#------------------------------------------------------------------------------ #$Date: 2019-02-12 05:35:00 +0200 (Tue, 12 Feb 2019) $ #$Revision: 213605 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/14/2021476.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021476 loop_ _publ_author_name 'Ja\'cimovi\'c, \H-imidazol-1-ide-5-carboxylato)-\k^2^N^1^,O:N^2^;\k^2^N^2^:N^1^,O-bis[triaquacobalt(II)] dihydrate' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens difmap _audit_creation_method SHELXL-2014/6 _cell_angle_alpha 90 _cell_angle_beta 102.930(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 8.9689(11) _cell_length_b 6.4035(8) _cell_length_c 16.4509(19) _cell_measurement_reflns_used 9652 _cell_measurement_temperature 200(2) _cell_measurement_theta_max 66.542 _cell_measurement_theta_min 4.782 _cell_volume 920.86(19) _computing_cell_refinement ; APEX2 (Bruker, 2008) ; _computing_data_collection ; SAINT (Bruker, 2008) ; _computing_data_reduction ; SAINT (Bruker, 2008) ; _computing_molecular_graphics ; ORTEP-3 (Farrugia, 2012) and Mercury (Macrae et al., 2008) ; _computing_publication_material ; PLATON (Spek, 2009) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 200(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker ApexII CCD' _diffrn_measurement_method 'phi and omegas scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0202 _diffrn_reflns_av_unetI/netI 0.0103 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 32322 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 33.289 _diffrn_reflns_theta_min 2.330 _diffrn_source 'Incoatec ImS' _exptl_absorpt_coefficient_mu 1.903 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2008) ; _exptl_crystal_colour pink _exptl_crystal_density_diffrn 2.063 _exptl_crystal_description prism _exptl_crystal_F_000 580 _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _refine_diff_density_max 0.545 _refine_diff_density_min -0.231 _refine_ls_extinction_coef 0.0055(6) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.065 _refine_ls_hydrogen_treatment refU _refine_ls_matrix_type full _refine_ls_number_parameters 158 _refine_ls_number_reflns 3531 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.065 _refine_ls_R_factor_all 0.0193 _refine_ls_R_factor_gt 0.0181 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0219P)^2^+0.4119P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0481 _refine_ls_wR_factor_ref 0.0486 _reflns_number_gt 3366 _reflns_number_total 3531 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yo3057sup1.cif _cod_data_source_block III _cod_database_code 2021476 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; 1 0 0 1497.35 30.70 -1 0 0 1258.37 30.40 1 0 0 1509.55 30.50 1 0 0 1536.35 31.20 -1 0 0 1512.85 30.30 1 0 0 1428.46 30.20 1 0 0 1328.57 30.10 -2 0 0 1003.70 21.50 -2 0 0 983.50 21.90 2 0 0 1016.30 22.00 2 0 0 1035.60 22.20 -2 0 0 1025.90 21.60 2 0 0 1004.00 21.30 2 0 0 982.10 21.70 -2 0 0 1019.90 21.90 2 0 0 992.30 21.20 2 0 0 1057.09 21.40 -2 0 0 1022.70 21.80 -3 0 0 3866.21 78.79 -3 0 0 3717.63 78.59 -3 0 0 3637.54 78.19 3 0 0 3863.61 80.69 3 0 0 3697.03 78.49 3 0 0 3600.34 77.59 -3 0 0 3638.04 77.49 3 0 0 3712.03 78.59 -3 0 0 3548.34 77.69 -4 0 0 476.05 10.40 -4 0 0 503.15 10.80 -4 0 0 487.65 10.50 -4 0 0 480.15 10.60 4 0 0 484.05 10.70 -4 0 0 473.75 10.30 4 0 0 486.35 10.50 4 0 0 492.25 11.30 5 0 0 2118.19 44.50 5 0 0 2082.89 45.30 -5 0 0 2066.99 44.60 -5 0 0 2104.49 43.60 -5 0 0 1992.10 44.50 5 0 0 2099.09 43.80 -5 0 0 2089.29 44.90 -5 0 0 2160.28 43.80 6 0 0 8.30 1.10 6 0 0 9.80 1.80 -6 0 0 8.10 0.80 -6 0 0 8.00 1.10 6 0 0 7.50 0.80 -6 0 0 6.60 0.60 -6 0 0 8.80 0.80 -7 0 0 249.58 6.10 -7 0 0 242.68 6.30 -7 0 0 226.58 5.50 -7 0 0 244.28 6.00 7 0 0 241.28 6.10 7 0 0 247.68 7.60 7 0 0 245.08 6.30 -8 0 0 16.00 1.30 8 0 0 13.90 1.30 8 0 0 8.70 1.30 -8 0 0 10.00 1.10 -8 0 0 11.50 1.50 8 0 0 8.70 1.80 -9 0 0 161.78 4.90 9 0 0 173.78 6.50 -9 0 0 162.98 4.60 9 0 0 164.08 4.70 9 0 0 157.68 5.10 -9 0 0 160.58 5.20 10 0 0 186.08 7.60 -10 0 0 192.98 5.60 10 0 0 186.08 5.50 -10 0 0 190.48 5.90 10 0 0 179.88 5.70 11 0 0 27.90 3.80 11 0 0 25.60 1.90 -11 0 0 25.70 2.10 -12 0 0 363.26 9.60 12 0 0 369.46 12.00 -12 0 0 388.46 11.70 12 0 0 354.66 10.20 12 0 0 373.56 9.70 13 0 0 351.76 9.70 13 0 0 358.56 10.30 -13 0 0 372.26 11.70 13 0 0 366.56 12.80 0 -1 0 1.80 0.20 0 1 0 1.30 0.30 -1 -1 0 208.38 4.50 -1 -1 0 208.08 4.50 1 -1 0 212.78 4.60 -1 -1 0 208.88 4.60 1 -1 0 209.38 4.60 1 -1 0 209.68 4.70 -1 1 0 218.88 4.70 1 1 0 217.78 4.60 -1 1 0 213.98 4.80 1 1 0 206.28 4.50 1 1 0 209.38 4.70 -1 1 0 206.38 4.60 1 1 0 201.68 4.60 -2 -1 0 7.80 0.40 2 -1 0 9.10 0.80 2 -1 0 9.80 0.60 -2 -1 0 8.30 0.40 2 -1 0 8.90 0.40 2 -1 0 8.40 0.50 -2 1 0 8.70 0.70 -2 1 0 8.90 0.60 -2 1 0 8.70 0.50 2 1 0 9.40 0.30 2 1 0 9.30 0.70 2 1 0 8.40 0.30 2 1 0 8.00 0.50 2 1 0 8.80 0.80 -3 -1 0 1820.32 40.20 3 -1 0 1942.21 39.40 3 -1 0 1866.11 40.50 -3 -1 0 1840.52 40.30 3 -1 0 1925.51 39.70 -3 -1 0 1837.02 40.00 3 -1 0 1873.71 40.40 3 1 0 1897.91 41.00 -3 1 0 1888.31 40.50 3 1 0 1835.32 40.30 -3 1 0 1905.71 40.30 3 1 0 1877.71 40.90 -3 1 0 1851.51 40.00 4 -1 0 18.40 1.40 4 -1 0 20.30 1.00 -4 -1 0 19.20 0.90 4 -1 0 18.10 1.00 4 -1 0 18.10 1.10 -4 -1 0 22.10 1.00 -4 -1 0 18.50 0.90 4 1 0 20.40 1.00 -4 1 0 21.10 1.00 -4 1 0 19.80 0.80 4 1 0 18.00 1.40 -4 1 0 20.80 1.40 4 1 0 20.40 1.40 5 -1 0 1252.67 26.40 -5 -1 0 1247.38 26.30 -5 -1 0 1221.68 26.20 5 -1 0 1217.48 26.40 5 -1 0 1238.98 26.40 5 -1 0 1275.17 27.30 -5 -1 0 1251.27 26.40 -5 1 0 1208.98 26.10 -5 1 0 1281.47 26.80 -5 1 0 1257.67 26.10 -5 1 0 1244.68 26.50 5 1 0 1251.07 26.30 5 1 0 1276.07 27.40 -5 1 0 1229.58 26.40 5 1 0 1251.77 26.70 6 -1 0 836.42 18.10 6 -1 0 859.61 19.30 6 -1 0 816.42 18.10 -6 -1 0 839.22 18.20 6 -1 0 832.72 18.20 -6 -1 0 849.32 18.20 -6 -1 0 817.42 18.10 -6 1 0 852.61 18.60 -6 1 0 827.42 18.10 6 1 0 833.92 18.00 -6 1 0 822.12 17.80 6 1 0 844.72 18.50 6 1 0 829.42 19.30 -6 1 0 834.82 18.20 7 -1 0 393.56 9.30 -7 -1 0 378.66 9.10 7 -1 0 393.66 9.10 7 -1 0 390.86 10.30 -7 -1 0 397.36 9.20 7 -1 0 393.16 9.20 -7 -1 0 395.86 9.10 7 1 0 391.16 9.00 7 1 0 383.66 10.40 7 1 0 394.66 9.50 -7 1 0 383.56 9.10 -7 1 0 382.96 9.10 -7 1 0 355.56 8.40 -7 1 0 384.26 8.80 -7 1 0 398.26 9.70 -8 -1 0 59.29 2.40 8 -1 0 61.19 2.80 -8 -1 0 61.09 2.50 8 -1 0 54.49 2.50 8 -1 0 63.69 4.00 8 -1 0 60.89 2.50 -8 -1 0 62.69 2.60 -8 1 0 62.49 2.20 -8 1 0 55.39 2.50 8 1 0 62.39 2.40 -8 1 0 59.99 2.30 8 1 0 61.29 3.00 -8 1 0 65.59 2.90 8 1 0 61.99 4.10 9 -1 0 21.80 1.70 -9 -1 0 26.60 2.00 9 -1 0 23.50 1.80 -9 -1 0 19.40 1.60 9 -1 0 21.70 2.60 -9 -1 0 20.20 1.60 9 -1 0 22.30 2.00 9 1 0 20.60 2.10 -9 1 0 22.30 1.80 -9 1 0 19.80 2.10 9 1 0 24.70 3.20 9 1 0 19.20 1.50 10 -1 0 72.39 3.20 -10 -1 0 70.79 3.10 -10 -1 0 72.89 3.00 10 -1 0 81.79 4.60 10 -1 0 73.19 3.60 -10 1 0 66.49 3.40 -10 1 0 70.89 3.20 10 1 0 69.29 4.60 10 1 0 83.89 3.00 10 1 0 68.99 3.60 -11 -1 0 59.29 2.80 -11 -1 0 61.29 3.80 11 -1 0 55.09 4.30 11 -1 0 55.69 3.10 11 -1 0 59.09 3.50 11 1 0 70.19 5.80 11 1 0 59.59 3.50 -11 1 0 56.49 3.80 11 1 0 54.79 2.70 -11 1 0 59.79 3.20 -12 -1 0 0.40 1.00 12 -1 0 -0.10 1.90 -12 -1 0 2.60 1.70 12 -1 0 -1.10 1.60 12 -1 0 -2.40 1.20 12 1 0 0.00 1.30 -12 1 0 -0.40 1.00 12 1 0 1.40 2.30 13 -1 0 17.30 3.70 13 -1 0 18.30 1.90 -13 -1 0 12.50 1.70 -13 -1 0 21.70 3.40 13 -1 0 15.80 2.10 13 1 0 17.10 4.10 -13 1 0 18.20 2.00 -13 1 0 16.50 2.70 13 1 0 16.30 2.00 0 -2 0 1114.89 23.70 0 -2 0 1122.59 23.80 0 -2 0 1087.99 23.80 0 -2 0 1156.88 23.90 0 2 0 1050.79 24.30 0 2 0 1114.99 24.00 0 2 0 1085.99 23.70 0 2 0 1150.98 23.50 1 -2 0 1935.91 42.20 -1 -2 0 1971.80 42.00 -1 -2 0 2001.70 42.30 -1 -2 0 2040.90 43.00 1 -2 0 2036.00 42.40 1 -2 0 1998.20 42.30 -1 -2 0 1964.40 42.30 1 -2 0 1975.20 42.10 1 2 0 2018.80 42.50 1 2 0 1972.40 42.30 1 2 0 1910.51 41.80 -1 2 0 1966.10 43.10 1 2 0 1912.01 42.20 -1 2 0 1948.51 43.10 -1 2 0 1927.81 42.70 -2 -2 0 30.70 1.00 2 -2 0 31.00 1.30 2 -2 0 29.90 1.10 -2 -2 0 32.00 1.10 2 -2 0 29.60 1.20 -2 -2 0 28.80 1.00 -2 2 0 32.00 1.40 2 2 0 29.80 1.10 -2 2 0 30.40 1.30 2 2 0 29.20 1.30 -2 2 0 33.50 1.10 2 2 0 30.30 1.10 -3 -2 0 132.69 3.20 -3 -2 0 140.89 3.50 3 -2 0 138.69 3.80 -3 -2 0 132.69 3.30 -3 -2 0 136.09 3.50 3 -2 0 142.69 3.50 3 -2 0 137.79 3.50 3 2 0 138.99 3.20 3 2 0 134.29 3.70 -3 2 0 145.99 3.90 3 2 0 127.39 2.90 -3 2 0 136.09 3.40 -3 2 0 141.19 3.70 3 2 0 139.19 3.40 3 2 0 135.99 3.90 4 -2 0 343.07 7.90 4 -2 0 343.57 7.90 -4 -2 0 341.77 7.70 4 -2 0 352.06 8.40 -4 -2 0 342.77 8.00 -4 2 0 349.17 8.20 4 2 0 347.87 8.60 4 2 0 340.57 7.80 -4 2 0 335.37 7.80 -4 2 0 343.07 8.30 4 2 0 355.26 8.30 -5 -2 0 48.70 1.70 -5 -2 0 46.80 1.50 -5 -2 0 48.70 2.00 5 -2 0 45.40 2.30 5 -2 0 49.30 1.90 5 -2 0 47.50 2.00 5 2 0 52.59 2.60 5 2 0 45.80 2.40 5 2 0 45.90 1.70 -5 2 0 49.20 2.30 -5 2 0 51.69 2.20 -5 2 0 49.40 1.90 -6 -2 0 66.29 2.50 6 -2 0 59.69 2.20 6 -2 0 61.19 2.90 6 -2 0 61.19 2.50 -6 -2 0 65.99 2.10 6 2 0 63.09 3.00 -6 2 0 65.19 2.80 -6 2 0 64.79 2.30 6 2 0 68.09 3.60 -6 2 0 64.09 2.70 6 2 0 64.09 2.30 7 -2 0 166.98 5.80 -7 -2 0 167.18 4.80 7 -2 0 166.88 4.80 7 -2 0 161.48 4.60 -7 -2 0 164.78 4.40 7 2 0 165.58 5.80 -7 2 0 161.58 4.60 -7 2 0 168.58 5.30 -7 2 0 157.88 4.30 7 2 0 163.68 5.10 7 2 0 165.38 4.50 -7 2 0 164.48 5.00 -8 -2 0 399.26 9.70 8 -2 0 385.56 9.40 8 -2 0 381.16 9.60 8 -2 0 398.06 10.80 8 2 0 395.66 10.20 8 2 0 390.16 9.30 -8 2 0 386.86 9.40 8 2 0 392.46 11.20 -8 2 0 399.76 10.20 -8 2 0 386.16 9.70 9 -2 0 158.78 4.90 9 -2 0 157.48 6.30 -9 -2 0 162.78 5.60 -9 -2 0 164.18 4.90 -9 -2 0 161.88 5.10 9 -2 0 152.98 4.90 9 2 0 157.98 5.60 -9 2 0 150.48 4.90 9 2 0 165.38 6.90 9 2 0 160.08 4.80 -9 2 0 161.98 5.50 -9 2 0 153.28 4.90 -10 -2 0 30.00 2.70 -10 -2 0 32.90 2.10 -10 -2 0 30.90 2.40 10 -2 0 30.90 2.10 10 -2 0 32.10 3.10 10 -2 0 29.10 2.40 10 2 0 31.70 2.80 10 2 0 29.50 2.20 -10 2 0 35.10 3.00 10 2 0 31.90 3.30 -10 2 0 32.90 2.20 -11 -2 0 205.48 7.30 11 -2 0 210.48 6.30 -11 -2 0 204.68 6.00 11 -2 0 200.38 6.30 11 -2 0 203.68 7.80 11 2 0 209.48 8.40 -11 2 0 196.78 6.90 -11 2 0 204.38 6.10 11 2 0 198.78 5.90 11 2 0 200.18 6.70 -12 -2 0 82.79 3.70 -12 -2 0 79.69 4.60 12 -2 0 76.19 3.80 12 -2 0 87.79 5.80 12 -2 0 71.59 3.70 12 2 0 75.39 6.00 12 2 0 73.19 3.30 -12 2 0 74.69 3.50 12 2 0 79.69 4.40 -13 -2 0 35.10 3.80 13 -2 0 36.90 2.80 13 -2 0 30.00 2.60 13 -2 0 33.00 4.10 13 2 0 39.70 5.00 -13 2 0 35.40 2.70 -13 2 0 34.90 4.00 0 -3 0 0.20 0.40 0 -3 0 0.20 0.30 0 -3 0 0.40 0.40 0 3 0 0.60 0.40 0 3 0 0.80 0.60 0 3 0 0.00 0.20 0 3 0 1.30 0.40 0 3 0 0.00 0.30 1 -3 0 451.45 9.90 -1 -3 0 445.86 9.80 1 -3 0 448.86 9.70 1 -3 0 454.75 9.70 -1 -3 0 458.55 10.00 1 -3 0 446.06 9.90 -1 -3 0 442.56 9.80 -1 3 0 454.25 10.40 1 3 0 427.16 9.40 -1 3 0 445.46 10.00 1 3 0 449.86 9.80 1 3 0 461.75 10.20 1 3 0 455.65 10.00 -1 3 0 444.06 9.90 2 -3 0 622.84 13.50 -2 -3 0 613.24 13.20 2 -3 0 617.14 13.30 2 -3 0 607.44 13.30 -2 -3 0 619.34 13.50 -2 -3 0 617.44 13.40 2 -3 0 625.64 13.60 2 3 0 637.04 13.50 -2 3 0 621.04 13.70 2 3 0 643.24 13.70 -2 3 0 640.24 14.10 2 3 0 623.34 13.70 -2 3 0 621.64 13.60 -3 -3 0 732.93 16.00 3 -3 0 746.63 16.50 -3 -3 0 731.43 16.10 3 -3 0 748.03 16.20 3 -3 0 743.03 16.00 3 -3 0 755.42 16.20 -3 -3 0 750.52 16.00 -3 3 0 740.83 16.20 3 3 0 759.52 16.20 3 3 0 773.42 16.10 -3 3 0 758.52 16.80 3 3 0 744.33 16.50 -3 3 0 734.23 16.50 4 -3 0 1770.92 37.30 -4 -3 0 1725.83 37.30 -4 -3 0 1787.72 37.10 4 -3 0 1806.52 37.80 4 -3 0 1779.22 37.40 -4 3 0 1762.02 37.30 4 3 0 1750.92 36.90 -4 3 0 1763.52 37.80 4 3 0 1801.52 37.80 -4 3 0 1788.12 38.00 4 3 0 1772.72 37.30 4 3 0 1787.72 38.10 5 -3 0 1355.36 29.30 5 -3 0 1337.67 28.70 5 -3 0 1340.67 28.70 -5 -3 0 1353.16 28.40 -5 -3 0 1288.57 28.70 -5 -3 0 1367.36 28.90 -5 3 0 1385.46 29.40 -5 3 0 1323.27 29.10 -5 3 0 1337.97 28.70 5 3 0 1356.96 28.60 5 3 0 1344.17 29.70 5 3 0 1345.07 29.20 6 -3 0 934.31 21.10 6 -3 0 924.11 20.30 -6 -3 0 881.91 20.40 -6 -3 0 933.61 20.00 -6 -3 0 926.41 20.50 6 -3 0 937.71 20.30 6 3 0 961.80 21.60 6 3 0 946.61 20.10 -6 3 0 914.31 20.90 -6 3 0 913.51 20.90 6 3 0 938.41 21.00 -6 3 0 916.31 20.30 7 -3 0 25.60 2.20 -7 -3 0 22.00 1.90 7 -3 0 20.60 1.50 -7 -3 0 24.40 1.60 -7 -3 0 22.30 1.80 7 -3 0 21.00 1.60 7 3 0 22.90 2.40 7 3 0 24.20 2.10 -7 3 0 26.10 1.60 -7 3 0 21.90 1.90 7 3 0 24.50 1.60 -7 3 0 27.30 2.30 -8 -3 0 268.87 7.20 8 -3 0 257.87 8.00 8 -3 0 267.47 7.20 -8 -3 0 258.27 6.60 -8 -3 0 248.18 7.40 8 -3 0 254.57 6.80 -8 3 0 256.57 7.30 -8 3 0 253.37 6.80 -8 3 0 255.57 7.50 8 3 0 268.37 7.80 8 3 0 254.47 8.60 8 3 0 260.67 6.70 -9 -3 0 165.78 4.80 9 -3 0 159.68 5.30 9 -3 0 161.28 5.00 -9 -3 0 163.18 5.80 -9 -3 0 162.68 5.20 9 -3 0 173.28 6.40 9 3 0 161.78 7.00 9 3 0 162.98 4.90 -9 3 0 162.38 6.00 -9 3 0 165.28 5.10 9 3 0 164.78 5.70 -9 3 0 160.58 5.50 -10 -3 0 94.79 4.30 -10 -3 0 95.69 4.10 10 -3 0 94.09 4.10 10 -3 0 97.59 5.30 10 -3 0 92.59 3.90 -10 -3 0 95.89 3.90 -10 3 0 95.29 4.00 10 3 0 92.79 3.60 10 3 0 93.59 4.40 -10 3 0 96.79 4.90 10 3 0 92.89 5.50 11 -3 0 125.79 6.30 -11 -3 0 111.69 4.40 11 -3 0 118.79 4.40 -11 -3 0 110.99 5.40 11 -3 0 118.09 4.80 -11 -3 0 120.19 4.70 11 3 0 114.69 6.30 -11 3 0 111.39 4.30 11 3 0 112.39 4.00 -11 3 0 114.59 5.20 11 3 0 110.19 5.40 12 -3 0 8.10 2.80 -12 -3 0 3.40 2.10 12 -3 0 3.70 1.60 12 -3 0 3.50 1.90 12 3 0 1.90 3.40 12 3 0 3.20 2.20 -12 3 0 4.10 1.30 0 -4 0 50.49 1.80 0 -4 0 47.60 1.90 0 -4 0 48.80 1.70 0 4 0 48.90 1.70 0 4 0 45.50 1.70 0 4 0 47.50 1.80 0 4 0 52.79 2.30 1 -4 0 537.15 11.90 1 -4 0 529.85 11.60 1 -4 0 530.75 11.50 -1 -4 0 536.65 11.70 -1 -4 0 541.55 11.80 -1 -4 0 546.85 12.00 1 -4 0 543.25 11.90 1 4 0 549.74 12.40 1 4 0 545.75 11.90 -1 4 0 534.95 11.90 -1 4 0 530.25 11.90 1 4 0 488.15 11.20 1 4 0 528.15 12.00 -1 4 0 543.25 12.70 -2 -4 0 2.50 0.50 -2 -4 0 1.60 0.50 2 -4 0 2.30 0.40 2 -4 0 1.80 0.70 2 -4 0 1.30 0.80 2 -4 0 4.10 0.60 -2 4 0 1.70 1.30 2 4 0 3.40 1.00 -2 4 0 2.20 0.70 -2 4 0 2.30 0.70 2 4 0 1.30 0.50 2 4 0 1.30 0.70 -3 -4 0 86.39 2.60 3 -4 0 85.29 2.90 3 -4 0 88.59 2.90 -3 -4 0 84.69 2.40 3 -4 0 83.79 2.50 -3 -4 0 85.99 2.80 3 -4 0 85.59 2.50 3 4 0 90.29 2.90 -3 4 0 89.39 3.50 -3 4 0 89.29 3.10 3 4 0 87.39 2.80 3 4 0 85.89 3.20 -3 4 0 87.59 2.90 4 -4 0 2.00 1.00 4 -4 0 1.10 0.60 -4 -4 0 0.70 0.80 -4 -4 0 0.70 0.50 -4 -4 0 0.30 0.50 4 -4 0 0.00 0.50 4 4 0 1.40 0.70 -4 4 0 0.40 0.60 -4 4 0 0.90 1.00 4 4 0 0.50 1.20 -4 4 0 0.50 0.80 4 4 0 2.30 1.10 4 4 0 0.50 0.50 -5 -4 0 8.80 1.10 5 -4 0 12.20 1.10 -5 -4 0 10.60 1.40 -5 -4 0 10.90 1.00 5 -4 0 10.30 1.20 5 -4 0 9.50 1.30 5 -4 0 10.90 1.00 -5 4 0 8.50 1.00 5 4 0 11.90 1.10 5 4 0 12.10 1.50 5 4 0 11.80 1.60 5 4 0 10.20 0.90 -5 4 0 7.80 1.50 -5 4 0 8.60 1.60 6 -4 0 5.50 0.90 -6 -4 0 5.20 1.00 -6 -4 0 5.20 1.20 6 -4 0 4.80 1.00 6 -4 0 5.80 1.20 -6 -4 0 7.20 1.00 6 4 0 3.60 1.30 6 4 0 6.10 1.70 -6 4 0 5.30 1.80 -6 4 0 4.60 0.90 -6 4 0 8.30 1.40 6 4 0 5.00 1.00 7 -4 0 21.40 1.90 -7 -4 0 21.10 1.90 7 -4 0 20.80 1.60 -7 -4 0 21.70 1.80 7 -4 0 27.90 2.50 -7 -4 0 21.40 1.60 7 4 0 21.20 1.50 7 4 0 24.80 2.50 -7 4 0 22.00 2.10 7 4 0 21.60 2.40 -7 4 0 18.70 1.60 -7 4 0 19.70 2.00 -8 -4 0 155.88 5.10 -8 -4 0 148.59 5.10 8 -4 0 155.48 5.80 8 -4 0 150.08 4.90 -8 -4 0 152.38 4.50 8 -4 0 157.08 5.00 -8 4 0 156.28 4.90 -8 4 0 150.38 5.80 -8 4 0 145.79 5.40 8 4 0 154.58 4.70 8 4 0 153.18 5.60 8 4 0 148.59 6.50 9 -4 0 42.00 3.00 -9 -4 0 43.10 3.00 9 -4 0 46.40 2.80 9 -4 0 40.60 3.10 -9 -4 0 42.80 3.00 -9 -4 0 38.80 2.10 9 4 0 41.40 3.20 -9 4 0 39.60 3.00 -9 4 0 41.30 3.50 9 4 0 44.10 3.90 -9 4 0 41.90 2.80 9 4 0 45.00 2.30 10 -4 0 1.70 1.50 -10 -4 0 2.80 1.60 -10 -4 0 4.00 1.70 -10 -4 0 2.70 1.30 10 -4 0 1.90 2.10 10 -4 0 1.20 1.20 10 4 0 1.50 2.20 10 4 0 1.60 0.90 -10 4 0 3.40 1.90 -10 4 0 2.70 1.20 -10 4 0 1.90 1.50 10 4 0 -0.70 2.00 11 -4 0 125.09 4.70 -11 -4 0 122.69 5.30 -11 -4 0 130.79 5.10 11 -4 0 126.79 5.80 11 -4 0 127.49 5.20 -11 -4 0 115.99 4.90 -11 4 0 127.99 4.80 11 4 0 153.58 6.60 11 4 0 121.59 6.80 11 4 0 120.19 6.00 12 -4 0 -0.80 1.50 -12 -4 0 -0.10 1.70 12 -4 0 5.10 1.90 12 4 0 1.30 2.30 12 4 0 2.00 2.60 -12 4 0 2.70 1.80 0 -5 0 1.30 0.60 0 -5 0 1.50 0.60 0 -5 0 1.30 0.40 0 5 0 -0.80 1.30 0 5 0 0.80 0.60 0 5 0 0.90 0.60 0 5 0 0.00 0.60 -1 -5 0 6.90 0.80 -1 -5 0 7.60 1.00 1 -5 0 7.10 0.80 -1 -5 0 7.00 1.00 1 -5 0 7.60 0.90 1 -5 0 5.70 1.00 1 5 0 7.50 1.20 1 5 0 6.90 1.50 1 5 0 6.90 0.90 -1 5 0 8.70 0.90 -1 5 0 7.90 1.00 -1 5 0 6.40 0.80 -1 5 0 9.00 1.70 2 -5 0 13.80 1.10 -2 -5 0 15.10 1.20 -2 -5 0 15.50 1.20 2 -5 0 16.20 0.90 2 -5 0 18.30 1.40 2 -5 0 16.40 1.30 2 5 0 16.60 1.60 2 5 0 17.80 1.60 -2 5 0 16.40 1.50 -2 5 0 15.90 1.40 2 5 0 15.50 1.20 -2 5 0 16.70 2.10 3 -5 0 355.66 8.40 -3 -5 0 372.26 8.80 3 -5 0 360.76 8.80 3 -5 0 354.86 8.20 3 -5 0 371.26 8.90 -3 -5 0 376.96 8.80 -3 5 0 374.36 9.20 3 5 0 377.16 8.80 3 5 0 384.66 9.20 -3 5 0 363.46 8.90 3 5 0 375.46 9.10 -3 5 0 372.46 10.00 3 5 0 373.16 9.30 4 -5 0 458.85 10.80 4 -5 0 429.26 10.20 -4 -5 0 430.46 10.10 -4 -5 0 467.35 10.60 4 -5 0 449.46 10.30 -4 -5 0 471.55 10.80 4 -5 0 456.25 10.80 4 5 0 462.45 10.70 4 5 0 457.95 11.30 -4 5 0 452.25 11.10 -4 5 0 459.75 11.90 -4 5 0 461.75 10.90 4 5 0 478.95 10.90 5 -5 0 187.38 5.40 -5 -5 0 192.78 5.20 5 -5 0 186.98 5.40 5 -5 0 184.98 4.90 -5 -5 0 181.28 4.90 5 5 0 182.08 5.00 -5 5 0 193.88 5.40 5 5 0 191.98 5.30 -5 5 0 194.48 5.90 5 5 0 201.08 6.20 -5 5 0 189.58 6.30 5 5 0 192.08 6.20 6 -5 0 145.99 4.50 6 -5 0 144.19 4.20 -6 -5 0 146.69 4.30 -6 -5 0 145.49 4.80 6 -5 0 139.59 4.50 -6 5 0 135.99 5.40 -6 5 0 141.69 4.60 6 5 0 148.09 4.50 6 5 0 146.69 5.50 6 5 0 144.49 5.50 -6 5 0 146.99 5.30 7 -5 0 283.27 7.80 -7 -5 0 312.97 8.60 7 -5 0 306.77 8.20 -7 -5 0 322.87 7.90 7 -5 0 306.47 8.30 7 5 0 320.87 8.10 -7 5 0 311.27 9.50 7 5 0 325.67 9.30 -7 5 0 323.87 9.10 7 5 0 308.27 9.70 -7 5 0 309.47 8.20 8 -5 0 174.38 6.30 -8 -5 0 177.48 6.10 8 -5 0 177.18 5.80 -8 -5 0 180.28 5.30 8 -5 0 179.48 5.70 8 -5 0 175.78 5.70 8 5 0 166.98 6.80 -8 5 0 170.38 6.20 8 5 0 181.58 6.50 8 5 0 179.58 5.40 -8 5 0 177.18 5.70 -8 5 0 182.48 6.50 -9 -5 0 275.67 7.50 -9 -5 0 293.47 8.60 9 -5 0 283.27 8.00 9 -5 0 277.07 7.90 -9 5 0 272.77 9.00 9 5 0 280.07 8.90 9 5 0 288.67 10.20 -9 5 0 269.07 7.90 -9 5 0 294.87 8.90 10 -5 0 34.10 2.80 -10 -5 0 30.40 2.20 -10 -5 0 45.50 3.60 10 -5 0 36.00 3.10 10 -5 0 30.00 2.40 -10 5 0 37.80 3.30 -10 5 0 36.40 2.70 -10 5 0 40.20 3.50 10 5 0 40.80 4.60 10 5 0 32.20 2.60 10 5 0 35.30 3.40 11 -5 0 6.80 1.60 11 -5 0 10.30 2.00 -11 -5 0 9.80 2.30 11 -5 0 7.50 1.90 11 5 0 8.70 2.90 11 5 0 7.00 2.80 -11 5 0 9.00 1.70 0 -6 0 1459.35 31.30 0 -6 0 1483.25 31.90 0 -6 0 1460.15 31.70 0 6 0 1489.75 31.90 0 6 0 1481.75 31.80 0 6 0 1502.85 32.90 1 -6 0 746.33 16.80 1 -6 0 752.52 16.90 1 -6 0 726.03 16.30 -1 -6 0 747.53 16.50 -1 -6 0 758.42 16.80 -1 -6 0 751.82 16.90 -1 6 0 761.92 16.90 1 6 0 735.03 16.80 -1 6 0 750.32 18.00 1 6 0 760.52 17.20 -1 6 0 741.33 16.80 1 6 0 762.52 17.80 -2 -6 0 360.76 8.70 2 -6 0 375.66 9.10 2 -6 0 360.86 9.10 2 -6 0 353.26 8.40 -2 -6 0 380.26 9.00 -2 6 0 371.46 9.20 2 6 0 363.66 8.90 2 6 0 372.76 9.80 -2 6 0 348.67 10.10 -2 6 0 374.76 9.20 2 6 0 368.56 9.50 -2 6 0 366.16 8.90 -3 -6 0 192.28 5.30 3 -6 0 180.58 5.40 3 -6 0 186.68 5.30 -3 -6 0 184.68 5.20 3 -6 0 180.48 4.70 -3 6 0 189.58 5.70 3 6 0 188.68 6.00 -3 6 0 191.48 5.40 -3 6 0 173.98 6.30 3 6 0 182.48 5.10 3 6 0 187.88 5.80 3 6 0 180.88 5.60 -4 -6 0 135.69 4.20 4 -6 0 131.59 4.30 4 -6 0 128.29 4.30 4 6 0 140.09 5.20 -4 6 0 131.69 5.70 -4 6 0 139.79 4.40 4 6 0 138.79 4.50 4 6 0 138.79 4.60 -4 6 0 133.59 4.60 5 -6 0 139.39 4.70 5 -6 0 136.79 4.50 -5 -6 0 143.39 5.20 -5 -6 0 142.19 4.40 -5 6 0 140.49 6.00 5 6 0 141.79 4.60 -5 6 0 132.49 4.90 5 6 0 139.19 5.70 -5 6 0 138.29 4.80 5 6 0 157.08 5.70 6 -6 0 84.19 3.50 -6 -6 0 92.19 4.20 -6 -6 0 87.09 3.40 6 -6 0 83.99 3.70 -6 6 0 89.09 5.10 6 6 0 89.69 3.50 6 6 0 78.99 4.30 -6 6 0 89.09 3.60 6 6 0 87.89 4.70 -6 6 0 81.49 4.30 7 -6 0 102.49 4.00 7 -6 0 100.79 3.90 -7 -6 0 108.69 3.80 -7 -6 0 101.49 4.40 7 6 0 100.89 5.50 -7 6 0 102.39 5.50 7 6 0 98.29 3.70 7 6 0 101.09 5.30 -7 6 0 94.19 4.50 -7 6 0 103.39 4.00 -8 -6 0 52.19 2.80 8 -6 0 48.70 2.80 -8 -6 0 52.19 3.20 8 -6 0 49.40 3.30 -8 6 0 52.89 4.30 8 6 0 48.90 2.80 -8 6 0 48.10 3.80 -8 6 0 49.10 3.40 8 6 0 57.09 4.30 8 6 0 53.29 4.10 9 -6 0 14.40 2.20 -9 -6 0 13.00 2.70 9 -6 0 11.30 2.00 -9 -6 0 12.10 2.00 9 6 0 13.40 3.00 -9 6 0 15.10 3.00 9 6 0 11.20 1.60 -9 6 0 15.60 2.00 9 6 0 11.30 3.40 -9 6 0 14.70 2.70 10 -6 0 282.17 8.30 10 -6 0 233.88 7.90 -10 -6 0 293.77 8.90 -10 6 0 279.17 8.30 10 6 0 277.17 10.30 -10 6 0 279.97 9.30 10 6 0 286.97 9.90 0 -7 0 0.60 1.30 0 -7 0 -0.20 0.70 0 -7 0 -0.50 1.20 0 7 0 -0.50 1.20 0 7 0 1.00 2.00 0 7 0 0.00 1.00 -1 -7 0 38.10 2.00 1 -7 0 40.20 2.60 -1 -7 0 36.70 2.50 -1 -7 0 39.70 2.80 1 -7 0 36.40 2.70 -1 7 0 39.90 2.70 1 7 0 39.50 2.60 1 7 0 42.70 3.10 -1 7 0 38.50 3.20 -1 7 0 35.40 2.50 1 7 0 39.20 2.90 -2 -7 0 67.49 2.80 2 -7 0 62.29 2.90 2 -7 0 67.19 3.00 -2 -7 0 63.79 2.80 2 7 0 67.29 3.30 2 7 0 59.59 3.80 -2 7 0 66.49 3.00 -2 7 0 67.09 3.00 2 7 0 60.59 2.70 -2 7 0 69.19 4.00 -3 -7 0 10.10 1.20 -3 -7 0 8.80 1.40 3 -7 0 9.40 1.30 3 -7 0 8.90 1.60 -3 7 0 7.40 1.30 3 7 0 8.50 1.70 3 7 0 8.20 1.40 3 7 0 9.20 1.60 3 7 0 9.40 2.10 -3 7 0 10.40 2.10 -3 7 0 9.60 1.20 -4 -7 0 7.50 1.40 4 -7 0 8.30 1.40 4 -7 0 8.20 1.60 4 7 0 8.40 2.20 4 7 0 5.80 1.90 4 7 0 9.10 1.60 -4 7 0 6.70 1.80 -4 7 0 9.20 2.80 -4 7 0 7.80 1.40 5 -7 0 132.99 4.70 -5 -7 0 139.49 4.50 -5 -7 0 141.39 5.30 5 -7 0 138.69 5.10 -5 7 0 139.39 6.10 5 7 0 130.79 5.90 5 7 0 133.29 5.60 5 7 0 143.79 4.70 -5 7 0 141.89 5.10 -5 7 0 137.49 5.40 -6 -7 0 1.00 1.30 6 -7 0 1.60 1.50 6 -7 0 2.50 1.60 -6 -7 0 2.00 1.30 -6 7 0 3.10 1.90 6 7 0 1.10 1.60 -6 7 0 0.40 1.10 6 7 0 -0.40 1.20 -6 7 0 1.40 2.60 6 7 0 1.40 1.70 7 -7 0 6.90 1.40 -7 -7 0 4.00 1.40 -7 -7 0 5.60 2.10 7 -7 0 5.30 1.90 7 7 0 3.10 1.10 -7 7 0 3.10 1.70 7 7 0 5.10 2.60 -7 7 0 5.60 2.90 7 7 0 7.30 2.80 -8 -7 0 1.50 1.40 8 -7 0 0.50 1.50 8 -7 0 0.10 1.60 8 7 0 -1.80 2.50 -8 7 0 1.10 2.80 8 7 0 0.20 1.90 -8 7 0 -0.10 1.80 9 -7 0 14.30 2.30 9 -7 0 17.80 3.60 -9 -7 0 15.20 2.30 9 7 0 16.50 3.40 -9 7 0 12.70 2.00 9 7 0 17.80 3.20 -9 7 0 14.10 2.70 0 -8 0 122.29 4.60 0 -8 0 124.99 4.90 0 8 0 127.79 4.70 0 8 0 126.89 4.70 0 8 0 126.49 6.00 -1 -8 0 62.29 3.30 1 -8 0 68.29 3.70 1 -8 0 69.09 3.20 1 8 0 66.69 4.00 -1 8 0 58.69 4.10 -1 8 0 72.29 3.60 -1 8 0 64.19 3.10 1 8 0 63.59 3.00 1 8 0 68.89 3.90 -2 -8 0 47.00 2.90 2 -8 0 46.80 3.10 2 -8 0 44.00 3.10 -2 8 0 52.09 3.20 2 8 0 48.10 2.60 2 8 0 52.09 3.80 -2 8 0 49.10 4.30 2 8 0 52.29 3.90 -2 8 0 48.10 3.00 3 -8 0 46.70 3.20 -3 -8 0 51.59 3.00 3 -8 0 52.19 3.30 -3 8 0 51.89 4.40 -3 8 0 53.19 3.40 3 8 0 44.40 3.40 3 8 0 49.99 3.40 3 8 0 52.89 3.50 -4 -8 0 24.30 2.50 4 -8 0 19.90 2.10 -4 -8 0 21.40 2.10 4 -8 0 24.70 2.50 -4 8 0 23.80 2.20 4 8 0 24.20 2.40 -4 8 0 26.00 3.20 4 8 0 30.90 3.40 5 -8 0 45.20 3.50 5 -8 0 33.20 2.70 -5 -8 0 34.90 3.00 -5 -8 0 37.80 2.40 5 8 0 42.30 3.50 -5 8 0 33.50 4.20 -5 8 0 38.10 3.00 5 8 0 37.40 2.60 5 8 0 32.00 3.20 6 -8 0 5.50 2.00 -6 -8 0 6.30 1.60 6 -8 0 3.40 1.30 -6 -8 0 3.90 2.20 -6 8 0 4.50 1.50 6 8 0 5.10 1.70 6 8 0 1.20 2.70 -6 8 0 4.70 2.30 6 8 0 8.50 2.70 -7 -8 0 5.90 1.90 7 -8 0 6.70 2.10 7 -8 0 6.80 1.90 7 8 0 2.10 2.80 7 8 0 3.80 2.90 -7 8 0 4.90 2.00 -7 8 0 4.40 2.40 0 -9 0 0.90 1.50 0 9 0 -1.30 1.30 0 9 0 0.10 1.50 0 9 0 -0.20 2.50 1 -9 0 8.70 1.60 -1 -9 0 6.30 1.40 1 -9 0 7.00 1.90 -1 9 0 5.00 1.90 -1 9 0 8.30 2.40 1 9 0 9.20 1.90 1 9 0 9.30 1.60 1 9 0 8.70 2.20 -1 9 0 10.40 1.70 2 -9 0 42.90 2.90 -2 -9 0 39.90 3.10 2 -9 0 44.00 3.00 2 9 0 43.80 3.20 2 9 0 42.60 3.80 -2 9 0 47.60 4.60 -2 9 0 42.70 3.00 2 9 0 42.20 3.70 3 -9 0 11.30 1.80 3 -9 0 13.40 1.80 -3 -9 0 10.10 1.90 -3 -9 0 11.20 1.90 -3 9 0 9.80 1.80 3 9 0 11.30 2.80 -3 9 0 9.30 3.20 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201.68 4.40 0 1 -3 201.18 4.60 0 1 3 200.98 4.60 0 1 -3 199.88 4.20 -1 -1 -3 1636.94 33.60 1 -1 3 1582.94 34.40 -1 -1 -3 1629.04 34.70 1 -1 3 1641.64 33.90 1 -1 3 1616.64 34.50 -1 -1 -3 1656.43 34.80 1 -1 3 1595.64 33.80 -1 1 -3 1556.64 33.70 1 1 3 1525.05 33.80 -1 1 -3 1638.24 33.90 1 1 3 1612.44 35.40 1 1 3 1621.54 33.50 -1 1 -3 1593.04 34.80 -1 1 -3 1616.64 33.80 -1 1 -3 1586.54 34.60 -1 1 -3 1581.14 34.40 2 -1 3 580.74 12.70 -2 -1 -3 564.64 12.20 2 -1 3 573.24 12.00 2 -1 3 573.04 12.20 -2 -1 -3 567.54 12.20 -2 -1 -3 563.14 12.20 -2 1 -3 567.24 12.20 -2 1 -3 579.54 12.50 -2 1 -3 561.64 12.40 2 1 3 580.94 12.30 2 1 3 563.64 12.60 2 1 3 573.54 12.50 -3 -1 -3 1953.10 41.20 3 -1 3 1974.50 40.40 3 -1 3 1918.11 40.00 -3 -1 -3 1881.91 41.00 3 -1 3 1913.01 40.80 -3 -1 -3 1870.81 40.50 3 -1 3 1875.41 41.20 -3 1 -3 1879.41 41.20 -3 1 -3 1873.11 40.00 3 1 3 1965.50 40.40 3 1 3 1927.41 41.30 -3 1 -3 1852.21 40.10 -3 1 -3 1905.51 41.30 3 1 3 1938.01 40.20 4 -1 3 2009.10 42.80 -4 -1 -3 1955.50 42.50 -4 -1 -3 1992.10 42.50 4 -1 3 2008.80 41.90 4 -1 3 2049.59 42.60 4 -1 3 1990.10 42.30 -4 -1 -3 1916.21 41.70 4 1 3 2029.00 42.80 -4 1 -3 1933.71 41.80 -4 1 -3 2010.80 42.00 -4 1 -3 1995.90 42.00 -4 1 -3 2004.20 41.70 4 1 3 2037.80 42.60 4 1 3 2016.30 42.20 5 -1 3 295.17 6.90 -5 -1 -3 304.87 6.90 5 -1 3 298.47 7.30 -5 -1 -3 298.37 7.00 -5 -1 -3 304.27 7.00 5 -1 3 308.17 8.00 5 -1 3 290.87 7.00 -5 -1 -3 280.77 6.40 -5 1 -3 295.97 7.30 5 1 3 290.17 8.10 5 1 3 293.87 7.00 -5 1 -3 294.97 7.00 5 1 3 299.37 7.50 -5 1 -3 293.07 6.40 -5 1 -3 295.07 7.10 5 1 3 286.47 6.40 6 -1 3 628.74 15.00 6 -1 3 620.24 13.90 -6 -1 -3 584.34 13.00 -6 -1 -3 626.54 13.90 -6 -1 -3 606.04 13.70 6 -1 3 621.04 14.10 -6 -1 -3 638.74 13.70 -6 1 -3 623.94 13.90 6 1 3 629.04 13.90 6 1 3 641.14 15.20 -6 1 -3 601.44 13.10 6 1 3 635.44 14.50 -6 1 -3 597.74 13.80 -6 1 -3 627.94 14.30 -7 -1 -3 552.54 13.00 7 -1 3 568.14 12.70 7 -1 3 559.14 14.10 -7 -1 -3 551.44 12.90 7 -1 3 549.54 13.10 7 -1 3 575.44 12.90 -7 -1 -3 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2 4 215.08 7.00 -9 -2 -4 136.39 4.40 -9 -2 -4 152.08 5.20 9 -2 4 146.09 6.40 9 -2 4 143.19 4.60 9 -2 4 142.49 4.70 -9 2 -4 148.09 5.60 9 2 4 153.98 4.90 9 2 4 146.99 6.50 -9 2 -4 146.59 4.80 9 2 4 149.19 5.60 -10 -2 -4 30.30 2.40 10 -2 4 35.10 2.40 10 -2 4 29.40 2.30 10 -2 4 33.40 3.40 10 2 4 39.90 4.60 10 2 4 35.10 3.30 10 2 4 31.50 2.20 -10 2 -4 32.60 2.30 -11 -2 -4 182.08 5.90 11 -2 4 177.98 5.80 11 -2 4 193.78 8.10 11 2 4 161.88 7.70 -11 2 -4 172.48 6.70 11 2 4 181.38 5.80 -11 2 -4 167.18 5.70 11 2 4 178.28 6.90 -12 -2 -4 33.70 3.50 12 -2 4 33.10 3.70 12 -2 4 37.80 3.00 -12 -2 -4 33.20 2.80 -12 2 -4 44.40 3.20 12 2 4 35.20 3.60 -12 2 -4 36.40 3.40 12 2 4 41.10 3.10 12 2 4 43.60 5.20 13 -3 -4 4.20 1.60 13 -3 -4 4.20 1.60 13 -3 -4 3.40 1.80 -13 -3 4 1.40 1.30 -13 -3 4 3.00 2.30 -13 3 4 3.70 2.60 -13 3 4 2.30 1.60 13 3 -4 5.50 3.40 12 -3 -4 -0.10 1.90 12 -3 -4 0.20 1.50 -12 -3 4 3.20 1.40 12 -3 -4 -0.30 1.30 -12 -3 4 1.70 1.60 -12 3 4 1.70 1.50 12 3 -4 1.80 3.10 -12 3 4 4.80 2.40 12 3 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810.42 19.40 -7 3 4 842.92 18.30 6 -3 -4 26.80 1.80 -6 -3 4 26.10 1.20 6 -3 -4 25.60 2.00 -6 -3 4 26.90 1.80 6 -3 -4 29.80 1.70 6 -3 -4 27.80 1.60 -6 -3 4 26.40 1.90 6 3 -4 26.00 2.00 6 3 -4 26.50 1.20 -6 3 4 25.40 1.70 6 3 -4 29.50 2.40 -6 3 4 28.10 2.30 6 3 -4 29.10 1.10 -5 -3 4 577.94 12.70 -5 -3 4 585.24 13.50 5 -3 -4 589.94 13.30 -5 -3 4 574.24 13.60 5 -3 -4 599.84 13.50 5 -3 -4 599.44 13.20 -5 3 4 594.14 13.20 5 3 -4 612.84 12.90 -5 3 4 584.54 14.00 5 3 -4 581.14 12.80 5 3 -4 597.74 13.40 4 -3 -4 115.69 3.50 -4 -3 4 114.79 3.60 -4 -3 4 117.89 2.90 4 -3 -4 117.29 3.30 -4 -3 4 114.29 3.50 4 -3 -4 122.19 3.30 4 -3 -4 117.39 3.60 4 3 -4 117.89 3.50 4 3 -4 120.49 3.00 -4 3 4 113.09 3.50 4 3 -4 121.99 3.30 -4 3 4 114.49 2.60 -4 3 4 119.69 4.00 -4 3 4 115.49 3.30 4 3 -4 116.89 2.80 3 -3 -4 600.24 13.20 -3 -3 4 578.54 13.20 -3 -3 4 595.34 12.60 -3 -3 4 589.94 13.30 3 -3 -4 603.04 13.10 3 -3 -4 590.64 13.20 -3 -3 4 585.74 13.30 3 3 -4 611.24 13.20 3 3 -4 619.94 13.20 3 3 -4 584.74 12.60 -3 3 4 599.64 13.10 3 3 -4 584.34 12.80 -3 3 4 572.84 12.60 -3 3 4 603.54 13.10 3 3 -4 587.44 12.60 -3 3 4 595.64 13.80 -2 -3 4 2548.95 55.49 2 -3 -4 2517.75 54.69 2 -3 -4 2557.74 55.29 -2 -3 4 2672.33 54.99 -2 -3 4 2520.45 54.99 2 -3 -4 2634.44 55.89 -2 -3 4 2550.94 54.99 -2 3 4 2617.84 54.29 2 3 -4 2586.14 55.19 -2 3 4 2559.94 54.59 2 3 -4 2607.24 54.09 2 3 -4 2586.84 55.09 -2 3 4 2495.75 55.39 -2 3 4 2594.64 55.49 1 -3 -4 147.99 3.90 -1 -3 4 152.58 3.60 -1 -3 4 149.49 3.90 -1 -3 4 150.38 4.10 1 -3 -4 152.98 3.90 1 -3 -4 149.79 3.90 -1 3 4 150.18 3.90 -1 3 4 154.78 4.50 -1 3 4 145.59 3.40 1 3 -4 150.68 3.60 1 3 -4 150.08 3.70 -1 3 4 152.48 3.90 1 3 -4 154.18 4.20 0 -3 -4 337.57 7.80 0 -3 -4 338.37 7.70 0 -3 -4 337.97 7.80 0 -3 4 338.47 7.50 0 -3 4 340.87 8.00 0 -3 4 330.17 7.60 0 -3 4 335.27 7.50 0 3 4 336.67 7.90 0 3 -4 340.27 7.80 0 3 -4 337.47 7.10 0 3 4 334.87 7.70 0 3 4 351.96 8.20 0 3 -4 349.27 8.30 0 3 -4 343.87 7.60 -1 -3 -4 10.60 0.90 1 -3 4 9.10 0.60 1 -3 4 9.20 0.70 1 -3 4 10.70 0.90 -1 -3 -4 11.10 0.90 1 -3 4 11.90 0.80 -1 -3 -4 9.50 0.90 1 3 4 9.40 0.90 1 3 4 15.40 1.20 -1 3 -4 11.20 0.90 -1 3 -4 10.90 1.20 1 3 4 9.80 0.90 -1 3 -4 9.50 0.80 1 3 4 11.60 1.20 -2 -3 -4 381.36 8.70 2 -3 4 391.66 8.00 -2 -3 -4 383.66 8.80 2 -3 4 364.46 8.20 2 -3 4 388.66 9.10 2 -3 4 386.26 8.70 -2 -3 -4 384.86 8.80 2 -3 4 386.06 8.50 -2 3 -4 384.16 9.00 2 3 4 382.76 9.20 2 3 4 375.16 9.10 2 3 4 387.46 8.90 -2 3 -4 389.26 8.70 -2 3 -4 391.76 9.40 -3 -3 -4 485.25 11.00 3 -3 4 448.36 10.10 3 -3 4 481.35 10.60 -3 -3 -4 476.25 10.40 3 -3 4 483.15 11.50 3 -3 4 482.75 10.80 -3 -3 -4 485.85 10.90 -3 3 -4 488.55 10.80 3 3 4 484.35 11.00 -3 3 -4 498.05 11.30 -3 3 -4 483.55 11.50 3 3 4 493.75 11.50 3 3 4 479.35 11.50 4 -3 4 1336.87 29.40 4 -3 4 1362.76 28.60 4 -3 4 1329.77 28.30 -4 -3 -4 1336.17 28.50 -4 -3 -4 1342.37 28.70 4 3 4 1327.87 29.30 4 3 4 1317.87 28.70 -4 3 -4 1352.96 28.60 4 3 4 1364.46 29.50 -4 3 -4 1344.57 29.30 -4 3 -4 1339.67 29.10 -5 -3 -4 1999.00 41.90 -5 -3 -4 2010.00 42.40 -5 -3 -4 2011.70 42.60 5 -3 4 2013.00 43.50 5 -3 4 2027.40 42.50 5 -3 4 1959.40 42.20 -5 3 -4 1992.60 43.10 -5 3 -4 1996.30 43.00 5 3 4 2059.19 43.40 5 3 4 2025.00 42.60 5 3 4 2018.30 43.70 -5 3 -4 2052.69 42.60 -6 -3 -4 352.36 8.60 6 -3 4 346.47 8.40 6 -3 4 365.86 9.80 6 -3 4 359.06 8.70 6 3 4 369.76 9.70 6 3 4 360.66 8.70 -6 3 -4 352.56 8.70 -6 3 -4 367.66 9.30 -6 3 -4 345.77 9.30 6 3 4 347.47 9.90 7 -3 4 458.65 12.30 7 -3 4 456.85 11.20 -7 -3 -4 489.85 11.40 -7 -3 -4 473.35 11.10 7 -3 4 458.35 10.90 7 3 4 472.15 12.10 -7 3 -4 462.85 11.70 -7 3 -4 475.65 11.90 7 3 4 477.55 11.20 -7 3 -4 463.05 11.20 7 3 4 471.75 12.80 -8 -3 -4 397.26 9.70 8 -3 4 402.46 11.30 8 -3 4 392.86 9.90 8 -3 4 384.56 9.60 -8 -3 -4 401.56 9.90 8 3 4 394.06 9.80 -8 3 -4 377.36 10.60 -8 3 -4 391.26 9.90 8 3 4 400.66 11.70 -8 3 -4 388.66 10.30 8 3 4 397.96 11.00 -9 -3 -4 262.07 7.20 9 -3 4 264.17 7.20 9 -3 4 257.27 7.40 -9 -3 -4 277.87 7.50 9 -3 4 275.07 9.00 9 3 4 267.47 9.70 -9 3 -4 262.67 8.30 9 3 4 263.37 8.60 9 3 4 263.67 7.40 -9 3 -4 270.97 7.50 -10 -3 -4 244.58 7.20 10 -3 4 245.98 7.40 10 -3 4 242.78 8.90 -10 3 -4 247.98 8.00 10 3 4 246.18 7.20 10 3 4 240.88 8.40 10 3 4 264.87 10.00 -10 3 -4 245.88 7.40 11 -3 4 3.00 2.50 11 -3 4 3.00 1.70 -11 -3 -4 2.90 1.80 -11 -3 -4 1.90 1.60 -11 3 -4 2.70 1.70 11 3 4 4.40 2.70 11 3 4 2.30 1.50 -11 3 -4 -0.50 2.10 11 3 4 0.80 1.60 -12 -3 -4 3.90 1.60 12 -3 4 4.00 2.80 -12 -3 -4 3.50 1.40 12 -3 4 2.90 1.70 -12 3 -4 4.40 1.90 12 3 4 3.10 1.30 12 3 4 1.50 1.70 12 3 4 -0.80 3.40 12 -4 -4 45.60 3.60 -12 -4 4 46.10 3.40 -12 -4 4 49.50 3.60 12 -4 -4 47.30 3.20 12 4 -4 49.30 5.20 -12 4 4 46.00 3.30 -12 4 4 44.40 4.20 12 4 -4 41.80 3.80 11 -4 -4 2.70 1.50 11 -4 -4 6.00 1.60 -11 -4 4 6.60 2.10 11 -4 -4 7.60 2.20 -11 -4 4 3.70 1.50 -11 4 4 5.50 2.20 -11 4 4 6.40 1.40 11 4 -4 7.20 3.20 11 4 -4 8.00 1.90 -10 -4 4 41.10 2.90 10 -4 -4 42.80 2.50 10 -4 -4 42.30 2.90 -10 -4 4 38.60 3.30 10 -4 -4 40.70 3.30 10 4 -4 41.90 3.40 10 4 -4 36.00 3.60 -10 4 4 45.80 2.60 -10 4 4 43.60 3.60 -10 4 4 40.40 3.00 -9 -4 4 1.40 1.10 9 -4 -4 3.20 1.30 9 -4 -4 0.90 1.40 -9 -4 4 1.20 1.60 9 -4 -4 0.00 1.60 -9 4 4 3.50 1.40 9 4 -4 -1.00 2.20 9 4 -4 2.00 1.90 -9 4 4 -1.40 1.10 -9 4 4 5.50 1.50 8 -4 -4 43.40 2.90 -8 -4 4 43.90 3.00 -8 -4 4 41.80 1.90 8 -4 -4 42.70 2.30 8 -4 -4 42.10 2.70 -8 -4 4 40.80 2.90 8 4 -4 42.50 3.30 -8 4 4 54.59 3.60 8 4 -4 46.90 2.90 -8 4 4 42.60 2.30 8 4 -4 39.60 1.80 -7 -4 4 1.60 0.90 7 -4 -4 0.80 1.10 -7 -4 4 0.70 0.60 7 -4 -4 2.30 1.10 7 -4 -4 -0.20 1.10 7 -4 -4 2.10 1.10 -7 -4 4 1.00 0.90 7 4 -4 0.90 1.10 7 4 -4 0.10 0.60 -7 4 4 2.20 1.10 -7 4 4 4.00 1.80 7 4 -4 0.40 1.20 -6 -4 4 4.70 0.70 6 -4 -4 4.70 1.20 6 -4 -4 5.00 0.90 6 -4 -4 3.10 1.00 -6 -4 4 5.20 1.30 6 -4 -4 3.10 0.80 -6 -4 4 4.20 0.90 6 4 -4 4.10 1.20 6 4 -4 4.80 0.60 -6 4 4 4.70 1.70 -6 4 4 3.90 0.90 6 4 -4 5.40 1.10 -5 -4 4 129.29 3.40 -5 -4 4 129.39 4.10 5 -4 -4 130.29 4.20 5 -4 -4 135.79 4.00 5 -4 -4 124.39 3.90 -5 -4 4 130.19 4.20 5 4 -4 130.79 3.60 5 4 -4 128.49 4.10 -5 4 4 130.19 3.90 -5 4 4 140.69 5.10 5 4 -4 136.89 3.70 4 -4 -4 11.50 1.10 -4 -4 4 12.90 1.20 -4 -4 4 9.70 0.70 4 -4 -4 11.60 1.30 4 -4 -4 11.80 1.20 -4 -4 4 12.50 1.30 -4 4 4 11.80 1.00 4 4 -4 12.60 0.90 4 4 -4 12.30 0.40 4 4 -4 11.90 1.20 4 4 -4 11.80 1.20 -4 4 4 11.40 1.10 -4 4 4 11.00 1.60 -4 4 4 10.60 0.70 -3 -4 4 113.69 3.60 -3 -4 4 108.59 3.00 -3 -4 4 106.59 3.30 3 -4 -4 112.99 3.30 3 -4 -4 126.19 3.60 3 -4 -4 112.19 3.50 -3 4 4 105.89 4.00 3 4 -4 109.59 3.00 3 4 -4 109.29 2.70 3 4 -4 116.29 3.50 3 4 -4 110.99 3.50 -3 4 4 108.69 2.90 -3 4 4 109.39 3.10 -3 4 4 109.39 3.30 2 -4 -4 642.34 14.80 2 -4 -4 665.13 14.90 -2 -4 4 684.13 14.90 -2 -4 4 659.53 14.90 -2 -4 4 670.83 14.40 2 -4 -4 682.53 14.80 2 4 -4 698.63 15.20 -2 4 4 654.13 14.30 2 4 -4 668.83 14.30 2 4 -4 670.13 14.40 -2 4 4 652.93 14.50 -2 4 4 682.23 15.70 -2 4 4 665.73 14.80 -1 -4 4 39.80 1.70 1 -4 -4 47.60 2.10 -1 -4 4 43.50 1.90 -1 -4 4 42.70 1.60 1 -4 -4 41.90 1.80 1 -4 -4 40.90 1.80 -1 4 4 44.80 1.90 1 4 -4 46.00 1.70 1 4 -4 48.90 2.20 -1 4 4 42.40 1.10 -1 4 4 46.10 2.40 1 4 -4 44.30 1.70 -1 4 4 43.20 1.90 0 -4 4 20.10 1.40 0 -4 4 22.20 1.10 0 -4 4 21.00 1.20 0 -4 4 18.60 1.20 0 -4 -4 19.90 1.30 0 -4 -4 18.90 1.30 0 -4 -4 21.40 1.40 0 4 -4 20.20 1.30 0 4 4 22.10 1.90 0 4 -4 22.10 1.60 0 4 4 21.50 1.60 0 4 -4 19.60 1.20 0 4 4 21.90 1.40 1 -4 4 26.50 1.30 -1 -4 -4 24.00 1.60 1 -4 4 24.90 1.10 1 -4 4 25.40 1.30 1 -4 4 24.70 1.50 -1 -4 -4 28.20 1.60 -1 -4 -4 28.20 1.40 -1 4 -4 29.10 1.50 1 4 4 33.40 2.10 1 4 4 27.70 1.40 -1 4 -4 28.10 1.30 -1 4 -4 26.70 2.10 1 4 4 27.30 2.00 2 -4 4 98.09 2.90 -2 -4 -4 94.79 3.00 -2 -4 -4 95.59 3.00 2 -4 4 97.89 2.80 2 -4 4 90.99 2.60 -2 -4 -4 92.69 3.00 2 -4 4 96.89 3.20 2 4 4 93.69 3.40 2 4 4 96.49 3.20 -2 4 -4 100.19 3.20 2 4 4 97.59 3.30 -2 4 -4 101.09 3.80 2 4 4 93.89 3.20 -2 4 -4 94.49 2.90 3 -4 4 409.96 9.10 -3 -4 -4 374.86 8.40 3 -4 4 388.76 8.30 3 -4 4 400.26 9.60 3 -4 4 363.56 8.50 -3 -4 -4 401.86 9.40 3 -4 4 405.36 9.30 -3 -4 -4 371.66 8.50 -3 -4 -4 401.26 9.20 3 4 4 403.66 10.00 -3 4 -4 407.76 9.30 -3 4 -4 395.86 10.10 -3 4 -4 391.36 9.60 3 4 4 399.96 9.90 3 4 4 411.16 9.50 -4 -4 -4 47.90 2.00 4 -4 4 43.50 1.30 -4 -4 -4 44.70 1.70 4 -4 4 46.60 1.50 4 -4 4 48.30 2.20 4 -4 4 47.10 2.00 -4 -4 -4 48.80 2.20 -4 4 -4 44.40 2.60 -4 4 -4 53.39 2.30 4 4 4 47.80 2.10 4 4 4 46.70 2.70 -4 4 -4 47.10 2.50 4 4 4 44.50 2.60 -5 -4 -4 56.39 2.30 -5 -4 -4 55.69 2.40 5 -4 4 53.79 2.50 5 -4 4 57.69 2.30 5 -4 4 57.59 2.90 -5 -4 -4 48.80 2.10 -5 4 -4 52.19 3.20 -5 4 -4 53.79 3.00 5 4 4 53.29 3.40 5 4 4 55.59 3.50 5 4 4 54.29 2.50 -5 4 -4 49.20 2.40 6 -4 4 26.90 1.80 6 -4 4 25.20 1.80 -6 -4 -4 24.80 1.70 6 -4 4 26.30 2.50 -6 -4 -4 27.30 2.00 6 4 4 23.10 2.60 6 4 4 26.90 1.80 -6 4 -4 26.20 2.20 -6 4 -4 23.50 2.40 -6 4 -4 25.30 1.80 6 4 4 24.30 2.80 -7 -4 -4 3.20 1.30 7 -4 4 3.60 1.30 7 -4 4 1.70 1.00 7 -4 4 2.60 1.70 -7 -4 -4 3.10 1.10 -7 -4 -4 2.40 1.00 -7 4 -4 2.90 1.70 7 4 4 2.70 1.60 7 4 4 5.50 1.30 -7 4 -4 4.60 1.80 7 4 4 3.40 1.50 -7 4 -4 2.70 1.20 8 -4 4 147.09 4.70 -8 -4 -4 141.59 4.80 -8 -4 -4 153.38 4.90 -8 -4 -4 160.88 5.30 8 -4 4 153.38 5.10 8 -4 4 153.48 6.20 -8 4 -4 152.38 5.10 8 4 4 149.49 6.40 -8 4 -4 149.39 5.80 -8 4 -4 151.88 5.60 8 4 4 151.78 5.00 8 4 4 157.28 6.00 -9 -4 -4 3.60 1.50 -9 -4 -4 2.20 1.10 9 -4 4 4.90 2.20 9 -4 4 2.00 1.50 -9 -4 -4 3.60 1.50 -9 4 -4 4.10 2.20 9 4 4 4.60 1.50 9 4 4 4.10 2.40 -9 4 -4 0.60 1.30 9 4 4 2.40 3.00 -9 4 -4 1.60 1.60 10 -4 4 25.50 2.90 10 -4 4 27.00 2.30 -10 -4 -4 22.50 2.00 -10 -4 -4 25.30 2.50 -10 4 -4 23.90 2.20 10 4 4 26.00 4.20 10 4 4 24.10 2.10 -10 4 -4 23.50 2.70 10 4 4 25.10 3.40 11 -4 4 48.00 3.60 11 -4 4 41.80 4.10 -11 4 -4 53.59 3.80 11 4 4 49.30 4.00 11 4 4 41.60 3.20 11 4 4 53.99 5.40 11 -5 -4 2.80 1.30 -11 -5 4 6.20 2.20 11 -5 -4 1.90 2.10 11 5 -4 2.30 3.30 11 5 -4 3.70 1.90 -11 5 4 3.70 1.40 -11 5 4 4.40 1.70 10 -5 -4 19.80 2.60 10 -5 -4 21.80 2.00 -10 -5 4 21.60 2.40 10 -5 -4 22.70 2.40 -10 5 4 18.30 2.40 10 5 -4 19.70 3.00 -10 5 4 22.20 2.80 10 5 -4 17.80 2.90 -10 5 4 26.70 2.30 9 -5 -4 88.49 4.00 -9 -5 4 97.99 4.30 9 -5 -4 87.69 4.20 9 -5 -4 93.89 4.50 9 -5 -4 87.09 4.00 -9 5 4 101.39 4.70 -9 5 4 87.89 5.10 9 5 -4 97.79 4.60 -9 5 4 99.79 4.20 9 5 -4 89.39 5.80 -8 -5 4 133.89 5.20 8 -5 -4 123.19 4.40 8 -5 -4 134.99 5.10 8 -5 -4 128.49 4.70 -8 5 4 128.09 4.80 8 5 -4 119.69 6.00 -8 5 4 129.49 4.50 -8 5 4 126.49 5.40 8 5 -4 137.79 5.60 -7 -5 4 419.96 10.90 7 -5 -4 424.66 10.40 7 -5 -4 427.26 10.50 7 -5 -4 423.36 10.80 -7 -5 4 416.36 9.70 -7 -5 4 397.46 10.50 7 5 -4 417.86 9.80 -7 5 4 411.56 11.50 -7 5 4 423.86 10.50 7 5 -4 419.36 11.70 -7 5 4 404.06 10.70 7 5 -4 426.46 11.00 -6 -5 4 811.92 17.60 6 -5 -4 816.62 18.30 -6 -5 4 829.22 18.90 6 -5 -4 812.92 18.60 6 -5 -4 808.12 18.30 -6 -5 4 784.42 18.30 6 5 -4 790.82 19.40 -6 5 4 804.62 19.50 6 5 -4 811.52 18.70 -6 5 4 791.92 18.40 6 5 -4 816.42 17.70 -6 5 4 812.92 18.30 5 -5 -4 53.29 2.90 -5 -5 4 51.29 2.00 5 -5 -4 53.09 2.60 -5 -5 4 51.59 2.60 -5 -5 4 50.09 2.40 5 -5 -4 54.89 2.60 5 5 -4 51.09 2.90 5 5 -4 55.69 2.40 -5 5 4 54.79 2.60 5 5 -4 51.59 2.20 -5 5 4 55.39 3.70 -5 5 4 51.99 2.40 4 -5 -4 623.74 13.90 4 -5 -4 602.74 13.80 4 -5 -4 609.84 14.10 -4 -5 4 610.44 14.30 -4 -5 4 577.64 13.60 -4 -5 4 597.94 13.30 -4 5 4 603.64 15.00 4 5 -4 604.24 13.50 4 5 -4 618.64 13.90 4 5 -4 600.54 14.10 -4 5 4 599.44 13.90 -4 5 4 594.34 13.60 -3 -5 4 277.77 6.70 -3 -5 4 277.07 7.40 3 -5 -4 281.27 7.10 3 -5 -4 283.97 7.30 3 -5 -4 273.67 7.10 -3 5 4 277.77 7.10 -3 5 4 268.17 6.60 3 5 -4 285.27 6.70 3 5 -4 281.67 7.20 -3 5 4 271.37 6.70 -3 5 4 295.97 8.20 3 5 -4 298.67 7.60 -2 -5 4 250.97 6.40 -2 -5 4 249.68 6.60 -2 -5 4 251.07 6.10 2 -5 -4 248.38 6.60 2 -5 -4 256.47 6.50 2 -5 -4 255.97 6.50 -2 5 4 248.88 6.50 2 5 -4 250.87 5.90 2 5 -4 247.48 6.10 2 5 -4 271.27 7.10 2 5 -4 269.37 6.70 -2 5 4 260.27 7.40 -2 5 4 240.18 5.60 -2 5 4 243.08 6.30 -1 -5 4 495.15 11.10 -1 -5 4 476.65 10.80 1 -5 -4 467.95 11.20 -1 -5 4 474.95 11.20 1 -5 -4 480.65 11.20 1 -5 -4 490.65 11.10 -1 5 4 479.05 12.00 1 5 -4 484.85 11.80 1 5 -4 475.85 10.90 1 5 -4 493.05 10.80 -1 5 4 469.55 11.20 -1 5 4 480.95 11.20 0 -5 4 249.38 6.20 0 -5 -4 237.78 6.20 0 -5 -4 242.18 6.20 0 -5 4 243.38 6.00 0 -5 4 237.48 6.10 0 -5 4 231.78 6.00 0 -5 -4 240.68 6.20 0 5 -4 238.08 6.10 0 5 -4 241.18 6.00 0 5 -4 237.08 6.80 0 5 4 249.88 6.40 0 5 4 245.78 6.90 0 5 4 233.08 6.20 1 -5 4 88.39 2.90 1 -5 4 86.49 2.90 1 -5 4 85.29 2.80 -1 -5 -4 86.99 3.10 1 -5 4 87.49 2.80 -1 -5 -4 89.49 3.10 -1 -5 -4 86.19 3.00 1 5 4 85.69 3.70 1 5 4 89.09 3.10 -1 5 -4 92.69 3.70 -1 5 -4 85.59 3.10 1 5 4 94.79 3.60 -1 5 -4 85.89 2.90 2 -5 4 1.10 0.70 -2 -5 -4 2.10 0.90 2 -5 4 1.00 0.50 2 -5 4 2.50 0.80 -2 -5 -4 1.20 0.90 2 -5 4 1.60 0.80 -2 -5 -4 3.30 0.80 -2 5 -4 1.30 1.10 2 5 4 0.20 1.00 2 5 4 1.30 0.80 2 5 4 0.30 0.90 -2 5 -4 0.80 0.80 -2 5 -4 0.80 1.30 2 5 4 2.20 1.20 2 5 4 0.60 1.00 3 -5 4 137.29 4.00 3 -5 4 130.69 4.10 -3 -5 -4 139.79 4.20 -3 -5 -4 145.79 4.30 3 -5 4 129.09 4.00 3 5 4 135.89 4.40 -3 5 -4 137.69 4.10 -3 5 -4 138.89 5.20 3 5 4 145.09 4.50 3 5 4 135.29 4.60 -3 5 -4 134.49 4.60 3 5 4 140.79 5.00 4 -5 4 21.60 1.80 4 -5 4 22.50 1.70 -4 -5 -4 25.50 2.00 -4 -5 -4 22.00 1.60 4 -5 4 25.10 1.70 4 5 4 20.10 1.70 -4 5 -4 22.60 2.50 4 5 4 21.50 2.10 4 5 4 25.00 2.20 -4 5 -4 23.00 1.70 -4 5 -4 23.90 2.20 5 -5 4 115.59 3.90 5 -5 4 114.39 4.00 -5 -5 -4 115.29 4.00 -5 -5 -4 119.79 3.90 5 -5 4 112.69 3.70 -5 5 -4 118.59 4.70 -5 5 -4 115.89 4.70 5 5 4 125.19 5.10 5 5 4 119.09 4.10 5 5 4 116.59 5.00 -5 5 -4 112.59 3.90 6 -5 4 213.88 5.90 -6 -5 -4 226.78 6.20 6 -5 4 215.38 6.20 -6 5 -4 215.78 6.80 6 5 4 215.38 7.40 -6 5 -4 219.08 7.30 6 5 4 227.38 6.30 6 5 4 210.88 7.30 -6 5 -4 221.48 6.20 -7 -5 -4 131.19 4.80 -7 -5 -4 118.09 4.30 7 -5 4 118.39 4.50 7 -5 4 126.29 4.20 -7 5 -4 131.49 5.10 -7 5 -4 118.79 5.10 7 5 4 130.09 4.60 7 5 4 120.79 5.30 -7 5 -4 120.49 4.50 7 5 4 120.99 6.00 -8 -5 -4 147.89 5.10 8 -5 4 143.79 5.00 -8 -5 -4 162.88 5.70 -8 5 -4 159.98 6.40 -8 5 -4 141.79 6.10 8 5 4 156.78 7.20 -8 5 -4 139.99 5.00 8 5 4 159.98 5.30 8 5 4 149.99 6.70 -9 -5 -4 57.39 3.30 9 -5 4 52.69 3.10 9 -5 4 52.69 3.80 -9 -5 -4 51.09 3.60 -9 5 -4 56.09 4.50 9 5 4 61.19 4.90 -9 5 -4 50.19 3.10 9 5 4 58.29 3.30 9 5 4 50.19 4.80 -10 -5 -4 90.99 4.20 10 -5 4 96.19 5.10 -10 -5 -4 96.19 4.60 10 -5 4 90.19 4.50 10 5 4 91.79 5.10 -10 5 -4 89.29 4.90 10 5 4 95.99 4.30 -10 5 -4 80.99 4.50 10 5 4 85.49 5.80 -11 6 4 175.48 6.50 11 6 -4 180.38 7.70 -10 -6 4 60.39 4.40 10 -6 -4 55.99 4.00 10 -6 -4 51.89 3.60 10 6 -4 54.59 4.70 -10 6 4 49.40 4.30 -10 6 4 50.19 3.60 -10 6 4 54.69 3.90 10 6 -4 54.19 4.00 -9 -6 4 178.28 6.80 9 -6 -4 172.78 6.30 9 -6 -4 180.08 5.80 9 6 -4 167.08 7.10 -9 6 4 164.78 6.10 -9 6 4 169.58 7.30 9 6 -4 170.68 8.00 -9 6 4 164.48 5.70 8 -6 -4 4.80 1.60 -8 -6 4 6.50 1.60 8 -6 -4 3.00 1.80 -8 6 4 5.10 2.00 8 6 -4 6.40 2.00 -8 6 4 4.40 1.70 8 6 -4 5.60 2.30 -8 6 4 7.10 1.70 7 -6 -4 75.39 3.40 7 -6 -4 79.29 3.60 -7 -6 4 74.39 4.00 7 -6 -4 80.09 3.90 -7 6 4 52.39 3.60 7 6 -4 70.49 3.80 -7 6 4 76.39 3.70 -7 6 4 74.09 4.40 7 6 -4 73.39 4.70 6 -6 -4 41.40 2.60 6 -6 -4 39.40 2.60 6 -6 -4 43.80 2.80 -6 -6 4 43.10 2.80 -6 -6 4 44.80 1.90 -6 6 4 44.90 3.90 6 6 -4 48.60 3.40 6 6 -4 41.10 3.50 -6 6 4 41.40 2.80 6 6 -4 39.90 2.10 -5 -6 4 2.90 1.10 -5 -6 4 2.80 0.80 5 -6 -4 2.30 0.90 5 -6 -4 1.20 1.40 5 -6 -4 3.00 1.00 -5 6 4 1.50 1.00 5 6 -4 2.60 1.50 -5 6 4 1.70 1.60 5 6 -4 1.10 0.60 5 6 -4 2.70 1.20 4 -6 -4 13.50 1.80 -4 -6 4 14.80 1.30 -4 -6 4 14.70 1.90 4 -6 -4 14.10 1.50 4 -6 -4 10.80 1.30 -4 6 4 13.00 1.50 4 6 -4 11.70 1.50 4 6 -4 11.30 1.30 4 6 -4 15.40 1.80 -4 6 4 10.50 2.40 -3 -6 4 944.81 21.40 3 -6 -4 926.71 20.80 -3 -6 4 957.40 20.50 3 -6 -4 930.41 21.00 3 -6 -4 947.81 21.20 -3 6 4 944.41 21.10 3 6 -4 973.30 21.50 3 6 -4 929.91 20.50 3 6 -4 955.60 21.30 -3 6 4 938.61 22.40 -3 6 4 915.71 20.60 2 -6 -4 266.67 6.80 2 -6 -4 259.47 6.90 -2 -6 4 262.87 6.60 2 -6 -4 256.97 7.00 -2 -6 4 260.97 7.20 2 6 -4 271.67 7.70 -2 6 4 254.87 6.80 2 6 -4 263.77 7.10 -2 6 4 265.97 8.20 -2 6 4 244.18 6.90 2 6 -4 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435.96 11.30 -3 4 -9 438.26 10.30 -3 4 -9 446.36 11.10 3 4 9 412.56 11.10 3 4 9 442.26 10.70 -3 4 -9 438.96 11.40 -4 -4 -9 7.90 1.00 4 -4 9 9.50 1.80 -4 -4 -9 9.10 1.20 4 -4 9 7.70 1.10 -4 -4 -9 9.70 1.30 -4 4 -9 8.50 1.70 4 4 9 11.00 1.30 4 4 9 8.10 1.70 -4 4 -9 10.00 1.30 -4 4 -9 9.90 1.90 4 4 9 10.40 2.00 5 -4 9 665.83 15.30 -5 -4 -9 675.43 15.40 -5 -4 -9 676.43 15.50 5 4 9 665.73 16.60 5 4 9 618.34 16.50 -5 4 -9 676.33 16.50 5 4 9 659.43 15.50 -5 4 -9 661.23 15.30 -5 4 -9 657.93 16.10 -6 -4 -9 848.82 19.10 6 -4 9 831.62 18.90 -6 -4 -9 836.82 19.20 6 4 9 805.02 20.50 -6 4 -9 820.32 18.90 -6 4 -9 840.82 19.90 6 4 9 839.22 20.50 6 4 9 833.62 19.20 -6 4 -9 824.22 20.00 7 -4 9 357.76 11.00 -7 -4 -9 374.86 10.00 -7 -4 -9 382.86 9.90 7 -4 9 372.46 9.70 -7 4 -9 354.86 10.60 7 4 9 383.06 10.10 -7 4 -9 386.66 10.80 7 4 9 386.06 11.40 -7 4 -9 384.26 9.80 7 4 9 358.66 11.30 8 -4 9 120.69 4.50 8 -4 9 117.89 6.00 -8 -4 -9 122.49 4.50 8 4 9 122.89 6.80 8 4 9 124.29 4.70 -8 4 -9 116.39 5.10 8 4 9 112.59 5.60 -8 4 -9 119.79 5.80 -8 4 -9 126.19 4.60 9 -4 9 8.00 2.10 -9 -4 -9 7.70 1.90 9 -4 9 5.90 1.90 9 4 9 3.50 3.00 9 4 9 6.60 1.90 -9 4 -9 13.60 2.30 9 4 9 9.90 2.30 -9 4 -9 6.30 1.90 -10 -4 -9 110.49 5.00 10 -4 9 109.39 5.80 10 -4 9 104.99 4.60 10 4 9 112.59 6.40 -10 4 -9 114.39 5.60 -10 4 -9 110.59 4.70 10 4 9 117.59 6.60 11 -5 -9 16.80 2.40 -11 -5 9 21.70 2.60 11 -5 -9 17.10 2.20 -11 -5 9 15.50 2.80 11 -5 -9 18.20 2.20 -11 5 9 18.10 2.30 11 5 -9 16.10 3.00 11 5 -9 15.50 2.80 -11 5 9 17.10 2.70 10 -5 -9 49.00 3.80 10 -5 -9 46.00 3.00 10 -5 -9 52.09 3.80 -10 -5 9 40.50 3.60 -10 -5 9 51.59 3.60 10 5 -9 50.69 4.70 -10 5 9 49.90 3.20 -10 5 9 48.50 3.80 10 5 -9 45.10 3.30 -9 -5 9 15.90 2.20 9 -5 -9 13.50 2.10 9 -5 -9 16.50 2.00 9 -5 -9 13.80 2.30 -9 -5 9 18.50 2.50 9 5 -9 16.20 2.10 -9 5 9 20.40 2.10 9 5 -9 14.80 3.10 -9 5 9 17.00 2.40 -9 5 9 16.80 2.40 8 -5 -9 13.20 2.30 8 -5 -9 13.20 2.20 -8 -5 9 14.60 2.30 8 -5 -9 13.00 1.50 -8 -5 9 14.40 1.90 8 5 -9 12.90 1.80 8 5 -9 17.90 2.80 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187.68 5.50 2 5 -9 192.18 6.20 2 5 -9 189.98 5.20 -2 5 9 198.58 5.60 -2 5 9 190.28 5.40 2 5 -9 190.88 4.80 1 -5 -9 560.74 13.10 1 -5 -9 556.64 13.00 -1 -5 9 573.24 13.60 -1 -5 9 560.14 12.40 -1 -5 9 554.94 12.90 1 -5 -9 558.74 13.20 1 5 -9 565.34 13.90 1 5 -9 556.74 12.40 1 5 -9 557.44 12.90 -1 5 9 546.55 13.00 -1 5 9 551.04 13.20 0 -5 9 632.44 14.70 0 -5 -9 651.73 15.10 0 -5 9 659.53 15.60 0 -5 -9 647.74 15.00 0 -5 9 660.93 14.50 0 -5 -9 645.94 15.00 0 5 -9 659.73 16.00 0 5 9 642.14 14.90 0 5 9 653.23 15.40 0 5 -9 671.13 14.50 0 5 -9 661.93 15.00 -1 -5 -9 530.75 12.10 -1 -5 -9 517.35 12.10 -1 -5 -9 499.55 12.10 1 -5 9 526.75 12.70 1 -5 9 511.25 11.60 1 -5 9 488.85 11.50 -1 5 -9 500.15 13.00 1 5 9 458.75 11.90 1 5 9 510.65 12.80 -1 5 -9 522.65 11.70 -1 5 -9 534.45 12.40 1 5 9 521.15 12.50 -2 -5 -9 61.59 3.00 -2 -5 -9 59.59 2.80 2 -5 9 64.19 3.10 2 -5 9 65.89 2.70 -2 -5 -9 59.99 2.60 -2 5 -9 63.89 3.20 2 5 9 58.59 3.00 2 5 9 65.09 3.30 -2 5 -9 61.09 2.60 2 5 9 66.09 3.10 -2 5 -9 59.59 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19.80 2.50 8 5 9 19.00 2.10 8 5 9 25.90 3.70 -9 -5 -9 50.79 3.50 -9 -5 -9 51.29 3.70 9 -5 9 42.40 3.00 -9 5 -9 42.60 3.10 9 5 9 51.79 3.70 9 5 9 50.79 4.70 -9 5 -9 50.79 4.30 9 5 9 50.19 4.90 -9 5 -9 41.10 3.50 10 -6 -9 80.49 4.60 10 -6 -9 83.19 4.20 -10 -6 9 80.79 4.70 10 -6 -9 74.69 4.30 10 6 -9 82.09 4.60 -10 6 9 80.49 4.30 10 6 -9 74.49 6.10 9 -6 -9 8.30 1.80 9 -6 -9 9.20 2.50 -9 -6 9 5.90 1.80 9 -6 -9 6.70 2.10 9 6 -9 9.00 2.40 9 6 -9 9.30 2.40 -9 6 9 8.00 1.90 8 -6 -9 25.40 2.90 8 -6 -9 26.20 2.20 8 -6 -9 27.90 2.80 -8 -6 9 23.30 2.50 8 6 -9 29.10 3.60 -8 6 9 24.70 2.20 8 6 -9 29.90 3.00 7 -6 -9 19.70 2.50 7 -6 -9 17.50 2.00 -7 -6 9 17.70 2.20 7 -6 -9 16.60 1.90 -7 6 9 15.00 2.00 7 6 -9 18.30 2.50 -7 6 9 29.30 3.60 -6 -6 9 4.10 1.40 6 -6 -9 2.90 1.50 6 -6 -9 1.20 1.60 6 -6 -9 1.50 1.80 -6 6 9 6.20 2.50 6 6 -9 3.00 1.70 -6 6 9 3.00 1.50 5 -6 -9 17.20 1.90 5 -6 -9 20.80 2.20 -5 -6 9 19.20 2.30 5 -6 -9 19.90 2.30 -5 6 9 26.20 2.90 -5 6 9 21.30 2.10 5 6 -9 19.00 1.90 5 6 -9 20.40 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38.60 3.00 -7 6 -9 29.80 3.20 -7 6 -9 31.30 3.50 -7 6 -9 30.80 2.80 7 6 9 29.70 3.70 7 6 9 28.00 2.80 7 6 9 26.00 3.90 -8 -6 -9 7.60 1.70 8 -6 9 6.50 2.00 8 6 9 9.30 3.20 -8 6 -9 8.50 2.20 8 6 9 5.00 2.30 8 6 9 7.00 1.60 -8 6 -9 4.30 2.70 -8 6 -9 7.90 2.00 9 -7 -9 82.29 4.40 -9 -7 9 85.29 5.50 9 -7 -9 74.79 4.30 -9 7 9 88.49 4.50 9 7 -9 77.39 5.40 9 7 -9 74.39 4.50 -8 -7 9 2.80 2.20 8 -7 -9 5.70 2.00 8 -7 -9 5.60 1.80 8 -7 -9 5.20 1.50 -8 7 9 6.10 1.50 8 7 -9 7.00 2.40 8 7 -9 5.30 2.90 7 -7 -9 4.00 1.60 -7 -7 9 2.20 2.10 7 -7 -9 1.80 1.30 7 -7 -9 0.50 1.20 -7 7 9 2.70 2.80 -7 7 9 1.80 1.30 7 7 -9 1.80 2.10 6 -7 -9 13.50 1.90 6 -7 -9 11.00 2.10 6 -7 -9 7.50 1.90 -6 -7 9 12.00 2.00 6 7 -9 8.00 2.10 -6 7 9 16.40 2.80 -6 7 9 12.70 2.10 -5 -7 9 50.99 3.60 5 -7 -9 48.90 2.90 5 -7 -9 48.90 3.40 5 -7 -9 54.29 3.70 5 7 -9 53.19 3.20 -5 7 9 52.49 4.20 -5 7 9 52.29 3.10 4 -7 -9 45.90 3.20 4 -7 -9 47.20 3.40 -4 -7 9 47.50 3.00 4 -7 -9 48.40 3.20 4 7 -9 45.00 3.00 -4 7 9 49.60 3.30 4 7 -9 52.59 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-10 41.50 2.60 -4 -4 10 42.90 2.60 4 -4 -10 43.70 2.00 4 4 -10 45.20 2.10 -4 4 10 39.90 2.10 -4 4 10 46.00 2.30 4 4 -10 47.20 2.70 3 -4 -10 3.30 0.70 -3 -4 10 8.10 1.20 -3 -4 10 5.30 1.00 3 -4 -10 4.20 1.00 3 -4 -10 8.50 1.50 -3 -4 10 4.80 0.50 -3 4 10 4.40 0.70 -3 4 10 4.70 0.80 3 4 -10 4.70 0.40 -3 4 10 6.10 0.90 3 4 -10 5.30 1.30 3 4 -10 5.00 1.00 -2 -4 10 58.59 1.80 2 -4 -10 58.29 2.30 -2 -4 10 64.59 3.00 2 -4 -10 61.39 2.70 2 -4 -10 61.59 2.90 -2 -4 10 60.79 2.60 2 4 -10 58.39 3.10 -2 4 10 59.49 2.40 2 4 -10 62.49 2.60 -2 4 10 63.39 2.50 2 4 -10 59.69 1.80 -1 -4 10 168.88 4.70 1 -4 -10 166.98 4.70 1 -4 -10 171.48 4.80 1 -4 -10 166.18 5.00 -1 -4 10 164.78 4.10 -1 -4 10 168.88 5.30 -1 4 10 172.98 5.10 -1 4 10 171.78 4.80 1 4 -10 165.68 4.90 1 4 -10 170.88 4.20 1 4 -10 164.88 5.50 -1 4 10 157.18 4.20 0 -4 10 94.59 3.90 0 -4 -10 93.29 3.40 0 -4 10 91.69 3.00 0 -4 -10 97.59 3.30 0 -4 10 93.19 2.80 0 -4 -10 96.79 3.20 0 4 10 92.09 3.50 0 4 -10 107.19 3.70 0 4 -10 91.49 3.80 0 4 10 81.29 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0.30 1.60 9 -6 -14 0.70 1.10 9 6 -14 -0.70 1.80 9 6 -14 -1.30 1.90 -9 6 14 -0.60 1.70 -9 6 14 0.20 1.50 8 -6 -14 58.09 3.10 8 -6 -14 56.99 4.10 -8 -6 14 66.79 4.70 8 -6 -14 66.89 4.40 -8 6 14 61.09 4.90 -8 6 14 59.19 3.20 8 6 -14 60.99 4.10 -7 -6 14 35.50 3.10 7 -6 -14 37.30 3.00 7 -6 -14 34.30 2.40 7 -6 -14 38.50 3.40 -7 6 14 35.10 4.30 7 6 -14 34.30 2.80 -7 6 14 32.70 2.70 6 -6 -14 186.48 6.90 6 -6 -14 188.78 6.10 -6 -6 14 179.48 6.60 6 -6 -14 179.58 6.60 6 6 -14 187.38 6.40 -6 6 14 190.98 6.20 5 -6 -14 130.99 4.70 5 -6 -14 135.99 5.10 -5 -6 14 128.79 5.20 -5 -6 14 134.99 5.30 5 -6 -14 131.59 5.30 -5 6 14 145.79 5.10 5 6 -14 133.59 5.60 -4 -6 14 93.79 4.70 4 -6 -14 98.59 3.80 4 -6 -14 98.59 4.40 4 -6 -14 91.79 4.00 -4 -6 14 93.89 4.40 4 6 -14 94.39 4.80 -4 6 14 90.69 3.80 -3 -6 14 248.68 7.60 3 -6 -14 254.57 7.50 3 -6 -14 262.37 7.40 3 -6 -14 260.77 7.80 -3 -6 14 259.97 8.10 -3 6 14 270.97 7.50 3 6 -14 256.77 8.50 -2 -6 14 220.48 6.90 -2 -6 14 228.18 7.70 2 -6 -14 228.08 6.80 2 -6 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7.20 1.50 -2 3 -22 3.50 2.40 -2 3 -22 9.40 2.30 6 -4 -22 6.20 2.60 -6 -4 22 1.90 2.30 -6 4 22 6.50 3.40 6 4 -22 2.70 1.80 6 4 -22 1.50 1.40 -5 -4 22 -0.10 1.50 5 -4 -22 3.00 2.40 5 4 -22 0.00 1.30 5 4 -22 0.80 1.60 -5 4 22 -0.60 2.00 4 -4 -22 0.50 2.10 -4 -4 22 -1.80 2.20 4 4 -22 -0.40 1.60 4 4 -22 0.10 1.90 -4 4 22 3.40 2.90 3 -4 -22 26.40 3.10 -3 -4 22 26.00 3.40 3 4 -22 30.40 3.30 -3 4 22 33.10 4.60 3 4 -22 30.80 3.90 -2 -4 22 6.00 2.50 2 -4 -22 3.50 2.10 2 4 -22 5.50 2.30 2 4 -22 2.30 1.90 -2 4 22 5.40 3.00 -1 -4 22 45.50 4.30 1 -4 -22 49.99 4.00 1 -4 -22 40.50 2.60 1 -4 -22 39.60 3.10 -1 4 22 40.40 2.70 -1 4 22 45.00 4.80 1 4 -22 37.10 3.30 1 4 -22 42.90 4.00 0 -4 -22 9.40 1.90 0 -4 -22 9.30 2.30 0 -4 -22 7.10 2.30 0 -4 22 9.30 2.90 0 4 -22 5.00 2.90 0 4 22 10.50 2.50 0 4 -22 12.30 2.80 0 4 22 9.70 1.90 1 -4 22 11.40 2.50 -1 -4 -22 8.50 1.90 -1 -4 -22 10.40 1.90 -1 -4 -22 9.80 1.60 1 4 22 13.80 2.10 -1 4 -22 9.30 2.70 -1 4 -22 10.40 2.40 8 0 -23 1.30 2.10 -8 0 23 -0.90 1.70 -7 0 23 -2.10 1.50 7 0 -23 2.60 2.10 -7 0 23 -1.30 2.40 -6 0 23 2.00 1.70 6 0 -23 1.70 1.90 -6 0 23 1.00 1.80 -5 0 23 -0.70 2.40 5 0 -23 1.50 1.80 5 0 -23 -0.80 2.20 -5 0 23 2.50 1.90 -4 0 23 -0.60 2.30 4 0 -23 3.80 1.80 4 0 -23 -1.90 1.50 -4 0 23 -1.70 1.70 3 0 -23 -0.40 1.10 3 0 -23 1.50 1.70 -3 0 23 0.10 1.30 -3 0 23 0.10 2.20 -2 0 23 -0.70 1.50 -2 0 23 -0.20 1.80 2 0 -23 2.90 1.70 -1 0 23 1.80 1.50 1 0 -23 0.90 1.60 -1 0 23 0.40 2.00 0 0 23 1.20 1.50 0 0 23 2.30 2.00 0 0 -23 0.70 1.60 -1 0 -23 1.40 2.20 1 0 23 0.10 1.50 2 0 23 1.50 2.30 -2 0 -23 -1.00 2.30 -8 -1 23 61.29 4.80 -8 -1 23 48.70 3.90 8 -1 -23 50.09 3.80 -8 1 23 49.80 4.70 8 1 -23 47.30 3.70 7 -1 -23 98.09 5.30 -7 -1 23 100.99 5.10 -7 -1 23 111.39 6.70 -7 1 23 108.49 7.00 -6 -1 23 33.10 3.60 6 -1 -23 36.50 3.30 -6 -1 23 40.30 3.50 6 1 -23 43.50 4.00 -6 1 23 43.80 4.30 -5 -1 23 293.57 9.60 5 -1 -23 304.37 9.30 -5 -1 23 296.97 10.50 5 1 -23 323.27 10.40 -5 1 23 311.07 11.40 -5 1 23 294.17 9.10 4 -1 -23 372.06 10.60 -4 -1 23 380.96 12.10 -4 -1 23 359.36 11.10 4 -1 -23 374.36 11.90 -4 1 23 357.06 10.60 -4 1 23 377.56 12.80 4 1 -23 396.06 11.90 3 -1 -23 90.99 5.10 -3 -1 23 94.09 5.30 3 -1 -23 89.89 4.40 -3 -1 23 88.99 5.20 -3 1 23 86.29 4.40 3 1 -23 97.09 5.00 -3 1 23 95.99 6.10 -2 -1 23 114.89 5.50 -2 -1 23 115.79 6.10 2 -1 -23 105.59 5.40 2 -1 -23 104.89 4.70 -2 1 23 115.89 6.40 2 1 -23 106.99 5.40 -2 1 23 107.09 5.40 -1 -1 23 58.19 4.50 1 -1 -23 49.30 3.30 -1 -1 23 51.69 4.30 1 -1 -23 62.89 4.70 1 1 -23 54.49 4.00 -1 1 23 55.59 4.70 -1 1 23 46.40 3.80 0 -1 -23 48.50 4.10 0 -1 23 50.69 4.10 0 -1 23 46.00 4.20 0 -1 -23 49.20 3.10 0 1 23 43.90 4.00 0 1 23 47.30 4.00 0 1 -23 46.70 3.80 -1 -1 -23 91.59 4.90 1 -1 23 95.19 5.50 -1 1 -23 89.49 5.00 1 1 23 87.39 5.50 -2 -1 -23 2.10 2.30 2 -1 23 6.00 2.60 -2 1 -23 -0.70 2.20 2 1 23 2.90 2.30 -2 1 -23 1.60 1.70 7 -2 -23 58.29 4.60 -7 -2 23 70.69 5.60 -7 -2 23 67.39 4.50 -7 2 23 64.59 5.80 7 2 -23 66.39 4.20 -6 -2 23 3.40 2.60 -6 -2 23 5.20 2.20 6 -2 -23 7.40 2.50 -6 2 23 8.50 2.60 6 2 -23 7.30 1.90 -5 -2 23 3.20 1.60 5 -2 -23 5.00 2.30 -5 -2 23 3.50 1.90 -5 2 23 3.90 2.80 5 2 -23 6.10 2.40 -4 -2 23 27.60 3.70 4 -2 -23 27.10 3.00 -4 -2 23 36.80 3.50 -4 2 23 31.00 4.30 4 2 -23 29.60 3.00 -3 -2 23 6.50 2.30 3 -2 -23 6.60 1.70 -3 -2 23 3.20 2.40 3 -2 -23 7.20 2.10 3 2 -23 7.40 2.50 -3 2 23 5.50 2.80 2 -2 -23 69.59 4.10 -2 -2 23 73.59 5.00 -2 -2 23 69.19 4.60 2 -2 -23 69.79 4.50 2 2 -23 88.29 4.70 -2 2 23 78.09 5.60 1 -2 -23 114.89 4.90 -1 -2 23 114.19 5.90 1 -2 -23 110.99 5.50 -1 -2 23 122.49 5.60 -1 2 23 111.89 5.40 1 2 -23 116.89 5.50 -1 2 23 111.99 6.00 1 2 -23 127.29 6.80 0 -2 23 33.00 3.50 0 -2 23 42.10 3.70 0 -2 -23 34.40 3.70 0 -2 -23 35.30 2.90 0 2 23 29.70 3.30 0 2 -23 35.60 3.30 0 2 -23 35.50 3.60 0 2 23 35.50 3.40 -1 -2 -23 112.49 5.40 -1 -2 -23 89.49 4.10 1 -2 23 103.29 5.90 -1 2 -23 103.89 5.80 1 2 23 101.09 5.30 -1 2 -23 104.79 5.30 -2 -2 -23 149.99 5.30 -2 -2 -23 164.78 7.20 -2 -2 -23 145.89 6.60 2 -2 23 144.19 7.60 -2 2 -23 150.98 6.50 -2 2 -23 156.48 7.40 2 2 23 148.49 7.00 2 2 23 129.09 5.30 -6 -3 23 36.50 3.70 -6 -3 23 36.20 4.20 6 -3 -23 42.10 3.50 -6 3 23 50.79 5.50 6 3 -23 37.90 3.30 6 3 -23 45.30 4.30 5 -3 -23 3.50 2.30 -5 -3 23 4.10 2.60 -5 -3 23 3.10 1.70 5 3 -23 5.40 2.50 5 3 -23 1.60 2.10 -5 3 23 2.40 2.20 -4 -3 23 4.30 2.30 4 -3 -23 1.80 1.50 4 3 -23 0.50 2.10 4 3 -23 2.50 1.80 -4 3 23 1.80 2.10 -3 -3 23 6.70 2.60 3 -3 -23 9.70 1.90 3 3 -23 10.20 3.00 -3 3 23 10.70 2.70 3 3 -23 8.70 2.50 -2 -3 23 4.10 1.90 2 -3 -23 6.40 2.10 2 -3 -23 3.50 1.80 -2 3 23 4.80 2.20 2 3 -23 5.30 2.10 2 3 -23 6.30 2.00 1 -3 -23 4.00 1.50 -1 -3 23 3.00 1.80 1 -3 -23 6.90 2.40 1 3 -23 4.40 2.40 1 3 -23 2.80 1.90 -1 3 23 4.30 2.60 0 -3 -23 -1.60 2.00 0 -3 -23 -0.90 1.70 0 -3 23 -3.30 2.30 0 3 -23 2.50 2.00 0 3 23 -0.90 1.70 0 3 -23 0.40 2.30 -1 -3 -23 9.60 2.20 -1 -3 -23 10.40 2.60 -1 -3 -23 5.00 2.40 1 -3 23 11.00 3.10 -1 3 -23 4.90 1.90 -1 3 -23 11.40 2.50 1 3 23 7.10 1.90 -4 -4 23 3.90 1.90 4 -4 -23 1.80 1.70 4 4 -23 1.80 2.40 4 4 -23 3.70 1.60 -4 4 23 4.70 2.40 -3 -4 23 4.80 2.50 3 -4 -23 0.10 2.10 3 4 -23 -0.50 1.90 -3 4 23 2.90 3.00 3 4 -23 1.70 2.40 2 -4 -23 78.19 4.70 2 -4 -23 83.69 5.40 -2 -4 23 78.99 5.70 2 4 -23 77.59 5.00 -2 4 23 83.99 6.50 2 4 -23 81.19 5.80 -7 0 24 29.40 2.90 7 0 -24 29.20 3.10 -7 0 24 21.20 3.30 -6 0 24 93.99 4.90 6 0 -24 107.19 5.10 -6 0 24 102.29 6.60 -5 0 24 337.07 10.10 -5 0 24 322.07 11.80 5 0 -24 313.57 9.40 5 0 -24 348.37 11.40 -4 0 24 312.17 9.90 4 0 -24 311.87 10.50 -4 0 24 340.77 11.70 -3 0 24 18.40 3.40 -3 0 24 16.20 2.80 3 0 -24 16.60 2.60 -2 0 24 14.00 2.60 -2 0 24 18.00 2.50 2 0 -24 18.40 3.10 -1 0 24 19.50 3.00 -1 0 24 17.90 3.00 1 0 -24 18.60 3.20 0 0 -24 33.60 3.30 0 0 24 30.90 3.50 0 0 24 35.20 4.30 -1 0 -24 43.90 3.70 1 0 24 41.90 3.90 -7 -1 24 41.30 4.30 7 -1 -24 48.80 3.90 -7 -1 24 48.80 3.80 7 1 -24 42.80 4.10 -7 1 24 51.49 4.90 6 -1 -24 0.70 2.00 -6 -1 24 0.30 1.80 -6 -1 24 1.50 2.40 6 1 -24 -0.40 2.20 -6 1 24 -0.70 2.60 -5 -1 24 63.99 4.10 -5 -1 24 63.59 5.40 5 -1 -24 70.69 4.30 5 1 -24 63.59 5.10 -5 1 24 67.69 5.80 -4 -1 24 3.60 2.10 4 -1 -24 2.00 1.40 4 -1 -24 2.10 2.60 -4 -1 24 5.70 2.70 -4 1 24 1.40 1.90 -4 1 24 0.60 1.70 4 1 -24 1.90 2.40 -3 -1 24 15.60 2.40 3 -1 -24 14.90 3.00 -3 -1 24 17.60 2.80 3 -1 -24 15.30 2.30 3 1 -24 17.90 2.60 -3 1 24 20.70 3.50 -3 1 24 17.60 2.60 -2 -1 24 93.19 5.50 -2 -1 24 94.49 5.70 2 -1 -24 89.29 4.30 2 -1 -24 89.89 5.10 -2 1 24 100.39 6.10 -2 1 24 89.69 4.70 2 1 -24 84.99 5.60 -1 -1 24 56.39 4.60 1 -1 -24 46.80 3.90 -1 -1 24 55.79 4.00 1 -1 -24 50.29 4.30 -1 1 24 49.10 4.00 -1 1 24 50.69 4.60 1 1 -24 57.29 4.50 0 -1 -24 -1.90 2.20 0 -1 24 1.90 2.20 0 1 24 0.90 2.00 0 1 24 -1.10 3.10 0 1 -24 2.10 2.30 -1 -1 -24 14.70 2.90 1 -1 24 15.70 3.20 -1 1 -24 17.70 2.90 1 1 24 11.60 2.70 -1 1 -24 16.30 3.10 -6 -2 24 84.29 5.50 -6 -2 24 92.39 4.80 6 2 -24 90.29 5.00 -6 2 24 98.69 6.40 -5 -2 24 75.09 5.00 5 -2 -24 90.39 5.00 -5 -2 24 89.29 6.00 5 2 -24 85.99 5.40 -5 2 24 94.59 6.70 -4 -2 24 44.80 4.10 -4 -2 24 43.90 3.60 4 -2 -24 41.30 3.50 -4 2 24 40.00 4.80 4 2 -24 43.40 3.90 3 -2 -24 4.40 2.00 -3 -2 24 2.60 2.20 -3 -2 24 4.60 2.50 3 -2 -24 2.70 1.50 3 2 -24 5.30 2.50 -3 2 24 0.40 2.60 -2 -2 24 1.80 2.40 2 -2 -24 0.30 1.80 -2 -2 24 0.50 1.60 2 -2 -24 0.90 1.80 -2 2 24 0.60 2.50 2 2 -24 1.50 1.70 -1 -2 24 18.20 2.60 1 -2 -24 17.60 2.40 1 -2 -24 20.80 2.70 -1 -2 24 16.10 3.10 1 2 -24 15.90 2.80 -1 2 24 19.00 3.40 1 2 -24 18.50 3.10 0 -2 -24 42.10 2.90 0 -2 24 37.50 4.20 0 -2 -24 39.20 3.90 0 2 -24 33.20 3.80 0 2 -24 43.50 4.50 0 2 24 40.30 3.90 -4 -3 24 55.19 4.20 4 -3 -24 58.59 3.80 4 3 -24 60.39 4.70 -4 3 24 60.09 5.20 4 3 -24 47.60 4.60 3 -3 -24 183.48 7.60 -3 -3 24 183.38 8.00 3 -3 -24 183.58 6.70 -3 3 24 191.18 8.80 3 3 -24 199.98 8.60 3 3 -24 192.18 7.40 2 -3 -24 212.38 8.30 -2 -3 24 226.08 9.10 2 -3 -24 223.08 7.70 -2 3 24 236.78 9.70 2 3 -24 237.98 9.60 2 3 -24 229.78 8.70 5 0 -25 -2.60 2.20 -5 0 25 -1.70 1.70 -5 0 25 -1.80 1.60 -4 0 25 -0.30 1.80 -4 0 25 0.90 1.80 4 0 -25 0.20 1.80 -3 0 25 0.20 1.40 3 0 -25 0.50 1.70 -3 0 25 -0.10 2.40 2 0 -25 -1.20 2.40 -2 0 25 0.70 2.30 -2 0 25 -1.00 1.80 1 0 -25 1.20 2.50 -1 0 25 4.50 2.20 -1 0 25 0.10 2.20 4 -1 -25 0.30 1.80 -4 -1 25 -1.30 1.60 4 -1 -25 1.50 2.40 -4 -1 25 0.00 1.90 4 1 -25 1.40 1.70 -4 1 25 1.50 1.90 -3 -1 25 70.39 5.40 -3 -1 25 71.09 5.00 3 -1 -25 74.49 4.20 3 -1 -25 66.69 5.40 3 1 -25 76.79 5.40 -3 1 25 76.19 5.70 -3 1 25 69.59 4.20 -2 -1 25 78.79 4.90 2 -1 -25 83.39 5.00 -2 -1 25 67.39 4.60 2 1 -25 75.39 5.50 -2 1 25 78.69 4.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 96424 _shelx_res_file ; TITL zeljko2017_1_0m_a.res in P2(1)/c CELL 0.71073 8.9689 6.4035 16.4509 90.000 102.930 90.000 ZERR 2.00 0.0011 0.0008 0.0019 0.000 0.002 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H CO N O UNIT 16 36 4 12 32 temp -73 MERG 2 FMAP 2 PLAN 10 ACTA BOND $H HTAB O5 O8 EQIV $3 -x+1, y+1/2, -z+3/2 HTAB O5 O2_$3 EQIV $4 x, y-1, z HTAB O6 O7_$4 EQIV $5 x+1, y, z HTAB O6 O3_$5 HTAB O6 O8 HTAB O7 O1_$3 EQIV $6 -x, -y+1, -z+1 HTAB O7 O4_$6 HTAB O7 O5_$3 EQIV $7 -x+1, y-1/2, -z+3/2 HTAB O8 O2_$7 HTAB O8 O2_$5 HTAB O8 O3_$5 LIST 6 L.S. 8 WGHT 0.021900 0.411900 EXTI 0.005461 FVAR 0.61179 CO1 3 0.540385 0.423447 0.616172 11.00000 0.00962 0.01590 = 0.00893 0.00088 0.00177 -0.00178 N1 4 0.301531 0.443695 0.442948 11.00000 0.01092 0.01592 = 0.00950 0.00006 0.00195 -0.00130 N2 4 0.338775 0.404879 0.526216 11.00000 0.01024 0.01514 = 0.00935 0.00062 0.00245 -0.00106 N3 4 -0.053512 0.229777 0.468725 11.00000 0.01044 0.01171 = 0.01919 -0.00269 0.00329 -0.00102 O1 5 0.384621 0.301675 0.681191 11.00000 0.01381 0.04021 = 0.01274 0.00769 0.00091 -0.00679 O2 5 0.142727 0.220619 0.676548 11.00000 0.01611 0.02830 = 0.01665 0.00344 0.00704 -0.00469 O3 5 -0.097881 0.164384 0.529245 11.00000 0.01594 0.02238 = 0.02512 0.00083 0.00990 -0.00369 O4 5 -0.135428 0.234380 0.397205 11.00000 0.01394 0.02975 = 0.02130 -0.00363 -0.00283 -0.00415 O5 5 0.709865 0.390600 0.726567 11.00000 0.01665 0.02179 = 0.01469 -0.00045 -0.00175 0.00117 AFIX 3 H51 2 0.769958 0.292001 0.730521 11.00000 0.03078 H52 2 0.753561 0.484204 0.754521 11.00000 0.04086 AFIX 0 O6 5 0.596083 0.117265 0.580706 11.00000 0.01723 0.01920 = 0.03867 0.00033 0.00451 -0.00035 AFIX 3 H61 2 0.552793 0.006310 0.591653 11.00000 0.08309 H62 2 0.677893 0.077810 0.598153 11.00000 0.07625 AFIX 0 O7 5 0.485220 0.732977 0.653198 11.00000 0.01863 0.02677 = 0.01722 -0.00492 0.00594 0.00161 AFIX 3 H71 2 0.520411 0.752819 0.703386 11.00000 0.04353 H72 2 0.397011 0.750719 0.646986 11.00000 0.04675 AFIX 0 O8 5 0.873973 0.049842 0.703918 11.00000 0.02218 0.02675 = 0.03517 0.00527 0.01398 0.00311 AFIX 3 H81 2 0.887290 -0.054575 0.734435 11.00000 0.03764 H82 2 0.958991 0.071125 0.687636 11.00000 0.04367 AFIX 0 C1 1 0.219060 0.321735 0.550796 11.00000 0.00983 0.01299 = 0.01168 0.00040 0.00304 -0.00090 C2 1 0.098597 0.306108 0.479398 11.00000 0.00903 0.01271 = 0.01344 -0.00076 0.00240 -0.00156 C3 1 0.156604 0.384160 0.413773 11.00000 0.01135 0.01626 = 0.01177 -0.00028 0.00153 -0.00163 C4 1 0.246621 0.276262 0.642242 11.00000 0.01395 0.01757 = 0.01263 0.00203 0.00370 -0.00160 H3 2 0.106731 0.396195 0.356934 11.00000 0.02604 HKLF 4 REM zeljko2017_1_0m_a.res in P2(1)/c REM R1 = 0.0181 for 3366 Fo > 4sig(Fo) and 0.0193 for all 3531 data REM 158 parameters refined using 0 restraints END WGHT 0.0219 0.4119 REM Highest difference peak 0.545, deepest hole -0.231, 1-sigma level 0.054 Q1 1 0.1204 0.3428 0.4451 11.00000 0.05 0.55 Q2 1 0.9196 0.0633 0.7424 11.00000 0.05 0.53 Q3 1 0.1553 0.3037 0.5187 11.00000 0.05 0.49 Q4 1 0.2340 0.2907 0.5972 11.00000 0.05 0.47 Q5 1 0.2747 0.3556 0.5384 11.00000 0.05 0.45 Q6 1 0.2305 0.4169 0.4303 11.00000 0.05 0.40 Q7 1 0.0244 0.2731 0.4733 11.00000 0.05 0.35 Q8 1 0.3175 0.2756 0.6630 11.00000 0.05 0.31 Q9 1 0.4035 0.4105 0.5561 11.00000 0.05 0.30 Q10 1 0.4834 0.6359 0.6672 11.00000 0.05 0.28 ; _shelx_res_checksum 28890 _shelxl_version_number 2014/6 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy Co Co1 0.54038(2) 0.42345(2) 0.61617(2) 0.01153(4) Uani d 1 N N1 0.30153(8) 0.44370(11) 0.44295(4) 0.01216(12) Uani d 1 N N2 0.33878(8) 0.40488(11) 0.52622(4) 0.01154(12) Uani d 1 N N3 -0.05351(8) 0.22978(11) 0.46872(5) 0.01379(12) Uani d 1 O O1 0.38462(8) 0.30168(14) 0.68119(4) 0.02258(15) Uani d 1 O O2 0.14273(8) 0.22062(12) 0.67655(4) 0.01982(13) Uani d 1 O O3 -0.09788(8) 0.16438(12) 0.52924(5) 0.02031(13) Uani d 1 O O4 -0.13543(8) 0.23438(13) 0.39720(5) 0.02273(14) Uani d 1 O O5 0.70987(8) 0.39060(11) 0.72657(4) 0.01854(13) Uani d 1 H H51 0.7700 0.2920 0.7305 0.031(4) Uiso d 1 H H52 0.7536 0.4842 0.7545 0.041(5) Uiso d 1 O O6 0.59608(9) 0.11727(12) 0.58071(6) 0.02531(15) Uani d 1 H H61 0.5528 0.0063 0.5917 0.083(8) Uiso d 1 H H62 0.6779 0.0778 0.5982 0.076(8) Uiso d 1 O O7 0.48522(8) 0.73298(12) 0.65320(4) 0.02057(13) Uani d 1 H H71 0.5204 0.7528 0.7034 0.044(5) Uiso d 1 H H72 0.3970 0.7507 0.6470 0.047(5) Uiso d 1 O O8 0.87397(9) 0.04984(13) 0.70392(6) 0.02685(16) Uani d 1 H H81 0.8873 -0.0546 0.7344 0.038(5) Uiso d 1 H H82 0.9590 0.0711 0.6876 0.044(5) Uiso d 1 C C1 0.21906(9) 0.32173(12) 0.55080(5) 0.01140(13) Uani d 1 C C2 0.09860(9) 0.30611(13) 0.47940(5) 0.01174(13) Uani d 1 C C3 0.15660(9) 0.38416(13) 0.41377(5) 0.01329(13) Uani d 1 C C4 0.24662(10) 0.27626(14) 0.64224(5) 0.01460(14) Uani d 1 H H3 0.1067(18) 0.396(2) 0.3569(10) 0.026(4) Uiso d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Co1 0.00962(5) 0.01590(6) 0.00893(5) -0.00178(3) 0.00177(4) 0.00088(4) N1 0.0109(3) 0.0159(3) 0.0095(3) -0.0013(2) 0.0020(2) 0.0001(2) N2 0.0102(3) 0.0151(3) 0.0094(3) -0.0011(2) 0.0025(2) 0.0006(2) N3 0.0104(3) 0.0117(3) 0.0192(3) -0.0010(2) 0.0033(2) -0.0027(2) O1 0.0138(3) 0.0402(4) 0.0127(3) -0.0068(3) 0.0009(2) 0.0077(3) O2 0.0161(3) 0.0283(3) 0.0166(3) -0.0047(2) 0.0070(2) 0.0034(2) O3 0.0159(3) 0.0224(3) 0.0251(3) -0.0037(2) 0.0099(2) 0.0008(3) O4 0.0139(3) 0.0297(4) 0.0213(3) -0.0042(3) -0.0028(2) -0.0036(3) O5 0.0167(3) 0.0218(3) 0.0147(3) 0.0012(2) -0.0018(2) -0.0004(2) O6 0.0172(3) 0.0192(3) 0.0387(4) -0.0003(3) 0.0045(3) 0.0003(3) O7 0.0186(3) 0.0268(3) 0.0172(3) 0.0016(3) 0.0059(2) -0.0049(2) O8 0.0222(3) 0.0268(4) 0.0352(4) 0.0031(3) 0.0140(3) 0.0053(3) C1 0.0098(3) 0.0130(3) 0.0117(3) -0.0009(2) 0.0030(2) 0.0004(2) C2 0.0090(3) 0.0127(3) 0.0134(3) -0.0016(2) 0.0024(2) -0.0008(2) C3 0.0113(3) 0.0163(3) 0.0118(3) -0.0016(3) 0.0015(2) -0.0003(3) C4 0.0139(3) 0.0176(4) 0.0126(3) -0.0016(3) 0.0037(3) 0.0020(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N2 Co1 N1 . 3_666 105.56(3) yes N2 Co1 O1 . . 76.55(3) yes N1 Co1 O5 3_666 . 90.47(3) yes O1 Co1 O5 . . 87.56(3) yes N2 Co1 O5 . . 163.76(3) yes N1 Co1 O1 3_666 . 176.78(3) yes O6 Co1 O7 . . 179.48(3) yes N2 Co1 O6 . . 88.41(3) ? N1 Co1 O6 3_666 . 91.27(3) ? O1 Co1 O6 . . 91.22(3) ? O5 Co1 O6 . . 88.63(3) ? N2 Co1 O7 . . 92.05(3) ? N1 Co1 O7 3_666 . 88.83(3) ? O1 Co1 O7 . . 88.66(3) ? O5 Co1 O7 . . 90.87(3) ? C3 N1 N2 . . 108.05(7) ? C3 N1 Co1 . 3_666 131.37(6) ? N2 N1 Co1 . 3_666 120.57(5) ? C1 N2 N1 . . 110.14(7) ? C1 N2 Co1 . . 116.01(5) ? N1 N2 Co1 . . 133.59(5) ? O3 N3 O4 . . 123.21(8) ? O3 N3 C2 . . 119.59(7) ? O4 N3 C2 . . 117.20(7) ? C4 O1 Co1 . . 118.47(6) ? Co1 O5 H51 . . 118.6 ? Co1 O5 H52 . . 125.9 ? H51 O5 H52 . . 107.5 ? Co1 O6 H61 . . 124.4 ? Co1 O6 H62 . . 117.5 ? H61 O6 H62 . . 95.1 ? Co1 O7 H71 . . 111.3 ? Co1 O7 H72 . . 112.6 ? H71 O7 H72 . . 104.9 ? H81 O8 H82 . . 107.1 ? N2 C1 C2 . . 107.05(7) ? N2 C1 C4 . . 114.66(7) ? C2 C1 C4 . . 138.27(7) ? C3 C2 C1 . . 105.71(7) ? C3 C2 N3 . . 122.83(7) ? C1 C2 N3 . . 131.45(7) ? N1 C3 C2 . . 109.04(7) ? N1 C3 H3 . . 122.6(9) ? C2 C3 H3 . . 128.3(9) ? O2 C4 O1 . . 123.48(8) ? O2 C4 C1 . . 122.62(8) ? O1 C4 C1 . . 113.89(7) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Co1 N1 3_666 2.0729(7) yes Co1 N2 . 2.0679(7) yes Co1 O1 . 2.0911(7) yes Co1 O5 . 2.1018(7) yes Co1 O6 . 2.1365(8) yes Co1 O7 . 2.1632(8) yes N1 C3 . 1.3364(10) ? N1 N2 . 1.3583(10) ? N1 Co1 3_666 2.0730(7) ? N2 C1 . 1.3395(10) ? N3 O3 . 1.2257(10) ? N3 O4 . 1.2402(10) ? N3 C2 . 1.4226(10) ? O1 C4 . 1.2705(10) ? O2 C4 . 1.2446(10) ? O5 H51 . 0.8232 ? O5 H52 . 0.8023 ? O6 H61 . 0.8481 ? O6 H62 . 0.7683 ? O7 H71 . 0.8251 ? O7 H72 . 0.7830 ? O8 H81 . 0.8286 ? O8 H82 . 0.8736 ? C1 C2 . 1.4103(11) ? C1 C4 . 1.4975(11) ? C2 C3 . 1.3919(11) ? C3 H3 . 0.945(16) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA O5 H51 O8 . 0.82 1.91 2.7041(11) 161.7 O5 H52 O2 2_656 0.80 1.99 2.7949(10) 178.6 O6 H61 O7 1_545 0.85 2.17 2.9995(12) 164.1 O6 H62 O3 1_655 0.77 2.58 3.0629(11) 122.6 O6 H62 O8 . 0.77 2.19 2.8716(12) 148.7 O7 H71 O1 2_656 0.83 1.92 2.7488(10) 176.3 O7 H72 O4 3_566 0.78 2.30 3.0675(11) 167.9 O7 H72 O5 2_656 0.78 2.63 3.0889(10) 118.8 O8 H81 O2 2_646 0.83 2.11 2.9096(12) 161.1 O8 H82 O2 1_655 0.87 1.95 2.7739(11) 156.9 O8 H82 O3 1_655 0.87 2.61 3.0304(12) 110.7 _cod_database_fobs_code 2021476