#------------------------------------------------------------------------------
#$Date: 2018-12-07 05:37:15 +0200 (Fri, 07 Dec 2018) $
#$Revision: 212436 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/83/2108348.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2108348
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   23.9430
_cell_length_b                   20.2680
_cell_length_c                   6.3130
_exptl_crystal_F_000             4042.52
_reflns_d_resolution_high        0.9747
_cod_data_source_file            ps5074CuPbOXO4sup10.hkl
_cod_data_source_block           CuPbOXO4
_shelx_title                     ' shelxt_a.res in C2/m             New: Cmmm'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            1829.43
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'x, -y, -z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z'
'x+1/2, -y+1/2, -z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, y, -z'
'-x, y, z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z'
'-x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
4 0 0 6188.27 33543.51 2485.23 o
6 0 0 28779.53 37408.56 3913.70 o
8 0 0 59972.48 49298.55 4092.00 o
10 0 0 1548255.62 1573432.50 29339.95 o
12 0 0 95804.71 131207.33 6531.04 o
14 0 0 4872.59 5777.93 2732.64 o
16 0 0 277831.47 296901.25 10585.42 o
18 0 0 4298.07 4534.19 3039.45 o
20 0 0 64844.94 68892.12 7159.03 o
22 0 0 27686.61 21822.24 4717.51 o
24 0 0 3441.18 15300.51 4774.35 o
3 1 0 9076.11 57084.75 2288.44 o
5 1 0 68680.41 77688.40 2678.40 o
7 1 0 108828.83 119376.12 3858.50 o
9 1 0 16473.91 20698.67 2200.44 o
11 1 0 10265.36 4646.10 1669.99 o
13 1 0 63858.22 82594.00 3987.70 o
15 1 0 313095.53 348187.59 7970.68 o
17 1 0 57045.41 61436.86 4032.90 o
19 1 0 22508.20 27433.59 4531.93 o
21 1 0 3404.02 4771.27 2379.59 o
23 1 0 35560.12 32971.15 3966.92 o
0 2 0 1571.21 3808.32 838.92 o
2 2 0 325.57 15387.10 800.62 o
4 2 0 413360.09 484216.59 8303.78 o
6 2 0 332466.12 378626.72 6602.36 o
8 2 0 42046.29 54254.18 2853.47 o
10 2 0 85211.95 73261.06 3523.20 o
12 2 0 479.25 1257.19 1549.73 o
14 2 0 824162.44 882049.81 14167.40 o
16 2 0 11796.01 8174.85 2262.50 o
18 2 0 1259.92 1042.00 2100.50 o
20 2 0 81402.44 96525.36 4930.90 o
22 2 0 202583.05 221013.59 7494.84 o
24 2 0 738.45 939.30 2539.19 o
1 3 0 18054.58 6889.30 652.98 o
3 3 0 61962.05 68035.40 2190.70 o
5 3 0 68095.10 41184.36 1938.51 o
7 3 0 660251.94 685913.06 10569.92 o
9 3 0 200775.33 186995.45 4916.63 o
11 3 0 19090.44 27306.06 2559.80 o
13 3 0 1148.72 207.43 1587.01 o
15 3 0 9495.60 3203.48 1891.11 o
17 3 0 4549.62 5094.04 2112.58 o
19 3 0 1686.71 1354.70 2089.89 o
21 3 0 80598.36 84056.34 4842.16 o
23 3 0 24340.08 21024.45 3613.55 o
0 4 0 38831.59 38971.64 1898.58 o
2 4 0 294.25 1184.89 645.37 o
4 4 0 145565.52 123082.54 2972.60 o
6 4 0 720951.81 760379.62 17290.83 o
8 4 0 1115631.12 1093331.50 22410.69 o
10 4 0 304821.34 362470.12 7382.57 o
12 4 0 963.91 323.37 1475.11 o
14 4 0 59407.93 46865.56 4094.35 o
16 4 0 152840.66 144010.28 5368.05 o
18 4 0 204863.75 242538.94 7114.81 o
20 4 0 352.91 -336.68 2086.34 o
22 4 0 2270.36 -676.79 2394.35 o
1 5 0 115764.22 74162.97 2013.73 o
3 5 0 9842.21 13466.46 1089.36 o
5 5 0 79064.68 51133.52 3361.22 o
7 5 0 823360.50 909587.25 16971.38 o
9 5 0 12454.13 3191.55 1366.32 o
11 5 0 5581.66 2722.77 1430.25 o
13 5 0 33320.66 43908.89 3217.19 o
15 5 0 360.64 -1008.61 1757.67 o
17 5 0 123484.18 107370.82 7912.28 o
19 5 0 41889.04 36456.90 3636.61 o
21 5 0 2702.67 2771.87 2474.89 o
23 5 0 2282.14 2993.57 2750.48 o
0 6 0 50700.46 81358.59 3186.28 o
2 6 0 22049.35 42142.36 1754.33 o
4 6 0 11083.18 30690.50 1845.20 o
6 6 0 6088.92 3110.93 1128.07 o
8 6 0 56192.15 46122.01 2984.74 o
10 6 0 13137.91 2481.75 1388.19 o
12 6 0 624.35 5738.68 1692.07 o
14 6 0 519785.50 497862.19 10174.90 o
16 6 0 66209.94 54692.22 5242.79 o
18 6 0 10151.64 7289.24 2413.09 o
20 6 0 92203.47 86657.89 4965.62 o
22 6 0 125762.64 122315.54 6288.80 o
1 7 0 42392.03 69572.44 2266.56 o
3 7 0 17583.97 17681.43 1529.75 o
5 7 0 154321.17 125592.86 3519.62 o
7 7 0 83561.31 65949.34 2824.85 o
9 7 0 109055.27 120197.20 3963.26 o
11 7 0 30740.23 30326.31 3392.99 o
13 7 0 44449.08 42113.98 3230.83 o
15 7 0 368229.97 354988.22 11482.03 o
17 7 0 50891.90 43958.64 3785.48 o
19 7 0 28435.92 19211.51 4079.29 o
21 7 0 34011.15 21917.85 3484.29 o
23 7 0 13829.72 15193.23 4846.01 o
0 8 0 2102275.75 1930764.88 33569.27 o
2 8 0 138696.25 155979.23 3618.85 o
4 8 0 52101.76 86048.38 2570.70 o
6 8 0 6297.92 1843.13 1206.13 o
8 8 0 71737.63 83153.18 3649.76 o
10 8 0 72561.56 63354.22 5178.14 o
12 8 0 1143.29 1719.79 1642.72 o
14 8 0 17057.68 12449.03 3471.04 o
16 8 0 65090.70 55827.32 4010.66 o
18 8 0 1419.42 71.02 2112.37 o
20 8 0 13420.27 17996.98 3321.84 o
22 8 0 442.83 127.75 2806.22 o
1 9 0 170930.44 170439.56 3933.94 o
3 9 0 13251.37 9356.35 1395.82 o
5 9 0 61927.56 67000.58 3542.84 o
7 9 0 223673.25 228244.44 5481.27 o
9 9 0 105011.16 115172.02 5647.54 o
11 9 0 57342.37 72998.23 4192.78 o
13 9 0 184267.83 173942.00 8426.23 o
15 9 0 32881.11 41848.18 3890.41 o
17 9 0 2900.52 1233.57 2217.34 o
19 9 0 206599.67 202747.62 12173.20 o
21 9 0 35029.63 35270.75 4941.26 o
0 10 0 235709.50 267934.22 7588.88 o
2 10 0 30951.20 26461.44 1957.53 o
4 10 0 50731.68 52484.93 2310.65 o
6 10 0 236429.52 260034.67 5996.48 o
8 10 0 6578.81 5223.55 1667.28 o
10 10 0 37911.64 40705.63 3058.59 o
12 10 0 4687.03 4330.97 2038.31 o
14 10 0 82707.38 91753.90 5350.50 o
16 10 0 7114.36 5214.72 2331.16 o
18 10 0 23325.60 24813.08 3529.22 o
20 10 0 4375.73 351.82 2807.30 o
1 11 0 339388.75 349356.91 6592.05 o
3 11 0 173973.72 168431.67 5294.41 o
5 11 0 39570.39 37753.02 2607.77 o
7 11 0 474721.03 475379.28 9199.57 o
9 11 0 280378.75 314585.44 7315.14 o
11 11 0 105606.58 111722.52 4561.17 o
13 11 0 13918.42 12677.52 2506.01 o
15 11 0 70265.11 62867.76 4283.07 o
17 11 0 7560.47 8552.56 2607.06 o
19 11 0 346.03 -149.33 2642.65 o
0 12 0 254792.50 270246.31 8180.07 o
2 12 0 369.38 -146.87 1205.19 o
4 12 0 46007.55 50225.38 3571.31 o
6 12 0 60390.70 55267.51 6069.24 o
8 12 0 349952.62 378181.03 8242.19 o
10 12 0 88720.25 81000.04 4015.12 o
12 12 0 50390.45 59091.21 4389.48 o
14 12 0 32528.74 33653.03 3492.54 o
16 12 0 4191.38 1290.67 2486.27 o
18 12 0 31586.93 38866.04 4082.25 o
1 13 0 243468.84 262464.69 5939.94 o
3 13 0 26170.37 22765.37 2318.79 o
5 13 0 479954.97 497040.28 9812.74 o
7 13 0 128041.35 124254.18 6241.58 o
9 13 0 1002.00 589.71 1798.19 o
11 13 0 87957.84 88502.20 4448.32 o
13 13 0 47603.47 49185.12 6679.29 o
15 13 0 13282.15 11181.23 3945.52 o
17 13 0 16782.76 17299.81 3385.86 o
19 13 0 3654.24 6423.53 3343.55 o
0 14 0 78530.41 76958.07 4663.35 o
2 14 0 86709.25 90975.80 3659.22 o
4 14 0 19739.80 26054.65 2219.62 o
6 14 0 36783.05 36904.62 3029.90 o
8 14 0 46392.64 55062.70 3643.79 o
10 14 0 99.31 -1058.62 1816.15 o
12 14 0 783.51 -355.09 2001.33 o
14 14 0 205928.86 215566.61 11808.07 o
16 14 0 42775.49 46284.62 4311.52 o
18 14 0 44599.11 41045.36 4854.01 o
1 15 0 1375.86 4593.66 1740.81 o
3 15 0 2402.26 3649.21 1542.55 o
5 15 0 238844.75 251863.36 6836.44 o
7 15 0 23897.66 27056.99 3544.70 o
9 15 0 129278.66 132076.25 6276.58 o
11 15 0 24184.16 22560.98 3344.95 o
13 15 0 6509.62 5059.07 2587.63 o
15 15 0 205194.66 221703.67 10300.78 o
0 16 0 272853.34 252647.66 11380.14 o
2 16 0 142702.56 154997.95 4999.12 o
4 16 0 81929.36 99665.73 5923.98 o
6 16 0 182.15 369.97 1822.36 o
8 16 0 13241.90 10174.73 2401.90 o
10 16 0 379.51 809.65 2071.89 o
12 16 0 1100.08 -449.30 2271.59 o
14 16 0 32906.31 35851.43 6351.66 o
1 17 0 56799.37 48663.44 3466.42 o
3 17 0 9032.48 9476.81 1879.62 o
5 17 0 3821.41 2612.89 2039.55 o
7 17 0 90854.55 80737.68 4691.72 o
9 17 0 47824.66 38733.07 5810.62 o
11 17 0 10461.15 9975.39 2763.86 o
13 17 0 93836.02 112308.27 7884.52 o
0 18 0 222463.56 252080.12 14503.99 o
2 18 0 8868.37 7619.09 2016.62 o
4 18 0 24033.69 22243.68 4028.40 o
6 18 0 32013.32 29970.53 3332.56 o
8 18 0 1975.05 3337.35 2353.58 o
10 18 0 60111.22 61317.10 9843.62 o
12 18 0 40664.68 37985.56 6988.77 o
1 19 0 3169.37 7367.89 2064.13 o
3 19 0 48927.86 42112.48 4588.63 o
5 19 0 18496.07 19644.59 3397.58 o
7 19 0 77449.38 77920.80 5274.22 o
9 19 0 22915.27 28700.10 3923.61 o
0 20 0 24294.22 19732.56 4677.49 o
2 20 0 403.19 -188.97 2007.25 o
4 20 0 61636.01 64800.03 5748.59 o
6 20 0 2470.37 -27.54 3010.47 o
0 0 1 5254.72 -2156.48 1078.24 o
2 0 1 1456.56 2469.93 1036.78 o
6 0 1 133694.88 313143.28 4915.24 o
8 0 1 45834.31 56637.27 1693.98 o
10 0 1 70794.42 50229.55 2093.00 o
12 0 1 52474.86 85973.79 3602.55 o
14 0 1 552322.38 565105.06 17204.05 o
16 0 1 88605.08 77354.54 5082.35 o
18 0 1 88219.91 99772.98 4146.60 o
20 0 1 130438.54 144048.97 12392.69 o
22 0 1 65176.85 82136.36 8326.27 o
24 0 1 33346.13 54226.43 7199.56 o
1 1 1 6404.47 8635.86 860.88 o
3 1 1 19100.25 8575.17 1661.53 o
5 1 1 53107.89 17269.87 1351.70 o
7 1 1 5227.78 -258.84 455.88 o
9 1 1 254394.27 243100.64 2827.32 o
11 1 1 65032.36 58107.44 1721.51 o
13 1 1 53142.34 69190.83 1847.88 o
15 1 1 50327.62 38890.93 1729.87 o
17 1 1 10524.11 11289.19 1530.15 o
19 1 1 91534.39 105598.98 4054.60 o
21 1 1 2234.90 651.55 1557.51 o
23 1 1 1780.75 1294.39 1652.89 o
0 2 1 631241.31 432477.78 15273.17 o
2 2 1 9948.58 27285.74 2832.59 o
4 2 1 5415.57 5761.46 1072.34 o
6 2 1 80037.17 62184.84 1665.50 o
8 2 1 325505.62 258028.89 2804.21 o
10 2 1 190796.05 163783.31 2436.83 o
12 2 1 57604.37 65370.29 1875.00 o
14 2 1 19553.24 7274.78 1108.71 o
16 2 1 3002.04 628.85 1090.57 o
18 2 1 187452.31 196035.98 7578.72 o
20 2 1 380.49 305.38 1506.99 o
22 2 1 1214.49 -946.19 1563.20 o
24 2 1 40648.01 51769.90 5110.24 o
1 3 1 4408.46 14298.62 1056.69 o
3 3 1 8209.86 12266.65 970.24 o
5 3 1 56035.95 70055.67 2028.86 o
7 3 1 136712.02 142210.14 1809.02 o
9 3 1 26316.54 33238.08 1161.03 o
11 3 1 79049.95 99062.60 2001.54 o
13 3 1 142527.72 150526.95 3812.26 o
15 3 1 5041.29 1762.51 1037.27 o
17 3 1 2105.40 1787.38 1158.07 o
19 3 1 60080.49 66594.95 3436.14 o
21 3 1 19838.35 23965.34 2814.26 o
23 3 1 11611.47 11842.53 2180.04 o
0 4 1 42479.81 28219.11 1338.31 o
2 4 1 279149.34 331033.62 4575.15 o
4 4 1 622950.88 601537.19 8570.63 o
6 4 1 227322.14 203611.61 2510.27 o
8 4 1 10999.49 7681.86 912.93 o
10 4 1 29263.30 21536.23 1085.39 o
12 4 1 14.14 70.89 773.09 o
14 4 1 67864.36 76344.15 2207.41 o
16 4 1 1222.21 1048.02 1066.64 o
18 4 1 185.89 653.26 1329.35 o
20 4 1 31104.85 43664.77 2717.95 o
22 4 1 215944.78 240901.42 7807.64 o
1 5 1 106337.37 147534.53 1835.08 o
3 5 1 642457.50 663254.56 8667.63 o
5 5 1 41718.01 55321.26 1374.71 o
7 5 1 414248.59 447463.06 4152.77 o
9 5 1 31013.01 35296.82 1217.24 o
11 5 1 502.62 -376.43 705.01 o
13 5 1 52387.67 50093.62 1791.79 o
15 5 1 190199.50 228246.72 5841.38 o
17 5 1 4341.40 3475.50 1166.88 o
19 5 1 6208.55 4358.57 1503.23 o
21 5 1 275.11 289.47 1660.78 o
23 5 1 12462.73 17328.17 2301.16 o
0 6 1 651914.38 675717.69 9359.54 o
2 6 1 90233.91 83465.48 1307.90 o
4 6 1 134019.75 146304.30 1936.84 o
6 6 1 306914.16 320305.28 4461.04 o
8 6 1 10542.66 11220.87 897.12 o
10 6 1 100352.86 116149.42 2354.74 o
12 6 1 3645.39 2440.54 989.52 o
14 6 1 53872.57 51811.18 2982.63 o
16 6 1 28380.94 34057.11 2073.23 o
18 6 1 13790.09 9249.13 1748.67 o
20 6 1 38972.11 30380.15 3123.24 o
22 6 1 15809.68 12867.97 2145.61 o
1 7 1 247427.16 270165.81 2856.33 o
3 7 1 12128.37 18037.85 810.62 o
5 7 1 463600.16 450631.94 5426.11 o
7 7 1 51764.81 57509.29 1565.59 o
9 7 1 45217.27 47101.82 1551.72 o
11 7 1 211033.17 231444.64 4698.13 o
13 7 1 31262.44 24750.84 1569.33 o
15 7 1 3031.36 4358.48 1252.78 o
17 7 1 452.82 461.98 1460.89 o
19 7 1 6263.83 5099.07 1766.06 o
21 7 1 2101.07 -329.75 1741.23 o
0 8 1 67925.52 117254.84 2510.15 o
2 8 1 62108.25 109719.64 1669.74 o
4 8 1 156202.31 150249.42 2173.53 o
6 8 1 22013.69 20771.91 991.93 o
8 8 1 902.15 1326.23 616.40 o
10 8 1 71489.33 89585.45 2242.50 o
12 8 1 11500.14 12441.32 1356.03 o
14 8 1 147299.14 143897.58 4010.93 o
16 8 1 31992.29 37598.97 2442.25 o
18 8 1 383.76 101.67 1591.61 o
20 8 1 72117.05 69424.91 5056.91 o
22 8 1 8993.75 15856.95 2386.47 o
1 9 1 202067.84 167662.59 2272.42 o
3 9 1 1625.74 1028.64 580.05 o
5 9 1 128333.64 107959.73 1914.28 o
7 9 1 5928.42 3781.66 705.92 o
9 9 1 410166.72 412698.19 5213.99 o
11 9 1 26794.97 43520.90 1848.58 o
13 9 1 29647.48 29044.51 2022.46 o
15 9 1 58309.36 66657.43 4288.83 o
17 9 1 32070.21 28809.24 2461.13 o
19 9 1 99181.99 115116.71 7578.71 o
21 9 1 17706.82 11888.57 2365.31 o
0 10 1 6126.78 6015.02 1026.58 o
2 10 1 164.44 1177.95 585.48 o
4 10 1 53812.30 55435.20 1470.88 o
6 10 1 10428.27 10651.54 885.66 o
8 10 1 323850.81 325016.84 5206.48 o
10 10 1 12023.56 12218.14 1289.80 o
12 10 1 9917.22 11926.28 1435.07 o
14 10 1 6076.50 2688.47 1449.50 o
16 10 1 43535.99 37367.77 3369.50 o
18 10 1 93348.99 98157.33 6479.17 o
20 10 1 6753.50 4145.90 1900.59 o
1 11 1 309.58 678.66 659.71 o
3 11 1 24585.88 31656.18 1278.10 o
5 11 1 125995.28 119328.73 2314.81 o
7 11 1 116259.84 125991.42 2484.25 o
9 11 1 21520.80 18964.77 1162.68 o
11 11 1 12237.50 12980.55 1369.13 o
13 11 1 310756.34 304687.41 5892.12 o
15 11 1 8230.07 6403.96 1781.70 o
17 11 1 30080.82 24272.45 3111.48 o
19 11 1 41324.00 38625.97 4221.61 o
0 12 1 99150.23 110190.20 2917.60 o
2 12 1 25486.08 27808.62 1286.05 o
4 12 1 40471.76 41197.80 1633.35 o
6 12 1 3088.89 3688.32 896.70 o
8 12 1 10578.88 13680.22 1123.33 o
10 12 1 23795.35 27175.68 1709.34 o
12 12 1 251.30 246.41 1322.88 o
14 12 1 6337.53 7013.94 1787.92 o
16 12 1 308.39 -1755.93 1688.58 o
18 12 1 14114.31 6362.15 2084.20 o
1 13 1 23169.37 19036.95 1256.14 o
3 13 1 168579.11 167378.56 3008.98 o
5 13 1 293.45 1251.11 873.75 o
7 13 1 6895.95 4618.05 1011.27 o
9 13 1 80349.23 91716.37 2605.89 o
11 13 1 9871.24 7170.51 1525.27 o
13 13 1 86279.20 92300.09 6009.05 o
15 13 1 107898.23 133108.75 7413.05 o
17 13 1 79349.20 79510.82 5721.83 o
0 14 1 104155.32 97088.60 3911.39 o
2 14 1 67563.46 72352.28 2140.03 o
4 14 1 32701.59 32017.76 2389.73 o
6 14 1 1336.71 2617.86 1081.36 o
8 14 1 40676.96 46935.47 2106.99 o
10 14 1 1080.64 -350.70 1091.84 o
12 14 1 1829.55 2081.52 1577.10 o
14 14 1 17398.91 12786.94 2141.89 o
16 14 1 4847.84 1506.01 1888.20 o
1 15 1 61564.87 54970.19 2444.89 o
3 15 1 968.34 76.66 1019.19 o
5 15 1 149628.86 155962.62 3711.99 o
7 15 1 15914.60 9860.67 1395.48 o
9 15 1 26873.58 30222.26 2315.97 o
11 15 1 42934.67 46441.24 2794.41 o
13 15 1 43112.60 44924.56 4030.31 o
15 15 1 4375.45 1846.17 1839.98 o
0 16 1 87412.87 84868.03 4079.62 o
2 16 1 11936.54 10075.54 1575.85 o
4 16 1 1722.61 1110.60 1268.58 o
6 16 1 37200.89 35830.75 3128.01 o
8 16 1 20262.33 19497.64 1912.77 o
10 16 1 27312.59 20667.92 2723.67 o
12 16 1 6176.82 7126.71 1895.80 o
14 16 1 1612.54 -406.85 1783.34 o
1 17 1 71076.98 64462.40 2757.27 o
3 17 1 17368.46 18037.30 1706.41 o
5 17 1 50567.93 56188.89 2800.11 o
7 17 1 45463.54 52149.89 2444.06 o
9 17 1 96175.08 103591.70 3767.73 o
11 17 1 1399.08 391.45 1691.21 o
13 17 1 5542.16 2359.21 1893.42 o
0 18 1 47894.77 49091.04 4693.46 o
2 18 1 27642.71 31194.69 2259.26 o
4 18 1 105243.82 110252.21 3336.53 o
6 18 1 1017.07 2132.99 1425.82 o
8 18 1 9642.73 9674.93 1918.74 o
10 18 1 34821.09 33817.07 2720.71 o
1 19 1 35556.37 34638.95 2587.28 o
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