#------------------------------------------------------------------------------ #$Date: 2025-02-11 01:12:30 +0200 (Tue, 11 Feb 2025) $ #$Revision: 297669 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/38/1573869.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573869 loop_ _publ_author_name 'Gao, Shengxiang' 'Wu, Chunxiao' 'Zhang, Ming' 'Li, Feng' _publ_section_title ; Stable Luminescent Diphenylamine Biphenylmethyl Radicals with \a-Type D₀\\rightarrow D₁ Transition and Antiferromagnetic Properties ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC08026B _journal_year 2025 _chemical_formula_moiety 'C25 H14 Cl6 N' _chemical_formula_sum 'C25 H14 Cl6 N' _chemical_formula_weight 541.07 _chemical_name_systematic 2PhN-BTM _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2024-06-27 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2024-09-16 deposited with the CCDC. 2025-01-30 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 103.423(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 16.4717(16) _cell_length_b 8.3566(9) _cell_length_c 17.0028(18) _cell_measurement_reflns_used 9595 _cell_measurement_temperature 125(2) _cell_measurement_theta_max 27.521 _cell_measurement_theta_min 2.731 _cell_volume 2276.5(4) _computing_cell_refinement 'SAINT V8.40A (?, 2016)' _computing_data_reduction 'SAINT V8.40A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _diffrn_ambient_temperature 125.0 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'CCD area detector' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0321 _diffrn_reflns_av_unetI/netI 0.0139 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 64972 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.548 _diffrn_reflns_theta_min 2.496 _exptl_absorpt_coefficient_mu 0.770 _exptl_absorpt_correction_T_max 27.521 _exptl_absorpt_correction_T_min 2.731 _exptl_crystal_colour 'metallic dark black' _exptl_crystal_colour_lustre metallic _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary black _exptl_crystal_density_diffrn 1.579 _exptl_crystal_description block _exptl_crystal_F_000 1092 _refine_diff_density_max 0.402 _refine_diff_density_min -0.318 _refine_diff_density_rms 0.048 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.056 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 289 _refine_ls_number_reflns 5228 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.056 _refine_ls_R_factor_all 0.0283 _refine_ls_R_factor_gt 0.0248 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0203P)^2^+1.7507P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0577 _refine_ls_wR_factor_ref 0.0595 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4808 _reflns_number_total 5228 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL mo in P21/c #14 mo.res created by SHELXL-2018/3 at 21:05:17 on 27-Jun-2024 REM reset to P21/c #14 CELL 0.71073 16.4717 8.3566 17.0028 90 103.423 90 ZERR 4 0.0016 0.0009 0.0018 0 0.004 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N Cl UNIT 100 56 4 24 L.S. 4 0 0 PLAN 20 TEMP -148.15 BOND fmap 2 53 acta REM REM REM WGHT 0.020300 1.750700 FVAR 0.16178 CL1 4 0.107015 0.920709 0.327310 11.00000 0.02156 0.01246 = 0.02759 0.00129 0.00659 0.00015 CL2 4 0.293115 0.938051 0.247912 11.00000 0.02609 0.02393 = 0.01516 0.00176 0.00540 -0.00701 CL3 4 0.258589 0.607873 0.514623 11.00000 0.02350 0.02404 = 0.02045 0.00754 0.00599 -0.00178 CL4 4 -0.093817 0.479002 0.407237 11.00000 0.01705 0.02464 = 0.03730 -0.00549 0.01253 -0.00560 CL5 4 0.193808 0.286882 0.345893 11.00000 0.02323 0.01253 = 0.04230 0.00355 0.01597 0.00199 CL6 4 0.427516 1.159226 0.545608 11.00000 0.02835 0.03234 = 0.02522 -0.01232 0.00441 -0.01114 C0AA 1 0.361806 0.545352 0.302703 11.00000 0.01567 0.01611 = 0.01653 -0.00372 0.00435 -0.00007 C2 1 0.280956 0.773850 0.382806 11.00000 0.01346 0.01406 = 0.01755 -0.00099 0.00570 0.00093 C3 1 0.294921 0.769018 0.467641 11.00000 0.01480 0.01729 = 0.01870 0.00317 0.00579 0.00193 N1 3 0.273173 0.570175 0.278588 11.00000 0.01573 0.01571 = 0.01484 -0.00063 0.00508 0.00098 C5 1 0.014284 0.684730 0.364498 11.00000 0.01650 0.01750 = 0.02006 -0.00259 0.00377 0.00087 AFIX 43 H5 2 -0.024074 0.767069 0.369202 11.00000 -1.20000 AFIX 0 C6 1 0.412668 0.600435 0.253612 11.00000 0.02036 0.03213 = 0.01578 -0.00101 0.00472 -0.00234 AFIX 43 H6 2 0.388880 0.656121 0.205016 11.00000 -1.20000 AFIX 0 C7 1 0.150210 0.603858 0.339204 11.00000 0.01616 0.01471 = 0.01382 -0.00047 0.00402 -0.00185 C8 1 0.338784 0.886125 0.517646 11.00000 0.01961 0.02573 = 0.01548 -0.00090 0.00395 0.00176 AFIX 43 H8 2 0.345861 0.879641 0.574619 11.00000 -1.20000 AFIX 0 C9 1 0.482678 0.441237 0.396568 11.00000 0.02250 0.02288 = 0.02086 -0.00245 0.00264 0.00483 AFIX 43 H9 2 0.506783 0.387451 0.445659 11.00000 -1.20000 AFIX 0 C10 1 0.360746 1.025520 0.399996 11.00000 0.01588 0.01590 = 0.02128 -0.00116 0.00599 -0.00154 AFIX 43 H10 2 0.383767 1.112808 0.376699 11.00000 -1.20000 AFIX 0 C11 1 0.396731 0.467061 0.375074 11.00000 0.02062 0.01821 = 0.01945 -0.00029 0.00751 0.00220 AFIX 43 H11 2 0.362319 0.431683 0.409382 11.00000 -1.20000 AFIX 0 C12 1 0.160328 0.600459 0.157838 11.00000 0.02256 0.02011 = 0.02007 0.00186 0.00573 0.00190 AFIX 43 H12 2 0.140554 0.691417 0.181250 11.00000 -1.20000 AFIX 0 C13 1 0.315025 0.907899 0.351867 11.00000 0.01631 0.01797 = 0.01444 -0.00072 0.00478 0.00000 C14 1 0.257976 0.381752 0.166147 11.00000 0.02099 0.01600 = 0.02352 -0.00231 0.00662 -0.00169 AFIX 43 H14 2 0.304728 0.323277 0.195503 11.00000 -1.20000 AFIX 0 C15 1 -0.003512 0.526002 0.376546 11.00000 0.01373 0.02187 = 0.01832 -0.00351 0.00400 -0.00414 C16 1 0.050238 0.404367 0.366267 11.00000 0.01771 0.01544 = 0.01969 -0.00012 0.00386 -0.00343 AFIX 43 H16 2 0.035692 0.295504 0.371434 11.00000 -1.20000 AFIX 0 C17 1 0.089710 0.720273 0.345355 11.00000 0.01859 0.01324 = 0.01612 -0.00108 0.00309 -0.00171 C18 1 0.125460 0.444173 0.348347 11.00000 0.01740 0.01400 = 0.01836 -0.00019 0.00496 0.00064 C19 1 0.120000 0.549926 0.080657 11.00000 0.02354 0.03028 = 0.02122 0.00388 0.00122 -0.00170 AFIX 43 H19 2 0.072649 0.606989 0.051448 11.00000 -1.20000 AFIX 0 C20 1 0.229924 0.516819 0.200609 11.00000 0.01692 0.01531 = 0.01579 -0.00002 0.00514 -0.00345 C21 1 0.372036 1.012417 0.483260 11.00000 0.01657 0.02050 = 0.02028 -0.00641 0.00335 -0.00137 C22 1 0.217321 0.333370 0.088940 11.00000 0.03002 0.01968 = 0.02607 -0.00831 0.01007 -0.00744 AFIX 43 H22 2 0.236867 0.242401 0.065342 11.00000 -1.20000 AFIX 0 C23 1 0.233714 0.648755 0.331057 11.00000 0.01764 0.01548 = 0.01956 -0.00126 0.00745 -0.00145 C24 1 0.148262 0.416952 0.045901 11.00000 0.02962 0.03014 = 0.01935 -0.00416 0.00339 -0.01250 AFIX 43 H24 2 0.120590 0.383381 -0.006901 11.00000 -1.20000 AFIX 0 C25 1 0.498267 0.574045 0.275623 11.00000 0.01909 0.04289 = 0.02344 -0.00349 0.00915 -0.00514 AFIX 43 H25 2 0.532892 0.611199 0.241890 11.00000 -1.20000 AFIX 0 C26 1 0.533302 0.493342 0.346943 11.00000 0.01653 0.03402 = 0.02545 -0.00875 0.00322 0.00097 AFIX 43 H26 2 0.591706 0.473965 0.361626 11.00000 -1.20000 AFIX 0 HKLF 4 REM mo in P21/c #14 REM wR2 = 0.0595, GooF = S = 1.056, Restrained GooF = 1.056 for all data REM R1 = 0.0248 for 4808 Fo > 4sig(Fo) and 0.0283 for all 5228 data REM 289 parameters refined using 0 restraints END WGHT 0.0203 1.7507 REM Highest difference peak 0.402, deepest hole -0.318, 1-sigma level 0.048 Q1 1 0.2640 0.5514 0.4759 11.00000 0.05 0.40 Q2 1 0.2584 0.7102 0.3590 11.00000 0.05 0.33 Q3 1 0.4411 1.0796 0.5651 11.00000 0.05 0.32 Q4 1 0.2059 0.6943 0.2989 11.00000 0.05 0.31 Q5 1 0.3601 1.0173 0.4420 11.00000 0.05 0.31 Q6 1 0.1185 0.6563 0.3407 11.00000 0.05 0.30 Q7 1 0.1388 0.5248 0.3385 11.00000 0.05 0.29 Q8 1 0.3399 0.9593 0.3792 11.00000 0.05 0.29 Q9 1 0.3807 0.5036 0.3360 11.00000 0.05 0.29 Q10 1 0.4588 0.6160 0.2786 11.00000 0.05 0.28 Q11 1 0.1976 0.5599 0.1757 11.00000 0.05 0.28 Q12 1 0.0187 0.4631 0.3641 11.00000 0.05 0.28 Q13 1 0.2832 0.7805 0.4213 11.00000 0.05 0.28 Q14 1 0.0022 0.6006 0.3604 11.00000 0.05 0.27 Q15 1 0.3601 0.9412 0.4988 11.00000 0.05 0.27 Q16 1 0.2399 0.4452 0.1850 11.00000 0.05 0.27 Q17 1 0.1376 0.5609 0.1243 11.00000 0.05 0.27 Q18 1 0.1936 0.6198 0.3407 11.00000 0.05 0.26 Q19 1 0.2230 0.3432 0.1368 11.00000 0.05 0.26 Q20 1 0.3121 0.8306 0.4893 11.00000 0.05 0.26 REM The information below was added by Olex2. REM REM R1 = 0.0248 for 4808 Fo > 4sig(Fo) and 0.0283 for all 67187 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.40, deepest hole -0.32 REM Mean Shift 0, Max Shift -0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0283 REM R1_gt = 0.0248 REM wR_ref = 0.0595 REM GOOF = 1.056 REM Shift_max = -0.001 REM Shift_mean = 0 REM Reflections_all = 67187 REM Reflections_gt = 4808 REM Parameters = n/a REM Hole = -0.32 REM Peak = 0.40 REM Flack = n/a ; _cod_data_source_file d4sc08026b2.cif _cod_data_source_block mo _cod_database_code 1573869 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C5(H5), C6(H6), C8(H8), C9(H9), C10(H10), C11(H11), C12(H12), C14(H14), C16(H16), C19(H19), C22(H22), C24(H24), C25(H25), C26(H26) ; _olex2_exptl_crystal_mounting_method no _olex2_submission_original_sample_id 2PhN-BTM _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.10702(2) 0.92071(4) 0.32731(2) 0.02039(8) Uani 1 1 d . . . . . Cl2 Cl 0.29312(2) 0.93805(4) 0.24791(2) 0.02163(8) Uani 1 1 d . . . . . Cl3 Cl 0.25859(2) 0.60787(4) 0.51462(2) 0.02252(8) Uani 1 1 d . . . . . Cl4 Cl -0.09382(2) 0.47900(4) 0.40724(2) 0.02531(8) Uani 1 1 d . . . . . Cl5 Cl 0.19381(2) 0.28688(4) 0.34589(2) 0.02465(8) Uani 1 1 d . . . . . Cl6 Cl 0.42752(2) 1.15923(5) 0.54561(2) 0.02893(9) Uani 1 1 d . . . . . C0AA C 0.36181(8) 0.54535(16) 0.30270(8) 0.0160(3) Uani 1 1 d . . . . . C2 C 0.28096(8) 0.77385(15) 0.38281(8) 0.0147(2) Uani 1 1 d . . . . . C3 C 0.29492(8) 0.76902(16) 0.46764(8) 0.0166(3) Uani 1 1 d . . . . . N1 N 0.27317(7) 0.57017(13) 0.27859(7) 0.0152(2) Uani 1 1 d . . . . . C5 C 0.01428(8) 0.68473(16) 0.36450(8) 0.0181(3) Uani 1 1 d . . . . . H5 H -0.024074 0.767069 0.369202 0.022 Uiso 1 1 calc R . . . . C6 C 0.41267(9) 0.60043(19) 0.25361(8) 0.0227(3) Uani 1 1 d . . . . . H6 H 0.388880 0.656121 0.205016 0.027 Uiso 1 1 calc R . . . . C7 C 0.15021(8) 0.60386(16) 0.33920(8) 0.0148(2) Uani 1 1 d . . . . . C8 C 0.33878(9) 0.88612(18) 0.51765(8) 0.0203(3) Uani 1 1 d . . . . . H8 H 0.345861 0.879641 0.574619 0.024 Uiso 1 1 calc R . . . . C9 C 0.48268(9) 0.44124(18) 0.39657(9) 0.0225(3) Uani 1 1 d . . . . . H9 H 0.506783 0.387451 0.445659 0.027 Uiso 1 1 calc R . . . . C10 C 0.36075(8) 1.02552(16) 0.40000(8) 0.0174(3) Uani 1 1 d . . . . . H10 H 0.383767 1.112808 0.376699 0.021 Uiso 1 1 calc R . . . . C11 C 0.39673(9) 0.46706(17) 0.37507(8) 0.0190(3) Uani 1 1 d . . . . . H11 H 0.362319 0.431683 0.409382 0.023 Uiso 1 1 calc R . . . . C12 C 0.16033(9) 0.60046(17) 0.15784(9) 0.0208(3) Uani 1 1 d . . . . . H12 H 0.140554 0.691417 0.181250 0.025 Uiso 1 1 calc R . . . . C13 C 0.31502(8) 0.90790(16) 0.35187(8) 0.0160(3) Uani 1 1 d . . . . . C14 C 0.25798(9) 0.38175(17) 0.16615(9) 0.0199(3) Uani 1 1 d . . . . . H14 H 0.304728 0.323277 0.195503 0.024 Uiso 1 1 calc R . . . . C15 C -0.00351(8) 0.52600(17) 0.37655(8) 0.0179(3) Uani 1 1 d . . . . . C16 C 0.05024(8) 0.40437(16) 0.36627(8) 0.0177(3) Uani 1 1 d . . . . . H16 H 0.035692 0.295504 0.371434 0.021 Uiso 1 1 calc R . . . . C17 C 0.08971(8) 0.72027(16) 0.34536(8) 0.0161(3) Uani 1 1 d . . . . . C18 C 0.12546(8) 0.44417(16) 0.34835(8) 0.0165(3) Uani 1 1 d . . . . . C19 C 0.12000(10) 0.54993(19) 0.08066(9) 0.0257(3) Uani 1 1 d . . . . . H19 H 0.072649 0.606989 0.051448 0.031 Uiso 1 1 calc R . . . . C20 C 0.22992(8) 0.51682(16) 0.20061(8) 0.0158(3) Uani 1 1 d . . . . . C21 C 0.37204(9) 1.01242(17) 0.48326(8) 0.0193(3) Uani 1 1 d . . . . . C22 C 0.21732(10) 0.33337(18) 0.08894(9) 0.0247(3) Uani 1 1 d . . . . . H22 H 0.236867 0.242401 0.065342 0.030 Uiso 1 1 calc R . . . . C23 C 0.23371(8) 0.64875(16) 0.33106(8) 0.0170(3) Uani 1 1 d . . . . . C24 C 0.14826(10) 0.41695(19) 0.04590(9) 0.0267(3) Uani 1 1 d . . . . . H24 H 0.120590 0.383381 -0.006901 0.032 Uiso 1 1 calc R . . . . C25 C 0.49827(9) 0.5740(2) 0.27562(9) 0.0278(3) Uani 1 1 d . . . . . H25 H 0.532892 0.611199 0.241890 0.033 Uiso 1 1 calc R . . . . C26 C 0.53330(9) 0.4933(2) 0.34694(9) 0.0256(3) Uani 1 1 d . . . . . H26 H 0.591706 0.473965 0.361626 0.031 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.02156(16) 0.01246(14) 0.02759(17) 0.00129(12) 0.00659(13) 0.00015(12) Cl2 0.02609(17) 0.02393(17) 0.01516(15) 0.00176(12) 0.00540(13) -0.00701(13) Cl3 0.02350(16) 0.02404(17) 0.02045(16) 0.00754(13) 0.00599(13) -0.00178(13) Cl4 0.01705(16) 0.02464(17) 0.0373(2) -0.00549(15) 0.01253(14) -0.00560(13) Cl5 0.02323(17) 0.01253(15) 0.0423(2) 0.00355(14) 0.01597(15) 0.00199(12) Cl6 0.02835(18) 0.0323(2) 0.02522(18) -0.01232(15) 0.00441(14) -0.01114(15) C0AA 0.0157(6) 0.0161(6) 0.0165(6) -0.0037(5) 0.0044(5) -0.0001(5) C2 0.0135(6) 0.0141(6) 0.0176(6) -0.0010(5) 0.0057(5) 0.0009(5) C3 0.0148(6) 0.0173(6) 0.0187(6) 0.0032(5) 0.0058(5) 0.0019(5) N1 0.0157(5) 0.0157(5) 0.0148(5) -0.0006(4) 0.0051(4) 0.0010(4) C5 0.0165(6) 0.0175(6) 0.0201(6) -0.0026(5) 0.0038(5) 0.0009(5) C6 0.0204(7) 0.0321(8) 0.0158(6) -0.0010(6) 0.0047(5) -0.0023(6) C7 0.0162(6) 0.0147(6) 0.0138(6) -0.0005(5) 0.0040(5) -0.0019(5) C8 0.0196(6) 0.0257(7) 0.0155(6) -0.0009(5) 0.0040(5) 0.0018(6) C9 0.0225(7) 0.0229(7) 0.0209(7) -0.0025(6) 0.0026(6) 0.0048(6) C10 0.0159(6) 0.0159(6) 0.0213(6) -0.0012(5) 0.0060(5) -0.0015(5) C11 0.0206(7) 0.0182(6) 0.0195(6) -0.0003(5) 0.0075(5) 0.0022(5) C12 0.0226(7) 0.0201(7) 0.0201(7) 0.0019(5) 0.0057(5) 0.0019(6) C13 0.0163(6) 0.0180(6) 0.0144(6) -0.0007(5) 0.0048(5) 0.0000(5) C14 0.0210(7) 0.0160(6) 0.0235(7) -0.0023(5) 0.0066(5) -0.0017(5) C15 0.0137(6) 0.0219(7) 0.0183(6) -0.0035(5) 0.0040(5) -0.0041(5) C16 0.0177(6) 0.0154(6) 0.0197(6) -0.0001(5) 0.0039(5) -0.0034(5) C17 0.0186(6) 0.0132(6) 0.0161(6) -0.0011(5) 0.0031(5) -0.0017(5) C18 0.0174(6) 0.0140(6) 0.0184(6) -0.0002(5) 0.0050(5) 0.0006(5) C19 0.0235(7) 0.0303(8) 0.0212(7) 0.0039(6) 0.0012(6) -0.0017(6) C20 0.0169(6) 0.0153(6) 0.0158(6) 0.0000(5) 0.0051(5) -0.0034(5) C21 0.0166(6) 0.0205(7) 0.0203(6) -0.0064(5) 0.0033(5) -0.0014(5) C22 0.0300(8) 0.0197(7) 0.0261(7) -0.0083(6) 0.0101(6) -0.0074(6) C23 0.0176(6) 0.0155(6) 0.0196(6) -0.0013(5) 0.0074(5) -0.0015(5) C24 0.0296(8) 0.0301(8) 0.0194(7) -0.0042(6) 0.0034(6) -0.0125(6) C25 0.0191(7) 0.0429(9) 0.0234(7) -0.0035(7) 0.0091(6) -0.0051(6) C26 0.0165(6) 0.0340(8) 0.0254(7) -0.0087(6) 0.0032(6) 0.0010(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C6 C0AA N1 119.64(12) . . ? C6 C0AA C11 120.14(13) . . ? C11 C0AA N1 120.21(12) . . ? C3 C2 C13 114.90(12) . . ? C3 C2 C23 122.12(12) . . ? C13 C2 C23 122.98(12) . . ? C2 C3 Cl3 120.04(10) . . ? C8 C3 Cl3 116.80(10) . . ? C8 C3 C2 123.15(13) . . ? C20 N1 C0AA 118.44(11) . . ? C23 N1 C0AA 118.83(11) . . ? C23 N1 C20 122.70(11) . . ? C15 C5 C17 118.15(13) . . ? C25 C6 C0AA 120.04(14) . . ? C17 C7 C18 114.52(12) . . ? C17 C7 C23 121.66(12) . . ? C18 C7 C23 123.62(12) . . ? C21 C8 C3 118.83(13) . . ? C26 C9 C11 120.61(14) . . ? C13 C10 C21 118.18(13) . . ? C9 C11 C0AA 119.32(13) . . ? C19 C12 C20 119.62(14) . . ? C2 C13 Cl2 119.24(10) . . ? C10 C13 Cl2 117.01(10) . . ? C10 C13 C2 123.58(12) . . ? C22 C14 C20 119.83(14) . . ? C5 C15 Cl4 119.22(11) . . ? C5 C15 C16 121.40(13) . . ? C16 C15 Cl4 119.36(11) . . ? C18 C16 C15 118.86(13) . . ? C5 C17 Cl1 116.11(10) . . ? C5 C17 C7 123.71(12) . . ? C7 C17 Cl1 120.18(10) . . ? C7 C18 Cl5 120.41(10) . . ? C16 C18 Cl5 116.22(10) . . ? C16 C18 C7 123.15(12) . . ? C24 C19 C12 120.68(14) . . ? C12 C20 N1 120.13(12) . . ? C12 C20 C14 119.84(13) . . ? C14 C20 N1 120.03(12) . . ? C8 C21 Cl6 119.09(11) . . ? C8 C21 C10 121.32(13) . . ? C10 C21 Cl6 119.58(11) . . ? C14 C22 C24 120.52(14) . . ? N1 C23 C2 117.45(11) . . ? N1 C23 C7 122.10(12) . . ? C7 C23 C2 120.34(11) . . ? C19 C24 C22 119.50(14) . . ? C6 C25 C26 120.10(14) . . ? C9 C26 C25 119.76(14) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C17 1.7382(14) . ? Cl2 C13 1.7383(13) . ? Cl3 C3 1.7412(14) . ? Cl4 C15 1.7319(14) . ? Cl5 C18 1.7374(14) . ? Cl6 C21 1.7362(14) . ? C0AA N1 1.4369(17) . ? C0AA C6 1.391(2) . ? C0AA C11 1.3945(19) . ? C2 C3 1.4075(18) . ? C2 C13 1.4084(18) . ? C2 C23 1.4679(18) . ? C3 C8 1.3847(19) . ? N1 C20 1.4233(17) . ? N1 C23 1.3852(17) . ? C5 C15 1.3839(19) . ? C5 C17 1.3876(19) . ? C6 C25 1.390(2) . ? C7 C17 1.4138(18) . ? C7 C18 1.4144(18) . ? C7 C23 1.4630(18) . ? C8 C21 1.380(2) . ? C9 C11 1.394(2) . ? C9 C26 1.387(2) . ? C10 C13 1.3845(18) . ? C10 C21 1.3887(19) . ? C12 C19 1.392(2) . ? C12 C20 1.3944(19) . ? C14 C20 1.3987(19) . ? C14 C22 1.388(2) . ? C15 C16 1.3854(19) . ? C16 C18 1.3835(19) . ? C19 C24 1.389(2) . ? C22 C24 1.390(2) . ? C25 C26 1.390(2) . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -3 0 0 12.79 0.41 -3 0 0 12.63 0.4 -3 0 0 12.6 0.43 -3 0 0 13.04 0.38 -3 0 0 12.78 0.4 3 0 0 12.5 0.44 3 0 0 12.18 0.43 3 0 0 12.5 0.38 3 0 0 11.84 0.38 4 0 0 3.71 0.23 4 0 0 3.5 0.2 4 0 0 3.82 0.22 -4 0 0 3.96 0.23 -4 0 0 4.12 0.24 -4 0 0 3.63 0.22 -4 0 0 4.15 0.29 -4 0 0 3.46 0.2 4 0 0 4.29 0.33 -5 0 0 300.25 7.36 -5 0 0 313.62 7.38 -5 0 0 303.74 7.42 -5 0 0 301.86 7.34 -5 0 0 292.56 7.37 5 0 0 306.35 7.37 5 0 0 303.38 7.41 5 0 0 300.43 7.32 5 0 0 313.74 7.37 -6 0 0 245.63 6.11 6 0 0 252.17 6.11 6 0 0 254.21 6 6 0 0 240.99 6.02 -6 0 0 250.03 6.06 -6 0 0 238.34 6.02 6 0 0 252.85 6.06 -6 0 0 252.55 6.07 -6 0 0 237.78 6.05 -7 0 0 92.73 2.36 7 0 0 94.55 2.4 -7 0 0 90.13 2.46 -7 0 0 91.87 2.41 -7 0 0 88.32 2.39 -7 0 0 89.55 2.39 7 0 0 91.85 2.45 7 0 0 90.74 2.33 7 0 0 90.96 2.32 -8 0 0 117.51 3.06 8 0 0 114.62 3.05 -8 0 0 128.54 3.63 8 0 0 116.04 3.11 8 0 0 120.68 2.96 -8 0 0 121.17 3.08 -8 0 0 111.95 3.05 -8 0 0 111.97 3.01 -9 0 0 6.78 0.43 -9 0 0 6.3 0.38 9 0 0 7.73 0.43 9 0 0 6.14 0.33 -9 0 0 7.2 0.52 -9 0 0 7.03 0.51 9 0 0 6.26 0.48 -9 0 0 7.68 0.43 -10 0 0 182.22 4.51 10 0 0 175.03 4.56 10 0 0 166.94 4.34 -10 0 0 166.1 4.55 -10 0 0 170.23 4.43 -10 0 0 174.85 4.49 -10 0 0 181.21 4.49 10 0 0 179.38 4.48 -11 0 0 115.7 3.03 11 0 0 107.79 3.11 -11 0 0 110.96 3.01 -11 0 0 111.68 3.12 -11 0 0 104.81 2.99 11 0 0 108.77 3.08 -11 0 0 116.02 2.97 -12 0 0 5.72 0.47 -12 0 0 5.07 0.6 12 0 0 5.51 0.51 12 0 0 5.29 0.48 -12 0 0 6 0.47 -12 0 0 5.27 0.43 -12 0 0 5.56 0.47 12 0 0 4.86 0.56 -13 0 0 68.61 2.06 13 0 0 68.46 2.13 -13 0 0 68.99 1.99 -13 0 0 68.46 2.07 13 0 0 62.82 2 13 0 0 66.4 2.02 -13 0 0 69.32 2.17 -13 0 0 64.3 2.02 -14 0 0 3.68 0.43 14 0 0 5.08 0.53 -14 0 0 3.71 0.5 -14 0 0 4.5 0.54 -14 0 0 4.07 0.49 14 0 0 4.53 0.56 14 0 0 3.61 0.49 -15 0 0 37.27 1.43 -15 0 0 40.34 1.44 -15 0 0 40.37 1.59 -15 0 0 37.22 1.37 15 0 0 40.29 1.55 -15 0 0 38.9 1.46 15 0 0 40.33 1.43 -16 0 0 1.22 0.35 -16 0 0 2.06 0.38 -16 0 0 1.12 0.42 -16 0 0 2.06 0.42 16 0 0 1.65 0.44 16 0 0 1.39 0.39 -16 0 0 1.76 0.39 17 0 0 0.49 0.37 -17 0 0 0.41 0.41 17 0 0 -0.36 0.4 17 0 0 0.01 0.42 -17 0 0 -0.18 0.32 -17 0 0 -0.21 0.3 -17 0 0 0.23 0.36 -17 0 0 0.79 0.34 -18 0 0 6.82 0.91 18 0 0 6.74 0.85 -18 0 0 7.48 0.76 18 0 0 8.47 0.86 18 0 0 7.5 0.84 -18 0 0 8.1 0.78 -18 0 0 7.21 0.73 -18 0 0 7.26 0.79 19 0 0 28.64 1.79 -19 0 0 25.98 1.34 -19 0 0 27.72 1.31 -19 0 0 25.73 1.5 -19 0 0 29.84 1.41 19 0 0 27.12 1.37 -19 0 0 26.6 1.31 -20 0 0 27.96 1.39 -20 0 0 26.51 1.54 -20 0 0 29.01 1.38 -20 0 0 28.03 1.45 20 0 0 25.8 1.59 -20 0 0 28.48 1.62 -1 -1 0 205.37 4.8 1 -1 0 196.6 4.86 -1 -1 0 198 4.81 -1 -1 0 191.1 4.8 -1 -1 0 201.79 4.81 1 -1 0 197.57 4.82 -1 1 0 202.42 4.89 -1 1 0 202.56 4.96 -2 -1 0 0.23 0.07 -2 -1 0 0.41 0.08 2 -1 0 0.31 0.09 -2 -1 0 0.31 0.07 -2 -1 0 0.23 0.07 2 -1 0 0.32 0.08 2 -1 0 0.32 0.09 2 -1 0 0.2 0.09 2 -1 0 0.25 0.09 -2 1 0 0.18 0.06 2 1 0 0.32 0.07 -2 1 0 0.26 0.09 -2 1 0 0.27 0.1 2 1 0 0.3 0.06 -2 1 0 0.17 0.1 -2 1 0 0.03 0.08 2 1 0 0.45 0.07 3 -1 0 49.04 1.33 -3 -1 0 49.07 1.29 3 -1 0 47.77 1.36 -3 -1 0 53.46 1.29 3 -1 0 50.3 1.3 3 -1 0 50.36 1.33 -3 -1 0 48.57 1.27 -3 -1 0 50.45 1.26 3 1 0 48.43 1.29 -3 1 0 48.81 1.34 -3 1 0 48.75 1.37 -3 1 0 50.34 1.33 -3 1 0 49.9 1.33 4 -1 0 918.66 21.08 -4 -1 0 846.33 20.99 4 -1 0 863.03 21.11 4 1 0 879.3 21.03 -4 1 0 868.87 21.07 -4 1 0 867.54 21.12 -4 1 0 928.42 21.08 -5 -1 0 1.28 0.14 5 -1 0 1.03 0.18 -5 -1 0 1.63 0.19 -5 -1 0 1.21 0.15 -5 -1 0 1.25 0.16 5 -1 0 1.06 0.17 5 -1 0 1.05 0.15 5 -1 0 1.08 0.2 5 1 0 1.59 0.2 5 1 0 1.29 0.16 -5 1 0 0.85 0.16 -5 1 0 0.93 0.18 -5 1 0 1.1 0.18 -5 1 0 1.17 0.16 5 1 0 1.49 0.16 -5 1 0 1.43 0.17 6 -1 0 335.38 7.83 -6 -1 0 322.79 7.83 6 -1 0 323.68 7.89 6 -1 0 315.85 7.95 -6 -1 0 311.68 7.82 -6 -1 0 329.81 7.84 -6 -1 0 314.44 7.8 6 -1 0 323.47 7.89 -6 -1 0 324.32 7.86 -6 1 0 325.47 7.9 -6 1 0 318.97 7.89 -6 1 0 323.89 7.97 6 1 0 334.02 7.84 6 1 0 315.55 7.83 6 1 0 314.8 7.83 -6 1 0 318.38 7.85 -6 1 0 331.35 7.9 -7 -1 0 134.12 3.35 -7 -1 0 130.57 3.28 7 -1 0 132.72 3.38 7 -1 0 133.39 3.37 -7 -1 0 130.52 3.33 -7 -1 0 127.95 3.3 7 -1 0 131.89 3.45 7 -1 0 127.28 3.3 -7 -1 0 130.24 3.31 7 1 0 128.91 3.32 7 1 0 129.11 3.32 7 1 0 130.16 3.32 -7 1 0 130.34 3.37 -7 1 0 130.65 3.38 -7 1 0 129.61 3.32 -7 1 0 129.78 3.48 -7 1 0 131.88 3.38 -8 -1 0 8.35 0.47 8 -1 0 7.56 0.47 -8 -1 0 8.43 0.42 8 -1 0 7.76 0.44 -8 -1 0 8.98 0.46 8 -1 0 7.76 0.39 8 -1 0 7.85 0.51 -8 -1 0 8.38 0.42 8 -1 0 8.15 0.42 -8 -1 0 7.98 0.39 -8 1 0 7.89 0.46 -8 1 0 7.89 0.45 8 1 0 8.82 0.43 -8 1 0 7.29 0.46 -8 1 0 7.45 0.4 8 1 0 9.18 0.47 8 1 0 9.14 0.44 -8 1 0 8.17 0.55 -9 -1 0 37 1.13 9 -1 0 32.43 1.13 9 -1 0 31.92 1.06 9 -1 0 33.26 1.21 -9 -1 0 33.45 1.13 -9 -1 0 32.66 1.07 -9 -1 0 34.41 1.09 9 -1 0 33.31 1.04 -9 -1 0 31.69 1.04 9 -1 0 35.46 1.13 9 1 0 36.77 1.09 -9 1 0 31.03 1.06 -9 1 0 35.09 1.24 -9 1 0 34.42 1.13 9 1 0 34.15 1.08 -9 1 0 33.06 1.13 9 1 0 33.8 1.11 -9 1 0 35.53 1.14 -10 -1 0 19.74 0.77 -10 -1 0 20.07 0.81 -10 -1 0 21.29 0.85 10 -1 0 21.57 0.77 10 -1 0 19.83 0.81 -10 -1 0 20.46 0.78 10 -1 0 20.57 0.91 10 -1 0 19.24 0.82 10 -1 0 20.12 0.73 -10 -1 0 20.1 0.75 10 1 0 21.19 0.79 -10 1 0 20.57 0.93 10 1 0 20.51 0.79 -10 1 0 21.59 0.84 -10 1 0 20.65 0.84 10 1 0 19.37 0.82 -10 1 0 20.26 0.83 -10 1 0 20.39 0.77 11 -1 0 2.92 0.45 -11 -1 0 2.81 0.33 11 -1 0 2.69 0.34 -11 -1 0 2.65 0.35 -11 -1 0 2.4 0.31 11 -1 0 3.09 0.36 11 -1 0 3.83 0.5 -11 -1 0 2.9 0.36 -11 -1 0 3.01 0.37 -11 1 0 3.07 0.44 -11 1 0 3.04 0.38 -11 1 0 3.36 0.41 11 1 0 2.74 0.58 -11 1 0 3.39 0.37 -11 1 0 3.29 0.39 11 1 0 2.97 0.34 11 1 0 2.71 0.33 12 -1 0 1.01 0.3 -12 -1 0 0.62 0.23 12 -1 0 0.42 0.25 12 -1 0 0.7 0.24 -12 -1 0 0.74 0.24 -12 -1 0 0.95 0.23 12 -1 0 0.74 0.25 -12 -1 0 0.78 0.26 -12 -1 0 0.93 0.29 -12 1 0 0.92 0.27 -12 1 0 0.58 0.32 12 1 0 1.11 0.28 12 1 0 0.09 0.24 -12 1 0 0.78 0.23 12 1 0 1.03 0.26 -12 1 0 0.31 0.22 -12 1 0 0.38 0.22 -13 -1 0 28.25 1.06 -13 -1 0 24.9 1.02 -13 -1 0 27.24 1 13 -1 0 27.59 1.11 13 -1 0 30.4 1.08 13 -1 0 27.05 0.95 -13 -1 0 28.19 1.09 -13 -1 0 26.53 1.13 13 -1 0 26.89 1.22 13 -1 0 24.86 1.22 -13 1 0 28.03 1.1 13 1 0 27.98 1.05 13 1 0 27.44 1.12 13 1 0 26.1 1.03 -13 1 0 26.7 1.12 -13 1 0 27.28 1.1 -13 1 0 26.47 1.24 -13 1 0 27.36 1.07 -14 -1 0 41.93 1.54 14 -1 0 44.08 1.65 14 -1 0 39.76 1.63 -14 -1 0 42.33 1.47 -14 -1 0 43.04 1.43 -14 -1 0 39.41 1.38 -14 -1 0 41.26 1.47 14 1 0 42.48 1.42 -14 1 0 43.34 1.66 14 1 0 40.82 1.5 14 1 0 39.01 1.41 -14 1 0 42.53 1.51 -14 1 0 44.33 1.55 -14 1 0 42.45 1.52 -14 1 0 42.17 1.44 -15 -1 0 7.17 0.6 -15 -1 0 8.72 0.65 -15 -1 0 8.08 0.75 15 -1 0 7.4 0.79 -15 -1 0 7.2 0.59 -15 -1 0 8.91 0.66 -15 1 0 7.25 0.83 15 1 0 8.23 0.87 -15 1 0 6.58 0.63 15 1 0 6.67 0.62 -15 1 0 7.78 0.7 15 1 0 9.22 0.63 -15 1 0 7.96 0.69 -15 1 0 7.93 0.63 -16 -1 0 1.02 0.35 -16 -1 0 1.12 0.33 -16 -1 0 0.77 0.33 -16 -1 0 1.05 0.33 16 -1 0 0.76 0.41 -16 -1 0 0.61 0.37 -16 1 0 0.79 0.36 -16 1 0 0.98 0.55 -16 1 0 0.68 0.36 16 1 0 0.59 0.36 -16 1 0 1.6 0.35 -16 1 0 0.79 0.35 17 -1 0 38.49 1.6 -17 -1 0 33.66 1.33 -17 -1 0 32.84 1.34 -17 -1 0 36.97 1.44 -17 -1 0 34.02 1.41 17 -1 0 29.83 1.51 -17 -1 0 35.25 1.52 -17 1 0 35.76 1.65 17 1 0 34.6 1.37 -17 1 0 32.88 1.36 -17 1 0 34.95 1.51 -17 1 0 35.66 1.43 -17 1 0 33.28 1.44 17 1 0 34.68 1.46 17 1 0 32.79 1.36 -18 -1 0 3.9 0.56 -18 -1 0 4.55 0.63 18 -1 0 4.08 0.58 -18 -1 0 4.41 0.56 18 -1 0 4.31 1.01 -18 -1 0 4.41 0.55 18 -1 0 3.35 0.64 -18 -1 0 4.07 0.61 -18 1 0 4.69 0.62 -18 1 0 5.13 0.6 18 1 0 4.52 0.57 -18 1 0 4.65 0.65 -18 1 0 4.14 0.55 18 1 0 3.49 0.57 -18 1 0 3.68 0.63 18 1 0 4.8 0.61 19 -1 0 0.06 0.6 -19 -1 0 0.66 0.4 -19 -1 0 -0.25 0.41 -19 -1 0 0.29 0.44 19 -1 0 -0.18 0.43 -19 -1 0 -0.31 0.46 -19 1 0 -0.38 0.41 19 1 0 0.23 0.43 -19 1 0 0.44 0.45 -19 1 0 0.96 0.44 19 1 0 -0.36 0.49 -19 1 0 0.24 0.45 -19 1 0 -0.06 0.55 -20 -1 0 3.8 0.74 -20 -1 0 4.86 0.65 -20 -1 0 5.08 0.65 -20 -1 0 5.44 0.72 -20 1 0 3.99 0.76 -20 1 0 4.65 0.73 -20 1 0 4.74 0.71 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5.25 -4 -2 0 213.43 5.11 -4 -2 0 220.81 5.17 4 -2 0 202.62 5.16 4 2 0 209.44 5.16 -4 2 0 209.77 5.22 -4 2 0 204.11 5.25 4 2 0 211.54 5.09 -4 2 0 207.78 5.24 -4 2 0 211.64 5.18 -4 2 0 212.49 5.22 5 -2 0 451.25 11.16 5 -2 0 462.36 11.12 5 -2 0 471.97 11.06 -5 -2 0 449.52 11.02 -5 -2 0 449.36 11.03 -5 -2 0 459.62 11 5 -2 0 470.54 11.13 5 -2 0 435.02 11.09 -5 -2 0 449.69 11.08 -5 2 0 453.48 11.13 -5 2 0 446.13 11.19 -5 2 0 469.38 11.07 5 2 0 466.89 11.03 -5 2 0 462.08 11.12 5 2 0 475.42 11.05 -5 2 0 443.96 11.12 6 -2 0 16.45 0.67 -6 -2 0 18.32 0.61 6 -2 0 16.91 0.68 -6 -2 0 17.81 0.63 6 -2 0 16.73 0.73 -6 -2 0 17.68 0.62 6 -2 0 17.12 0.62 -6 -2 0 17.35 0.58 6 -2 0 16.26 0.69 -6 2 0 17.32 0.7 -6 2 0 17.17 0.76 -6 2 0 16.65 0.71 -6 2 0 17.3 0.64 -6 2 0 19.22 0.88 6 2 0 17.26 0.61 6 2 0 17.92 0.63 7 -2 0 1.77 0.25 7 -2 0 2.54 0.31 -7 -2 0 1.78 0.22 7 -2 0 1.82 0.27 7 -2 0 1.75 0.28 -7 -2 0 2.17 0.25 -7 -2 0 2.14 0.23 -7 -2 0 1.82 0.21 7 2 0 1.93 0.25 -7 2 0 2.05 0.27 -7 2 0 1.54 0.24 -7 2 0 1.49 0.28 -7 2 0 1.75 0.26 7 2 0 2.18 0.26 -7 2 0 1.79 0.23 -8 -2 0 345.76 8.58 -8 -2 0 334.47 8.54 8 -2 0 353.18 8.59 8 -2 0 352.77 8.69 -8 -2 0 345.57 8.58 -8 -2 0 349.19 8.53 -8 -2 0 343.38 8.61 8 -2 0 364.16 8.65 8 -2 0 350.77 8.69 8 -2 0 342.27 8.76 -8 2 0 363.05 8.72 8 2 0 337.57 8.57 -8 2 0 349.86 8.69 -8 2 0 365.88 8.63 -8 2 0 350.4 8.7 8 2 0 366.3 8.59 -8 2 0 349.83 8.79 -9 -2 0 1.31 0.22 9 -2 0 1.44 0.3 9 -2 0 1.24 0.24 9 -2 0 1.47 0.23 -9 -2 0 1.13 0.26 -9 -2 0 1.58 0.25 9 -2 0 1.54 0.25 9 -2 0 1.69 0.3 -9 -2 0 1.13 0.2 -9 -2 0 1.16 0.22 -9 2 0 1.45 0.32 9 2 0 1.61 0.24 -9 2 0 0.8 0.2 9 2 0 1.25 0.23 -9 2 0 1.77 0.3 -9 2 0 1.14 0.26 9 2 0 1.03 0.19 -9 2 0 1.35 0.27 10 -2 0 1.94 0.33 10 -2 0 1.7 0.27 10 -2 0 2.01 0.28 10 -2 0 1.78 0.35 -10 -2 0 2.67 0.32 -10 -2 0 2.18 0.29 -10 -2 0 2.74 0.31 -10 -2 0 2.37 0.28 -10 -2 0 2.36 0.3 10 -2 0 1.86 0.31 -10 2 0 1.43 0.3 -10 2 0 1.96 0.37 -10 2 0 1.22 0.24 10 2 0 2.15 0.27 -10 2 0 1.67 0.31 -10 2 0 1.48 0.29 10 2 0 1.93 0.28 10 2 0 2.15 0.28 11 -2 0 11.98 1.29 11 -2 0 12.95 0.69 -11 -2 0 12.06 0.59 11 -2 0 12.32 0.59 -11 -2 0 11.47 0.6 11 -2 0 11.25 0.62 11 -2 0 12.03 0.72 -11 -2 0 14.01 0.66 -11 -2 0 14.83 0.63 -11 2 0 12.09 0.71 -11 2 0 11.85 0.85 -11 2 0 10.99 0.69 -11 2 0 12.31 0.7 11 2 0 12.52 0.63 11 2 0 13.29 0.63 -11 2 0 11.63 0.63 11 2 0 13.23 0.63 -12 -2 0 0.12 0.23 -12 -2 0 1.11 0.26 -12 -2 0 0.67 0.23 -12 -2 0 0.42 0.2 12 -2 0 0.29 0.19 12 -2 0 0 0.22 12 -2 0 0.29 0.31 -12 -2 0 0.37 0.2 12 -2 0 0.31 0.23 12 -2 0 -0.06 0.27 -12 2 0 0.68 0.31 -12 2 0 0.23 0.25 -12 2 0 0.36 0.26 -12 2 0 -0.31 0.22 12 2 0 0.11 0.2 12 2 0 0.44 0.25 12 2 0 0.21 0.24 -13 -2 0 17.83 0.82 13 -2 0 18.07 0.8 -13 -2 0 17.95 0.85 -13 -2 0 16.65 0.77 -13 -2 0 15.89 0.75 13 -2 0 18.97 0.87 13 -2 0 17.27 0.73 13 -2 0 18.92 0.93 13 -2 0 15.81 0.98 -13 -2 0 16.8 0.82 -13 2 0 17.77 0.84 -13 2 0 17.19 1.07 13 2 0 16.28 0.82 -13 2 0 17.97 0.9 13 2 0 17.57 0.8 -13 2 0 17.41 0.9 -13 2 0 17.47 0.9 13 2 0 15.98 0.79 14 -2 0 5.04 0.63 14 -2 0 5.36 0.56 -14 -2 0 6.34 0.52 -14 -2 0 6.45 0.63 -14 -2 0 5.97 0.51 -14 -2 0 6.27 0.68 -14 -2 0 6.07 0.54 14 -2 0 5.52 0.46 14 -2 0 4.94 0.59 14 -2 0 5.57 0.53 -14 2 0 5.89 0.63 -14 2 0 5.71 0.56 -14 2 0 6.18 0.74 -14 2 0 4.54 0.89 14 2 0 5.45 0.54 14 2 0 5.39 0.55 -14 2 0 5.5 0.6 14 2 0 5.68 0.64 15 -2 0 29.4 1.42 -15 -2 0 27.22 1.12 -15 -2 0 31.21 1.2 15 -2 0 30.34 1.25 15 -2 0 28.67 1.05 -15 -2 0 27.35 1.12 -15 -2 0 29.68 1.23 -15 -2 0 29.35 1.19 15 -2 0 28.83 1.08 -15 2 0 28.81 1.21 -15 2 0 31.41 1.31 -15 2 0 28.76 1.3 -15 2 0 28.42 1.28 15 2 0 29.54 1.18 15 2 0 29.25 1.13 -16 -2 0 12.66 0.76 -16 -2 0 15.38 0.86 -16 -2 0 14.47 0.86 -16 -2 0 12.85 0.78 -16 -2 0 14.09 0.9 16 -2 0 15.09 0.91 -16 2 0 14.74 1.11 16 2 0 13.66 0.83 -16 2 0 14.62 1.11 -16 2 0 13.79 0.93 16 2 0 12.5 0.83 -16 2 0 13.93 0.9 -16 2 0 12.07 0.84 16 2 0 13.98 0.78 17 -2 0 3.17 0.53 -17 -2 0 4.08 0.54 17 -2 0 3.15 1 -17 -2 0 3.54 0.51 -17 -2 0 4.4 0.55 -17 -2 0 3.79 0.49 -17 -2 0 3.73 0.48 17 -2 0 4.3 0.64 17 2 0 3.01 0.48 17 2 0 4.08 0.51 17 2 0 4.9 0.55 -17 2 0 4.03 0.58 -17 2 0 2.83 0.47 -17 2 0 2.95 0.58 -17 2 0 3.4 0.62 -17 2 0 3.27 0.54 -18 -2 0 6.35 0.7 18 -2 0 5.45 0.77 -18 -2 0 6.62 0.86 -18 -2 0 6.11 0.73 -18 -2 0 7.25 0.91 -18 -2 0 5.85 0.68 -18 2 0 8.57 0.88 -18 2 0 6.92 0.82 -18 2 0 5.5 0.7 18 2 0 5.35 0.56 18 2 0 4.59 0.61 -18 2 0 5.88 0.82 -19 -2 0 14.09 0.98 -19 -2 0 13.59 1.07 -19 -2 0 14.62 1.03 -19 -2 0 13.15 0.95 -19 -2 0 13.36 0.91 19 2 0 12.71 0.95 19 2 0 13.15 0.99 -19 2 0 14.04 1.08 -19 2 0 15.76 1.15 -19 2 0 13.17 1.02 -19 2 0 15.03 1.08 -19 2 0 14.93 1.31 -20 -2 0 5.83 0.68 -20 -2 0 6.41 0.77 -20 -2 0 6.71 0.73 -20 -2 0 8.54 1.22 -20 -2 0 7.25 0.79 -20 2 0 6.33 0.8 -20 2 0 6.81 0.82 -20 2 0 5.76 0.88 -20 2 0 4.87 0.82 20 2 0 4.33 0.68 0 -3 0 0.14 0.13 0 -3 0 0.29 0.16 0 -3 0 0.51 0.13 0 -3 0 0.18 0.11 0 -3 0 0.1 0.12 0 3 0 0.53 0.16 0 3 0 0.22 0.12 0 3 0 0.28 0.15 0 3 0 0.45 0.15 0 3 0 0.33 0.14 1 -3 0 751 18.11 1 -3 0 717.88 17.89 -1 -3 0 759.08 17.96 -1 -3 0 737.48 17.94 -1 -3 0 741.72 17.92 1 -3 0 740.32 17.98 -1 -3 0 749.41 17.81 1 -3 0 730.17 17.94 1 -3 0 793.72 17.94 -1 -3 0 768.27 17.93 -1 3 0 712.57 17.93 -1 3 0 747.68 17.98 1 3 0 735.39 17.95 1 3 0 735.25 17.9 1 3 0 760.89 17.92 1 3 0 777.84 17.95 -1 3 0 730.44 17.9 -2 -3 0 48.47 1.39 -2 -3 0 49.01 1.37 2 -3 0 45.78 1.4 2 -3 0 48.57 1.39 2 -3 0 48.64 1.38 -2 -3 0 47.33 1.37 -2 -3 0 49.36 1.36 2 -3 0 47.39 1.41 -2 3 0 46.72 1.42 -2 3 0 47.67 1.38 -2 3 0 49.52 1.43 2 3 0 46.16 1.34 2 3 0 48.01 1.38 2 3 0 46.63 1.34 2 3 0 48.04 1.39 -2 3 0 47.04 1.4 3 -3 0 71.36 2 3 -3 0 72.54 1.98 3 -3 0 69.72 1.97 -3 -3 0 68.55 1.91 3 -3 0 70.62 1.99 3 -3 0 74.93 2.25 -3 -3 0 70.73 1.9 -3 -3 0 70.47 1.91 3 3 0 69.5 1.88 -3 3 0 68.31 1.99 3 3 0 72.65 1.87 3 3 0 71.35 1.92 3 3 0 71.95 1.94 -3 3 0 69.53 2.34 -3 3 0 70.7 1.99 -4 -3 0 13.73 0.54 4 -3 0 14.51 0.63 4 -3 0 13.79 0.56 4 -3 0 14.52 0.63 -4 -3 0 14.02 0.57 4 -3 0 14.13 0.61 -4 -3 0 14.01 0.55 -4 -3 0 14.36 0.55 -4 3 0 13.89 0.77 -4 3 0 14.23 0.63 4 3 0 14.09 0.51 4 3 0 14.24 0.57 -4 3 0 13.6 0.62 -4 3 0 13.49 0.57 -4 3 0 14.33 0.63 4 3 0 13.81 0.5 5 -3 0 2.19 0.3 5 -3 0 2.04 0.26 5 -3 0 1.93 0.28 -5 -3 0 1.97 0.25 -5 -3 0 2.22 0.25 5 -3 0 2.31 0.26 -5 -3 0 2.79 0.26 -5 -3 0 2.05 0.24 5 -3 0 2.04 0.28 -5 3 0 2.22 0.45 5 3 0 1.98 0.22 -5 3 0 1.38 0.25 5 3 0 2.31 0.26 -5 3 0 2.17 0.26 5 3 0 2.02 0.21 -5 3 0 2.61 0.33 -5 3 0 2.04 0.28 -6 -3 0 54.19 1.53 -6 -3 0 52.49 1.5 6 -3 0 52.18 1.58 6 -3 0 53.11 1.61 6 -3 0 51.56 1.61 6 -3 0 52.29 1.65 6 -3 0 52.02 1.53 -6 -3 0 51.56 1.5 -6 -3 0 53.12 1.48 6 3 0 54.21 1.5 -6 3 0 50.56 1.6 -6 3 0 50.3 1.61 -6 3 0 53.14 1.67 -6 3 0 51.15 1.61 -7 -3 0 34.38 1.03 7 -3 0 30.85 1.12 7 -3 0 31.55 1.17 -7 -3 0 33.24 1.05 7 -3 0 32.24 1.05 -7 -3 0 30.71 1.01 7 -3 0 30.94 1.09 -7 -3 0 31.75 0.99 7 -3 0 30.63 1.12 7 3 0 30.35 1.02 7 3 0 32.61 1.02 -7 3 0 30.78 1.07 -7 3 0 29.86 1.12 -7 3 0 30.3 1.13 -7 3 0 30.83 1.11 -7 3 0 31.69 1.2 -8 -3 0 7.09 0.43 -8 -3 0 6.96 0.4 8 -3 0 7.48 0.44 -8 -3 0 7.09 0.45 8 -3 0 6.18 0.48 8 -3 0 7.34 0.53 8 -3 0 7.24 0.5 8 -3 0 6.43 0.59 8 3 0 6.21 0.42 8 3 0 6.16 0.43 -8 3 0 6.92 0.47 -8 3 0 7.46 0.53 -8 3 0 7.43 0.53 -8 3 0 7.15 0.52 -8 3 0 7.74 0.64 9 -3 0 46.22 1.49 9 -3 0 44.99 1.61 9 -3 0 46.83 1.42 -9 -3 0 44.73 1.42 -9 -3 0 43.6 1.39 -9 -3 0 43.4 1.4 -9 -3 0 44.29 1.36 9 -3 0 47.24 1.55 9 -3 0 46.99 1.53 -9 3 0 47.19 1.55 -9 3 0 46.12 1.55 9 3 0 45.4 1.39 -9 3 0 44.9 1.46 9 3 0 47.21 1.42 -9 3 0 46.85 1.57 -9 3 0 46.87 1.65 -10 -3 0 0.81 0.23 10 -3 0 0.66 0.31 -10 -3 0 1.13 0.25 10 -3 0 0.85 0.28 10 -3 0 0.8 0.26 -10 -3 0 1.16 0.25 -10 -3 0 1.1 0.23 10 -3 0 1.01 0.22 -10 3 0 1.38 0.32 -10 3 0 0.74 0.28 -10 3 0 1.3 0.39 10 3 0 1.34 0.25 10 3 0 1.02 0.26 -10 3 0 1.02 0.26 -10 3 0 0.8 0.27 11 -3 0 12.06 0.71 11 -3 0 12.01 0.62 11 -3 0 12.91 0.79 -11 -3 0 10.59 0.61 -11 -3 0 11.68 0.6 11 -3 0 11.39 0.83 -11 -3 0 10.72 0.62 -11 -3 0 10.61 0.57 11 -3 0 11.75 0.68 -11 3 0 11.94 0.66 -11 3 0 11.51 0.73 -11 3 0 12.29 0.73 11 3 0 10.25 0.59 11 3 0 12.27 0.63 -11 3 0 12.17 0.86 -11 3 0 11.78 0.73 12 -3 0 69.4 1.99 -12 -3 0 67.67 1.97 12 -3 0 66.87 2.12 -12 -3 0 68.59 1.97 12 -3 0 67.17 2.16 12 -3 0 68.09 2.05 12 -3 0 63.95 2.24 -12 -3 0 68.03 2.03 -12 -3 0 67.51 2.03 -12 3 0 64.77 2.16 -12 3 0 70.2 2.32 12 3 0 65.15 1.97 -12 3 0 63.1 2.12 -12 3 0 65.92 2.06 -12 3 0 67.11 2.16 -13 -3 0 27.94 1.11 13 -3 0 28.49 1.06 13 -3 0 29.44 1.26 13 -3 0 30.28 1.21 13 -3 0 27.8 1.33 13 -3 0 28.95 1.14 -13 -3 0 28.73 1.07 -13 -3 0 26.18 1.08 -13 -3 0 26.08 1.04 -13 3 0 29.1 1.24 13 3 0 28.18 1.06 -13 3 0 26.22 1.13 13 3 0 28.58 1.07 -13 3 0 26.94 1.22 -13 3 0 28.39 1.24 -13 3 0 29.24 1.42 -14 -3 0 1.94 0.33 -14 -3 0 2.68 0.39 14 -3 0 1.52 0.38 -14 -3 0 2.46 0.37 14 -3 0 2.5 0.36 14 -3 0 2.51 0.43 14 -3 0 1.88 0.46 -14 -3 0 2.32 0.34 -14 -3 0 2.66 0.38 14 -3 0 0.55 0.45 -14 3 0 2.54 0.46 -14 3 0 1.81 0.43 -14 3 0 1.55 0.39 14 3 0 1.85 0.34 -14 3 0 1.3 0.44 -14 3 0 1.96 0.41 14 3 0 1.99 0.38 15 -3 0 5.12 0.66 -15 -3 0 6.85 0.62 -15 -3 0 6.37 0.61 15 -3 0 6.89 0.72 -15 -3 0 6.24 0.63 -15 -3 0 6.59 0.6 -15 -3 0 6.41 0.57 15 -3 0 5.44 0.54 15 3 0 6.3 0.59 -15 3 0 7.53 0.73 -15 3 0 6.73 0.74 -15 3 0 6.81 0.76 -15 3 0 6.21 0.66 -15 3 0 5.92 0.75 -16 -3 0 2.67 0.43 -16 -3 0 3.24 0.42 16 -3 0 2.82 0.53 -16 -3 0 3.04 0.42 16 -3 0 1.3 1 -16 -3 0 3.28 0.47 16 -3 0 3.31 0.44 16 -3 0 3.13 0.58 -16 3 0 2.27 0.52 -16 3 0 2.93 0.48 16 3 0 3.4 0.45 -16 3 0 2.98 0.53 -16 3 0 3.32 0.55 -16 3 0 1.56 0.54 16 3 0 3.07 0.54 -17 -3 0 1.33 0.42 -17 -3 0 1.92 0.43 -17 -3 0 1.74 0.39 17 -3 0 1.21 0.64 17 -3 0 1.29 0.45 -17 -3 0 1.97 0.45 17 -3 0 1.53 0.37 17 -3 0 1.79 0.56 -17 3 0 2.13 0.56 -17 3 0 1.73 0.52 17 3 0 2.01 0.43 -17 3 0 1.44 0.63 17 3 0 2.18 0.47 -17 3 0 1.57 0.49 -17 3 0 1.84 0.53 -18 -3 0 3.33 0.55 18 -3 0 3.34 0.56 -18 -3 0 2.04 0.47 -18 -3 0 3.18 0.46 -18 -3 0 3.23 0.54 18 3 0 3.22 0.51 -18 3 0 2.93 0.74 -18 3 0 2.71 0.56 -18 3 0 2.71 0.62 -18 3 0 3.11 0.6 -18 3 0 2.67 0.6 -19 -3 0 14.47 0.96 -19 -3 0 10.19 1.34 -19 -3 0 14.23 1.07 -19 -3 0 15.05 1.05 19 -3 0 10.05 1.06 -19 3 0 15.65 1.43 -19 3 0 11.53 1.44 19 3 0 12.37 0.9 -19 3 0 14.06 1.15 -20 -3 0 8.2 0.94 -20 -3 0 9.43 1.01 -20 3 0 7.65 0.91 0 -4 0 9.49 0.49 0 -4 0 8.81 0.5 0 -4 0 10 0.53 0 -4 0 9.9 0.45 0 -4 0 9.33 0.5 0 4 0 9.73 0.53 0 4 0 9.75 0.47 0 4 0 9.48 0.48 0 4 0 9.51 0.53 1 -4 0 24.97 0.87 1 -4 0 23.82 0.84 1 -4 0 23.25 0.88 1 -4 0 23.3 0.9 -1 -4 0 25.62 0.89 -1 -4 0 25.22 0.9 -1 -4 0 24.47 0.86 -1 -4 0 23.82 0.75 1 -4 0 23.08 0.91 -1 -4 0 24.88 0.91 -1 4 0 23.06 0.86 -1 4 0 23.27 0.84 -1 4 0 23.91 0.91 1 4 0 24.55 0.85 -1 4 0 23.96 0.88 1 4 0 24.97 0.79 -1 4 0 22.33 0.9 1 4 0 25.96 0.91 2 -4 0 32.85 1.43 -2 -4 0 29.28 0.99 -2 -4 0 29.73 1.02 2 -4 0 30.87 1.06 2 -4 0 30.56 1.02 -2 -4 0 29.27 1 -2 -4 0 31.62 1.05 2 -4 0 29.43 1.01 -2 4 0 30.45 1.06 2 4 0 29.92 1.04 2 4 0 29.83 1.03 -2 4 0 30.77 1.04 2 4 0 29.71 0.98 -2 4 0 30.22 1.03 -3 -4 0 4.16 0.37 3 -4 0 4.66 0.4 -3 -4 0 4.26 0.36 3 -4 0 4.94 0.49 3 -4 0 4.88 0.44 3 -4 0 4.2 0.4 -3 -4 0 4.87 0.35 -3 -4 0 3.71 0.35 3 -4 0 4.9 0.36 3 4 0 4.43 0.38 -3 4 0 4.67 0.45 3 4 0 4.94 0.4 3 4 0 4.14 0.33 -3 4 0 4.78 0.37 -3 4 0 5.03 0.41 -3 4 0 4.57 0.41 -3 4 0 5.27 0.43 3 4 0 3.9 0.33 4 -4 0 25.95 0.94 -4 -4 0 26.86 0.93 -4 -4 0 28.03 0.94 4 -4 0 26.26 1.01 -4 -4 0 26.02 0.92 4 -4 0 25.52 1.01 -4 -4 0 27.7 0.97 4 -4 0 25.83 1 -4 4 0 26.7 1.03 4 4 0 27.53 0.88 4 4 0 27.95 0.89 4 4 0 27.06 0.95 -4 4 0 27.55 0.98 4 4 0 26.34 0.95 -4 4 0 26.09 1.26 -4 4 0 27.01 1.02 5 -4 0 -0.15 0.19 5 -4 0 -0.01 0.15 -5 -4 0 0.13 0.16 -5 -4 0 0.11 0.16 5 -4 0 0.29 0.21 -5 -4 0 0.38 0.17 5 -4 0 0.3 0.21 5 -4 0 0.07 0.21 -5 -4 0 0.15 0.16 -5 4 0 0.13 0.16 -5 4 0 0.1 0.21 5 4 0 0.31 0.14 -5 4 0 0.27 0.21 5 4 0 0.14 0.15 -5 4 0 0.2 0.22 -5 4 0 0.57 0.24 5 4 0 0.14 0.16 -6 -4 0 19.61 0.78 -6 -4 0 19.08 0.78 -6 -4 0 19.7 0.81 6 -4 0 20.75 0.88 6 -4 0 21.46 0.91 -6 -4 0 19.93 0.76 6 -4 0 21.82 0.92 6 -4 0 20.66 0.93 6 -4 0 22.2 0.82 -6 4 0 22.11 0.97 6 4 0 21.52 0.82 -6 4 0 19.23 0.84 -6 4 0 21.33 0.92 -6 4 0 19.42 0.9 -6 4 0 21.12 0.91 -7 -4 0 98 2.68 7 -4 0 100.89 2.9 7 -4 0 101.7 2.83 -7 -4 0 100.39 2.72 7 -4 0 102.2 2.86 -7 -4 0 100.97 2.75 -7 -4 0 98.33 2.7 7 -4 0 98.77 2.86 7 -4 0 102.57 2.76 -7 4 0 96.98 2.87 -7 4 0 96.66 2.78 -7 4 0 99.6 2.87 -7 4 0 98.91 2.92 -7 4 0 103.24 2.87 7 4 0 100.1 2.73 7 4 0 101.67 2.71 8 -4 0 1.73 0.34 -8 -4 0 1.08 0.25 -8 -4 0 1.28 0.25 8 -4 0 1.19 0.33 -8 -4 0 1.53 0.25 8 -4 0 1.37 0.4 8 -4 0 1.5 0.28 -8 -4 0 1.13 0.24 8 -4 0 1.89 0.36 -8 4 0 0.81 0.24 -8 4 0 1.86 0.37 8 4 0 1.09 0.31 -8 4 0 1.5 0.32 -8 4 0 1.96 0.35 8 4 0 1.54 0.27 -8 4 0 1.48 0.32 9 -4 0 0.73 0.24 9 -4 0 0.86 0.29 9 -4 0 0.84 0.29 -9 -4 0 1.32 0.28 -9 -4 0 1.25 0.26 9 -4 0 0.93 0.3 -9 -4 0 1.47 0.27 9 -4 0 0.66 0.34 -9 -4 0 1.28 0.26 9 4 0 1.02 0.27 9 4 0 1.38 0.27 -9 4 0 0.94 0.25 -9 4 0 1.08 0.37 -9 4 0 1.29 0.33 -9 4 0 1.28 0.34 -9 4 0 0.64 0.29 -10 -4 0 162.17 4.22 10 -4 0 161.63 4.45 10 -4 0 166.63 4.43 -10 -4 0 164.28 4.26 -10 -4 0 162.02 4.29 10 -4 0 157.22 4.29 -10 -4 0 163.29 4.3 10 -4 0 160.99 4.53 10 4 0 159.63 4.26 -10 4 0 162.63 4.48 -10 4 0 166.78 4.59 -10 4 0 161.22 4.46 10 4 0 158.68 4.23 -10 4 0 168.36 4.38 -10 4 0 166.67 4.45 -11 -4 0 79.93 2.4 -11 -4 0 83 2.46 11 -4 0 86.74 2.55 11 -4 0 83.53 2.6 -11 -4 0 79.64 2.45 11 -4 0 86.22 2.73 -11 -4 0 83.7 2.39 11 -4 0 89.79 2.66 11 -4 0 89.16 2.47 -11 4 0 84.68 2.55 -11 4 0 85.61 2.66 11 4 0 87.57 2.47 -11 4 0 87.19 2.77 -11 4 0 86.49 2.64 11 4 0 78.51 2.41 -11 4 0 88.28 2.64 -12 -4 0 55.67 1.78 12 -4 0 58.33 1.97 12 -4 0 52.56 2.05 12 -4 0 54.59 1.76 12 -4 0 57.23 1.85 -12 -4 0 52.81 1.71 -12 -4 0 53.64 1.76 12 -4 0 57.07 1.93 -12 -4 0 51.57 1.7 -12 4 0 55.63 1.95 -12 4 0 56.46 1.96 -12 4 0 56.58 2.14 -12 4 0 55.06 1.92 12 4 0 54.38 1.73 -12 4 0 53.1 1.85 12 4 0 60.01 1.81 13 -4 0 20.01 0.99 -13 -4 0 17.74 0.89 -13 -4 0 20.47 0.93 13 -4 0 19.46 0.92 13 -4 0 20.69 1.12 13 -4 0 20.35 1.03 -13 -4 0 20.43 0.93 -13 -4 0 19.11 0.88 -13 4 0 20.58 1.1 13 4 0 20.88 0.9 -13 4 0 22.44 1.62 -13 4 0 19.82 1.28 13 4 0 18.65 0.89 -13 4 0 22.71 1.03 14 -4 0 1.88 0.51 14 -4 0 2.53 0.46 14 -4 0 2.86 0.42 14 -4 0 4.28 0.51 -14 -4 0 2.09 0.39 -14 -4 0 2.56 0.4 -14 -4 0 2.64 0.4 -14 -4 0 2.94 0.43 -14 4 0 3.53 0.55 -14 4 0 1.51 0.51 -14 4 0 3.17 0.55 -14 4 0 2.99 0.47 14 4 0 2.68 0.4 -14 4 0 2.96 0.52 15 -4 0 0.93 0.43 -15 -4 0 1.59 0.36 -15 -4 0 1.49 0.33 -15 -4 0 1.82 0.39 -15 -4 0 2.07 0.39 15 -4 0 1.02 0.35 15 -4 0 1.03 0.84 15 -4 0 1.36 0.55 15 -4 0 1.05 0.41 -15 4 0 1.06 0.4 15 4 0 1.62 0.38 -15 4 0 0.25 0.42 -15 4 0 1.77 0.49 -15 4 0 0.65 0.42 -15 4 0 0.86 0.46 -16 -4 0 11.22 0.75 -16 -4 0 12.31 0.87 16 -4 0 11.4 1.05 -16 -4 0 11.43 0.77 16 -4 0 12.38 1.19 16 -4 0 11.93 0.88 -16 -4 0 10.87 0.81 16 -4 0 11.17 0.75 16 -4 0 12.17 0.96 -16 4 0 13.14 0.97 16 4 0 9.69 0.79 -16 4 0 13.22 0.97 16 4 0 11 0.8 -16 4 0 13.92 1.05 -16 4 0 11.5 1.13 -16 4 0 12.06 1.02 17 -4 0 5.44 0.58 -17 -4 0 5.37 0.62 -17 -4 0 5.61 0.64 -17 -4 0 5.72 0.72 17 -4 0 5.31 0.7 17 -4 0 4.29 0.58 -17 4 0 5.72 0.76 -17 4 0 5.06 0.78 -17 4 0 5.34 0.71 -17 4 0 5.09 0.7 17 4 0 5.69 0.71 -17 4 0 5.09 0.73 -18 -4 0 5.53 0.64 18 -4 0 5.7 0.62 18 -4 0 4.91 0.65 -18 -4 0 4.32 0.65 -18 -4 0 5.57 0.7 18 -4 0 5.21 0.77 -18 4 0 4.98 0.75 18 4 0 5.91 0.6 -18 4 0 4.28 0.81 -18 4 0 6.15 0.84 -18 4 0 4.98 0.72 19 -4 0 19.53 1.05 19 -4 0 20.55 1.16 -19 -4 0 21.84 1.18 -19 -4 0 16.9 1.04 -19 -4 0 21.1 1.27 -19 4 0 22.63 1.84 -19 4 0 20.05 1.34 -19 4 0 21.33 1.68 -19 4 0 22.41 1.48 0 -5 0 -0.17 0.19 0 -5 0 0.39 0.23 0 -5 0 0.17 0.18 0 -5 0 -0.06 0.18 0 -5 0 -0.05 0.15 0 5 0 -0.14 0.22 0 5 0 0.23 0.21 0 5 0 0.15 0.21 0 5 0 -0.23 0.16 0 5 0 -0.06 0.2 -1 -5 0 112.57 3.05 1 -5 0 106.1 3.04 -1 -5 0 107.23 3.09 -1 -5 0 108.1 3.06 1 -5 0 115.59 3.13 -1 -5 0 110.76 2.89 -1 -5 0 109.44 3.05 1 -5 0 109.63 3.07 1 -5 0 110.34 3.09 1 -5 0 112.17 2.98 1 5 0 110.78 3.02 1 5 0 109.61 3.09 -1 5 0 126.11 3.56 1 5 0 111.91 3.03 -1 5 0 107.3 3.11 -1 5 0 113.41 3.08 1 5 0 114.66 3.09 -1 5 0 114.49 3.12 -1 5 0 110.48 3.05 1 5 0 112.85 2.91 2 -5 0 1.37 0.25 -2 -5 0 1.23 0.27 2 -5 0 1.38 0.26 2 -5 0 1.78 0.32 2 -5 0 1.56 0.31 -2 -5 0 1.29 0.27 -2 -5 0 1.28 0.32 -2 -5 0 1.07 0.24 2 -5 0 1.58 0.28 2 5 0 0.94 0.24 2 5 0 1.51 0.26 -2 5 0 1.58 0.29 2 5 0 1.49 0.28 -2 5 0 1.78 0.32 -2 5 0 1.88 0.33 -2 5 0 1.72 0.31 -2 5 0 1.42 0.27 -3 -5 0 14.49 0.69 -3 -5 0 13.5 0.71 -3 -5 0 14.14 0.68 3 -5 0 15.7 0.75 -3 -5 0 14.15 0.7 3 -5 0 15.31 0.7 3 -5 0 14.97 0.74 3 -5 0 15.3 0.78 3 5 0 13.68 0.64 -3 5 0 15.26 0.73 -3 5 0 14.79 0.76 3 5 0 14.63 0.72 3 5 0 13.73 0.71 -3 5 0 14.84 0.76 -3 5 0 14.9 0.78 4 -5 0 73.09 2.15 -4 -5 0 70.13 2.11 -4 -5 0 68.76 2.06 4 -5 0 68.24 2.13 4 -5 0 74.45 2.21 -4 -5 0 71.27 2.07 -4 -5 0 67.99 2.06 4 -5 0 70.58 2.18 4 -5 0 72.77 2.1 -4 5 0 71.22 2.16 -4 5 0 70.09 2.2 4 5 0 72.18 2.1 4 5 0 71.05 2.01 -4 5 0 71.65 2.12 -4 5 0 70.99 2.18 -4 5 0 69 2.15 4 5 0 71.93 2.1 5 -5 0 43.53 1.44 -5 -5 0 43.86 1.42 5 -5 0 43.21 1.53 -5 -5 0 46.36 1.48 5 -5 0 43.72 1.53 -5 -5 0 45.45 1.45 5 -5 0 42.84 1.51 -5 -5 0 44 1.42 5 -5 0 44.13 1.56 -5 5 0 42.89 1.56 -5 5 0 44.11 1.54 5 5 0 45.18 1.34 -5 5 0 40.64 1.51 5 5 0 44.95 1.44 5 5 0 46.24 1.46 -5 5 0 40.99 1.52 -5 5 0 40.83 1.46 6 -5 0 193.6 5.17 -6 -5 0 188.62 4.99 -6 -5 0 186.81 4.97 6 -5 0 198.44 5.05 6 -5 0 194.65 5.15 6 -5 0 201.07 5.17 -6 -5 0 196.77 5.02 -6 -5 0 196.01 5.05 -6 5 0 203.31 5.18 -6 5 0 191.48 5.16 -6 5 0 194.89 5.18 -6 5 0 189.13 5.13 -6 5 0 194.98 5.16 6 5 0 190.84 5.21 6 5 0 183.06 4.85 7 -5 0 30.46 1.26 -7 -5 0 31.18 1.12 7 -5 0 29.94 1.21 7 -5 0 29.41 1.26 7 -5 0 29.68 1.15 -7 -5 0 29.98 1.1 7 -5 0 32.89 1.33 -7 -5 0 30.62 1.13 -7 -5 0 32.88 1.17 -7 5 0 30.71 1.19 -7 5 0 31.15 1.27 -7 5 0 30.47 1.31 -7 5 0 28.5 1.23 -7 5 0 31.1 1.28 7 5 0 30.75 1.14 -8 -5 0 0.6 0.26 -8 -5 0 0.44 0.22 8 -5 0 0.78 0.31 -8 -5 0 0.34 0.24 -8 -5 0 0.87 0.27 8 -5 0 0.58 0.3 8 -5 0 0.55 0.36 8 -5 0 0.59 0.22 8 -5 0 0.55 0.34 -8 5 0 0.36 0.27 -8 5 0 0.37 0.29 -8 5 0 0.58 0.28 8 5 0 0.1 0.23 -8 5 0 0.41 0.32 -8 5 0 0.2 0.28 8 5 0 0.63 0.26 -9 -5 0 116.38 3.26 9 -5 0 118.22 3.45 9 -5 0 119.38 3.43 9 -5 0 119.57 3.28 -9 -5 0 116.87 3.27 -9 -5 0 109.02 3.2 9 -5 0 121.31 3.39 -9 -5 0 115.83 3.2 9 -5 0 114.07 3.46 9 5 0 119.02 3.26 -9 5 0 116.56 3.45 9 5 0 117.3 3.22 -9 5 0 119.75 3.53 -9 5 0 120.33 3.43 -9 5 0 121.83 3.46 -9 5 0 118.82 3.36 10 -5 0 0.69 0.3 10 -5 0 0.82 0.35 -10 -5 0 0.51 0.25 -10 -5 0 0.43 0.26 10 -5 0 0.83 0.37 -10 -5 0 0.54 0.28 -10 -5 0 0.53 0.26 10 -5 0 0.26 0.34 10 -5 0 0.62 0.28 -10 5 0 0.62 0.34 -10 5 0 0.61 0.34 -10 5 0 -0.19 0.34 10 5 0 0.15 0.26 -10 5 0 0.28 0.33 -10 5 0 0.74 0.33 10 5 0 0.16 0.27 11 -5 0 6.31 0.75 -11 -5 0 5.92 0.55 -11 -5 0 5.84 0.55 11 -5 0 6.3 0.68 11 -5 0 5.67 0.67 -11 -5 0 6.58 0.54 11 -5 0 4.71 0.63 11 -5 0 5.64 0.57 11 5 0 6.09 0.59 -11 5 0 6.2 0.68 -11 5 0 5.08 1.09 -11 5 0 5.7 0.69 11 5 0 7.09 0.59 -11 5 0 5.19 0.64 -11 5 0 5.68 0.85 -12 -5 0 37.04 1.37 -12 -5 0 39.68 1.45 -12 -5 0 40.88 1.52 12 -5 0 40.24 1.64 -12 -5 0 39.97 1.42 12 -5 0 37.8 1.56 12 -5 0 36.26 1.5 12 -5 0 38.3 1.43 -12 5 0 38.14 1.62 -12 5 0 39.45 1.98 12 5 0 40.03 1.39 -12 5 0 38.17 1.54 -12 5 0 42.64 1.8 -12 5 0 40.01 1.63 13 -5 0 14.13 0.95 -13 -5 0 13.56 0.76 13 -5 0 13.85 1 -13 -5 0 11.47 0.78 -13 -5 0 12.23 0.79 13 -5 0 13.21 0.8 13 -5 0 13.27 0.89 -13 -5 0 11.6 0.76 -13 5 0 13.4 0.94 -13 5 0 13.11 0.97 -13 5 0 11.62 1.09 13 5 0 11.98 0.75 -13 5 0 12.09 0.88 -13 5 0 13.62 1 -14 -5 0 24.09 1.03 -14 -5 0 25.31 1.11 14 -5 0 23.32 1.21 -14 -5 0 24 1.12 -14 -5 0 23.95 1.05 14 -5 0 22.89 1.08 14 -5 0 24.2 1.24 -14 5 0 23.92 1.56 -14 5 0 25.42 1.47 -14 5 0 20.84 1.25 14 5 0 21.38 1.03 -14 5 0 22.51 1.27 -14 5 0 26.6 1.34 14 5 0 20.85 1.2 -15 -5 0 18.55 0.98 -15 -5 0 20.26 1.04 -15 -5 0 18.69 1.04 15 -5 0 20.29 1.19 15 -5 0 17.15 1.37 15 -5 0 20.51 1.26 -15 -5 0 17.47 0.93 15 -5 0 20.19 1.14 15 5 0 19.09 0.98 -15 5 0 19.72 1.21 15 5 0 18.06 0.99 -15 5 0 21.17 1.2 -15 5 0 19.88 1.25 -15 5 0 18.8 1.23 -15 5 0 18.96 1.38 -16 -5 0 38.3 1.48 16 -5 0 37.62 1.65 -16 -5 0 34.72 1.39 16 -5 0 39.28 1.5 16 -5 0 38.3 1.62 -16 -5 0 36.16 1.47 -16 5 0 36.87 1.73 -16 5 0 36.56 1.75 -16 5 0 37.12 1.94 16 5 0 33.68 1.38 -16 5 0 35.57 1.68 -17 -5 0 11.89 0.94 17 -5 0 11.56 0.88 -17 -5 0 11.87 1.01 17 -5 0 13.33 1.11 -17 -5 0 12.89 0.95 -17 5 0 15.05 1.23 -17 5 0 10.78 1.06 -17 5 0 12.51 1.35 -17 5 0 13.12 1.19 17 5 0 10 0.85 -18 -5 0 6.82 0.74 -18 -5 0 6.55 0.77 -18 -5 0 6.37 0.75 -18 -5 0 7.51 0.92 18 -5 0 7.7 1.07 18 -5 0 6.28 0.69 -18 5 0 6.01 0.96 -18 5 0 7.52 0.9 -18 5 0 7.55 0.97 0 -6 0 94.88 2.8 0 -6 0 92.76 2.58 0 -6 0 96.79 2.78 0 -6 0 96.29 2.72 0 6 0 92.98 2.72 0 6 0 97.94 2.79 0 6 0 90.29 2.77 0 6 0 96.04 2.71 0 6 0 92.94 2.61 -1 -6 0 22.76 1.01 1 -6 0 22.58 1.03 1 -6 0 22.14 0.91 1 -6 0 22.08 1.02 1 -6 0 22.25 1.05 -1 -6 0 22.7 1.01 -1 -6 0 22.38 1.11 1 -6 0 23.5 0.98 -1 -6 0 22.48 0.84 -1 -6 0 22.3 0.96 1 6 0 23.11 1.03 -1 6 0 22.69 0.96 -1 6 0 22.97 1.03 1 6 0 21.48 0.94 -1 6 0 21.84 1.04 -1 6 0 23.44 0.97 1 6 0 24.45 0.99 1 6 0 21.48 1.19 1 6 0 23.86 0.89 -1 6 0 22.47 1 2 -6 0 84.85 2.65 -2 -6 0 87.7 2.59 2 -6 0 86.89 2.51 2 -6 0 89.78 2.64 2 -6 0 88.77 2.58 2 -6 0 89.65 2.63 -2 -6 0 86.01 2.55 -2 -6 0 88.1 2.63 -2 -6 0 84.66 2.57 -2 6 0 84.78 2.65 -2 6 0 88.89 2.77 -2 6 0 87.83 2.88 2 6 0 85.83 2.78 2 6 0 86.23 2.5 -2 6 0 92.98 2.58 2 6 0 88.05 2.6 2 6 0 91.46 2.54 -2 6 0 90.14 2.62 3 -6 0 -0.03 0.25 3 -6 0 0.28 0.28 3 -6 0 0.75 0.29 -3 -6 0 0.1 0.27 3 -6 0 0.81 0.25 -3 -6 0 0.6 0.28 3 -6 0 1 0.32 -3 -6 0 0.39 0.48 -3 -6 0 0.44 0.26 -3 6 0 0.34 0.3 -3 6 0 0.5 0.33 -3 6 0 0.78 0.32 3 6 0 0.43 0.24 -3 6 0 0.45 0.29 3 6 0 -0.13 0.2 3 6 0 0.13 0.25 -3 6 0 0.2 0.23 3 6 0 0.17 0.25 4 -6 0 0.54 0.34 -4 -6 0 0.11 0.23 4 -6 0 0.32 0.23 4 -6 0 -0.24 0.26 -4 -6 0 0.05 0.25 4 -6 0 0.6 0.27 4 -6 0 0.53 0.3 -4 -6 0 0.31 0.27 -4 -6 0 -0.17 0.26 -4 6 0 0.45 0.3 -4 6 0 0.37 0.31 4 6 0 0.08 0.21 -4 6 0 0.44 0.31 4 6 0 0.19 0.26 -4 6 0 0.31 0.29 4 6 0 0.12 0.23 -4 6 0 0.52 0.26 4 6 0 -0.15 0.24 -5 -6 0 220.44 5.78 5 -6 0 216.45 5.82 -5 -6 0 223.14 5.73 5 -6 0 245.31 6.57 5 -6 0 219.93 5.87 5 -6 0 216.92 5.75 -5 -6 0 218.59 5.74 -5 -6 0 214.67 5.71 5 -6 0 222.02 5.88 -5 6 0 223.33 5.86 -5 6 0 223.64 5.87 5 6 0 217.46 5.74 -5 6 0 222.31 5.91 -5 6 0 223.12 5.87 5 6 0 220.57 5.77 5 6 0 219.49 5.6 5 6 0 217.87 5.6 -5 6 0 209.52 5.78 6 -6 0 11.58 0.71 6 -6 0 11.59 0.81 6 -6 0 10.57 0.79 6 -6 0 12.14 0.84 6 -6 0 11.29 0.78 -6 -6 0 10.58 0.67 -6 -6 0 10.17 0.7 -6 -6 0 10.39 0.68 -6 -6 0 10.97 0.71 6 6 0 10.5 0.58 6 6 0 10.49 0.7 -6 6 0 10.19 0.71 -6 6 0 11.5 0.83 6 6 0 11.34 0.71 -6 6 0 11.61 0.81 -6 6 0 10.91 0.84 6 6 0 11.01 0.58 -6 6 0 11.57 0.81 -7 -6 0 35.54 1.35 7 -6 0 36.84 1.49 7 -6 0 36.56 1.5 -7 -6 0 38.29 1.36 7 -6 0 37.72 1.36 7 -6 0 37.27 1.66 7 -6 0 36.48 1.44 -7 -6 0 33.99 1.68 -7 -6 0 37.65 1.32 -7 6 0 36.08 1.5 -7 6 0 35.03 1.39 7 6 0 34.2 1.35 -7 6 0 35.35 1.47 -7 6 0 36.22 1.53 -7 6 0 37.43 1.48 -8 -6 0 5.2 0.81 8 -6 0 3.67 0.52 8 -6 0 2.9 0.52 8 -6 0 4.27 0.55 8 -6 0 3.4 0.45 8 -6 0 2.88 0.51 -8 -6 0 4.63 0.5 -8 -6 0 3.96 0.5 -8 -6 0 4 0.52 8 6 0 3.96 0.58 8 6 0 3.29 0.45 -8 6 0 3.44 0.53 -8 6 0 3.18 0.52 -8 6 0 3.58 0.51 -8 6 0 3.64 0.56 -8 6 0 3.65 0.53 9 -6 0 63.68 2.14 -9 -6 0 65.46 2.53 -9 -6 0 64.63 1.96 9 -6 0 63.87 2.03 9 -6 0 59.75 2.14 -9 -6 0 61.73 1.97 -9 -6 0 63.29 2.03 9 -6 0 62.85 2.2 9 -6 0 62.4 2.22 -9 6 0 60.42 2.15 -9 6 0 62.75 2.28 9 6 0 62.98 1.98 -9 6 0 56.53 2.89 -9 6 0 61.09 2.19 10 -6 0 3 0.56 10 -6 0 3.35 0.53 -10 -6 0 4.08 0.51 10 -6 0 2.78 0.5 10 -6 0 3.56 0.59 -10 -6 0 3.89 0.5 -10 -6 0 3.16 0.45 10 -6 0 2.82 0.54 -10 -6 0 2.63 0.44 -10 6 0 4.12 0.61 -10 6 0 4.29 0.58 -10 6 0 3.71 0.58 -10 6 0 3.66 0.66 10 6 0 3.85 0.49 -11 -6 0 -0.02 0.28 11 -6 0 -0.18 0.41 11 -6 0 0.1 0.36 -11 -6 0 0.1 0.32 11 -6 0 0.1 0.38 11 -6 0 -0.04 0.31 -11 -6 0 0.21 0.33 11 -6 0 -0.4 0.4 -11 -6 0 0.41 0.32 11 6 0 -0.43 0.32 -11 6 0 0.07 0.55 -11 6 0 0.11 0.36 -11 6 0 -0.5 0.4 -11 6 0 -0.09 0.37 -11 6 0 -0.48 0.4 12 -6 0 9.74 0.97 12 -6 0 11.11 0.88 -12 -6 0 9.68 0.75 12 -6 0 7.72 1.36 -12 -6 0 8.23 0.7 -12 -6 0 11.04 0.8 12 -6 0 9.31 0.76 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0 30.33 1.37 -2 7 0 31.47 1.27 -2 7 0 28.76 1.23 2 7 0 31.75 1.31 2 7 0 33.11 1.25 2 7 0 29.56 1.29 3 -7 0 0.54 0.31 3 -7 0 0.02 0.33 3 -7 0 -0.06 0.29 3 -7 0 0.36 0.33 -3 -7 0 0.25 0.33 -3 -7 0 0.02 0.29 3 -7 0 1.08 0.31 -3 -7 0 0.66 0.32 -3 -7 0 0.44 0.3 -3 7 0 0.58 0.36 -3 7 0 0.51 0.34 3 7 0 0.59 0.34 3 7 0 0.37 0.31 -3 7 0 0.54 0.35 3 7 0 0.13 0.27 -3 7 0 0.13 0.33 3 7 0 0.48 0.29 -3 7 0 0.21 0.32 -4 -7 0 21.59 1.05 4 -7 0 23.19 1.11 4 -7 0 23.24 1.17 4 -7 0 22.66 1.19 -4 -7 0 23.53 1.07 4 -7 0 25.77 1.11 -4 -7 0 23.24 1.11 -4 -7 0 22.13 1.08 4 -7 0 21.36 1.15 4 7 0 22.91 0.99 4 7 0 23.81 1.13 4 7 0 21.85 1.07 -4 7 0 24.61 1.17 -4 7 0 24.24 1.17 -4 7 0 24.1 1.19 -4 7 0 23.28 1.1 -4 7 0 23.42 1.2 4 7 0 23.3 1 5 -7 0 0.63 0.35 -5 -7 0 0.65 0.31 -5 -7 0 0.27 0.28 5 -7 0 1.06 0.4 5 -7 0 1.43 0.41 5 -7 0 1.55 0.38 -5 -7 0 1.05 0.38 -5 -7 0 0.84 0.35 5 7 0 1.09 0.38 -5 7 0 0.57 0.32 -5 7 0 1.37 0.38 5 7 0 0.98 0.34 -5 7 0 1.25 0.42 -5 7 0 1.14 0.44 5 7 0 1.06 0.32 -5 7 0 1.15 0.4 5 7 0 0.73 0.29 -6 -7 0 1.9 0.44 6 -7 0 1.86 0.48 6 -7 0 1.71 0.89 6 -7 0 3.04 0.52 -6 -7 0 2.83 0.54 6 -7 0 3.07 0.49 -6 -7 0 1.86 0.38 -6 -7 0 2.61 0.43 6 -7 0 2.27 0.65 -6 7 0 3.4 0.54 6 7 0 3.02 0.38 -6 7 0 2 0.8 -6 7 0 2.44 0.46 6 7 0 2.78 0.45 -6 7 0 2.5 0.5 6 7 0 2.38 0.37 -6 7 0 2.17 0.5 -7 -7 0 2.32 0.38 -7 -7 0 3.69 0.49 7 -7 0 1.5 0.43 -7 -7 0 2.61 0.4 7 -7 0 3.38 0.56 7 -7 0 3.26 0.48 7 -7 0 4.66 0.6 7 -7 0 3.69 0.56 -7 -7 0 3.54 0.47 -7 7 0 2.78 0.52 -7 7 0 3.98 0.59 -7 7 0 3.19 0.54 -7 7 0 4.58 0.63 7 7 0 2.78 0.43 -8 -7 0 14.5 0.88 8 -7 0 14.44 1.04 -8 -7 0 14.21 0.88 8 -7 0 15.53 1.02 8 -7 0 13.76 1.04 -8 -7 0 13.94 0.85 8 -7 0 13.99 0.88 -8 -7 0 14.91 0.86 -8 7 0 12.68 1.01 -8 7 0 16.33 1.35 -8 7 0 16.26 1.07 -8 7 0 13.5 1.03 -9 -7 0 0.68 0.38 -9 -7 0 0.9 0.35 9 -7 0 0.83 0.38 -9 -7 0 1.11 0.37 -9 -7 0 0.48 0.34 9 -7 0 1.03 0.43 9 -7 0 0.43 0.45 9 -7 0 0.47 0.46 9 7 0 1.46 0.41 -9 7 0 1.01 0.46 -9 7 0 1.19 0.52 -9 7 0 0.51 0.44 -9 7 0 1.1 0.49 -10 -7 0 3.84 0.54 -10 -7 0 4.05 0.56 10 -7 0 4.05 0.73 -10 -7 0 4.06 0.52 10 -7 0 6.93 0.88 -10 -7 0 5.05 0.65 10 -7 0 5.04 0.71 10 -7 0 4.66 0.6 10 -7 0 4.96 0.66 -10 7 0 4.07 0.71 -10 7 0 5.05 0.72 10 7 0 4.67 0.57 -10 7 0 4.77 0.69 -11 -7 0 8.3 0.8 -11 -7 0 9.58 0.91 11 -7 0 9.82 0.81 -11 -7 0 8.71 0.77 11 -7 0 8.47 1 11 -7 0 9.66 1.09 11 -7 0 7.37 1.27 -11 -7 0 8.95 0.76 11 -7 0 8.19 0.92 -11 7 0 11.36 1 11 7 0 9.57 0.86 -11 7 0 7.96 1.05 -11 7 0 9.44 1.06 -11 7 0 7.94 0.93 11 7 0 7.03 0.84 -11 7 0 8.5 0.95 -12 -7 0 0.7 0.45 12 -7 0 0.95 0.54 12 -7 0 -0.07 0.54 -12 -7 0 0.97 0.41 -12 -7 0 0.64 0.47 12 -7 0 -0.01 0.39 -12 -7 0 -0.49 0.37 12 -7 0 0.56 0.52 -12 7 0 0.08 0.53 -12 7 0 -0.17 0.52 -12 7 0 0.25 0.61 12 7 0 0 0.41 -12 7 0 0.12 0.52 12 7 0 0.04 0.45 -12 7 0 -0.12 0.54 -13 -7 0 2.22 0.51 13 -7 0 2.15 0.64 -13 -7 0 2.42 0.56 13 -7 0 2.98 0.57 -13 -7 0 2.17 0.54 13 -7 0 2.1 0.7 -13 -7 0 2.96 0.49 13 -7 0 3.15 0.63 -13 7 0 2.82 0.73 -13 7 0 2.09 0.62 13 7 0 2.51 0.53 -13 7 0 3.35 0.77 -13 7 0 2.3 0.67 -14 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9.49 0.7 6 -8 0 7.42 0.9 6 -8 0 8.99 0.89 -6 -8 0 8.92 0.82 -6 -8 0 7.62 0.8 6 -8 0 8.2 0.92 -6 -8 0 8.11 0.78 -6 -8 0 6.59 0.77 6 -8 0 8.19 0.77 6 8 0 9.06 0.81 -6 8 0 8.99 0.87 -6 8 0 9.24 0.98 -6 8 0 7.83 1.02 -6 8 0 9.51 0.92 6 8 0 7.53 0.66 -6 8 0 9.71 0.92 6 8 0 9.7 0.66 7 -8 0 8.74 0.79 -7 -8 0 10.08 0.84 7 -8 0 8.04 0.96 7 -8 0 8.4 0.96 -7 -8 0 9.21 0.84 -7 -8 0 9.68 0.81 7 -8 0 10.46 0.94 -7 -8 0 8.9 0.82 7 -8 0 10.41 0.98 -7 8 0 8.78 0.95 7 8 0 9.23 0.84 -7 8 0 9.34 0.9 -7 8 0 8.1 0.99 -7 8 0 9.13 1.02 -7 8 0 10.37 0.98 8 -8 0 1.28 0.56 8 -8 0 1.3 0.51 -8 -8 0 1.78 0.49 8 -8 0 0.92 0.42 8 -8 0 0.73 0.53 8 -8 0 1.77 0.57 -8 -8 0 1.22 0.44 -8 -8 0 1.45 0.47 -8 -8 0 1.42 0.43 -8 8 0 1.18 0.53 -8 8 0 0.55 0.57 -8 8 0 1.42 0.55 -8 8 0 1.44 0.52 -8 8 0 1.72 0.52 8 8 0 1.34 0.49 9 -8 0 1.26 0.51 9 -8 0 0.78 0.57 9 -8 0 0.94 0.58 -9 -8 0 0.44 0.41 -9 -8 0 0.07 0.44 9 -8 0 0.22 0.4 9 -8 0 -0.29 0.54 -9 -8 0 0.83 0.45 -9 -8 0 0.6 0.43 -9 8 0 0.7 0.57 -9 8 0 0.21 0.5 -9 8 0 -0.12 0.52 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