50 3.00 -1 8 -4 2.00 2.20 -1 8 -4 7.20 2.60 -1 8 -4 3.40 2.20 1 8 4 4.10 2.30 -1 8 -4 4.00 3.10 1 8 4 2.10 2.70 1 8 4 3.40 2.20 -1 8 -4 3.70 2.40 1 8 4 4.40 3.20 -1 8 -4 9.70 2.10 1 8 4 5.10 3.40 -1 8 -4 5.90 2.20 1 8 4 5.60 3.40 1 8 4 3.90 2.60 -2 -8 -4 54.69 9.10 2 -8 4 45.70 9.80 2 -8 4 46.70 9.70 -2 -8 -4 45.20 8.90 -2 -8 -4 37.90 7.90 2 -8 4 54.19 9.30 -2 -8 -4 51.49 8.40 2 -8 4 47.60 9.20 2 -8 4 53.29 8.50 -2 8 -4 58.09 8.20 -2 8 -4 63.59 9.40 2 8 4 50.89 8.80 2 8 4 30.10 8.60 2 8 4 62.79 11.50 -2 8 -4 55.29 8.50 2 8 4 53.09 10.50 2 8 4 38.60 9.50 2 8 4 36.40 8.50 -2 8 -4 64.29 9.10 2 8 4 37.50 8.50 -2 8 -4 67.19 8.90 -2 8 -4 38.00 7.60 3 -8 4 14.60 5.40 3 -8 4 22.60 6.30 3 -8 4 7.10 4.60 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4 56.39 9.20 1 -9 -4 40.50 8.10 -1 9 4 55.79 9.20 1 9 -4 45.80 9.00 1 9 -4 47.10 8.60 1 9 -4 39.90 8.80 1 9 -4 34.80 8.70 1 9 -4 54.39 8.90 -1 9 4 55.99 9.10 -1 9 4 43.40 7.60 -1 9 4 46.60 8.60 1 9 -4 33.00 7.50 0 -9 4 9.20 3.20 0 -9 -4 10.10 3.80 0 -9 -4 8.10 3.80 0 -9 4 12.80 4.00 0 -9 4 4.00 3.40 0 -9 4 11.40 4.00 0 -9 -4 13.10 4.10 0 9 -4 9.90 3.10 0 9 -4 8.50 3.30 0 9 4 17.00 4.00 0 9 4 8.00 3.50 0 9 4 12.50 4.50 0 9 -4 20.80 5.10 0 9 -4 10.30 3.90 0 9 4 15.70 4.40 0 9 -4 15.10 4.40 0 9 -4 10.40 3.30 -1 -9 -4 31.00 7.50 1 -9 4 37.20 8.70 1 -9 4 44.90 8.60 1 -9 4 54.19 9.30 -1 -9 -4 31.50 7.80 -1 -9 -4 54.29 8.60 -1 -9 -4 37.40 8.30 -1 9 -4 63.69 8.80 -1 9 -4 44.40 7.70 -1 9 -4 53.69 7.80 1 9 4 43.60 8.60 1 9 4 31.40 8.40 1 9 4 52.69 9.70 -1 9 -4 43.40 6.90 1 9 4 54.99 9.80 -1 9 -4 43.80 8.10 -1 9 -4 45.40 7.40 2 -9 4 78.29 13.80 2 -9 4 86.49 15.00 -2 -9 -4 84.99 12.70 -2 -9 -4 81.59 13.30 -2 -9 -4 110.69 14.50 -2 -9 -4 97.89 13.00 2 -9 4 86.69 13.70 2 -9 4 98.89 14.80 2 -9 4 89.29 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4 -6.60 7.80 5 9 4 17.00 9.00 -5 9 -4 -6.40 4.00 -5 9 -4 10.80 6.20 -5 9 -4 2.20 5.00 5 9 4 -2.20 7.20 4 -10 -4 -2.10 5.20 -4 -10 4 8.60 6.40 4 -10 -4 -0.10 5.80 -4 -10 4 -2.00 4.10 -4 -10 4 -0.90 4.40 4 -10 -4 3.40 6.10 4 10 -4 2.80 6.70 4 10 -4 11.10 7.10 -4 10 4 2.00 3.90 4 10 -4 -3.30 6.00 4 10 -4 1.70 5.10 4 10 -4 0.60 8.00 -4 10 4 -3.40 4.40 -4 10 4 -2.50 6.20 3 -10 -4 8.10 5.50 3 -10 -4 15.00 6.40 -3 -10 4 27.70 7.30 -3 -10 4 15.70 7.20 3 -10 -4 13.60 6.40 -3 -10 4 21.00 6.20 -3 -10 4 17.60 6.40 3 10 -4 18.10 7.30 -3 10 4 21.70 6.00 3 10 -4 23.00 9.10 3 10 -4 3.30 6.30 3 10 -4 21.00 7.20 3 10 -4 22.00 8.50 3 10 -4 27.70 9.20 -3 10 4 30.10 7.00 -3 10 4 26.20 6.70 2 -10 -4 7.80 5.20 -2 -10 4 14.90 5.20 -2 -10 4 17.30 5.70 2 -10 -4 7.40 4.60 2 -10 -4 16.50 5.10 2 -10 -4 10.70 5.40 -2 -10 4 13.80 5.30 2 10 -4 3.00 4.80 2 10 -4 16.30 5.80 2 10 -4 18.40 6.50 2 10 -4 7.50 4.90 2 10 -4 28.20 7.10 -2 10 4 13.20 4.60 -2 10 4 6.80 3.40 2 10 -4 14.90 5.30 -2 10 4 15.00 5.20 -1 -10 4 187.48 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2.20 2.70 3 -2 9 0.40 3.30 3 -2 9 -3.30 2.90 -3 -2 -9 6.80 2.80 3 -2 9 7.50 3.80 3 -2 9 12.80 4.20 3 -2 9 5.40 3.20 -3 -2 -9 5.70 3.40 -3 -2 -9 -1.00 2.60 -3 -2 -9 12.40 4.00 3 -2 9 -1.20 3.10 -3 2 -9 3.20 3.00 3 2 9 0.40 3.10 3 2 9 4.90 3.10 3 2 9 1.70 3.60 -3 2 -9 4.60 2.70 3 2 9 3.40 3.90 -3 2 -9 6.60 3.00 3 2 9 -2.70 3.00 3 2 9 3.10 3.80 3 2 9 3.80 3.80 3 2 9 7.10 3.50 -3 2 -9 4.40 2.80 3 2 9 0.90 2.90 3 2 9 9.10 4.10 -3 2 -9 2.00 2.70 3 2 9 2.00 2.80 4 -2 9 25.80 7.50 -4 -2 -9 21.00 6.40 4 -2 9 18.60 6.70 4 -2 9 16.00 6.80 4 -2 9 33.10 8.20 4 -2 9 44.30 9.10 4 -2 9 16.70 7.60 -4 -2 -9 25.20 6.30 -4 -2 -9 32.00 6.60 4 -2 9 9.20 5.30 -4 -2 -9 26.30 6.40 -4 -2 -9 31.60 7.40 4 2 9 22.60 7.20 -4 2 -9 32.50 7.00 4 2 9 6.70 6.70 4 2 9 25.70 7.10 4 2 9 13.10 5.70 4 2 9 20.90 6.90 -4 2 -9 30.60 6.80 -4 2 -9 43.50 7.30 4 2 9 27.60 8.50 4 2 9 24.90 7.40 -4 2 -9 29.80 6.50 4 2 9 15.70 6.50 -4 2 -9 18.10 5.80 5 -2 9 -2.40 6.40 5 -2 9 15.20 6.90 5 -2 9 6.30 8.80 -5 -2 -9 13.90 5.80 -5 -2 -9 8.50 5.40 -5 -2 -9 4.50 4.70 5 -2 9 13.00 6.80 -5 -2 -9 6.10 5.40 5 -2 9 7.70 6.00 5 2 9 12.10 6.30 5 2 9 8.10 6.90 5 2 9 0.70 5.30 -5 2 -9 7.90 5.50 5 2 9 9.50 6.80 -5 2 -9 9.80 5.60 -5 2 -9 8.10 5.30 5 2 9 0.60 7.80 -5 2 -9 3.30 4.60 5 -3 -9 7.50 6.20 5 -3 -9 6.20 5.80 -5 -3 9 -1.40 6.00 5 -3 -9 3.80 7.90 -5 -3 9 -3.90 4.30 5 -3 -9 -8.30 6.70 5 -3 -9 5.50 8.80 -5 -3 9 3.40 4.00 -5 -3 9 11.70 5.80 5 3 -9 6.60 5.60 5 3 -9 4.80 7.80 -5 3 9 3.30 5.40 -5 3 9 0.30 5.50 -5 3 9 2.90 5.40 5 3 -9 -0.70 6.60 -5 3 9 2.20 4.20 5 3 -9 0.50 5.70 5 3 -9 2.70 7.10 4 -3 -9 1.70 4.70 -4 -3 9 4.00 3.50 4 -3 -9 -0.50 3.90 -4 -3 9 -0.20 3.30 4 -3 -9 -6.20 4.90 4 -3 -9 -0.30 5.50 4 -3 -9 -2.50 4.10 -4 -3 9 0.30 3.90 -4 3 9 5.20 3.50 4 3 -9 6.70 5.40 4 3 -9 -2.20 4.20 4 3 -9 -0.10 5.30 4 3 -9 -3.10 5.00 -4 3 9 -0.80 4.30 -4 3 9 -2.70 3.40 -4 3 9 2.90 3.60 4 3 -9 1.90 5.30 3 -3 -9 20.80 5.30 -3 -3 9 15.20 4.30 3 -3 -9 6.10 4.50 3 -3 -9 8.60 4.30 3 -3 -9 11.80 4.00 -3 -3 9 16.00 4.80 3 -3 -9 13.80 4.80 -3 -3 9 8.70 3.70 3 -3 -9 8.40 4.50 3 3 -9 10.30 5.00 -3 3 9 11.70 4.20 -3 3 9 13.00 3.90 3 3 -9 10.70 5.00 -3 3 9 5.80 3.50 3 3 -9 6.30 4.10 3 3 -9 13.50 4.80 3 3 -9 5.30 3.70 -3 3 9 15.90 4.70 3 3 -9 8.50 5.10 -2 -3 9 152.68 22.80 -2 -3 9 181.68 23.20 -2 -3 9 171.68 23.10 2 -3 -9 159.88 22.90 -2 -3 9 172.58 22.80 2 -3 -9 157.88 23.00 2 -3 -9 170.98 22.90 2 -3 -9 162.78 22.70 2 -3 -9 176.08 22.70 2 -3 -9 156.18 23.40 2 -3 -9 192.48 23.10 2 -3 -9 164.78 22.60 2 3 -9 174.48 23.20 2 3 -9 163.18 23.30 -2 3 9 167.48 23.00 2 3 -9 178.08 23.30 -2 3 9 184.38 23.10 2 3 -9 154.28 23.40 2 3 -9 167.08 22.00 2 3 -9 157.88 22.90 -2 3 9 183.78 22.90 2 3 -9 197.08 23.50 -2 3 9 171.98 22.60 -2 3 9 168.68 22.50 1 -3 -9 279.57 38.10 -1 -3 9 306.97 38.10 -1 -3 9 317.57 38.40 -1 -3 9 307.67 38.20 1 -3 -9 267.07 37.70 1 -3 -9 281.67 38.30 1 -3 -9 277.77 38.40 -1 -3 9 284.97 38.20 -1 -3 9 289.77 38.00 -1 -3 9 315.27 38.10 1 -3 -9 282.57 37.70 1 -3 -9 287.67 38.20 1 3 -9 294.77 38.10 1 3 -9 289.07 38.20 1 3 -9 309.37 38.20 1 3 -9 275.57 38.30 1 3 -9 306.97 38.40 -1 3 9 293.87 37.50 1 3 -9 309.17 38.30 -1 3 9 306.67 38.30 -1 3 9 311.17 38.40 -1 3 9 280.87 38.00 -1 3 9 289.27 38.20 -1 3 9 287.67 38.20 0 -3 -9 38.40 7.40 0 -3 9 49.20 7.10 0 -3 -9 43.30 6.20 0 -3 9 46.50 7.30 0 -3 -9 46.90 6.60 0 -3 -9 39.20 7.50 0 -3 9 42.10 7.60 0 -3 -9 67.49 8.10 0 -3 9 65.09 8.60 0 -3 9 47.30 7.60 0 3 9 38.80 7.50 0 3 9 56.69 7.90 0 3 -9 50.09 7.20 0 3 9 48.60 7.30 0 3 -9 50.69 7.30 0 3 9 42.60 7.80 0 3 -9 43.70 6.60 0 3 -9 58.89 7.50 0 3 9 52.39 7.60 0 3 -9 60.29 7.40 0 3 9 49.10 7.60 0 3 -9 39.80 6.40 1 -3 9 312.97 37.50 1 -3 9 303.17 37.20 -1 -3 -9 303.77 36.80 -1 -3 -9 289.67 37.10 1 -3 9 299.17 37.20 1 -3 9 294.27 36.70 -1 -3 -9 289.97 36.30 -1 -3 -9 287.67 37.20 -1 -3 -9 286.27 36.20 1 -3 9 300.57 37.20 -1 -3 -9 299.27 36.40 1 -3 9 285.57 36.10 -1 3 -9 276.77 36.00 1 3 9 280.67 36.50 1 3 9 260.87 36.40 -1 3 -9 266.47 36.80 1 3 9 238.48 36.40 1 3 9 295.57 37.20 1 3 9 271.47 37.00 1 3 9 237.58 36.70 1 3 9 300.37 37.20 -1 3 -9 306.07 36.50 -1 3 -9 281.77 36.40 1 3 9 268.47 36.30 -1 3 -9 287.27 36.60 -1 3 -9 256.67 36.50 1 3 9 282.37 36.80 1 3 9 280.37 37.20 1 3 9 278.67 37.00 2 -3 9 209.58 24.60 -2 -3 -9 161.18 23.20 2 -3 9 170.58 23.60 -2 -3 -9 205.78 24.10 2 -3 9 167.88 24.10 2 -3 9 178.68 24.00 -2 -3 -9 181.58 23.20 -2 -3 -9 174.48 23.30 2 -3 9 183.28 23.60 -2 -3 -9 181.08 23.20 2 -3 9 182.38 23.70 -2 -3 -9 178.28 23.80 -2 -3 -9 163.28 23.40 -2 -3 -9 183.78 23.60 2 3 9 156.88 23.60 2 3 9 174.68 23.70 2 3 9 181.68 23.60 -2 3 -9 178.08 23.30 2 3 9 181.38 23.60 2 3 9 172.58 24.20 -2 3 -9 151.58 23.20 2 3 9 170.68 23.70 2 3 9 161.68 23.70 2 3 9 191.38 24.00 -2 3 -9 178.08 23.20 2 3 9 192.08 24.10 2 3 9 170.38 23.90 -2 3 -9 171.28 23.00 2 3 9 147.69 23.50 -2 3 -9 172.58 23.40 3 -3 9 8.00 4.50 -3 -3 -9 9.80 4.20 -3 -3 -9 12.00 3.70 -3 -3 -9 4.80 3.60 3 -3 9 17.40 4.30 -3 -3 -9 14.60 4.70 -3 -3 -9 16.60 4.30 3 -3 9 12.70 4.70 -3 -3 -9 8.20 4.20 -3 -3 -9 1.20 3.40 -3 -3 -9 7.80 3.90 -3 -3 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4.00 5 3 9 -4.50 5.60 5 3 9 0.30 7.20 -5 3 -9 8.10 5.20 5 3 9 -2.00 4.80 5 3 9 23.50 8.00 5 -4 -9 29.40 11.10 -5 -4 9 8.30 5.40 5 -4 -9 18.30 7.20 -5 -4 9 11.00 8.10 -5 -4 9 20.00 6.60 5 -4 -9 -1.70 5.50 -5 -4 9 28.90 7.60 5 -4 -9 7.30 8.20 5 4 -9 14.60 6.70 -5 4 9 21.30 6.30 -5 4 9 11.60 6.20 5 4 -9 2.80 7.70 5 4 -9 36.90 13.70 -5 4 9 11.50 5.60 5 4 -9 -3.50 6.00 -5 4 9 4.30 10.30 4 -4 -9 2.40 4.40 4 -4 -9 5.70 5.70 4 -4 -9 4.50 6.00 -4 -4 9 9.60 4.50 4 -4 -9 0.10 5.90 4 -4 -9 2.70 4.90 -4 -4 9 5.40 3.90 -4 -4 9 4.90 4.50 -4 4 9 8.70 5.50 4 4 -9 -1.70 4.40 -4 4 9 6.50 4.20 4 4 -9 7.70 5.00 -4 4 9 3.50 3.40 -4 4 9 7.90 4.60 4 4 -9 7.40 5.40 -4 4 9 2.40 3.80 4 4 -9 1.80 5.90 4 4 -9 9.80 5.50 3 -4 -9 27.10 7.30 3 -4 -9 40.50 8.40 -3 -4 9 40.20 7.80 3 -4 -9 26.80 6.10 3 -4 -9 39.30 7.70 3 -4 -9 37.00 9.10 -3 -4 9 31.70 7.20 3 -4 -9 31.30 7.20 -3 -4 9 36.30 7.80 3 -4 -9 30.10 7.40 3 4 -9 30.60 7.30 -3 4 9 42.90 7.10 -3 4 9 39.30 6.90 3 4 -9 57.59 9.60 -3 4 9 42.10 7.30 3 4 -9 40.60 8.50 3 4 -9 33.30 8.10 3 4 -9 34.90 8.30 3 4 -9 26.00 7.80 -3 4 9 24.10 6.70 -2 -4 9 226.88 31.30 2 -4 -9 248.48 31.50 -2 -4 9 233.68 31.10 2 -4 -9 241.88 32.00 2 -4 -9 221.98 31.00 2 -4 -9 231.88 31.00 -2 -4 9 248.08 31.50 2 -4 -9 244.58 31.20 2 -4 -9 221.08 31.10 -2 -4 9 248.88 31.70 2 -4 -9 250.27 31.60 -2 4 9 263.97 31.60 2 4 -9 224.98 31.50 2 4 -9 221.38 32.00 -2 4 9 239.08 31.40 2 4 -9 250.97 31.80 2 4 -9 218.18 31.80 2 4 -9 214.58 31.10 -2 4 9 229.58 30.80 -2 4 9 236.68 31.10 -2 4 9 243.98 31.20 2 4 -9 242.88 31.70 2 4 -9 226.08 31.80 -1 -4 9 65.09 8.50 1 -4 -9 63.39 9.20 -1 -4 9 50.79 8.00 1 -4 -9 48.80 8.40 1 -4 -9 46.00 7.10 -1 -4 9 58.39 8.30 -1 -4 9 53.69 8.40 1 -4 -9 61.39 8.90 -1 -4 9 49.20 8.60 1 -4 -9 56.09 8.90 -1 -4 9 70.79 8.70 1 -4 -9 35.50 7.60 -1 4 9 39.40 8.30 1 4 -9 51.99 8.50 -1 4 9 54.09 8.60 1 4 -9 47.10 8.40 -1 4 9 47.00 8.00 -1 4 9 44.20 8.30 1 4 -9 60.79 9.10 -1 4 9 51.39 7.10 1 4 -9 63.59 8.50 1 4 -9 60.29 8.70 1 4 -9 53.89 8.50 -1 4 9 48.20 8.50 1 4 -9 66.29 9.10 0 -4 9 21.10 4.60 0 -4 -9 16.60 4.60 0 -4 -9 17.70 4.20 0 -4 -9 22.40 3.50 0 -4 9 27.00 4.50 0 -4 9 25.40 4.00 0 -4 -9 14.80 3.60 0 -4 9 14.90 3.70 0 -4 9 27.90 4.80 0 -4 9 16.00 3.10 0 -4 -9 16.80 4.10 0 4 -9 13.00 3.30 0 4 9 13.90 3.20 0 4 -9 23.10 3.80 0 4 -9 20.30 3.90 0 4 9 14.30 4.00 0 4 9 20.30 4.00 0 4 -9 24.20 4.10 0 4 -9 18.20 3.50 0 4 9 28.10 5.20 0 4 9 18.70 4.10 0 4 9 24.30 4.50 0 4 9 20.20 4.40 0 4 -9 16.50 3.50 0 4 -9 20.10 3.70 1 -4 9 71.29 9.40 -1 -4 -9 44.70 6.90 -1 -4 -9 48.30 7.00 -1 -4 -9 53.19 8.80 1 -4 9 48.50 6.80 1 -4 9 61.39 8.90 1 -4 9 52.69 8.80 -1 -4 -9 46.80 6.90 -1 -4 -9 58.59 8.70 1 -4 9 62.39 8.40 -1 -4 -9 57.89 8.70 -1 -4 -9 61.89 8.10 1 -4 9 59.09 9.00 1 4 9 50.49 7.90 -1 4 -9 61.09 8.10 1 4 9 46.90 7.40 -1 4 -9 47.40 6.90 -1 4 -9 48.60 8.10 1 4 9 36.20 8.10 1 4 9 46.90 8.20 1 4 9 54.59 9.10 -1 4 -9 49.70 7.10 1 4 9 46.40 8.40 1 4 9 46.50 8.40 1 4 9 51.89 8.70 -1 4 -9 55.39 7.90 1 4 9 57.69 8.20 -1 4 -9 61.19 8.10 1 4 9 44.40 7.40 1 4 9 42.40 7.30 2 -4 9 249.58 32.10 -2 -4 -9 241.88 31.70 -2 -4 -9 239.28 32.10 -2 -4 -9 246.58 32.30 2 -4 9 270.27 32.20 -2 -4 -9 271.97 31.70 2 -4 9 247.88 32.20 -2 -4 -9 221.48 31.80 -2 -4 -9 233.48 32.10 2 -4 9 252.37 32.70 -2 -4 -9 237.78 31.50 2 -4 9 231.58 32.60 2 -4 9 217.88 32.20 -2 -4 -9 265.37 32.30 -2 4 -9 240.98 31.70 -2 4 -9 250.27 31.40 2 4 9 247.38 32.40 2 4 9 234.58 31.90 -2 4 -9 261.37 31.70 2 4 9 251.57 32.30 2 4 9 202.28 32.00 2 4 9 251.77 32.90 2 4 9 251.27 32.30 -2 4 -9 234.88 31.80 2 4 9 224.48 32.10 2 4 9 246.98 31.90 2 4 9 224.78 32.50 -2 4 -9 215.38 31.70 2 4 9 237.48 32.00 2 4 9 232.68 32.20 -3 -4 -9 47.00 7.60 -3 -4 -9 32.50 7.00 -3 -4 -9 46.80 7.90 3 -4 9 29.40 8.00 -3 -4 -9 40.50 7.20 3 -4 9 37.20 8.20 -3 -4 -9 42.00 7.50 -3 -4 -9 28.40 6.60 -3 -4 -9 48.80 7.60 -3 -4 -9 56.19 8.00 3 -4 9 34.70 8.00 -3 -4 -9 30.70 7.00 -3 -4 -9 46.30 7.50 3 -4 9 33.10 7.80 3 -4 9 42.10 8.60 3 -4 9 28.60 6.80 -3 -4 -9 52.49 8.10 3 -4 9 36.50 7.60 3 4 9 47.00 9.80 3 4 9 26.00 7.20 3 4 9 33.40 7.80 3 4 9 33.70 8.00 3 4 9 19.00 6.60 3 4 9 32.20 8.50 3 4 9 21.80 6.60 3 4 9 26.30 7.40 3 4 9 24.70 6.60 -3 4 -9 32.00 6.80 3 4 9 30.20 7.10 -3 4 -9 48.70 7.80 -3 4 -9 43.10 7.50 -3 4 -9 42.40 6.90 3 4 9 24.70 7.00 -3 4 -9 38.60 7.50 -4 -4 -9 12.40 4.40 4 -4 9 4.20 4.40 4 -4 9 1.90 3.80 4 -4 9 8.40 5.60 -4 -4 -9 -0.40 3.50 -4 -4 -9 7.90 4.30 -4 -4 -9 7.20 4.60 -4 -4 -9 3.70 3.70 4 -4 9 0.40 4.90 -4 -4 -9 3.50 4.20 4 -4 9 4.50 4.80 4 -4 9 2.50 4.60 -4 4 -9 4.20 3.40 -4 4 -9 4.40 4.10 4 4 9 3.40 4.30 4 4 9 1.20 5.10 4 4 9 -1.40 5.30 -4 4 -9 5.10 4.00 4 4 9 3.50 4.90 4 4 9 2.50 5.80 4 4 9 -0.80 4.90 4 4 9 -1.30 4.00 -4 4 -9 5.10 4.10 4 4 9 0.80 4.60 -5 -4 -9 27.20 7.10 5 -4 9 7.30 5.50 -5 -4 -9 14.00 5.90 5 -4 9 3.20 6.30 -5 -4 -9 28.80 7.20 -5 -4 -9 7.40 5.60 5 -4 9 24.80 8.30 5 -4 9 35.70 15.50 -5 -4 -9 14.90 6.60 -5 4 -9 9.00 5.70 5 4 9 10.40 6.20 5 4 9 29.00 9.70 -5 4 -9 10.20 4.60 5 4 9 10.40 8.90 5 4 9 8.10 8.10 5 4 9 10.60 7.50 -5 4 -9 -0.90 4.30 5 4 9 5.70 5.60 5 -5 -9 5.70 6.90 -5 -5 9 0.10 4.10 -5 -5 9 0.40 5.60 5 -5 -9 11.10 7.60 -5 -5 9 5.30 5.20 -5 5 9 12.60 5.10 5 5 -9 6.00 6.40 -5 5 9 3.30 4.90 5 5 -9 5.70 5.40 5 5 -9 -1.90 6.10 -4 -5 9 29.90 7.10 4 -5 -9 18.50 6.40 4 -5 -9 21.70 7.40 -4 -5 9 15.30 6.10 -4 -5 9 16.50 6.30 4 5 -9 20.00 6.80 -4 5 9 25.00 7.20 -4 5 9 30.30 6.60 -4 5 9 17.60 5.80 4 5 -9 26.40 8.10 4 5 -9 17.80 6.40 4 5 -9 11.70 6.20 -4 5 9 23.50 6.50 4 5 -9 19.30 8.10 -3 -5 9 96.99 14.30 -3 -5 9 73.69 13.70 -3 -5 9 79.09 14.00 3 -5 -9 95.99 13.60 3 -5 -9 93.89 14.30 3 -5 -9 72.69 13.90 3 -5 -9 97.29 15.60 -3 5 9 110.49 13.80 -3 5 9 90.79 14.20 3 5 -9 66.19 13.90 3 5 -9 75.49 14.50 3 5 -9 69.69 14.00 3 5 -9 84.99 14.70 -3 5 9 96.89 13.70 -3 5 9 72.39 13.30 3 5 -9 71.69 15.00 -3 5 9 83.19 13.30 3 5 -9 111.19 16.50 3 5 -9 83.89 15.10 -2 -5 9 93.89 12.90 -2 -5 9 69.19 12.10 2 -5 -9 88.79 12.70 2 -5 -9 104.39 14.50 2 -5 -9 88.69 12.30 -2 -5 9 72.69 12.40 2 -5 -9 66.29 12.30 -2 -5 9 88.49 13.00 2 -5 -9 81.29 13.50 2 -5 -9 92.29 13.20 2 5 -9 67.89 12.80 2 5 -9 68.19 12.70 2 5 -9 70.39 12.60 2 5 -9 84.89 13.20 -2 5 9 68.39 12.20 2 5 -9 90.29 12.50 -2 5 9 106.99 13.10 2 5 -9 86.59 13.50 2 5 -9 71.29 13.30 -2 5 9 82.99 12.40 -2 5 9 79.19 11.20 -2 5 9 81.29 11.70 -2 5 9 67.19 12.30 1 -5 -9 213.88 30.50 -1 -5 9 229.78 30.20 1 -5 -9 243.78 30.70 1 -5 -9 229.18 30.00 1 -5 -9 229.98 30.40 -1 -5 9 228.18 30.10 -1 -5 9 245.68 30.30 -1 -5 9 223.88 30.10 1 -5 -9 252.27 30.50 -1 -5 9 240.58 30.50 -1 -5 9 248.88 30.20 -1 5 9 228.18 30.50 -1 5 9 196.88 29.30 -1 5 9 232.18 30.40 1 5 -9 231.98 30.20 1 5 -9 216.88 30.40 1 5 -9 259.67 30.70 -1 5 9 243.88 29.60 1 5 -9 212.38 30.50 1 5 -9 230.88 30.40 1 5 -9 223.38 29.90 1 5 -9 218.48 30.30 -1 5 9 229.08 30.40 -1 5 9 241.58 30.30 0 -5 -9 154.88 20.50 0 -5 9 150.38 19.90 0 -5 9 165.88 20.90 0 -5 9 161.58 20.30 0 -5 9 161.98 20.60 0 -5 -9 155.98 19.90 0 -5 -9 136.99 20.70 0 -5 9 147.49 20.10 0 -5 9 166.18 20.90 0 -5 -9 136.79 20.70 0 -5 -9 160.18 20.70 0 5 -9 140.99 20.20 0 5 9 143.59 19.90 0 5 -9 141.69 20.10 0 5 -9 165.48 20.30 0 5 9 165.78 20.90 0 5 9 142.99 20.90 0 5 -9 149.99 20.20 0 5 -9 142.19 20.10 0 5 -9 161.78 20.30 0 5 9 144.59 20.60 0 5 9 145.99 20.60 0 5 9 166.08 20.70 0 5 -9 152.08 20.20 1 -5 9 278.47 30.60 1 -5 9 251.37 29.90 -1 -5 -9 220.58 29.30 1 -5 9 239.88 30.60 -1 -5 -9 243.88 30.60 1 -5 9 221.28 30.30 1 -5 9 243.38 30.40 -1 -5 -9 227.88 30.40 -1 -5 -9 233.18 29.80 -1 -5 -9 254.57 30.40 -1 -5 -9 239.48 29.30 -1 -5 -9 210.28 29.20 1 -5 9 227.18 29.20 -1 5 -9 226.48 29.60 1 5 9 223.18 30.40 1 5 9 239.58 30.60 1 5 9 245.58 30.40 1 5 9 203.08 29.40 1 5 9 250.27 30.70 1 5 9 215.08 29.40 -1 5 -9 219.28 29.60 1 5 9 218.18 30.40 -1 5 -9 248.48 29.70 -1 5 -9 223.48 29.70 1 5 9 214.68 29.30 1 5 9 196.28 29.70 1 5 9 231.28 29.80 -1 5 -9 202.58 29.80 -1 5 -9 235.68 29.40 1 5 9 199.38 30.10 -2 -5 -9 74.79 11.30 2 -5 9 73.49 12.30 2 -5 9 80.79 12.40 -2 -5 -9 60.69 10.90 2 -5 9 75.79 12.90 -2 -5 -9 77.59 12.10 2 -5 9 97.79 13.50 -2 -5 -9 92.79 13.00 -2 -5 -9 62.99 11.40 -2 -5 -9 79.39 10.60 2 -5 9 87.39 12.20 2 5 9 65.99 12.50 -2 5 -9 68.99 11.20 2 5 9 74.29 11.80 -2 5 -9 78.89 10.50 2 5 9 73.09 12.30 2 5 9 86.19 13.30 2 5 9 71.29 11.40 2 5 9 52.79 11.20 2 5 9 74.89 11.90 2 5 9 77.59 11.60 -2 5 -9 74.69 11.50 2 5 9 75.19 12.20 -2 5 -9 63.99 11.00 2 5 9 83.19 12.80 -2 5 -9 82.99 10.90 2 5 9 72.69 12.20 3 -5 9 96.19 13.70 -3 -5 -9 78.49 12.40 3 -5 9 76.99 13.60 3 -5 9 86.69 15.00 -3 -5 -9 78.89 12.70 -3 -5 -9 86.79 12.40 -3 -5 -9 83.39 12.60 -3 -5 -9 90.19 12.60 -3 -5 -9 86.19 13.10 -3 -5 -9 68.09 12.40 -3 -5 -9 88.69 12.30 3 -5 9 101.79 14.50 3 -5 9 91.89 13.20 -3 -5 -9 65.59 11.60 3 -5 9 82.49 12.60 3 5 9 73.59 13.10 3 5 9 49.99 12.20 3 5 9 65.69 12.40 3 5 9 68.09 12.20 3 5 9 72.49 12.20 -3 5 -9 85.99 12.40 3 5 9 72.39 13.20 3 5 9 90.79 15.40 3 5 9 73.89 12.80 3 5 9 72.49 12.10 -3 5 -9 76.89 12.30 -3 5 -9 87.89 12.50 3 5 9 56.89 13.20 -3 5 -9 62.89 11.30 -3 5 -9 69.59 12.20 3 5 9 61.09 12.40 4 -5 9 25.80 7.20 4 -5 9 25.20 7.70 4 -5 9 25.30 8.00 4 -5 9 18.20 6.40 4 -5 9 13.10 6.20 -4 -5 -9 20.10 6.40 -4 -5 -9 19.60 6.50 4 -5 9 25.50 8.20 -4 -5 -9 19.20 6.40 -4 -5 -9 27.10 6.70 -4 -5 -9 30.90 6.60 -4 5 -9 17.60 6.00 4 5 9 23.80 7.50 4 5 9 16.90 7.10 4 5 9 17.80 7.30 -4 5 -9 29.40 6.80 4 5 9 35.60 10.10 -4 5 -9 20.90 5.90 -4 5 -9 15.80 5.20 4 5 9 9.00 5.30 4 5 9 12.00 6.50 4 5 9 19.00 8.20 5 -5 9 1.80 8.00 5 -5 9 -5.10 5.80 5 -5 9 15.90 6.50 -5 -5 -9 6.30 5.60 -5 -5 -9 6.10 5.10 -5 -5 -9 5.30 5.30 -5 -5 -9 3.20 5.30 -5 -5 -9 -3.70 5.50 5 -5 9 -3.70 5.40 -5 5 -9 9.20 5.60 5 5 9 8.10 7.90 -5 5 -9 2.60 4.50 5 5 9 1.00 6.90 5 5 9 -6.70 5.60 -5 5 -9 4.00 4.50 5 5 9 1.70 7.20 5 5 9 3.60 5.50 5 5 9 9.00 9.40 -5 -6 9 2.20 5.20 -5 -6 9 6.80 5.10 5 -6 -9 6.60 6.60 5 -6 -9 5.30 5.60 5 6 -9 -5.00 5.70 -5 6 9 -1.20 4.80 5 6 -9 2.60 7.00 5 6 -9 -3.80 5.50 -5 6 9 4.50 4.40 -4 -6 9 17.20 7.20 -4 -6 9 9.50 5.80 4 -6 -9 -3.50 4.70 4 -6 -9 4.20 5.80 -4 -6 9 15.20 5.20 4 6 -9 5.50 5.90 -4 6 9 14.40 5.40 4 6 -9 7.60 5.60 4 6 -9 22.20 7.50 -4 6 9 14.20 4.80 -4 6 9 18.70 5.80 4 6 -9 15.80 7.10 4 6 -9 18.70 7.40 3 -6 -9 69.59 10.60 -3 -6 9 51.69 10.70 -3 -6 9 51.69 10.00 3 -6 -9 68.39 12.20 -3 -6 9 40.10 10.00 3 -6 -9 36.50 9.90 3 -6 -9 50.59 10.70 3 6 -9 66.59 12.30 -3 6 9 71.09 10.90 3 6 -9 48.40 11.60 3 6 -9 52.99 11.80 -3 6 9 79.99 11.60 -3 6 9 64.59 10.20 -3 6 9 77.09 10.40 3 6 -9 62.09 11.80 3 6 -9 42.40 10.30 3 6 -9 61.29 11.50 2 -6 -9 5.70 3.40 -2 -6 9 7.10 3.80 -2 -6 9 9.90 3.60 -2 -6 9 11.10 3.90 2 -6 -9 2.70 2.80 2 -6 -9 9.10 3.40 2 -6 -9 1.80 3.30 -2 -6 9 14.60 4.00 2 -6 -9 12.70 5.20 -2 6 9 11.30 2.90 -2 6 9 9.00 3.70 2 6 -9 11.80 4.40 -2 6 9 7.10 3.80 2 6 -9 9.70 4.60 2 6 -9 9.80 3.80 2 6 -9 10.60 4.30 -2 6 9 8.30 3.50 2 6 -9 10.70 3.80 -2 6 9 12.70 3.70 2 6 -9 10.80 4.30 1 -6 -9 30.20 6.10 -1 -6 9 22.50 5.30 -1 -6 9 23.30 5.00 1 -6 -9 33.50 6.10 1 -6 -9 26.00 5.00 1 -6 -9 15.70 5.10 -1 -6 9 27.60 5.40 1 -6 -9 24.30 5.60 -1 -6 9 36.30 5.80 -1 -6 9 34.20 6.30 -1 6 9 25.60 4.50 -1 6 9 31.90 5.70 1 6 -9 33.20 5.10 1 6 -9 20.80 5.60 -1 6 9 25.50 5.80 -1 6 9 35.90 6.70 1 6 -9 33.70 6.20 1 6 -9 33.40 6.30 1 6 -9 31.00 5.90 -1 6 9 28.60 5.80 1 6 -9 33.10 6.30 1 6 -9 21.80 5.00 0 -6 9 170.48 22.70 0 -6 -9 158.68 22.70 0 -6 9 159.78 22.20 0 -6 9 175.58 22.10 0 -6 9 180.98 23.10 0 -6 -9 163.28 22.90 0 -6 9 170.68 22.30 0 -6 -9 149.88 22.80 0 -6 -9 181.88 22.60 0 -6 9 184.08 23.10 0 6 -9 173.28 22.40 0 6 -9 150.68 22.10 0 6 -9 177.58 22.50 0 6 -9 191.48 22.50 0 6 9 166.38 23.10 0 6 9 169.28 23.00 0 6 9 135.49 22.60 0 6 -9 169.18 22.20 0 6 9 152.08 22.80 0 6 -9 167.88 22.30 0 6 9 168.88 22.90 0 6 9 153.68 22.10 0 6 -9 194.08 22.70 -1 -6 -9 20.90 5.60 1 -6 9 21.40 5.80 -1 -6 -9 30.80 5.40 1 -6 9 30.00 6.10 1 -6 9 23.10 6.10 -1 -6 -9 32.20 6.50 1 -6 9 45.90 6.30 1 -6 9 27.20 6.10 -1 -6 -9 32.30 6.40 1 6 9 26.40 6.40 -1 6 -9 23.80 5.00 -1 6 -9 25.30 4.90 -1 6 -9 37.30 5.40 1 6 9 21.00 4.60 -1 6 -9 33.50 5.40 1 6 9 34.00 6.90 1 6 9 26.40 6.20 -1 6 -9 34.70 5.70 -1 6 -9 41.30 5.80 1 6 9 23.50 5.40 1 6 9 24.80 5.90 1 6 9 27.80 6.00 -2 -6 -9 14.00 4.50 -2 -6 -9 18.70 3.50 2 -6 9 7.20 3.70 2 -6 9 7.20 3.80 -2 -6 -9 14.10 4.30 -2 -6 -9 10.10 3.00 2 -6 9 14.00 4.50 -2 -6 -9 3.40 3.40 2 -6 9 9.40 4.40 2 -6 9 9.50 3.40 2 6 9 4.80 3.40 -2 6 -9 5.40 2.90 2 6 9 12.80 3.50 2 6 9 4.80 3.50 2 6 9 4.20 3.10 -2 6 -9 16.30 3.50 2 6 9 5.20 3.50 2 6 9 2.10 2.90 -2 6 -9 8.80 3.10 -2 6 -9 11.30 2.80 2 6 9 8.00 4.30 2 6 9 2.20 3.40 2 6 9 2.20 4.50 2 6 9 8.40 3.70 -2 6 -9 8.70 2.90 2 6 9 9.20 3.40 -3 -6 -9 33.90 8.40 3 -6 9 45.30 10.90 3 -6 9 50.89 10.00 -3 -6 -9 47.10 9.80 3 -6 9 61.29 10.30 3 -6 9 75.09 11.80 3 -6 9 60.69 10.80 -3 -6 -9 59.49 9.30 -3 -6 -9 49.30 9.00 -3 -6 -9 56.09 9.30 -3 -6 -9 49.60 9.90 -3 -6 -9 68.79 10.50 3 -6 9 62.69 10.10 3 6 9 24.30 8.40 3 6 9 51.29 9.50 -3 6 -9 58.39 9.10 -3 6 -9 52.19 8.90 3 6 9 32.00 9.10 3 6 9 55.59 9.70 3 6 9 33.60 9.30 3 6 9 57.79 11.50 -3 6 -9 51.49 8.80 3 6 9 47.70 11.30 3 6 9 51.69 10.40 -3 6 -9 51.99 9.00 -3 6 -9 48.80 9.20 4 -6 9 1.90 4.50 -4 -6 -9 16.80 5.40 4 -6 9 6.60 6.50 -4 -6 -9 8.80 4.70 -4 -6 -9 4.70 4.30 4 -6 9 7.10 5.00 4 -6 9 10.50 5.60 -4 -6 -9 12.80 5.00 -4 -6 -9 4.70 5.40 4 -6 9 7.30 5.20 4 6 9 6.30 5.80 -4 6 -9 6.50 4.50 4 6 9 11.60 6.10 4 6 9 20.60 8.60 4 6 9 2.10 5.90 4 6 9 5.40 5.80 -4 6 -9 10.40 4.40 -4 6 -9 -1.20 3.30 -4 6 -9 10.20 5.10 4 6 9 6.40 6.20 5 -6 9 -13.80 6.00 -5 -6 -9 -3.20 5.30 5 -6 9 -1.90 6.40 -5 -6 -9 5.70 5.30 -5 -6 -9 20.00 9.40 -5 -6 -9 7.50 5.20 5 -6 9 -4.80 8.60 5 -6 9 -1.50 5.20 -5 -6 -9 0.40 5.80 5 6 9 1.70 7.40 5 6 9 5.10 7.20 5 6 9 0.10 6.30 -5 6 -9 -6.30 4.00 -5 6 -9 4.00 5.50 5 6 9 -0.40 8.20 -5 6 -9 3.10 4.50 -5 -7 9 -5.50 4.60 -5 -7 9 -6.90 4.40 5 -7 -9 8.60 6.90 5 -7 -9 5.70 8.40 -5 7 9 4.30 5.20 5 7 -9 3.10 6.00 5 7 -9 -7.10 5.80 -5 7 9 -7.20 6.40 5 7 -9 7.40 6.60 4 -7 -9 -3.50 4.70 -4 -7 9 3.10 4.60 4 -7 -9 6.30 5.70 -4 -7 9 1.00 3.90 -4 -7 9 4.40 5.50 -4 7 9 -4.10 4.10 4 7 -9 6.80 5.30 4 7 -9 -0.90 3.80 4 7 -9 11.10 6.70 4 7 -9 1.30 5.20 4 7 -9 -5.80 5.90 -4 7 9 -0.40 4.50 4 7 -9 2.40 6.60 -4 7 9 0.50 3.60 3 -7 -9 15.20 5.80 -3 -7 9 22.50 6.20 -3 -7 9 10.30 5.60 3 -7 -9 19.50 7.10 3 -7 -9 11.00 4.90 3 -7 -9 28.30 7.70 -3 -7 9 36.00 6.80 3 7 -9 7.70 5.80 -3 7 9 15.20 5.10 -3 7 9 23.20 5.20 -3 7 9 19.70 5.80 3 7 -9 15.40 6.30 -3 7 9 21.00 5.50 3 7 -9 15.40 5.70 3 7 -9 12.30 5.60 3 7 -9 13.50 5.40 3 7 -9 10.20 6.50 -2 -7 9 11.60 4.10 2 -7 -9 10.10 3.80 -2 -7 9 3.70 3.40 -2 -7 9 10.00 3.30 -2 -7 9 11.80 3.80 2 -7 -9 8.60 5.10 2 -7 -9 11.60 4.20 2 -7 -9 8.60 3.40 2 7 -9 5.40 4.50 2 7 -9 6.60 4.30 2 7 -9 10.20 4.20 -2 7 9 11.20 4.30 -2 7 9 3.10 3.00 -2 7 9 3.30 2.40 2 7 -9 5.00 3.40 2 7 -9 0.90 2.40 -2 7 9 16.00 4.60 2 7 -9 14.30 5.00 -2 7 9 4.50 3.40 1 -7 -9 15.20 4.40 -1 -7 9 35.10 6.00 -1 -7 9 20.90 4.50 1 -7 -9 28.20 5.70 -1 -7 9 16.00 3.90 -1 -7 9 19.50 4.60 1 -7 -9 15.90 4.40 1 -7 -9 12.10 4.40 -1 -7 9 19.10 4.50 1 7 -9 13.80 4.40 -1 7 9 7.60 3.80 1 7 -9 11.30 4.50 -1 7 9 15.00 4.20 1 7 -9 8.50 3.90 1 7 -9 15.70 3.80 -1 7 9 30.00 5.50 1 7 -9 21.40 5.30 1 7 -9 17.90 4.30 -1 7 9 15.20 3.30 -1 7 9 22.30 5.30 0 -7 9 110.89 14.10 0 -7 9 118.09 16.30 0 -7 -9 109.89 14.50 0 -7 -9 118.29 15.90 0 -7 9 123.39 15.00 0 -7 -9 121.09 16.50 0 -7 9 103.19 15.70 0 -7 -9 107.89 15.90 0 -7 9 96.19 14.10 0 -7 9 100.29 14.00 0 7 9 96.29 15.70 0 7 -9 103.99 14.20 0 7 -9 100.79 14.00 0 7 -9 93.49 13.90 0 7 9 83.09 13.90 0 7 -9 103.99 14.40 0 7 -9 108.49 14.60 0 7 9 122.09 16.60 0 7 9 103.19 15.90 0 7 -9 102.79 14.40 0 7 -9 99.29 14.50 0 7 9 99.69 15.60 1 -7 9 18.70 4.60 1 -7 9 15.30 4.60 -1 -7 -9 21.10 5.70 1 -7 9 17.50 5.00 -1 -7 -9 12.00 4.30 -1 -7 -9 16.70 3.80 -1 -7 -9 10.80 4.10 1 -7 9 18.30 4.10 1 -7 9 16.30 4.70 1 7 9 9.70 4.50 -1 7 -9 11.60 3.50 -1 7 -9 21.50 4.10 -1 7 -9 20.50 4.20 1 7 9 17.00 5.10 -1 7 -9 23.60 4.10 1 7 9 24.80 4.90 1 7 9 17.70 4.80 -1 7 -9 16.20 3.90 -1 7 -9 16.70 3.60 1 7 9 9.70 4.70 1 7 9 8.70 4.40 -2 -7 -9 7.20 3.90 -2 -7 -9 2.50 3.50 2 -7 9 12.50 3.70 2 -7 9 13.20 5.10 -2 -7 -9 10.70 4.80 2 -7 9 6.40 3.70 2 -7 9 6.10 3.80 2 -7 9 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10 2.90 4.70 -4 -4 10 -4.20 3.30 4 -4 -10 3.20 5.70 -4 -4 10 7.80 4.30 4 -4 -10 -1.20 4.30 4 -4 -10 0.20 4.30 -4 -4 10 1.50 4.30 -4 4 10 5.10 4.20 4 4 -10 -0.50 5.50 -4 4 10 7.70 4.40 -4 4 10 1.10 3.80 4 4 -10 -0.90 4.40 4 4 -10 1.40 5.70 4 4 -10 -1.00 4.80 -4 4 10 1.50 3.30 4 4 -10 6.60 5.10 -4 4 10 -4.60 4.10 3 -4 -10 63.99 12.00 3 -4 -10 64.69 10.80 3 -4 -10 48.30 10.40 3 -4 -10 37.60 9.40 -3 -4 10 73.59 10.90 -3 -4 10 51.09 10.10 -3 -4 10 44.40 9.90 3 -4 -10 68.89 10.70 -3 4 10 62.49 9.70 3 4 -10 57.19 11.10 3 4 -10 57.69 10.50 3 4 -10 52.89 11.00 -3 4 10 58.99 10.20 -3 4 10 74.39 10.60 3 4 -10 63.99 11.70 3 4 -10 47.60 10.50 3 4 -10 45.70 10.70 -3 4 10 73.29 11.10 -2 -4 10 32.40 5.90 2 -4 -10 22.70 5.40 2 -4 -10 24.90 5.10 -2 -4 10 28.40 5.70 -2 -4 10 28.30 5.40 2 -4 -10 31.40 6.70 2 -4 -10 31.00 5.40 -2 -4 10 21.10 5.40 2 -4 -10 29.50 5.40 2 -4 -10 21.90 5.70 2 -4 -10 20.70 4.70 -2 4 10 34.80 5.80 2 4 -10 28.80 5.60 2 4 -10 24.10 5.80 -2 4 10 36.40 6.00 2 4 -10 22.80 5.90 2 4 -10 15.90 5.10 2 4 -10 34.60 6.80 2 4 -10 28.20 6.10 -2 4 10 19.90 5.30 -2 4 10 22.30 4.50 -2 4 10 15.50 4.80 -1 -4 10 4.80 2.50 -1 -4 10 13.10 3.10 -1 -4 10 8.20 2.40 1 -4 -10 3.80 2.30 1 -4 -10 8.70 3.10 1 -4 -10 4.80 2.60 -1 -4 10 7.40 2.40 1 -4 -10 8.50 1.90 -1 -4 10 10.00 2.60 1 -4 -10 10.90 3.30 1 -4 -10 6.00 2.40 -1 -4 10 9.00 2.60 -1 4 10 9.20 2.60 1 4 -10 6.30 2.60 -1 4 10 10.70 3.30 -1 4 10 2.60 2.70 1 4 -10 6.90 2.70 -1 4 10 7.00 2.60 1 4 -10 8.20 2.40 -1 4 10 6.40 1.60 1 4 -10 8.20 3.10 1 4 -10 11.60 3.00 1 4 -10 6.20 2.40 -1 4 10 7.30 2.80 1 4 -10 1.10 2.10 0 -4 -10 32.60 5.00 0 -4 10 44.00 6.70 0 -4 10 33.80 6.00 0 -4 10 36.40 6.40 0 -4 10 42.70 5.00 0 -4 10 40.40 5.60 0 -4 -10 29.50 5.50 0 -4 10 41.90 6.00 0 -4 -10 27.90 6.10 0 -4 -10 21.50 4.00 0 -4 -10 25.90 5.60 0 4 10 28.40 6.20 0 4 -10 30.20 5.00 0 4 -10 34.20 5.40 0 4 10 36.10 6.50 0 4 10 31.50 6.00 0 4 -10 36.30 5.50 0 4 -10 25.80 5.10 0 4 10 36.90 5.70 0 4 -10 33.20 5.30 0 4 10 29.00 5.60 0 4 -10 42.70 5.70 0 4 10 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6 12 97.09 13.40 -3 6 12 89.19 13.30 3 6 -12 88.19 14.50 3 6 -12 86.79 14.60 3 6 -12 69.29 13.60 -3 6 12 65.49 11.90 3 6 -12 72.39 13.30 -2 -6 12 9.90 4.50 -2 -6 12 12.80 4.00 -2 -6 12 16.50 4.50 2 -6 -12 11.80 4.40 -2 -6 12 9.10 4.00 2 -6 -12 12.60 4.40 2 -6 -12 6.50 3.80 -2 6 12 10.40 4.40 2 6 -12 9.50 4.40 -2 6 12 8.80 3.90 -2 6 12 8.50 3.60 2 6 -12 6.10 3.80 2 6 -12 8.90 4.90 2 6 -12 8.80 4.40 2 6 -12 15.80 4.80 2 6 -12 4.30 3.30 -2 6 12 19.60 5.20 -1 -6 12 31.40 5.70 -1 -6 12 32.70 6.30 1 -6 -12 30.30 6.50 -1 -6 12 29.90 6.00 1 -6 -12 19.60 5.90 -1 -6 12 35.40 6.70 1 -6 -12 35.40 6.80 1 -6 -12 19.60 6.20 -1 -6 12 34.60 6.20 -1 -6 12 33.10 6.20 1 6 -12 32.60 6.60 1 6 -12 34.50 6.50 1 6 -12 30.70 6.40 1 6 -12 33.70 6.80 1 6 -12 17.30 5.80 -1 6 12 20.10 5.70 -1 6 12 28.60 6.50 -1 6 12 26.40 6.40 -1 6 12 38.10 6.60 1 6 -12 32.80 6.30 1 6 -12 37.90 6.10 0 -6 -12 25.00 6.30 0 -6 -12 27.90 6.20 0 -6 12 30.90 5.90 0 -6 12 27.00 5.10 0 -6 -12 28.00 5.80 0 -6 -12 28.90 6.20 0 -6 12 22.80 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-4.70 5.80 -1 3 28 1.20 7.60 1 3 -28 -6.00 4.00 -1 3 28 16.60 7.60 -1 3 28 -4.40 7.00 1 3 -28 11.30 6.60 0 -3 28 9.30 6.70 0 -3 -28 4.60 5.00 0 -3 -28 -4.80 4.40 0 -3 28 -6.40 6.00 0 3 28 6.00 5.90 0 3 -28 1.70 5.10 0 3 28 -4.60 7.10 0 3 -28 1.60 4.90 0 3 28 -1.00 7.20 -1 -3 -28 6.40 6.70 1 -3 28 -2.30 7.30 1 -3 28 -5.30 5.70 -1 -3 -28 5.10 5.30 -1 3 -28 -0.50 4.70 1 3 28 13.30 6.00 -1 3 -28 7.90 5.10 1 3 28 5.60 8.10 1 -4 -28 3.60 5.40 -1 -4 28 8.00 7.90 1 -4 -28 2.50 6.10 1 4 -28 -3.50 4.10 -1 4 28 -10.80 6.30 -1 4 28 1.40 6.60 -1 4 28 -4.90 6.50 1 4 -28 4.30 5.70 0 -4 -28 -1.40 5.10 0 -4 28 -14.30 5.90 0 -4 -28 3.50 5.30 0 -4 28 -4.00 6.70 0 4 28 2.50 7.10 0 4 -28 -0.50 4.30 0 4 -28 -2.20 4.20 0 4 28 -4.10 6.80 0 4 28 -0.10 8.00 -1 -4 -28 1.50 4.50 1 -4 28 -1.30 6.00 1 -4 28 0.40 8.30 -1 -4 -28 -4.70 5.60 1 4 28 -8.10 7.30 -1 4 -28 5.40 5.60 1 4 28 2.10 5.40 -1 4 -28 6.40 4.70 1 4 28 -14.00 6.80 -1 4 -28 -0.80 4.80 0 -5 -28 2.50 5.20 0 -5 -28 3.20 6.10 0 -5 28 -3.70 7.30 0 -5 28 -1.80 6.40 0 5 -28 0.50 5.70 0 5 28 9.30 7.40 0 5 28 7.50 8.20 0 5 28 -2.20 5.90 0 5 -28 0.30 4.90 0 5 -28 3.00 4.50 1 0 -29 2.20 5.60 -1 0 29 5.30 7.10 -1 0 29 7.00 8.30 1 0 -29 -1.30 5.40 0 0 29 1.10 6.50 0 0 29 -8.90 5.70 0 0 -29 0.80 6.40 0 0 -29 13.40 6.90 0 0 -29 -2.20 4.00 -1 0 -29 5.00 6.10 1 0 29 -2.00 6.80 -1 0 -29 13.50 7.20 -1 0 -29 0.90 4.90 1 0 29 19.60 9.70 -1 -1 29 8.60 6.20 1 -1 -29 3.90 6.10 1 -1 -29 -0.70 6.10 -1 -1 29 4.00 7.90 -1 1 29 12.10 9.00 1 1 -29 0.50 5.30 1 1 -29 6.70 6.30 -1 1 29 -5.60 6.00 0 -1 -29 -1.60 5.10 0 -1 -29 -7.70 4.20 0 -1 29 3.40 7.00 0 -1 -29 5.00 5.90 0 -1 29 4.90 6.80 0 1 29 1.10 7.80 0 1 -29 1.50 4.30 0 1 29 -10.50 6.90 0 1 29 5.50 6.80 0 1 -29 -12.50 4.40 0 1 -29 -0.40 5.80 -1 -1 -29 5.10 5.50 -1 -1 -29 -1.70 5.40 -1 -1 -29 3.80 5.00 1 -1 29 2.80 7.30 1 -1 29 3.70 6.80 -1 1 -29 0.10 4.70 -1 1 -29 13.50 7.50 -1 1 -29 2.60 5.30 1 1 29 4.30 6.00 1 1 29 4.10 7.10 0 -2 -29 0.80 4.50 0 -2 29 -10.60 6.40 0 -2 -29 5.10 6.70 0 -2 29 -0.40 6.90 0 -2 -29 6.40 5.50 0 2 29 1.90 7.50 0 2 -29 -3.90 4.40 0 2 29 1.40 6.50 0 2 -29 8.80 5.50 0 2 -29 12.80 7.40 0 2 29 2.50 6.90 0 -3 -29 -3.90 4.70 0 -3 29 10.50 6.80 0 -3 -29 -3.70 5.80 0 3 -29 8.10 5.40 0 3 29 -0.30 7.50 0 3 29 -5.40 6.50 0 3 29 8.10 6.50 0 3 -29 -1.60 4.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 68149 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O001 O 0.6283(6) 0.5220(2) 0.47661(10) 0.0737(8) Uani 1 1 d . . . . . N002 N 0.3047(5) 0.50048(19) 0.40270(11) 0.0498(6) Uani 1 1 d . . . . . O003 O -0.0139(6) 0.47661(19) 0.32809(12) 0.0784(8) Uani 1 1 d . . . . . C004 C 0.5155(7) 0.5577(2) 0.43140(13) 0.0502(8) Uani 1 1 d . . . . . C005 C 0.5953(7) 0.6614(2) 0.40573(13) 0.0492(7) Uani 1 1 d . . . . . C006 C 0.2640(7) 0.6336(2) 0.32273(13) 0.0500(8) Uani 1 1 d . . . . . C007 C 0.4693(7) 0.6966(2) 0.35152(13) 0.0487(7) Uani 1 1 d . . . . . C008 C 0.1711(7) 0.5318(2) 0.34955(15) 0.0528(8) Uani 1 1 d . . . . . C009 C 0.2155(8) 0.3982(2) 0.42925(15) 0.0617(9) Uani 1 1 d . . . . . H00A H 0.011928 0.390494 0.424690 0.074 Uiso 1 1 calc R U . . . H00B H 0.257837 0.398692 0.471977 0.074 Uiso 1 1 calc R U . . . C00A C 0.3610(8) 0.3039(2) 0.40036(15) 0.0601(9) Uani 1 1 d . . . . . H00C H 0.563228 0.308469 0.407904 0.072 Uiso 1 1 calc R U . . . H00D H 0.332181 0.306844 0.357162 0.072 Uiso 1 1 calc R U . . . C00B C 0.5480(8) 0.7962(3) 0.32683(16) 0.0631(9) Uani 1 1 d . . . . . C00C C 0.1426(9) 0.6677(3) 0.26965(15) 0.0686(10) Uani 1 1 d . . . . . H00E H 0.008788 0.625455 0.250228 0.082 Uiso 1 1 calc R U . . . C00D C 0.7925(8) 0.7244(3) 0.43379(17) 0.0681(10) Uani 1 1 d . . . . . H00F H 0.876107 0.701156 0.469370 0.082 Uiso 1 1 calc R U . . . C00E C 0.4164(10) 0.8280(3) 0.27232(19) 0.0801(12) Uani 1 1 d . . . . . H00G H 0.466050 0.892911 0.255012 0.096 Uiso 1 1 calc R U . . . C00F C 0.2518(9) 0.1982(3) 0.42384(18) 0.0731(10) Uani 1 1 d . . . . . H00H H 0.289163 0.194144 0.466719 0.088 Uiso 1 1 calc R U . . . H00I H 0.047865 0.195617 0.418266 0.088 Uiso 1 1 calc R U . . . C00G C 0.7520(9) 0.8575(3) 0.3576(2) 0.0795(12) Uani 1 1 d . . . . . H00J H 0.807585 0.923013 0.341928 0.095 Uiso 1 1 calc R U . . . C00H C 0.2213(11) 0.7663(3) 0.24507(18) 0.0847(13) Uani 1 1 d . . . . . H00K H 0.137716 0.789433 0.209469 0.102 Uiso 1 1 calc R U . . . C00I C 0.8689(9) 0.8224(3) 0.4098(2) 0.0824(12) Uani 1 1 d . . . . . H00L H 1.001588 0.864480 0.429706 0.099 Uiso 1 1 calc R U . . . C00J C 0.3827(11) 0.1027(3) 0.39354(19) 0.0943(14) Uani 1 1 d . . . . . H00M H 0.342773 0.105086 0.351185 0.141 Uiso 1 1 calc R U . . . H00N H 0.304679 0.038613 0.410417 0.141 Uiso 1 1 calc R U . . . H00O H 0.584230 0.103596 0.399686 0.141 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.0881(18) 0.0745(17) 0.0583(14) 0.0038(12) -0.0155(14) 0.0089(16) N002 0.0548(15) 0.0406(13) 0.0539(14) 0.0021(11) 0.0056(13) -0.0007(13) O003 0.0806(18) 0.0571(14) 0.0975(18) -0.0048(13) -0.0227(15) -0.0114(15) C004 0.0511(18) 0.0524(18) 0.0471(17) -0.0072(15) 0.0024(16) 0.0072(15) C005 0.0508(18) 0.0437(16) 0.0530(17) -0.0101(14) 0.0051(15) 0.0012(14) C006 0.056(2) 0.0468(17) 0.0471(16) -0.0010(13) 0.0031(15) 0.0091(15) C007 0.0528(18) 0.0409(16) 0.0525(17) -0.0031(14) 0.0146(15) 0.0060(15) C008 0.0522(19) 0.0412(17) 0.065(2) -0.0069(15) 0.0016(17) 0.0026(16) C009 0.067(2) 0.0456(17) 0.072(2) 0.0088(16) 0.0133(19) 0.0005(17) C00A 0.063(2) 0.0442(17) 0.073(2) 0.0025(16) 0.0053(18) 0.0011(16) C00B 0.069(2) 0.0427(17) 0.078(2) 0.0019(17) 0.0243(19) 0.0065(18) C00C 0.076(3) 0.071(2) 0.059(2) 0.0005(17) -0.0059(19) 0.015(2) C00D 0.066(2) 0.068(2) 0.070(2) -0.0204(18) 0.0045(19) -0.008(2) C00E 0.094(3) 0.060(2) 0.086(3) 0.026(2) 0.031(3) 0.018(2) C00F 0.079(3) 0.050(2) 0.091(3) 0.0090(19) 0.009(2) -0.0059(19) C00G 0.080(3) 0.044(2) 0.114(3) -0.008(2) 0.032(3) -0.010(2) C00H 0.097(3) 0.089(3) 0.068(2) 0.025(2) 0.006(2) 0.028(3) C00I 0.073(3) 0.068(3) 0.106(3) -0.033(2) 0.014(3) -0.018(2) C00J 0.119(4) 0.048(2) 0.116(3) -0.002(2) 0.009(3) -0.001(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C004 N002 C008 124.7(3) . . ? C004 N002 C009 118.2(3) . . ? C008 N002 C009 117.1(3) . . ? O001 C004 N002 120.2(3) . . ? O001 C004 C005 122.1(3) . . ? N002 C004 C005 117.7(3) . . ? C00D C005 C007 119.5(3) . . ? C00D C005 C004 120.5(3) . . ? C007 C005 C004 120.0(3) . . ? C00C C006 C007 120.1(3) . . ? C00C C006 C008 119.4(3) . . ? C007 C006 C008 120.5(3) . . ? C006 C007 C005 120.2(3) . . ? C006 C007 C00B 120.1(3) . . ? C005 C007 C00B 119.8(3) . . ? O003 C008 N002 119.9(3) . . ? O003 C008 C006 123.3(3) . . ? N002 C008 C006 116.8(3) . . ? N002 C009 C00A 112.4(3) . . ? N002 C009 H00A 109.1 . . ? C00A C009 H00A 109.1 . . ? N002 C009 H00B 109.1 . . ? C00A C009 H00B 109.1 . . ? H00A C009 H00B 107.9 . . ? C009 C00A C00F 112.6(3) . . ? C009 C00A H00C 109.1 . . ? C00F C00A H00C 109.1 . . ? C009 C00A H00D 109.1 . . ? C00F C00A H00D 109.1 . . ? H00C C00A H00D 107.8 . . ? C00G C00B C007 118.2(4) . . ? C00G C00B C00E 124.1(4) . . ? C007 C00B C00E 117.7(4) . . ? C006 C00C C00H 119.8(4) . . ? C006 C00C H00E 120.1 . . ? C00H C00C H00E 120.1 . . ? C005 C00D C00I 120.8(4) . . ? C005 C00D H00F 119.6 . . ? C00I C00D H00F 119.6 . . ? C00H C00E C00B 121.5(4) . . ? C00H C00E H00G 119.3 . . ? C00B C00E H00G 119.3 . . ? C00J C00F C00A 113.7(3) . . ? C00J C00F H00H 108.8 . . ? C00A C00F H00H 108.8 . . ? C00J C00F H00I 108.8 . . ? C00A C00F H00I 108.8 . . ? H00H C00F H00I 107.7 . . ? C00I C00G C00B 121.0(4) . . ? C00I C00G H00J 119.5 . . ? C00B C00G H00J 119.5 . . ? C00E C00H C00C 120.8(4) . . ? C00E C00H H00K 119.6 . . ? C00C C00H H00K 119.6 . . ? C00G C00I C00D 120.6(4) . . ? C00G C00I H00L 119.7 . . ? C00D C00I H00L 119.7 . . ? C00F C00J H00M 109.5 . . ? C00F C00J H00N 109.5 . . ? H00M C00J H00N 109.5 . . ? C00F C00J H00O 109.5 . . ? H00M C00J H00O 109.5 . . ? H00N C00J H00O 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O001 C004 1.221(4) . ? N002 C004 1.382(4) . ? N002 C008 1.395(4) . ? N002 C009 1.472(4) . ? O003 C008 1.211(4) . ? C004 C005 1.468(4) . ? C005 C00D 1.370(5) . ? C005 C007 1.413(4) . ? C006 C00C 1.379(4) . ? C006 C007 1.403(4) . ? C006 C008 1.475(4) . ? C007 C00B 1.413(4) . ? C009 C00A 1.510(4) . ? C009 H00A 0.9700 . ? C009 H00B 0.9700 . ? C00A C00F 1.513(4) . ? C00A H00C 0.9700 . ? C00A H00D 0.9700 . ? C00B C00G 1.408(5) . ? C00B C00E 1.418(5) . ? C00C C00H 1.401(6) . ? C00C H00E 0.9300 . ? C00D C00I 1.386(5) . ? C00D H00F 0.9300 . ? C00E C00H 1.345(6) . ? C00E H00G 0.9300 . ? C00F C00J 1.506(5) . ? C00F H00H 0.9700 . ? C00F H00I 0.9700 . ? C00G C00I 1.357(6) . ? C00G H00J 0.9300 . ? C00H H00K 0.9300 . ? C00I H00L 0.9300 . ? C00J H00M 0.9600 . ? C00J H00N 0.9600 . ? C00J H00O 0.9600 . ?