#------------------------------------------------------------------------------ #$Date: 2019-11-12 10:30:17 +0200 (Tue, 12 Nov 2019) $ #$Revision: 227656 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/31/2243188.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243188 loop_ _publ_author_name 'Kenfack Tsobnang, Patrice' 'Tsamo Tontsa, Armelle' 'Mkounga, Pierre' 'Ephrem Nkengfack, Augustin' 'Tonl\'e Kenfack, Ignas' _publ_section_title ; Crystal structure of limonoid TS3, isolated from Trichilia rubescens ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 1083 _journal_page_last 1086 _journal_paper_doi 10.1107/S2056989018009775 _journal_volume 74 _journal_year 2018 _chemical_formula_iupac 'C26 H28 O5, 0.5H2 O1' _chemical_formula_moiety 'C26 H28 O5, 0.5(H2 O1)' _chemical_formula_sum 'C26 H29 O5.5' _chemical_formula_weight 429.49 _chemical_name_systematic ;(3aS,3bS,4aS,5aS,6S,7aR,8aR,8bS,11aR)-6-(Furan-3-yl)-3a,5a,8b,11a-tetramethyl-3a,4a,5,5a,6,7,7a,8b,11,11a-decahydrooxireno[2',3':4b,5]oxireno[2'',3'':2',3']cyclopenta[1',2':7,8]phenanthro[10,1-bc]furan-3(3aH)-one hemihydrate ; _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 91.7420(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.4711(2) _cell_length_b 12.0986(2) _cell_length_c 13.7645(2) _cell_measurement_reflns_used 30836 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 76.50 _cell_measurement_theta_min 3.55 _cell_volume 2075.87(6) _computing_cell_refinement ; SAINT (Bruker, 2013) ; _computing_data_collection ; APEX2 (Bruker, 2013) ; _computing_data_reduction ; SAINT (Bruker, 2013) ; _computing_molecular_graphics ; PLATON (Spek, 2009) ; _computing_publication_material ; SHELXL2018 (Sheldrick, 2015), publCIF (Westrip, 2010) and enCIFer (Allen et al., 2004) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Bruker D8 Venture Photon' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0372 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 33504 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 76.503 _diffrn_reflns_theta_min 3.546 _exptl_absorpt_coefficient_mu 0.776 _exptl_absorpt_correction_T_max 0.900 _exptl_absorpt_correction_T_min 0.869 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2013) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.374 _exptl_crystal_description needle _exptl_crystal_F_000 916 _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.11 _refine_diff_density_max 0.239 _refine_diff_density_min -0.237 _refine_ls_abs_structure_details ; Flack x determined using 3527 quotients [(I^+^)-(I^-^)]/[(I^+^)+(I^-^)] (Parsons et al., 2013) ; _refine_ls_abs_structure_Flack -0.05(5) _refine_ls_extinction_coef 0.0012(2) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; (SHELXL2018; Sheldrick, 2015) ; _refine_ls_goodness_of_fit_ref 1.021 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 585 _refine_ls_number_reflns 8304 _refine_ls_number_restraints 3 _refine_ls_restrained_S_all 1.022 _refine_ls_R_factor_all 0.0331 _refine_ls_R_factor_gt 0.0313 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0454P)^2^+0.3923P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0778 _refine_ls_wR_factor_ref 0.0797 _reflns_number_gt 8067 _reflns_number_total 8304 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file su5448sup1.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 21' _cod_original_formula_sum 'C26 H29 O5.50' _cod_database_code 2243188 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; 0 -14 0 44.70 3.23 0 -14 -1 1.39 0.59 0 -14 1 38.55 3.21 0 -14 -2 159.24 5.49 0 -14 3 47.29 3.21 0 -14 -3 45.54 3.01 0 -14 -4 155.48 5.41 0 -14 4 153.32 5.76 0 -14 -5 27.24 2.24 0 -14 5 26.82 2.46 0 -14 -6 79.51 3.42 0 -13 0 0.01 0.76 0 -13 0 -1.12 1.40 0 -13 1 52.08 4.58 0 -13 -1 45.69 3.87 0 -13 -1 48.50 3.74 0 -13 -2 37.46 3.38 0 -13 2 47.51 4.01 0 -13 2 45.11 4.47 0 -13 -3 62.00 4.43 0 -13 3 60.02 4.67 0 -13 3 62.45 5.30 0 -13 -4 14.93 2.28 0 -13 4 19.95 3.29 0 -13 -4 15.22 2.40 0 -13 4 15.04 2.54 0 -13 -5 12.28 2.03 0 -13 5 9.87 2.24 0 -13 -5 12.34 2.03 0 -13 -6 240.76 8.01 0 -13 -6 230.59 7.62 0 -13 6 246.47 8.81 0 -13 -7 25.00 2.44 0 -13 7 25.09 2.86 0 -13 -7 19.49 2.11 0 -13 -8 38.95 2.67 0 -13 -9 139.45 4.05 0 -12 0 78.95 6.02 0 -12 0 79.95 5.10 0 -12 -1 36.21 3.95 0 -12 1 35.39 4.36 0 -12 -1 39.78 3.77 0 -12 1 41.50 4.10 0 -12 2 29.40 4.06 0 -12 -2 30.02 3.80 0 -12 -2 25.33 3.09 0 -12 2 31.80 3.85 0 -12 3 127.69 7.51 0 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112.82 6.34 0 -7 12 125.82 9.78 0 -7 -12 119.10 6.01 0 -7 -13 111.58 4.34 0 -7 13 96.50 7.92 0 -7 -13 114.86 5.45 0 -7 13 110.45 5.68 0 -7 14 69.94 3.85 0 -7 -14 75.25 3.10 0 -7 -15 2.27 1.01 0 -7 15 3.33 0.73 0 -6 0 359.65 23.85 0 -6 1 1096.07 41.84 0 -6 -1 1022.49 40.04 0 -6 2 902.59 38.89 0 -6 -2 892.14 33.21 0 -6 -2 920.20 38.54 0 -6 -3 380.64 25.59 0 -6 3 393.45 26.78 0 -6 -3 376.93 22.81 0 -6 4 550.56 32.95 0 -6 -4 540.93 29.20 0 -6 -5 162.07 17.25 0 -6 5 172.45 19.46 0 -6 -6 62.76 11.64 0 -6 6 69.00 13.32 0 -6 -7 188.57 21.37 0 -6 7 195.70 22.92 0 -6 -8 216.48 23.94 0 -6 8 242.18 27.21 0 -6 -8 211.54 10.71 0 -6 -9 774.17 15.81 0 -6 -9 796.28 48.17 0 -6 9 663.15 47.44 0 -6 9 722.18 17.67 0 -6 -9 778.60 21.19 0 -6 9 770.69 17.35 0 -6 -9 782.33 21.30 0 -6 -9 690.71 12.67 0 -6 -10 122.44 5.44 0 -6 -10 132.65 8.85 0 -6 10 137.27 7.54 0 -6 10 151.20 11.15 0 -6 -10 142.94 9.24 0 -6 -10 133.89 8.62 0 -6 -10 135.70 6.86 0 -6 -11 53.12 5.58 0 -6 -11 51.08 4.23 0 -6 11 49.26 6.67 0 -6 -11 46.04 3.37 0 -6 -11 47.44 5.04 0 -6 11 48.41 4.54 0 -6 -12 -0.01 0.81 0 -6 -12 0.76 1.23 0 -6 -12 1.05 1.19 0 -6 12 -0.28 1.40 0 -6 -12 2.12 1.52 0 -6 -12 1.29 1.21 0 -6 12 0.14 2.47 0 -6 -13 28.61 2.47 0 -6 -13 32.19 3.79 0 -6 -13 30.56 3.17 0 -6 13 27.17 3.21 0 -6 13 17.23 4.11 0 -6 -13 28.99 3.54 0 -6 -14 11.19 1.45 0 -6 14 13.90 2.16 0 -6 15 3.54 1.03 0 -6 -15 8.30 1.07 0 -5 0 0.19 2.55 0 -5 -1 710.65 29.87 0 -5 1 660.67 29.04 0 -5 2 873.46 34.32 0 -5 -2 824.08 32.88 0 -5 -2 822.78 29.00 0 -5 -3 906.18 36.13 0 -5 3 825.99 35.25 0 -5 -3 853.60 31.37 0 -5 4 332.93 23.30 0 -5 -4 341.98 21.68 0 -5 5 32.99 7.90 0 -5 -5 29.93 7.30 0 -5 -6 2.49 3.38 0 -5 6 3.99 2.18 0 -5 7 340.50 28.72 0 -5 -7 342.38 27.01 0 -5 8 49.14 11.53 0 -5 -8 23.69 8.23 0 -5 9 162.28 7.94 0 -5 -9 160.02 7.12 0 -5 -9 143.66 8.83 0 -5 9 138.65 21.09 0 -5 -9 148.07 20.32 0 -5 -9 151.64 9.61 0 -5 -10 201.45 11.02 0 -5 -10 224.87 12.15 0 -5 -10 189.00 23.73 0 -5 10 211.98 26.72 0 -5 10 205.12 9.31 0 -5 10 205.38 12.80 0 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32.10 4.39 0 4 13 33.74 3.47 0 4 -13 32.86 5.47 0 4 -13 42.22 5.67 0 4 -13 36.91 5.49 0 4 -13 33.90 4.85 0 4 14 101.86 6.83 0 4 -14 98.93 7.79 0 4 -14 88.62 7.44 0 4 14 88.13 6.57 0 4 -14 99.84 7.42 0 4 -15 2.46 1.54 0 4 -15 -0.77 1.69 0 4 -15 0.45 1.85 0 4 15 0.31 1.37 0 4 -15 0.39 1.97 0 4 -16 298.11 8.72 0 4 16 282.79 7.89 0 5 0 -1.95 1.62 0 5 0 1.77 1.01 0 5 1 763.06 20.79 0 5 1 816.56 20.34 0 5 -1 797.83 24.12 0 5 -2 848.74 32.53 0 5 2 925.46 19.22 0 5 -2 842.19 26.56 0 5 2 916.78 34.27 0 5 -2 900.05 25.09 0 5 2 874.53 25.18 0 5 -3 862.71 28.76 0 5 3 842.05 27.83 0 5 -3 888.28 34.06 0 5 3 877.89 36.00 0 5 4 409.27 27.22 0 5 -4 369.56 22.81 0 5 -4 360.46 20.06 0 5 4 361.49 19.88 0 5 -5 31.34 6.98 0 5 5 30.25 6.30 0 5 -5 31.65 7.00 0 5 5 28.14 9.42 0 5 -6 8.02 4.50 0 5 6 10.96 5.66 0 5 6 4.79 3.18 0 5 -6 0.36 3.69 0 5 7 310.20 23.45 0 5 7 316.96 30.76 0 5 -7 334.77 26.64 0 5 -7 294.68 22.01 0 5 8 38.44 8.89 0 5 -8 24.13 7.01 0 5 -8 30.12 8.86 0 5 8 19.83 9.30 0 5 9 147.27 18.78 0 5 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15 6.18 1.68 0 6 -15 3.80 1.43 0 6 -15 3.52 1.10 0 7 0 0.74 1.18 0 7 -1 41.49 6.98 0 7 -1 38.81 8.52 0 7 -2 9.51 3.73 0 7 -2 0.16 2.03 0 7 2 16.29 6.91 0 7 -3 34.89 7.30 0 7 -3 50.16 9.63 0 7 3 31.66 9.83 0 7 3 46.06 7.03 0 7 4 107.46 11.88 0 7 -4 84.23 11.23 0 7 -4 98.95 14.27 0 7 4 87.92 15.59 0 7 5 240.92 27.22 0 7 5 258.68 20.30 0 7 -5 258.77 23.80 0 7 -5 233.85 19.92 0 7 -6 443.78 29.04 0 7 6 475.89 29.34 0 7 6 489.67 41.08 0 7 -6 490.64 34.29 0 7 -7 120.19 17.32 0 7 7 139.69 17.42 0 7 -7 123.69 16.35 0 7 7 145.06 24.94 0 7 8 -3.72 2.93 0 7 -8 6.53 3.80 0 7 8 3.43 9.94 0 7 -8 8.91 6.92 0 7 -9 253.56 12.33 0 7 -10 61.04 6.29 0 7 -10 54.39 7.21 0 7 -10 58.74 6.09 0 7 -11 117.94 8.18 0 7 -11 109.33 8.20 0 7 -11 114.32 8.37 0 7 -11 105.46 9.47 0 7 -12 116.92 7.93 0 7 -12 112.34 7.36 0 7 -12 116.74 8.04 0 7 -12 114.54 9.14 0 7 -12 109.96 8.74 0 7 -13 109.57 6.38 0 7 -13 115.91 7.30 0 7 -13 110.08 7.78 0 7 13 104.99 6.94 0 7 -13 101.38 8.11 0 7 -13 113.74 7.97 0 7 -14 74.92 5.81 0 7 -14 73.25 5.53 0 7 14 70.73 5.08 0 7 -14 78.62 5.28 0 7 14 72.61 5.13 0 7 15 1.74 0.70 0 7 -15 3.80 1.13 0 7 -15 1.65 0.84 0 7 15 3.13 1.12 0 8 0 109.41 15.93 0 8 -1 38.49 7.44 0 8 -1 39.12 9.49 0 8 -2 270.89 19.37 0 8 -2 293.03 26.20 0 8 2 290.90 27.28 0 8 -3 72.67 10.84 0 8 3 78.78 15.36 0 8 -3 87.90 14.03 0 8 -4 237.34 20.35 0 8 -4 257.60 24.82 0 8 4 270.82 29.11 0 8 5 262.70 30.55 0 8 -5 270.57 26.20 0 8 -5 226.28 20.76 0 8 -6 80.60 13.36 0 8 -6 69.17 13.57 0 8 6 115.28 21.54 0 8 7 67.36 19.17 0 8 7 82.40 13.13 0 8 -7 80.25 15.24 0 8 -7 80.85 13.94 0 8 -9 435.36 16.00 0 8 -10 77.09 6.83 0 8 -10 92.51 7.29 0 8 -10 77.38 7.02 0 8 -10 77.82 8.31 0 8 -11 141.51 10.36 0 8 -11 168.37 9.08 0 8 -11 160.80 9.37 0 8 -11 168.42 9.56 0 8 -12 5.62 1.96 0 8 -12 5.46 2.68 0 8 -12 4.07 2.14 0 8 -12 6.33 3.35 0 8 -13 1.85 1.56 0 8 13 8.69 2.15 0 8 -13 8.05 2.82 0 8 -13 4.93 1.65 0 8 -13 7.79 2.53 0 8 14 7.05 1.56 0 8 14 8.01 1.81 0 8 -14 7.75 1.56 0 8 -14 8.45 1.92 0 8 -14 7.78 1.85 0 9 0 6.73 4.35 0 9 1 108.61 16.87 0 9 -1 133.38 18.46 0 9 1 120.03 19.79 0 9 2 255.06 28.73 0 9 -2 249.72 20.10 0 9 -2 299.31 28.15 0 9 -3 54.08 11.91 0 9 3 54.34 14.24 0 9 -3 43.23 9.02 0 9 4 83.96 17.74 0 9 -4 54.94 10.27 0 9 -4 78.25 15.10 0 9 -5 82.08 15.06 0 9 -5 68.50 12.39 0 9 -9 24.58 4.03 0 9 -10 9.83 3.76 0 9 -10 15.40 3.13 0 9 -10 17.86 3.13 0 9 -11 100.85 6.73 0 9 -11 101.64 6.79 0 9 -11 90.20 7.68 0 9 -12 24.90 3.16 0 9 -12 27.62 3.96 0 9 12 21.78 2.88 0 9 -12 21.69 2.78 0 9 -12 24.75 3.77 0 9 -13 23.93 2.42 0 9 -13 25.77 3.40 0 9 13 25.52 2.64 0 9 -13 25.83 3.12 0 10 0 73.76 15.53 0 10 -1 78.06 14.73 0 10 1 51.88 14.45 0 10 2 9.09 7.18 0 10 -2 -0.48 2.80 0 10 -3 103.64 17.31 0 10 -9 13.79 2.88 0 10 -9 11.29 2.56 0 10 -10 9.67 2.31 0 10 -10 9.29 3.11 0 10 10 8.53 1.88 0 10 -10 7.60 2.15 0 10 -11 73.40 4.75 0 10 -11 70.47 5.94 0 10 11 62.88 4.41 0 10 -12 36.57 3.42 0 10 -12 37.17 4.16 0 10 -12 33.94 3.65 0 10 12 26.60 2.69 0 10 12 28.49 2.58 0 10 13 7.49 1.36 0 10 -13 7.03 1.38 0 11 -10 6.71 2.25 0 11 -11 42.00 3.76 0 11 -11 37.26 3.31 0 12 -9 80.85 5.61 0 12 10 17.24 2.08 0 12 -10 13.76 1.86 0 13 -8 24.18 2.59 1 -14 -6 15.25 1.58 1 -14 -5 26.20 2.22 1 -14 -4 50.77 3.21 1 -14 -3 3.33 1.13 1 -14 -2 46.60 3.10 1 -14 -1 175.32 5.71 1 -14 -1 176.49 6.24 1 -14 0 166.23 6.50 1 -14 0 0.73 0.36 1 -14 1 68.33 4.39 -1 -14 -2 -0.16 0.28 1 -14 2 2.74 0.80 1 -14 3 13.47 2.16 -1 -14 -3 17.08 1.79 1 -14 3 14.00 1.83 1 -14 4 40.70 3.06 -1 -14 -4 40.42 2.70 1 -14 5 79.54 4.08 -1 -14 -5 72.58 3.42 -1 -14 -6 5.39 0.92 1 -14 6 6.31 1.15 1 -13 -8 3.36 0.96 1 -13 -8 2.17 0.81 -1 -13 7 67.11 4.38 1 -13 -7 71.92 3.98 1 -13 -7 64.07 4.09 1 -13 -6 40.31 3.62 -1 -13 6 45.81 3.87 1 -13 -6 44.35 3.47 1 -13 -5 41.51 3.56 1 -13 -5 38.51 3.69 -1 -13 5 35.87 3.63 -1 -13 4 54.22 4.34 1 -13 -4 57.09 4.58 1 -13 -4 57.02 4.28 -1 -13 3 89.50 6.03 1 -13 -3 96.86 5.98 1 -13 -3 91.43 5.32 -1 -13 3 85.00 5.40 1 -13 -2 9.78 2.11 1 -13 -2 14.15 2.40 1 -13 -2 7.05 1.76 -1 -13 2 8.61 1.86 -1 -13 2 7.44 2.03 1 -13 -1 4.12 1.41 -1 -13 1 7.74 2.05 1 -13 -1 7.68 1.72 1 -13 -1 5.59 1.63 1 -13 0 17.72 2.28 1 -13 0 20.36 2.88 -1 -13 0 20.40 2.73 1 -13 1 20.81 2.38 -1 -13 -1 17.66 2.16 1 -13 1 19.03 3.03 1 -13 1 23.43 2.75 -1 -13 -2 39.25 3.36 1 -13 2 35.06 3.59 1 -13 2 35.19 4.05 -1 -13 -3 35.61 3.34 1 -13 3 36.65 4.15 1 -13 3 33.47 3.47 1 -13 4 1.63 1.75 -1 -13 -4 5.21 1.53 1 -13 4 2.11 1.51 1 -13 5 77.90 5.26 -1 -13 -5 77.91 4.63 1 -13 5 82.45 5.70 -1 -13 -6 11.64 1.88 1 -13 6 16.37 2.78 -1 -13 -7 21.28 2.27 1 -13 7 20.51 2.61 -1 -13 -8 21.42 1.97 1 -13 8 22.72 2.32 1 -12 -10 47.87 2.61 1 -12 -10 51.05 3.27 1 -12 -9 123.52 5.03 1 -12 -9 115.16 5.79 -1 -12 9 107.54 4.26 1 -12 -8 48.43 3.67 -1 -12 8 55.59 3.35 -1 -12 8 52.76 4.45 1 -12 -8 49.23 4.28 1 -12 -7 5.76 1.85 1 -12 -7 6.73 2.09 -1 -12 7 6.15 2.24 1 -12 -6 5.26 2.00 -1 -12 6 6.23 2.49 1 -12 -6 7.18 2.11 1 -12 -5 21.11 3.48 -1 -12 5 23.91 3.48 -1 -12 5 24.40 3.95 1 -12 -5 23.03 3.14 1 -12 -4 69.46 5.95 -1 -12 4 73.02 5.78 -1 -12 4 71.25 6.15 1 -12 -4 69.48 5.27 -1 -12 3 127.94 7.98 -1 -12 3 123.54 7.38 1 -12 -3 121.56 7.78 1 -12 -3 119.06 6.78 1 -12 -2 81.53 5.54 1 -12 -2 96.27 6.86 1 -12 -2 89.10 6.00 -1 -12 2 89.16 6.14 -1 -12 2 86.43 6.57 1 -12 -1 766.57 18.76 1 -12 -1 725.12 16.14 -1 -12 1 766.32 18.52 -1 -12 1 783.78 17.36 1 -12 -1 770.40 18.29 1 -12 0 62.01 5.53 1 -12 0 62.91 4.66 -1 -12 0 63.48 5.25 1 -12 0 69.30 5.62 1 -12 1 74.45 5.68 -1 -12 -1 71.05 4.87 1 -12 1 70.96 4.76 1 -12 1 76.15 6.20 1 -12 1 79.46 5.70 1 -12 2 158.44 8.25 -1 -12 -2 154.02 7.32 1 -12 2 159.51 8.98 1 -12 3 33.10 4.04 -1 -12 -3 29.67 3.43 1 -12 3 28.43 4.22 -1 -12 -4 74.10 5.24 1 -12 4 80.77 6.57 1 -12 4 74.82 5.94 1 -12 5 28.69 4.18 -1 -12 -5 27.13 3.38 1 -12 5 29.78 3.87 -1 -12 -5 24.51 3.02 1 -12 6 7.37 2.76 -1 -12 -6 5.11 1.62 -1 -12 -6 4.09 1.50 1 -12 6 7.56 2.15 1 -12 6 6.20 2.28 1 -12 7 65.78 5.27 1 -12 7 73.26 5.94 -1 -12 -7 58.54 4.31 -1 -12 -7 68.98 4.85 1 -12 8 107.07 6.55 -1 -12 -8 95.49 5.29 -1 -12 -8 101.78 5.16 1 -12 8 102.01 5.91 -1 -12 -9 86.96 4.33 1 -12 9 83.06 5.16 -1 -12 -9 80.02 4.25 1 -12 9 90.16 4.92 -1 -12 -10 16.38 1.65 1 -11 -11 6.98 1.57 1 -11 -11 7.90 1.19 -1 -11 11 6.95 1.33 -1 -11 10 17.16 2.63 1 -11 -10 25.69 3.16 1 -11 -10 21.97 2.34 -1 -11 9 182.28 8.32 1 -11 -9 169.58 6.91 1 -11 -9 162.36 8.26 1 -11 -8 7.49 2.45 -1 -11 8 13.59 2.90 1 -11 -8 5.95 1.77 -1 -11 8 8.85 2.55 -1 -11 7 235.83 10.78 1 -11 -7 210.76 10.54 -1 -11 7 246.64 11.52 1 -11 -7 215.63 8.87 1 -11 -6 73.67 6.45 1 -11 -6 65.09 5.16 -1 -11 6 69.63 6.06 -1 -11 6 71.37 6.50 1 -11 -5 17.74 2.99 -1 -11 5 20.19 3.84 1 -11 -5 19.57 3.72 -1 -11 5 21.65 3.70 -1 -11 4 261.38 11.98 1 -11 -4 250.41 10.08 -1 -11 4 265.60 11.46 1 -11 -4 251.79 11.81 -1 -11 3 140.11 8.74 -1 -11 3 143.07 8.28 1 -11 -3 138.05 8.62 1 -11 -3 136.34 7.54 1 -11 -3 138.05 7.56 1 -11 -2 67.62 6.03 -1 -11 2 78.08 6.06 -1 -11 2 79.48 6.43 1 -11 -2 70.64 5.34 1 -11 -2 75.90 5.86 1 -11 -1 92.26 6.93 1 -11 -1 85.99 6.51 1 -11 -1 82.35 5.75 -1 -11 1 92.21 6.33 -1 -11 1 92.39 6.79 -1 -11 0 61.96 4.54 1 -11 0 64.78 5.17 -1 -11 0 69.71 5.70 1 -11 0 69.46 5.86 1 -11 0 66.56 5.94 1 -11 0 62.39 4.86 1 -11 1 79.06 5.95 1 -11 1 70.57 5.01 -1 -11 -1 70.91 5.54 1 -11 1 79.18 6.52 -1 -11 -1 70.77 5.07 1 -11 1 74.94 6.04 1 -11 2 10.88 2.82 1 -11 2 8.55 2.33 1 -11 2 5.82 1.93 -1 -11 -2 6.61 1.75 1 -11 2 7.65 1.71 1 -11 3 10.62 2.91 1 -11 3 9.90 2.50 -1 -11 -3 11.73 2.31 1 -11 4 173.40 9.49 1 -11 4 158.58 9.50 -1 -11 -4 149.11 7.68 -1 -11 -4 176.42 9.32 1 -11 5 9.71 3.03 -1 -11 -5 8.16 2.32 1 -11 5 9.84 2.99 -1 -11 -5 6.54 2.07 -1 -11 -6 154.49 8.80 1 -11 6 138.90 8.66 -1 -11 -6 132.89 7.20 1 -11 6 153.03 8.89 -1 -11 -7 5.27 1.73 1 -11 7 8.36 2.78 -1 -11 -7 8.47 2.42 1 -11 7 9.39 2.81 1 -11 8 101.04 7.82 -1 -11 -8 89.94 5.58 1 -11 8 100.82 6.79 -1 -11 -8 88.25 6.29 1 -11 9 39.65 4.04 -1 -11 -9 38.35 3.47 -1 -11 -9 33.25 3.67 1 -11 9 37.87 4.66 1 -11 10 62.56 4.24 1 -11 10 57.37 5.03 -1 -11 -10 60.91 3.83 -1 -11 -10 60.00 4.35 -1 -11 -11 53.68 3.45 -1 -11 -11 56.90 3.13 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16.32 1.92 1 -10 10 17.90 2.80 1 -10 10 12.86 3.50 1 -10 11 4.13 2.35 1 -10 11 6.66 1.56 -1 -10 -11 3.83 1.43 -1 -10 -11 2.48 1.05 -1 -10 -11 3.37 0.92 -1 -10 -12 30.92 2.93 1 -10 12 25.80 3.18 -1 -10 -12 34.47 2.42 1 -9 -14 63.98 3.21 1 -9 -13 5.54 1.57 1 -9 -12 15.23 1.83 -1 -9 12 17.36 1.93 1 -9 -12 15.66 2.75 -1 -9 11 2.78 1.11 1 -9 -11 4.12 1.50 -1 -9 11 2.77 2.20 1 -9 -11 2.37 1.93 1 -9 -11 2.79 0.95 1 -9 -11 0.81 0.93 -1 -9 10 31.70 3.99 1 -9 -10 34.17 2.98 1 -9 -10 29.25 3.21 -1 -9 10 30.06 3.15 1 -9 -10 37.77 4.20 1 -9 -10 26.46 4.10 -1 -9 10 30.53 4.90 -1 -9 9 13.90 3.65 1 -9 -9 12.85 2.83 -1 -9 9 15.38 3.32 1 -9 -9 17.11 2.23 -1 -9 8 5.76 2.78 -1 -9 8 9.59 2.76 1 -9 -8 7.23 2.15 1 -9 -7 647.77 19.13 1 -9 -7 603.14 19.20 -1 -9 7 642.80 18.36 -1 -9 7 598.85 18.34 -1 -9 6 224.00 10.93 1 -9 -6 202.06 10.97 -1 -9 6 205.44 10.63 1 -9 -6 226.33 11.38 -1 -9 5 432.00 15.01 1 -9 -5 435.59 15.67 -1 -9 5 438.35 14.91 -1 -9 4 48.31 5.01 -1 -9 4 54.80 5.22 1 -9 -4 42.08 4.81 -1 -9 3 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7.99 -2 4 -13 116.55 8.42 -2 4 -13 121.17 8.75 -2 4 -13 108.33 8.29 -2 4 -13 122.62 8.89 -2 4 -13 117.89 9.54 -2 4 -14 38.65 4.94 2 4 14 41.09 3.75 -2 4 -14 35.18 4.02 -2 4 -14 34.64 4.51 2 4 15 41.48 3.14 -2 4 -15 41.36 4.28 -2 4 -15 42.67 4.46 2 4 15 37.30 3.65 -2 4 -15 35.13 3.75 -2 4 -16 105.89 5.34 -2 4 -16 102.81 5.11 -2 5 16 23.73 2.17 2 5 -16 23.01 2.06 -2 5 16 18.38 1.89 -2 5 16 18.22 1.89 -2 5 15 0.43 1.23 -2 5 15 1.17 0.92 -2 5 15 2.00 1.36 2 5 -15 -1.09 1.82 2 5 -14 14.67 2.83 2 5 -14 21.20 3.61 2 5 -14 17.71 2.62 2 5 -14 17.18 3.73 -2 5 14 19.27 3.34 -2 5 14 18.60 3.13 2 5 -13 16.86 3.78 2 5 -13 19.09 3.51 -2 5 13 19.64 3.73 2 5 -13 25.47 4.99 2 5 -12 178.39 10.91 2 5 -12 163.19 11.95 -2 5 12 159.79 9.65 2 5 -12 159.28 9.50 2 5 -12 171.94 10.54 2 5 -11 346.52 15.43 2 5 -11 362.22 15.81 2 5 -11 360.40 14.38 2 5 -11 345.48 13.60 2 5 -10 15.28 5.88 2 5 -10 19.76 7.98 -2 5 10 30.12 11.15 2 5 -10 20.45 4.40 -2 5 10 14.59 6.81 2 5 -10 22.02 3.69 2 5 -10 24.45 3.92 -2 5 9 168.32 20.48 2 5 -9 156.44 10.47 2 5 -9 161.85 9.12 2 5 -9 159.82 18.15 -2 5 9 154.71 25.13 2 5 -9 172.58 21.71 2 5 -8 169.35 20.07 -2 5 8 182.35 25.86 2 5 -8 177.62 18.84 -2 5 8 182.48 19.72 -2 5 7 657.22 34.99 -2 5 7 584.69 43.38 2 5 -7 600.68 32.39 2 5 -7 691.57 37.40 -2 5 6 393.63 24.93 -2 5 6 395.85 33.07 2 5 -6 399.91 26.35 -2 5 5 557.12 27.43 2 5 -5 640.29 30.55 -2 5 5 570.04 36.23 2 5 -4 33.19 6.74 -2 5 4 30.88 6.06 -2 5 4 21.77 6.65 -2 5 3 90.90 9.27 -2 5 3 84.01 11.83 -2 5 3 88.58 7.26 2 5 -3 87.69 9.77 -2 5 2 263.63 13.60 -2 5 2 289.46 14.55 2 5 -2 270.86 16.10 -2 5 1 1218.92 30.38 2 5 -1 1268.40 33.60 2 5 0 1613.15 37.41 -2 5 0 1632.88 36.19 -2 5 -1 84.17 10.35 2 5 1 76.55 8.04 2 5 1 78.35 6.40 -2 5 -1 79.42 8.44 -2 5 -2 1313.81 38.40 2 5 2 1338.35 40.23 -2 5 -2 1290.76 35.23 2 5 2 1279.08 35.63 -2 5 -2 1253.48 44.14 2 5 3 83.81 11.12 -2 5 -3 54.34 7.95 -2 5 -3 72.29 11.09 2 5 3 50.77 7.88 -2 5 -4 105.11 11.30 2 5 4 141.31 16.27 2 5 4 118.00 12.41 -2 5 -4 129.45 14.84 -2 5 -5 925.61 35.41 2 5 5 887.14 36.76 2 5 5 873.69 43.65 -2 5 -5 935.18 41.20 -2 5 -6 200.98 17.54 -2 5 -6 239.68 22.01 2 5 6 221.42 19.70 2 5 6 219.63 23.81 -2 5 -7 216.85 22.24 -2 5 -7 207.96 19.02 2 5 7 240.34 21.86 2 5 7 214.86 25.03 2 5 8 28.37 7.79 2 5 8 21.92 10.20 -2 5 -8 32.37 10.25 -2 5 -8 4.99 3.91 -2 5 -9 156.09 21.35 2 5 9 117.68 16.86 -2 5 -9 150.67 9.97 -2 5 -9 141.52 8.65 2 5 9 121.57 20.96 -2 5 -9 153.94 18.13 -2 5 -9 150.26 9.84 -2 5 -10 228.54 12.06 -2 5 -10 236.92 12.77 -2 5 -10 222.68 14.26 -2 5 -10 250.79 11.82 -2 5 -10 206.96 21.29 -2 5 -10 246.91 13.21 -2 5 -11 1.59 2.71 -2 5 -11 -0.27 3.13 -2 5 -11 1.68 1.85 -2 5 -11 1.16 1.80 -2 5 -12 327.40 14.61 -2 5 -12 315.66 16.15 -2 5 -12 323.15 14.65 -2 5 -12 329.56 14.54 -2 5 -12 320.13 13.07 -2 5 -13 0.64 2.03 -2 5 -13 0.28 2.26 -2 5 -13 -1.35 3.11 -2 5 -13 4.34 2.32 -2 5 -13 2.54 2.36 -2 5 -13 1.97 1.72 -2 5 -13 2.08 2.56 -2 5 -14 39.49 4.70 -2 5 -14 43.17 4.70 -2 5 -14 48.46 5.19 2 5 14 42.50 3.34 -2 5 -14 30.13 3.76 -2 5 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5.89 2 6 -3 232.48 16.74 -2 6 3 267.71 23.22 2 6 -3 270.66 18.85 -2 6 3 282.08 17.07 2 6 -2 271.83 16.89 2 6 -2 296.58 18.95 -2 6 2 311.38 23.82 -2 6 2 303.82 15.89 -2 6 2 305.99 15.75 2 6 -1 657.19 27.29 2 6 -1 588.63 23.02 -2 6 1 634.64 23.92 -2 6 0 517.58 22.49 2 6 0 506.28 19.59 2 6 0 518.43 24.04 2 6 0 482.15 19.58 -2 6 -1 62.75 8.57 -2 6 -1 79.91 10.72 2 6 1 63.06 7.83 2 6 1 66.05 6.43 -2 6 -2 54.06 8.79 -2 6 -2 53.50 8.27 -2 6 -2 46.57 9.73 2 6 2 38.73 6.63 2 6 2 54.32 9.80 2 6 3 10.31 3.74 -2 6 -3 13.74 4.99 -2 6 -3 11.41 5.08 2 6 3 11.57 5.75 2 6 4 204.81 17.32 2 6 4 201.27 20.72 -2 6 -4 205.61 17.20 -2 6 -4 206.29 20.47 2 6 5 97.46 12.79 2 6 5 119.28 17.66 -2 6 -5 110.16 15.88 -2 6 -5 91.33 12.25 -2 6 -6 761.98 36.58 2 6 6 773.25 38.25 -2 6 -6 807.93 43.31 2 6 6 720.90 45.67 -2 6 -7 45.83 10.96 2 6 7 56.33 10.72 2 6 7 48.65 13.93 -2 6 -7 53.21 10.35 2 6 8 9.56 5.14 -2 6 -8 28.28 9.45 -2 6 -8 21.50 4.05 2 6 8 7.74 6.91 -2 6 -8 22.10 3.34 -2 6 -8 37.69 8.89 -2 6 -9 20.50 3.65 2 6 9 19.96 6.21 2 6 9 25.45 9.75 -2 6 -9 23.18 4.64 -2 6 -9 25.75 9.50 -2 6 -9 19.12 6.77 -2 6 -9 22.90 3.69 -2 6 -10 77.78 7.54 -2 6 -10 71.50 7.27 -2 6 -10 88.86 7.46 -2 6 -10 78.58 6.65 -2 6 -11 4.77 2.09 -2 6 -11 7.01 3.00 -2 6 -11 6.22 3.63 -2 6 -11 4.17 2.51 -2 6 -12 31.75 4.74 -2 6 -12 28.73 4.66 -2 6 -12 26.79 5.22 -2 6 -12 33.68 5.17 -2 6 -12 30.24 4.01 -2 6 -13 24.54 4.04 -2 6 -13 23.30 4.23 -2 6 -13 21.86 3.73 -2 6 -13 30.56 3.70 -2 6 -13 25.74 3.88 -2 6 -13 23.10 4.40 -2 6 -13 32.12 4.69 -2 6 -14 10.57 2.78 -2 6 -14 11.91 2.79 -2 6 -14 8.28 2.19 -2 6 -14 7.35 1.98 -2 6 -15 29.48 3.03 2 6 15 31.51 3.01 -2 6 -15 31.46 3.09 -2 6 -15 27.78 2.85 -2 7 15 25.01 2.37 2 7 -15 26.63 2.44 -2 7 15 22.51 2.01 -2 7 15 26.62 2.39 2 7 -15 27.37 2.73 -2 7 15 25.92 2.54 -2 7 14 59.43 4.48 2 7 -14 54.50 3.85 2 7 -14 51.34 4.47 -2 7 14 46.99 4.15 2 7 -14 51.80 5.00 -2 7 14 51.91 4.31 2 7 -13 205.12 9.91 2 7 -13 207.06 11.45 -2 7 13 184.71 9.41 -2 7 13 198.52 9.25 2 7 -13 205.31 8.70 2 7 -12 19.76 3.17 -2 7 12 27.97 4.12 2 7 -12 29.62 4.22 2 7 -12 27.36 4.48 -2 7 11 7.54 2.47 2 7 -11 15.97 4.04 2 7 -11 15.48 3.41 2 7 -11 7.82 2.16 2 7 -10 52.14 5.31 2 7 -10 45.89 6.01 2 7 -9 557.80 17.03 2 7 -8 264.57 25.29 -2 7 8 267.87 25.78 2 7 -8 289.12 27.94 -2 7 8 248.88 33.47 2 7 -7 231.95 22.45 -2 7 7 240.06 22.85 -2 7 7 312.07 35.94 2 7 -7 306.95 26.95 -2 7 6 18.83 6.26 2 7 -6 4.88 4.20 2 7 -6 28.72 7.92 -2 7 6 17.56 9.18 2 7 -5 126.54 15.16 2 7 -5 169.66 17.95 -2 7 5 192.38 25.20 -2 7 5 171.86 16.62 2 7 -4 87.02 12.33 -2 7 4 103.28 16.98 2 7 -4 74.50 10.87 -2 7 4 90.15 10.82 2 7 -3 86.86 11.67 2 7 -3 65.33 9.72 -2 7 3 64.41 12.54 -2 7 2 203.84 21.58 2 7 -2 197.83 15.46 2 7 -2 216.92 18.00 2 7 -1 14.82 4.61 2 7 -1 10.53 3.56 -2 7 1 4.56 2.74 -2 7 0 133.49 12.67 2 7 0 141.59 14.27 2 7 0 110.82 9.94 -2 7 -1 58.70 10.18 -2 7 -1 59.69 8.97 2 7 1 73.53 11.88 -2 7 -1 59.33 12.57 2 7 1 54.18 8.71 2 7 2 316.59 19.41 -2 7 -2 303.02 20.63 2 7 2 330.91 25.28 -2 7 -2 300.82 26.17 -2 7 -2 324.15 22.27 2 7 3 668.13 30.25 -2 7 -3 634.99 38.47 -2 7 -3 619.40 30.70 2 7 3 698.91 39.04 -2 7 -4 360.26 29.19 -2 7 -4 331.13 23.61 2 7 4 344.22 29.34 2 7 4 367.23 23.99 2 7 5 202.00 19.17 -2 7 -5 201.73 22.68 -2 7 -5 178.87 18.19 2 7 5 200.82 24.36 2 7 6 63.70 15.37 -2 7 -6 75.22 14.03 2 7 6 62.91 11.40 -2 7 -6 74.07 12.63 2 7 7 227.23 22.49 -2 7 -7 248.56 26.26 2 7 7 245.57 30.85 -2 7 -7 252.21 23.46 -2 7 -7 220.08 10.53 2 7 8 165.94 19.81 -2 7 -8 138.96 18.32 -2 7 -8 180.92 23.18 2 7 8 128.73 22.85 -2 7 -8 152.88 10.45 -2 7 -8 170.40 9.51 -2 7 -9 85.57 7.93 -2 7 -9 88.98 7.73 -2 7 -9 87.26 6.94 -2 7 -10 149.48 10.22 -2 7 -10 156.83 10.63 -2 7 -10 172.43 9.54 -2 7 -11 105.83 8.36 -2 7 -11 112.22 10.03 -2 7 -11 111.38 7.44 -2 7 -11 113.91 8.80 -2 7 -12 100.32 7.57 -2 7 -12 96.71 8.71 -2 7 -12 99.74 7.75 -2 7 -12 90.18 7.32 -2 7 -12 111.23 6.90 -2 7 -13 13.88 2.74 -2 7 -13 11.50 2.18 -2 7 -13 20.46 3.81 -2 7 -13 13.84 3.04 -2 7 -13 16.92 3.64 -2 7 -13 11.42 2.73 -2 7 -13 14.38 2.99 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889.27 48.50 -2 8 -3 949.30 51.43 -2 8 -4 138.90 19.46 -2 8 -4 126.69 15.90 2 8 5 135.30 22.30 -2 8 -5 127.83 18.94 -2 8 -5 119.97 16.07 2 8 5 136.38 15.65 -2 8 -6 -2.16 2.54 2 8 6 -9.57 4.75 2 8 7 460.90 43.12 -2 8 -7 457.14 15.33 2 8 7 381.47 29.42 -2 8 -8 65.97 6.97 -2 8 -8 79.13 6.44 -2 8 -9 117.84 8.84 -2 8 -9 137.90 8.33 -2 8 -9 117.23 9.09 -2 8 -10 243.87 10.75 -2 8 -10 219.23 11.98 -2 8 -10 219.39 12.16 -2 8 -11 186.69 10.30 -2 8 -11 200.51 10.58 -2 8 -11 166.63 11.65 -2 8 -11 194.58 10.77 -2 8 -11 191.18 8.83 -2 8 -12 56.35 5.27 -2 8 -12 57.01 5.49 -2 8 -12 52.23 6.06 -2 8 -12 56.05 5.40 -2 8 -13 15.52 2.67 -2 8 -13 17.27 3.08 -2 8 -13 16.15 2.53 -2 8 -13 17.57 2.72 -2 8 -13 15.98 3.07 -2 8 -13 15.84 2.65 -2 8 -14 3.55 1.29 2 8 14 2.99 1.15 -2 8 -14 5.32 1.39 -2 9 13 2.57 1.01 2 9 -13 2.67 1.72 -2 9 13 2.56 1.54 -2 9 13 -0.48 1.21 2 9 -13 0.88 0.99 -2 9 13 2.36 1.08 -2 9 12 9.67 2.01 -2 9 12 6.18 2.38 2 9 -12 10.35 2.45 -2 9 12 6.22 1.82 2 9 -12 14.46 3.73 -2 9 11 92.03 5.95 2 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8.50 1.58 -4 12 -8 6.65 1.84 -4 12 -8 11.57 2.37 -4 12 -9 106.08 4.68 -4 12 -9 106.62 4.65 -4 12 -9 121.94 6.28 -4 12 -9 117.74 5.27 -4 13 7 5.92 1.53 -4 13 6 72.89 4.96 -4 13 5 2.91 1.38 -4 13 4 2.53 1.51 -4 13 -1 39.09 4.51 -4 13 -5 63.18 5.22 -4 13 -6 83.26 5.11 -4 13 -6 82.72 4.99 -4 13 -7 4.36 1.10 -4 13 -7 3.37 1.15 -4 14 1 30.72 3.52 5 -14 -4 74.95 3.26 5 -14 -4 112.64 3.58 5 -14 -3 38.76 2.56 5 -14 -3 38.65 2.31 5 -14 -2 2.90 0.81 5 -14 -2 4.08 1.05 5 -14 -2 3.85 0.93 5 -14 -1 10.90 1.59 5 -14 -1 12.81 1.68 5 -14 -1 12.38 1.42 5 -14 0 23.53 2.29 5 -14 0 23.59 2.14 5 -14 0 20.43 1.70 5 -14 1 63.03 3.26 5 -14 1 60.57 2.64 5 -14 2 9.71 1.49 5 -14 2 8.51 1.18 5 -14 3 90.62 3.99 5 -13 -7 42.19 2.76 5 -13 -7 40.79 2.09 5 -13 -6 67.80 3.28 -5 -13 6 62.00 2.75 5 -13 -5 121.30 5.82 5 -13 -5 123.52 4.84 5 -13 -4 39.14 3.05 5 -13 -4 41.14 3.71 5 -13 -4 36.79 2.96 5 -13 -3 30.41 3.37 5 -13 -3 30.13 2.97 5 -13 -3 31.52 2.89 5 -13 -2 73.66 4.87 5 -13 -2 82.28 5.46 5 -13 -2 73.59 4.33 5 -13 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14.52 2.33 5 -11 -6 7.23 1.88 5 -11 -6 7.22 2.82 -5 -11 5 108.71 5.77 5 -11 -5 85.81 5.55 5 -11 -5 89.23 6.96 5 -11 -5 88.76 6.11 5 -11 -4 10.59 2.31 5 -11 -4 9.73 3.07 5 -11 -3 13.15 3.15 5 -11 -3 13.92 2.67 5 -11 -3 14.79 2.86 5 -11 -2 138.63 7.46 5 -11 -2 140.15 8.83 -5 -11 2 132.20 6.63 5 -11 -2 139.44 8.49 5 -11 -1 69.35 6.13 -5 -11 1 65.12 4.61 5 -11 -1 65.26 5.24 5 -11 -1 67.83 6.30 5 -11 0 38.99 4.73 5 -11 0 41.48 4.99 5 -11 0 44.62 4.33 5 -11 1 10.96 2.45 5 -11 1 13.65 3.23 5 -11 1 11.80 2.59 5 -11 1 13.04 2.92 5 -11 2 204.35 9.91 5 -11 2 226.03 10.64 5 -11 2 210.90 8.67 5 -11 3 26.63 3.84 5 -11 3 22.26 3.52 -5 -11 -3 21.73 2.44 5 -11 3 23.69 3.68 5 -11 3 26.12 3.07 5 -11 4 105.00 6.85 5 -11 4 100.36 6.73 5 -11 4 117.54 7.50 -5 -11 -4 110.96 5.51 5 -11 4 115.17 5.88 5 -11 5 24.14 3.58 -5 -11 -5 23.23 2.53 5 -11 5 24.88 2.57 5 -11 5 22.56 3.26 5 -11 5 22.47 3.32 5 -11 6 181.30 8.15 5 -11 6 180.66 8.11 5 -11 6 198.90 9.09 -5 -11 -6 202.37 6.96 5 -11 7 165.12 7.08 5 -11 7 182.81 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5 -12 11.92 2.34 -8 5 -13 87.17 4.59 -8 5 -13 83.42 4.38 8 6 -13 64.72 3.31 -8 6 13 71.52 3.50 -8 6 13 70.99 3.90 -8 6 13 57.95 2.52 -8 6 13 70.27 3.61 -8 6 13 53.81 2.93 -8 6 12 -0.36 0.90 -8 6 12 0.29 0.98 -8 6 12 0.03 1.29 -8 6 12 0.63 0.70 -8 6 12 0.38 1.20 -8 6 12 0.65 1.12 8 6 -12 0.87 1.03 -8 6 11 79.41 5.61 8 6 -11 96.97 5.71 -8 6 11 94.89 4.65 -8 6 11 94.21 5.55 -8 6 11 102.08 6.63 -8 6 11 86.86 5.54 -8 6 11 97.48 6.54 -8 6 11 95.39 5.94 -8 6 11 90.93 6.15 8 6 -10 21.67 3.03 -8 6 10 26.06 2.73 -8 6 10 21.26 3.05 -8 6 10 21.68 3.83 -8 6 10 21.24 3.58 -8 6 10 21.27 3.74 -8 6 10 20.95 3.34 -8 6 10 21.94 3.83 8 6 -9 60.47 5.12 -8 6 9 64.47 4.35 -8 6 9 60.88 5.15 -8 6 9 57.21 5.73 -8 6 9 59.98 6.45 -8 6 9 58.52 6.06 -8 6 9 58.05 5.46 -8 6 9 59.81 6.22 -8 6 8 77.05 4.87 -8 6 8 73.84 5.74 -8 6 8 78.03 6.77 -8 6 8 71.11 7.41 -8 6 8 74.86 6.78 -8 6 8 71.20 6.10 -8 6 8 70.95 7.13 -8 6 7 111.88 5.88 -8 6 7 113.70 7.00 -8 6 7 114.21 8.18 -8 6 7 99.98 9.06 -8 6 7 114.18 8.51 -8 6 7 122.69 7.98 -8 6 7 101.68 8.38 -8 6 6 96.14 6.31 -8 6 6 111.27 8.01 -8 6 6 94.34 8.80 -8 6 6 94.92 7.66 -8 6 6 93.81 6.83 -8 6 6 99.14 8.22 -8 6 5 47.56 5.27 -8 6 5 52.51 6.94 -8 6 5 54.34 5.71 -8 6 5 49.58 5.00 -8 6 5 49.09 5.88 -8 6 4 26.76 4.97 -8 6 4 38.56 4.81 -8 6 4 31.44 3.79 -8 6 4 34.55 4.84 -8 6 3 179.60 10.49 -8 6 3 156.97 10.88 -8 6 3 172.90 9.73 -8 6 3 171.38 9.91 -8 6 2 178.26 10.23 -8 6 2 192.54 24.78 -8 6 2 194.50 11.59 -8 6 2 202.64 20.44 -8 6 2 189.10 10.04 -8 6 1 271.36 12.27 -8 6 1 269.14 24.10 -8 6 1 273.68 13.02 -8 6 1 258.39 11.40 -8 6 0 167.04 9.51 -8 6 0 143.46 18.24 -8 6 0 164.72 9.72 -8 6 0 152.77 21.44 -8 6 0 160.59 8.56 -8 6 0 160.69 9.77 -8 6 0 158.49 9.79 -8 6 -1 51.50 5.34 -8 6 -1 55.37 5.92 -8 6 -1 51.14 5.50 -8 6 -1 63.72 12.00 -8 6 -1 48.35 6.40 -8 6 -1 56.80 5.58 -8 6 -1 62.48 13.37 -8 6 -1 69.12 6.24 -8 6 -2 126.16 8.03 -8 6 -2 120.12 8.24 -8 6 -2 127.69 9.96 -8 6 -2 147.85 20.30 -8 6 -2 106.79 16.34 -8 6 -2 126.05 8.27 -8 6 -2 130.66 8.65 -8 6 -3 249.29 11.69 -8 6 -3 265.02 11.99 -8 6 -3 278.04 14.16 -8 6 -3 254.26 11.60 -8 6 -3 259.00 25.41 -8 6 -3 260.32 12.76 -8 6 -3 249.91 11.00 -8 6 -4 33.86 4.28 -8 6 -4 31.25 4.29 -8 6 -4 29.15 4.15 -8 6 -4 32.44 4.11 -8 6 -4 35.47 5.35 -8 6 -4 36.70 4.95 -8 6 -4 31.87 4.25 -8 6 -5 92.37 8.00 -8 6 -5 88.55 8.71 -8 6 -5 89.87 6.41 -8 6 -5 90.78 7.51 -8 6 -5 88.12 6.72 -8 6 -5 89.89 6.92 -8 6 -6 26.61 3.44 -8 6 -6 18.69 3.86 -8 6 -6 22.13 4.69 -8 6 -6 26.17 4.19 -8 6 -6 17.27 3.29 -8 6 -7 79.08 8.06 -8 6 -7 76.97 6.26 -8 6 -7 85.52 7.31 -8 6 -7 79.07 6.93 -8 6 -8 2.48 2.22 -8 6 -8 0.52 2.91 -8 6 -8 4.21 1.99 -8 6 -8 4.92 2.35 -8 6 -8 1.48 2.12 -8 6 -9 46.55 4.08 -8 6 -9 42.15 5.04 -8 6 -9 42.65 5.46 -8 6 -9 44.49 4.90 -8 6 -9 45.42 5.23 -8 6 -9 48.78 5.23 -8 6 -9 43.29 4.52 -8 6 -10 103.16 7.14 -8 6 -10 104.24 6.57 -8 6 -10 99.70 6.23 -8 6 -10 101.12 6.95 -8 6 -10 99.17 6.61 -8 6 -10 109.92 6.34 -8 6 -11 10.06 2.16 8 6 11 11.60 1.77 -8 6 -11 9.59 2.04 -8 6 -11 10.67 1.94 -8 6 -11 10.47 2.36 -8 6 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2.47 -9 11 5 7.24 1.80 -9 11 5 7.01 1.72 -9 11 5 4.77 1.09 -9 11 5 7.02 1.97 -9 11 5 5.62 1.33 -9 11 5 5.33 1.48 -9 11 4 3.92 1.63 -9 11 4 1.83 1.30 -9 11 4 2.99 1.12 -9 11 4 -0.14 1.54 -9 11 4 1.83 1.30 -9 11 3 23.95 2.42 -9 11 3 21.21 2.80 -9 11 3 22.47 3.53 -9 11 3 21.65 2.80 -9 11 3 22.85 2.93 -9 11 2 80.86 5.13 -9 11 2 79.37 6.37 -9 11 2 71.68 4.01 -9 11 2 71.25 5.15 -9 11 2 82.75 5.27 -9 11 2 79.05 5.09 -9 11 1 32.04 3.36 -9 11 1 35.47 3.42 -9 11 1 31.53 4.19 -9 11 1 37.34 3.90 -9 11 1 33.73 3.42 -9 11 0 29.74 3.23 -9 11 0 33.88 3.25 -9 11 0 35.44 4.38 -9 11 0 29.95 3.47 -9 11 0 26.44 3.06 -9 11 -1 10.24 2.16 -9 11 -1 13.47 2.90 -9 11 -1 12.15 2.09 -9 11 -1 12.92 2.40 -9 11 -2 36.35 3.40 -9 11 -2 34.77 3.86 -9 11 -2 29.97 3.93 -9 11 -2 35.63 3.52 -9 11 -3 9.35 1.93 -9 11 -3 5.18 2.11 -9 11 -3 9.75 1.97 -9 11 -3 6.30 1.52 -9 11 -4 16.78 2.14 -9 11 -4 15.64 2.72 -9 11 -4 19.56 2.18 -9 11 -4 14.00 2.26 -9 11 -5 125.31 5.67 -9 11 -5 128.70 6.32 -9 11 -5 117.62 5.36 -9 11 -5 121.89 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8.55 1.17 -10 -11 -2 9.87 1.22 10 -11 3 131.09 4.86 -10 -11 -3 118.30 3.70 10 -11 4 53.24 2.83 10 -10 -7 18.02 1.67 -10 -10 7 21.27 1.71 10 -10 -6 13.27 1.74 -10 -10 6 11.24 1.64 -10 -10 6 16.71 1.82 10 -10 -5 4.47 1.36 -10 -10 5 1.53 0.74 -10 -10 5 3.73 1.23 10 -10 -4 51.56 3.89 10 -10 -4 48.93 2.98 -10 -10 4 57.20 3.74 10 -10 -4 54.04 2.85 -10 -10 3 0.85 0.38 10 -10 -3 8.12 1.87 -10 -10 3 1.35 0.70 10 -10 -3 11.36 1.76 -10 -10 3 10.54 1.82 10 -10 -3 8.99 1.37 10 -10 -2 88.78 5.31 10 -10 -2 94.20 4.76 10 -10 -2 94.17 4.46 -10 -10 2 83.16 3.91 10 -10 -1 45.83 3.90 -10 -10 1 38.81 2.82 10 -10 -1 47.00 3.54 10 -10 -1 44.20 3.21 10 -10 0 15.89 2.35 10 -10 0 16.03 2.23 10 -10 0 15.12 2.03 -10 -10 0 16.02 1.88 10 -10 1 6.16 1.52 10 -10 1 4.89 1.56 -10 -10 -1 4.48 1.02 10 -10 2 78.83 4.25 10 -10 2 80.14 4.65 -10 -10 -2 77.44 4.18 -10 -10 -2 74.85 3.62 10 -10 3 61.84 3.99 -10 -10 -3 64.77 3.75 -10 -10 -4 46.85 2.80 10 -10 4 43.32 3.38 -10 -10 -4 44.11 2.94 -10 -10 -5 8.63 1.18 10 -10 5 7.35 1.34 -10 -10 -5 6.68 1.19 -10 -10 -6 45.33 2.20 -10 -10 -6 50.28 2.55 -10 -9 8 126.88 5.58 -10 -9 8 158.23 4.84 -10 -9 7 264.24 6.36 -10 -9 7 275.51 9.01 -10 -9 6 86.88 4.09 -10 -9 6 97.10 4.92 -10 -9 5 29.53 2.98 -10 -9 5 27.91 2.59 -10 -9 4 28.04 3.39 -10 -9 4 34.84 3.45 10 -9 -4 33.90 2.68 -10 -9 4 37.57 3.11 10 -9 -3 137.14 6.16 -10 -9 3 134.86 6.03 -10 -9 3 130.59 6.43 10 -9 -3 138.96 5.75 -10 -9 2 12.17 1.99 10 -9 -2 16.74 2.48 -10 -9 2 12.13 2.33 10 -9 -2 13.56 2.12 -10 -9 1 21.11 2.87 10 -9 -1 25.60 2.99 10 -9 -1 27.98 2.91 -10 -9 1 25.75 2.90 10 -9 0 130.79 6.92 10 -9 0 132.80 6.58 10 -9 0 137.82 6.26 -10 -9 0 134.96 6.35 10 -9 1 88.44 5.50 10 -9 1 82.69 4.74 10 -9 1 86.16 5.41 10 -9 1 88.00 4.97 -10 -9 -1 81.52 4.99 10 -9 2 3.78 1.25 10 -9 2 4.44 1.32 10 -9 2 4.91 1.87 -10 -9 -2 4.20 1.39 -10 -9 -3 3.66 1.28 10 -9 3 1.56 1.42 -10 -9 -4 7.82 1.48 -10 -9 -4 8.19 1.82 -10 -9 -5 24.57 2.50 -10 -9 -5 23.87 2.28 -10 -9 -6 3.43 0.91 -10 -9 -6 6.23 1.27 10 -9 6 6.93 1.49 -10 -9 -6 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3.27 -10 -7 -8 45.47 2.74 -10 -7 -8 51.44 3.32 -10 -7 -8 44.54 3.27 -10 -7 -9 2.39 0.90 -10 -7 -9 1.35 0.74 -10 -7 -9 1.77 0.53 -10 -7 -9 3.78 1.00 -10 -7 -10 16.92 1.28 -10 -7 -10 16.31 1.45 -10 -6 11 12.37 1.78 -10 -6 11 10.00 1.51 -10 -6 10 15.58 2.17 -10 -6 10 12.27 2.20 -10 -6 9 37.79 3.90 10 -6 -9 38.40 3.81 -10 -6 9 37.84 2.77 -10 -6 9 32.73 3.28 -10 -6 8 7.70 2.54 10 -6 -8 5.52 2.20 10 -6 -8 3.48 1.50 -10 -6 8 1.77 0.88 -10 -6 8 4.87 1.86 -10 -6 7 182.64 9.46 10 -6 -7 172.13 8.66 10 -6 -7 167.98 8.90 -10 -6 7 182.09 7.52 -10 -6 7 172.34 7.29 -10 -6 7 177.67 8.23 -10 -6 6 280.61 12.03 10 -6 -6 275.99 11.23 10 -6 -6 276.71 11.94 -10 -6 6 278.35 9.80 -10 -6 6 283.94 10.00 -10 -6 6 291.89 10.74 -10 -6 5 27.52 4.08 -10 -6 5 30.17 3.69 10 -6 -5 26.78 3.97 -10 -6 5 29.31 3.54 -10 -6 5 22.36 3.03 -10 -6 4 14.26 2.79 -10 -6 4 9.94 2.68 10 -6 -4 12.87 3.45 -10 -6 4 12.97 2.56 -10 -6 4 14.35 2.67 -10 -6 3 136.72 8.82 10 -6 -3 160.69 9.50 -10 -6 3 159.39 8.09 -10 -6 3 150.38 8.19 -10 -6 3 161.40 8.28 -10 -6 2 0.82 1.90 10 -6 -2 1.40 0.86 -10 -6 2 0.30 1.54 -10 -6 2 3.17 1.79 -10 -6 2 3.45 1.91 -10 -6 1 195.10 9.43 -10 -6 1 192.52 8.96 -10 -6 1 206.27 9.89 10 -6 -1 202.43 8.40 -10 -6 1 214.69 9.45 -10 -6 0 54.70 5.76 -10 -6 0 69.92 5.91 -10 -6 0 67.95 5.42 -10 -6 0 72.16 6.00 10 -6 0 67.18 5.01 -10 -6 0 76.22 5.69 10 -6 1 47.52 4.42 -10 -6 -1 43.26 4.77 -10 -6 -1 44.51 4.73 10 -6 1 43.42 4.06 -10 -6 -1 51.38 4.80 -10 -6 -2 126.74 7.16 10 -6 2 121.14 7.44 10 -6 2 119.30 6.92 -10 -6 -2 114.55 7.80 -10 -6 -2 123.59 7.25 10 -6 2 114.31 6.51 -10 -6 -3 27.99 3.36 10 -6 3 27.53 3.71 10 -6 3 30.40 3.64 -10 -6 -3 32.20 4.33 -10 -6 -3 30.12 3.77 -10 -6 -4 19.45 2.92 10 -6 4 18.82 3.23 10 -6 4 20.91 3.04 -10 -6 -4 22.25 3.71 -10 -6 -4 19.69 3.08 -10 -6 -5 71.49 5.24 10 -6 5 72.86 5.68 -10 -6 -5 73.27 6.38 -10 -6 -5 80.37 5.67 -10 -6 -6 9.35 2.17 10 -6 6 8.05 2.15 -10 -6 -6 5.38 1.74 -10 -6 -7 13.72 2.34 10 -6 7 10.54 2.26 -10 -6 -7 10.98 1.99 -10 -6 -8 153.83 6.20 -10 -6 -8 152.14 6.01 -10 -6 -8 155.28 6.71 -10 -6 -9 12.02 1.54 -10 -6 -9 11.45 1.68 -10 -6 -9 12.19 1.84 -10 -6 -9 14.06 1.75 -10 -6 -10 42.23 2.61 -10 -6 -10 41.00 2.29 -10 -6 -10 41.44 2.30 -10 -6 -10 42.34 2.80 -10 -5 12 4.99 1.10 -10 -5 11 49.09 3.57 10 -5 -11 61.33 4.07 -10 -5 11 53.73 3.57 -10 -5 10 3.54 1.59 -10 -5 10 3.28 1.44 10 -5 -10 0.82 1.29 10 -5 -10 2.20 1.29 -10 -5 9 322.07 11.28 10 -5 -9 313.88 10.98 10 -5 -9 301.55 10.89 -10 -5 9 332.74 10.73 -10 -5 8 11.53 2.92 10 -5 -8 5.92 2.06 -10 -5 8 8.26 1.75 10 -5 -8 7.83 2.36 -10 -5 8 7.59 1.52 -10 -5 8 11.48 2.00 -10 -5 7 52.40 5.75 10 -5 -7 37.66 4.44 -10 -5 7 37.58 3.65 10 -5 -7 37.22 4.61 -10 -5 7 42.79 3.77 -10 -5 7 40.72 3.90 -10 -5 7 42.39 4.41 -10 -5 6 86.89 7.06 10 -5 -6 77.05 6.25 -10 -5 6 87.05 5.69 10 -5 -6 89.12 7.02 -10 -5 6 92.45 5.70 -10 -5 6 89.36 6.00 -10 -5 6 94.50 6.47 -10 -5 5 9.52 2.35 -10 -5 5 8.61 2.90 10 -5 -5 6.60 2.28 -10 -5 5 9.93 2.17 10 -5 -5 5.43 2.27 -10 -5 5 7.84 2.00 -10 -5 5 6.99 1.89 -10 -5 4 370.07 14.56 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128.70 7.99 -10 2 -1 568.73 16.79 -10 2 -1 573.72 18.73 -10 2 -1 541.07 16.51 -10 2 -1 539.08 16.08 -10 2 -2 359.49 13.46 10 2 2 359.56 13.00 -10 2 -2 353.52 28.27 -10 2 -2 340.43 13.38 -10 2 -2 343.99 12.99 -10 2 -3 4.71 1.74 -10 2 -3 5.42 2.13 -10 2 -3 5.58 1.70 10 2 3 3.77 1.68 -10 2 -3 1.01 1.42 -10 2 -4 125.18 7.30 -10 2 -4 126.14 6.74 10 2 4 127.40 7.44 -10 2 -4 123.58 7.59 -10 2 -4 118.66 8.14 -10 2 -4 125.27 8.08 -10 2 -5 116.34 7.15 -10 2 -5 110.54 6.39 -10 2 -5 126.40 8.72 -10 2 -5 112.28 7.10 -10 2 -5 129.78 8.68 -10 2 -5 118.68 7.99 -10 2 -6 103.78 6.88 -10 2 -6 104.41 6.63 -10 2 -6 103.48 7.76 -10 2 -6 113.06 7.67 -10 2 -7 72.02 6.21 -10 2 -7 76.25 6.27 -10 2 -7 76.21 5.84 -10 2 -8 109.33 7.28 -10 2 -8 105.24 6.74 -10 2 -8 97.68 5.00 -10 2 -8 110.62 7.49 -10 2 -8 114.02 6.87 -10 2 -8 113.81 7.41 -10 2 -9 11.34 2.52 -10 2 -9 10.72 2.47 -10 2 -9 9.91 1.55 -10 2 -9 13.33 2.99 -10 2 -9 10.70 2.82 -10 2 -9 12.04 2.20 -10 2 -10 5.36 1.79 -10 2 -10 8.60 1.87 -10 2 -10 10.17 1.42 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176.09 9.83 -10 3 5 194.64 9.96 -10 3 5 186.32 8.24 -10 3 5 183.04 8.93 -10 3 5 185.23 10.75 -10 3 5 198.20 9.51 -10 3 5 188.95 10.39 -10 3 4 716.09 19.57 -10 3 4 710.51 19.18 -10 3 4 730.09 19.50 -10 3 4 723.37 15.97 -10 3 4 746.73 17.60 -10 3 4 735.12 21.27 -10 3 4 734.56 17.60 -10 3 4 730.61 20.04 -10 3 3 420.57 15.06 -10 3 3 419.59 14.95 -10 3 3 436.65 15.27 -10 3 3 441.51 13.26 -10 3 3 453.69 16.45 -10 3 3 434.80 13.18 -10 3 3 432.01 15.16 -10 3 3 425.47 14.20 -10 3 2 149.49 8.97 -10 3 2 168.31 9.51 -10 3 2 166.18 7.99 -10 3 2 166.37 10.08 -10 3 2 146.45 7.51 -10 3 2 154.49 9.07 -10 3 2 149.41 8.55 -10 3 2 152.25 9.11 -10 3 1 28.35 4.06 -10 3 1 30.53 4.11 -10 3 1 33.99 4.66 -10 3 1 40.43 4.92 -10 3 1 34.66 4.27 -10 3 1 31.24 4.04 -10 3 0 31.22 4.26 -10 3 0 31.50 4.40 -10 3 0 33.44 4.53 -10 3 0 35.73 5.07 -10 3 0 25.73 3.87 -10 3 0 35.24 4.32 -10 3 0 29.59 4.09 -10 3 -1 305.55 12.88 -10 3 -1 316.05 13.03 -10 3 -1 315.52 14.40 -10 3 -1 311.74 26.96 -10 3 -1 298.63 12.73 -10 3 -1 314.86 12.27 -10 3 -1 315.26 12.75 -10 3 -1 309.55 12.45 -10 3 -2 388.00 12.61 -10 3 -2 427.59 16.80 10 3 2 396.42 13.44 -10 3 -2 388.59 14.63 -10 3 -2 400.24 14.39 -10 3 -2 401.83 14.20 10 3 3 250.32 10.38 -10 3 -3 238.35 11.53 -10 3 -3 238.60 10.02 -10 3 -3 247.14 11.36 -10 3 -4 60.95 5.29 -10 3 -4 60.24 6.01 -10 3 -4 59.85 5.81 -10 3 -5 31.11 3.85 -10 3 -5 36.24 4.90 -10 3 -5 37.16 4.07 -10 3 -5 30.29 4.47 -10 3 -5 26.19 3.59 -10 3 -5 37.81 4.63 -10 3 -6 32.41 3.89 -10 3 -6 34.84 4.59 -10 3 -6 35.52 4.79 -10 3 -6 39.22 4.36 -10 3 -6 32.39 4.36 -10 3 -7 5.58 2.10 -10 3 -7 7.48 2.77 -10 3 -7 3.29 1.80 -10 3 -7 6.77 2.70 -10 3 -7 5.72 1.82 -10 3 -8 28.36 3.79 -10 3 -8 29.59 3.76 -10 3 -8 33.15 3.88 -10 3 -8 28.31 3.61 -10 3 -9 19.99 2.99 -10 3 -9 16.98 2.91 -10 3 -9 19.53 2.89 -10 3 -9 17.37 3.20 -10 3 -9 27.77 3.38 -10 3 -10 54.72 4.41 -10 3 -10 43.83 4.40 -10 3 -10 52.11 4.56 -10 3 -10 55.25 4.27 -10 3 -10 51.36 4.00 10 3 11 86.57 4.79 -10 3 -11 81.07 5.23 -10 3 -11 85.98 5.19 -10 3 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4 5 206.43 10.96 -10 4 5 202.83 9.92 -10 4 4 128.61 8.56 -10 4 4 136.88 8.78 -10 4 4 137.35 8.89 -10 4 4 148.18 7.69 -10 4 4 150.66 10.08 -10 4 4 135.76 7.54 -10 4 4 144.79 9.13 -10 4 4 143.42 8.46 -10 4 3 129.83 8.59 -10 4 3 132.41 8.72 -10 4 3 126.96 8.56 -10 4 3 129.73 7.08 -10 4 3 135.01 9.31 -10 4 3 139.45 9.40 -10 4 3 130.23 7.15 -10 4 3 127.88 8.38 -10 4 3 135.98 8.35 -10 4 2 118.09 8.15 -10 4 2 116.67 8.23 -10 4 2 109.94 8.00 -10 4 2 121.83 9.02 -10 4 2 123.19 8.66 -10 4 2 110.53 7.62 -10 4 2 115.02 7.79 -10 4 1 37.76 4.73 -10 4 1 35.33 4.73 -10 4 1 32.56 4.67 -10 4 1 37.95 5.51 -10 4 1 31.60 4.08 -10 4 1 34.19 4.36 -10 4 0 91.19 7.15 -10 4 0 91.58 7.27 -10 4 0 91.79 8.07 -10 4 0 91.86 6.84 -10 4 0 84.74 6.68 -10 4 0 86.94 7.13 -10 4 -1 140.49 8.75 -10 4 -1 148.81 7.89 -10 4 -1 151.21 9.35 -10 4 -1 143.96 9.07 -10 4 -1 169.61 10.95 -10 4 -1 133.95 8.78 -10 4 -1 142.63 8.64 -10 4 -1 155.79 8.66 -10 4 -2 450.62 15.35 -10 4 -2 443.57 13.75 -10 4 -2 446.46 15.65 -10 4 -2 482.49 18.20 10 4 2 446.97 13.94 -10 4 -2 450.98 16.02 -10 4 -2 459.55 15.48 -10 4 -3 108.26 7.64 -10 4 -3 110.37 7.00 -10 4 -3 116.42 9.04 -10 4 -3 101.46 7.39 -10 4 -3 112.52 8.19 -10 4 -4 235.98 10.21 -10 4 -4 227.40 12.05 -10 4 -4 224.09 10.74 -10 4 -4 224.72 11.57 -10 4 -5 87.47 6.36 -10 4 -5 78.10 7.12 -10 4 -5 88.55 7.29 -10 4 -5 85.35 6.49 -10 4 -5 88.26 6.80 -10 4 -6 98.06 6.68 -10 4 -6 101.19 8.00 -10 4 -6 101.94 7.79 -10 4 -6 90.76 6.62 -10 4 -6 99.47 7.01 -10 4 -7 17.60 3.00 -10 4 -7 17.97 3.09 -10 4 -7 16.06 3.34 -10 4 -7 17.82 3.74 -10 4 -7 19.55 3.23 -10 4 -8 48.58 4.72 -10 4 -8 42.34 4.27 -10 4 -8 44.68 4.49 -10 4 -8 44.78 4.42 -10 4 -9 139.05 7.16 -10 4 -9 133.56 6.99 -10 4 -9 136.79 7.62 -10 4 -9 132.22 7.10 -10 4 -9 132.33 6.57 -10 4 -10 25.01 2.84 -10 4 -10 26.65 3.44 -10 4 -10 23.88 3.20 -10 4 -10 22.67 2.79 -10 4 -10 21.96 2.35 -10 4 -11 135.23 5.23 10 4 11 140.09 5.61 -10 4 -11 132.97 6.31 -10 4 -11 135.00 6.09 -10 4 -11 125.40 5.36 10 4 12 68.91 3.07 -10 4 -12 73.47 3.79 -10 5 12 9.20 1.30 -10 5 12 9.95 1.35 -10 5 11 64.62 3.29 -10 5 11 64.52 3.87 -10 5 11 70.37 4.11 -10 5 11 62.87 3.94 -10 5 10 4.79 1.48 -10 5 10 3.72 1.16 -10 5 10 4.10 1.57 -10 5 10 0.80 1.43 -10 5 10 3.84 1.61 -10 5 9 312.21 10.89 -10 5 9 322.16 9.02 -10 5 9 328.58 10.34 -10 5 9 318.49 11.24 -10 5 9 336.48 10.77 -10 5 9 306.61 11.23 -10 5 8 10.08 2.56 -10 5 8 6.22 1.44 -10 5 8 10.18 2.22 -10 5 8 8.85 2.78 -10 5 8 10.33 2.25 -10 5 8 11.08 2.89 -10 5 7 35.06 4.07 -10 5 7 38.67 4.37 -10 5 7 32.19 4.21 -10 5 7 40.28 3.57 -10 5 7 38.19 3.89 -10 5 7 36.64 4.81 -10 5 7 41.73 4.31 -10 5 7 41.12 4.99 -10 5 6 85.42 6.69 -10 5 6 87.64 7.08 -10 5 6 89.82 6.93 -10 5 6 94.21 5.40 -10 5 6 92.72 5.99 -10 5 6 95.44 6.68 -10 5 6 87.07 7.49 -10 5 6 87.23 6.03 -10 5 6 96.37 7.52 -10 5 5 8.78 2.61 -10 5 5 10.61 2.76 -10 5 5 5.40 2.65 -10 5 5 6.52 1.65 -10 5 5 7.23 3.05 -10 5 5 9.27 2.14 -10 5 5 6.24 2.77 -10 5 5 8.90 2.37 -10 5 4 420.62 15.51 -10 5 4 404.77 15.39 -10 5 4 399.03 15.25 -10 5 4 394.42 15.90 -10 5 4 408.41 16.38 -10 5 4 427.11 12.78 -10 5 4 400.08 14.99 -10 5 4 422.58 14.91 -10 5 3 395.10 15.10 -10 5 3 376.26 14.86 -10 5 3 393.59 15.24 -10 5 3 384.23 16.25 -10 5 3 399.47 15.85 -10 5 3 401.21 14.72 -10 5 3 396.60 14.52 -10 5 2 24.29 4.19 -10 5 2 26.43 4.21 -10 5 2 24.16 4.01 -10 5 2 28.92 4.86 -10 5 2 26.62 4.39 -10 5 2 22.28 3.66 -10 5 2 26.82 3.99 -10 5 1 383.23 14.48 -10 5 1 390.79 15.11 -10 5 1 382.44 14.93 -10 5 1 391.67 16.71 -10 5 1 375.09 13.74 -10 5 1 386.68 14.46 -10 5 0 87.26 7.05 -10 5 0 95.48 7.62 -10 5 0 100.67 7.86 -10 5 0 101.87 8.82 -10 5 0 97.10 6.91 -10 5 0 94.79 7.26 -10 5 -1 103.46 7.58 -10 5 -1 121.24 7.37 -10 5 -1 106.09 7.93 -10 5 -1 110.06 8.00 -10 5 -1 114.33 9.23 -10 5 -1 105.86 8.02 -10 5 -1 130.33 7.80 -10 5 -1 106.85 7.64 -10 5 -2 137.29 8.59 -10 5 -2 114.77 7.21 -10 5 -2 121.62 8.41 -10 5 -2 121.80 8.35 -10 5 -2 122.59 9.47 -10 5 -2 131.99 8.50 -10 5 -2 118.76 8.55 -10 5 -3 313.43 12.69 -10 5 -3 289.77 11.42 -10 5 -3 296.19 14.22 -10 5 -3 309.84 14.11 -10 5 -3 289.60 13.17 -10 5 -3 302.52 12.62 -10 5 -4 59.99 5.31 -10 5 -4 56.15 6.33 -10 5 -4 62.53 6.48 -10 5 -4 71.32 6.78 -10 5 -4 61.21 5.60 -10 5 -5 201.93 9.47 -10 5 -5 204.15 11.43 -10 5 -5 201.77 9.80 -10 5 -5 203.24 10.89 -10 5 -5 180.82 9.52 -10 5 -6 121.37 8.79 -10 5 -6 136.85 8.79 -10 5 -6 118.79 7.70 -10 5 -6 124.16 7.40 -10 5 -6 126.11 7.50 -10 5 -7 70.17 5.51 -10 5 -7 58.94 6.03 -10 5 -7 74.72 6.42 -10 5 -7 69.45 5.71 -10 5 -7 70.60 5.39 -10 5 -8 21.02 3.21 -10 5 -8 24.87 3.29 -10 5 -8 20.40 3.13 -10 5 -8 24.20 2.88 -10 5 -9 36.91 3.57 -10 5 -9 37.59 4.15 -10 5 -9 35.90 3.73 -10 5 -9 39.12 3.76 -10 5 -10 27.60 2.62 -10 5 -10 28.76 3.12 -10 5 -10 28.44 3.03 10 5 11 14.59 1.64 -10 5 -11 17.70 2.23 -10 5 -11 17.80 2.08 -10 5 -11 15.84 1.89 -10 6 11 15.98 1.64 -10 6 11 16.15 1.80 -10 6 11 17.29 1.95 -10 6 10 10.40 1.86 -10 6 10 15.85 1.94 -10 6 10 15.11 2.15 -10 6 10 18.70 2.58 -10 6 9 36.86 3.79 -10 6 9 39.90 3.26 -10 6 9 37.00 3.89 -10 6 9 33.33 3.30 -10 6 9 34.90 3.80 -10 6 8 6.31 1.92 -10 6 8 4.95 2.17 -10 6 8 4.84 1.38 -10 6 8 5.69 2.19 -10 6 8 6.21 1.86 -10 6 8 3.87 2.44 -10 6 8 5.62 1.82 -10 6 7 174.78 8.73 -10 6 7 171.72 9.19 -10 6 7 177.46 8.96 -10 6 7 184.94 7.58 -10 6 7 178.27 9.85 -10 6 7 171.86 7.82 -10 6 7 170.50 9.32 -10 6 7 184.12 8.55 -10 6 6 271.89 11.78 -10 6 6 271.90 12.01 -10 6 6 272.82 11.95 -10 6 6 285.85 12.98 -10 6 6 296.18 10.34 -10 6 6 292.27 12.31 -10 6 5 21.00 3.77 -10 6 5 27.17 4.13 -10 6 5 27.08 4.29 -10 6 5 27.92 4.24 -10 6 5 28.58 4.78 -10 6 5 31.82 3.42 -10 6 5 32.41 4.55 -10 6 4 13.31 3.24 -10 6 4 9.30 3.11 -10 6 4 15.27 3.37 -10 6 4 13.26 3.51 -10 6 4 13.13 3.84 -10 6 4 10.11 3.09 -10 6 4 13.51 3.13 -10 6 3 161.74 9.68 -10 6 3 155.58 9.77 -10 6 3 151.26 9.61 -10 6 3 169.24 10.95 -10 6 3 164.84 10.25 -10 6 3 166.43 9.31 -10 6 3 153.39 9.20 -10 6 2 -1.20 2.36 -10 6 2 4.87 2.63 -10 6 2 2.48 2.09 -10 6 2 0.92 2.28 -10 6 2 1.95 2.09 -10 6 2 1.41 1.47 -10 6 2 2.58 2.34 -10 6 1 212.91 10.76 -10 6 1 203.95 11.12 -10 6 1 209.14 11.13 -10 6 1 187.14 11.95 -10 6 1 197.32 9.72 -10 6 1 197.31 10.52 -10 6 0 69.78 6.27 -10 6 0 61.26 6.17 -10 6 0 68.86 6.52 -10 6 0 63.62 7.16 -10 6 0 72.81 5.78 -10 6 0 55.14 5.69 -10 6 -1 46.56 5.23 -10 6 -1 45.18 5.35 -10 6 -1 51.26 5.55 -10 6 -1 54.19 6.64 -10 6 -1 50.88 5.70 -10 6 -1 42.78 4.33 -10 6 -1 42.41 4.95 -10 6 -2 121.51 7.99 -10 6 -2 119.69 7.41 -10 6 -2 124.08 8.33 -10 6 -2 124.84 9.54 -10 6 -2 137.14 9.48 -10 6 -2 126.18 8.19 -10 6 -2 117.28 8.65 -10 6 -2 127.50 8.48 -10 6 -3 27.71 3.71 -10 6 -3 27.46 3.89 -10 6 -3 31.26 5.10 -10 6 -3 31.41 4.88 -10 6 -3 27.62 4.51 -10 6 -3 32.73 4.40 -10 6 -4 21.26 3.43 -10 6 -4 24.80 3.55 -10 6 -4 20.23 4.15 -10 6 -4 26.30 4.47 -10 6 -4 21.12 3.93 -10 6 -5 79.09 5.94 -10 6 -5 76.87 7.14 -10 6 -5 75.70 6.72 -10 6 -5 77.55 5.89 -10 6 -6 8.03 2.30 -10 6 -6 7.97 2.08 -10 6 -6 8.58 2.13 -10 6 -6 3.38 2.29 -10 6 -6 6.83 2.83 -10 6 -6 7.79 2.42 -10 6 -7 11.33 2.57 -10 6 -7 11.24 1.95 -10 6 -7 11.90 2.30 -10 6 -7 8.39 2.43 -10 6 -7 13.71 3.51 -10 6 -7 8.78 2.39 -10 6 -8 142.94 6.79 -10 6 -8 154.47 7.28 -10 6 -8 147.60 7.10 -10 6 -8 144.51 7.53 -10 6 -9 11.02 2.07 -10 6 -9 13.30 1.93 -10 6 -9 8.29 1.58 -10 6 -9 9.99 2.13 -10 6 -9 15.52 2.57 -10 6 -10 31.95 2.26 10 6 10 40.59 2.79 -10 6 -10 42.08 3.34 -10 6 -11 9.17 1.38 -10 7 11 26.68 1.99 -10 7 10 14.11 1.84 -10 7 10 18.27 2.21 -10 7 9 96.71 5.47 -10 7 9 100.72 5.67 -10 7 9 117.47 5.13 -10 7 9 108.97 5.87 -10 7 8 16.91 2.46 -10 7 8 13.78 2.30 -10 7 8 14.19 2.62 -10 7 8 14.06 2.72 -10 7 8 14.70 2.14 -10 7 8 18.73 2.97 -10 7 8 16.25 2.29 -10 7 7 117.21 6.95 -10 7 7 116.47 7.22 -10 7 7 117.98 7.14 -10 7 7 128.16 7.98 -10 7 7 131.86 6.15 -10 7 7 133.67 7.72 -10 7 7 120.77 6.73 -10 7 6 81.95 6.38 -10 7 6 91.99 6.89 -10 7 6 88.23 6.67 -10 7 6 100.42 7.68 -10 7 6 94.16 5.23 -10 7 6 99.74 6.90 -10 7 6 88.01 6.33 -10 7 5 4.74 2.52 -10 7 5 2.66 2.08 -10 7 5 4.66 2.76 -10 7 5 4.17 2.35 -10 7 5 5.12 3.09 -10 7 5 3.02 2.08 -10 7 5 4.59 2.16 -10 7 4 12.34 3.22 -10 7 4 11.97 3.26 -10 7 4 11.18 2.90 -10 7 4 14.89 3.62 -10 7 4 14.62 3.78 -10 7 4 12.18 3.00 -10 7 4 11.75 3.01 -10 7 3 211.99 10.76 -10 7 3 202.02 10.95 -10 7 3 202.53 10.94 -10 7 3 191.15 11.63 -10 7 3 205.00 11.13 -10 7 3 203.97 9.87 -10 7 3 187.94 10.12 -10 7 2 327.98 13.20 -10 7 2 328.35 13.84 -10 7 2 327.72 13.84 -10 7 2 306.09 14.88 -10 7 2 329.41 13.61 -10 7 2 337.58 12.43 -10 7 2 325.45 13.29 -10 7 1 50.80 5.42 -10 7 1 53.74 5.98 -10 7 1 55.71 5.96 -10 7 1 44.85 6.22 -10 7 1 49.23 4.73 -10 7 1 46.90 5.33 -10 7 0 112.62 7.75 -10 7 0 101.67 7.84 -10 7 0 107.94 7.99 -10 7 0 110.09 9.20 -10 7 0 117.03 6.96 -10 7 0 112.57 7.99 -10 7 -1 542.91 16.32 -10 7 -1 546.41 17.31 -10 7 -1 551.75 19.65 -10 7 -1 538.36 17.98 -10 7 -1 546.38 17.41 -10 7 -1 544.47 17.01 -10 7 -2 70.70 5.89 -10 7 -2 77.48 5.99 -10 7 -2 74.73 6.42 -10 7 -2 69.37 6.22 -10 7 -2 75.88 7.40 -10 7 -2 66.39 6.65 -10 7 -2 75.72 6.90 -10 7 -2 74.83 6.35 -10 7 -3 67.50 5.67 -10 7 -3 68.43 7.05 -10 7 -3 68.61 6.80 -10 7 -3 75.38 6.87 -10 7 -3 66.84 5.94 -10 7 -3 66.07 5.48 -10 7 -4 87.67 6.29 -10 7 -4 91.04 7.53 -10 7 -4 71.17 6.89 -10 7 -4 87.18 7.19 -10 7 -4 87.89 6.02 -10 7 -5 184.90 8.73 -10 7 -5 174.00 10.21 -10 7 -5 204.90 10.34 -10 7 -5 183.68 8.11 -10 7 -6 53.88 4.77 -10 7 -6 61.00 5.05 -10 7 -6 51.19 5.50 -10 7 -6 64.97 5.80 -10 7 -6 56.71 5.13 -10 7 -6 64.07 4.40 -10 7 -7 57.80 4.59 -10 7 -7 55.47 4.26 -10 7 -7 55.66 4.56 -10 7 -7 56.02 5.41 -10 7 -7 64.54 5.36 -10 7 -7 61.87 5.14 -10 7 -8 41.17 3.23 -10 7 -8 48.37 3.85 -10 7 -8 49.07 3.83 -10 7 -8 47.33 4.10 -10 7 -9 1.75 0.78 -10 7 -9 -0.23 1.07 -10 7 -9 1.03 0.53 -10 7 -9 3.26 1.24 -10 7 -9 1.91 1.23 -10 7 -10 18.48 2.06 -10 7 -10 16.48 1.67 -10 7 -10 18.31 1.91 -10 8 10 24.10 1.99 -10 8 9 12.39 1.29 -10 8 9 15.06 2.00 -10 8 8 28.60 3.13 -10 8 8 26.60 2.74 -10 8 8 28.78 2.93 -10 8 8 30.15 3.38 -10 8 8 22.53 1.96 -10 8 8 27.88 3.05 -10 8 8 27.60 2.64 -10 8 7 4.87 1.86 -10 8 7 6.36 2.05 -10 8 7 6.89 2.17 -10 8 7 6.73 2.48 -10 8 7 9.95 2.26 -10 8 7 4.84 1.50 -10 8 6 15.85 2.97 -10 8 6 19.94 3.27 -10 8 6 17.61 2.97 -10 8 6 22.46 3.16 -10 8 6 22.98 3.77 -10 8 6 20.56 3.14 -10 8 6 21.00 3.01 -10 8 5 95.78 6.74 -10 8 5 98.55 6.91 -10 8 5 89.18 6.58 -10 8 5 92.83 6.97 -10 8 5 98.15 7.19 -10 8 5 97.76 6.25 -10 8 5 87.20 6.24 -10 8 4 40.40 4.66 -10 8 4 41.53 4.85 -10 8 4 38.07 4.73 -10 8 4 35.47 4.97 -10 8 4 36.42 4.79 -10 8 4 45.84 4.49 -10 8 4 36.12 4.30 -10 8 3 24.58 4.05 -10 8 3 35.02 4.76 -10 8 3 34.77 4.31 -10 8 3 27.73 4.76 -10 8 3 33.54 4.55 -10 8 3 29.97 3.55 -10 8 3 30.78 4.26 -10 8 2 103.50 7.12 -10 8 2 98.80 7.63 -10 8 2 99.80 7.54 -10 8 2 91.96 8.12 -10 8 2 102.15 7.29 -10 8 2 106.23 6.49 -10 8 2 94.97 7.14 -10 8 1 7.38 2.97 -10 8 1 8.45 3.00 -10 8 1 5.74 1.90 -10 8 1 3.98 3.37 -10 8 1 8.56 1.99 -10 8 1 4.03 2.36 -10 8 0 17.14 3.63 -10 8 0 22.10 3.85 -10 8 0 20.25 3.31 -10 8 0 18.13 4.54 -10 8 0 18.11 3.78 -10 8 0 21.84 3.70 -10 8 -1 45.72 5.07 -10 8 -1 43.31 4.87 -10 8 -1 48.23 6.24 -10 8 -1 42.57 4.42 -10 8 -1 41.25 5.18 -10 8 -1 46.34 5.16 -10 8 -2 60.82 5.08 -10 8 -2 55.80 5.00 -10 8 -2 60.93 5.60 -10 8 -2 58.94 6.72 -10 8 -2 47.36 5.56 -10 8 -2 54.47 5.89 -10 8 -2 58.13 5.49 -10 8 -3 185.58 8.76 -10 8 -3 181.62 10.39 -10 8 -3 155.90 9.65 -10 8 -3 193.77 10.08 -10 8 -3 174.53 8.83 -10 8 -3 190.59 8.30 -10 8 -4 13.22 2.11 -10 8 -4 12.42 3.19 -10 8 -4 11.26 3.05 -10 8 -4 9.81 2.81 -10 8 -4 13.13 2.82 -10 8 -5 22.53 3.19 -10 8 -5 20.55 3.60 -10 8 -5 18.42 3.28 -10 8 -5 22.04 3.41 -10 8 -6 10.46 2.36 -10 8 -6 10.85 2.18 -10 8 -6 8.83 2.65 -10 8 -6 13.46 2.75 -10 8 -6 16.11 2.67 -10 8 -7 57.75 4.11 -10 8 -7 51.76 3.49 -10 8 -7 54.51 4.12 -10 8 -7 49.57 4.73 -10 8 -7 63.20 4.75 -10 8 -8 5.23 1.40 -10 8 -8 4.19 1.13 -10 8 -8 3.56 1.13 -10 8 -8 5.36 1.59 -10 8 -9 1.80 0.72 -10 8 -9 2.48 0.91 -10 9 8 153.43 5.75 -10 9 8 131.84 4.84 -10 9 8 140.01 5.17 -10 9 8 154.09 5.44 -10 9 8 121.57 4.43 -10 9 7 338.20 9.51 -10 9 7 320.64 9.22 -10 9 7 332.77 9.53 -10 9 7 352.15 10.30 -10 9 7 337.28 8.94 -10 9 7 321.78 8.86 -10 9 6 95.03 5.56 -10 9 6 89.60 5.59 -10 9 6 92.15 5.71 -10 9 6 94.00 5.49 -10 9 6 102.28 6.16 -10 9 6 102.10 5.28 -10 9 6 92.47 5.39 -10 9 5 25.12 3.25 -10 9 5 26.73 3.51 -10 9 5 25.28 3.49 -10 9 5 28.04 3.71 -10 9 5 26.29 3.52 -10 9 5 26.30 2.88 -10 9 5 28.30 3.43 -10 9 4 34.31 3.80 -10 9 4 39.83 4.53 -10 9 4 37.62 4.38 -10 9 4 30.86 4.26 -10 9 4 30.75 3.82 -10 9 4 34.61 3.32 -10 9 4 27.00 3.60 -10 9 3 139.93 8.15 -10 9 3 136.41 7.92 -10 9 3 125.90 8.51 -10 9 3 129.58 6.19 -10 9 3 131.40 7.51 -10 9 3 133.02 7.18 -10 9 2 17.78 3.61 -10 9 2 10.12 2.65 -10 9 2 14.00 2.65 -10 9 2 16.48 3.92 -10 9 2 10.49 2.89 -10 9 1 29.13 3.44 -10 9 1 31.19 4.27 -10 9 1 27.44 3.97 -10 9 1 23.44 4.56 -10 9 1 26.70 4.06 -10 9 1 25.68 3.84 -10 9 0 141.04 7.28 -10 9 0 136.85 8.03 -10 9 0 144.40 8.12 -10 9 0 139.40 9.39 -10 9 0 136.47 8.41 -10 9 0 141.48 7.97 -10 9 -1 107.23 6.07 -10 9 -1 98.19 6.18 -10 9 -1 94.51 6.41 -10 9 -1 97.41 6.47 -10 9 -1 101.14 7.87 -10 9 -1 91.02 6.95 -10 9 -1 94.40 6.89 -10 9 -1 97.09 6.45 -10 9 -2 3.59 1.83 -10 9 -2 4.13 1.35 -10 9 -2 4.17 2.88 -10 9 -2 5.01 2.11 -10 9 -2 4.97 2.32 -10 9 -2 4.70 2.06 -10 9 -3 3.74 1.78 -10 9 -3 1.61 2.13 -10 9 -3 4.15 2.44 -10 9 -3 4.26 2.25 -10 9 -4 10.50 2.37 -10 9 -4 7.37 2.52 -10 9 -4 9.40 2.46 -10 9 -5 28.14 3.17 -10 9 -5 27.68 3.17 -10 9 -5 26.46 3.67 -10 9 -5 25.62 3.19 -10 9 -5 24.04 3.16 -10 9 -6 6.19 1.60 -10 9 -6 5.66 1.15 -10 9 -6 2.92 1.30 -10 9 -6 4.65 1.91 -10 9 -6 4.62 1.51 -10 9 -6 6.90 1.81 -10 9 -6 -0.06 0.41 -10 9 -7 37.66 2.89 -10 9 -7 31.13 2.61 -10 9 -7 43.29 3.74 -10 9 -7 39.26 3.25 -10 9 -8 25.70 2.24 -10 9 -8 24.51 1.89 -10 10 7 22.41 1.93 -10 10 7 18.47 1.79 -10 10 7 19.77 1.88 -10 10 7 18.81 1.71 -10 10 6 15.73 1.92 -10 10 6 15.29 2.07 -10 10 6 16.31 2.12 -10 10 6 10.86 1.32 -10 10 6 15.10 1.93 -10 10 5 5.90 1.65 -10 10 5 6.35 1.71 -10 10 5 2.52 1.09 -10 10 5 2.34 1.36 -10 10 5 1.82 0.64 -10 10 5 2.57 1.35 -10 10 4 60.32 4.03 -10 10 4 63.48 4.60 -10 10 4 59.91 4.42 -10 10 4 50.23 4.40 -10 10 4 56.06 4.21 -10 10 3 14.86 2.65 -10 10 3 11.85 2.42 -10 10 3 11.66 1.94 -10 10 3 10.01 2.65 -10 10 3 8.41 2.12 -10 10 2 90.50 5.02 -10 10 2 91.34 5.76 -10 10 2 91.35 5.72 -10 10 2 91.43 6.58 -10 10 2 83.98 5.77 -10 10 2 86.76 5.49 -10 10 1 49.69 3.71 -10 10 1 44.77 4.19 -10 10 1 46.21 4.19 -10 10 1 55.92 5.34 -10 10 1 46.08 4.48 -10 10 1 45.03 4.13 -10 10 0 19.99 2.69 -10 10 0 21.53 2.96 -10 10 0 19.23 2.70 -10 10 0 19.81 3.38 -10 10 0 16.57 2.68 -10 10 0 19.58 3.02 -10 10 0 19.37 2.85 -10 10 0 19.76 2.25 -10 10 -1 4.42 1.71 -10 10 -1 3.16 2.10 -10 10 -1 7.40 2.12 -10 10 -1 8.48 2.28 -10 10 -1 8.59 2.10 -10 10 -2 85.26 5.05 -10 10 -2 94.60 6.33 -10 10 -2 85.51 5.58 -10 10 -3 71.04 4.48 -10 10 -3 62.84 5.04 -10 10 -3 69.52 4.82 -10 10 -4 50.23 3.61 -10 10 -4 40.72 4.04 -10 10 -4 48.95 3.74 -10 10 -4 45.63 3.77 -10 10 -5 8.32 1.60 -10 10 -5 8.52 1.55 -10 10 -5 9.24 1.94 -10 10 -5 7.16 1.42 -10 10 -5 8.02 1.77 -10 10 -6 49.50 2.91 -10 10 -6 48.33 3.43 -10 10 -6 49.91 3.25 -10 11 5 77.67 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59.76 3.10 -11 -5 -9 50.91 2.42 -11 -5 -9 72.32 3.84 -11 -5 -10 92.18 3.20 -11 -5 -10 95.96 3.71 11 -4 -11 144.86 5.47 -11 -4 11 142.86 5.11 -11 -4 10 5.43 1.54 -11 -4 10 1.97 1.09 11 -4 -10 3.95 1.33 11 -4 -10 3.51 1.30 -11 -4 9 2.04 1.45 -11 -4 9 2.37 1.34 11 -4 -9 2.05 1.33 -11 -4 9 2.71 1.09 11 -4 -9 0.88 1.24 -11 -4 9 2.54 0.96 -11 -4 8 6.56 2.00 -11 -4 8 3.41 1.66 11 -4 -8 5.76 1.78 -11 -4 8 6.75 1.70 11 -4 -8 5.23 1.98 -11 -4 8 6.97 1.74 -11 -4 7 113.55 7.62 11 -4 -7 138.37 7.58 -11 -4 7 137.27 6.89 11 -4 -7 137.56 8.32 -11 -4 7 134.56 6.99 -11 -4 7 144.54 7.51 -11 -4 6 95.51 7.36 11 -4 -6 109.40 6.87 -11 -4 6 112.26 6.55 11 -4 -6 107.25 7.40 -11 -4 6 109.25 5.72 -11 -4 6 114.26 6.76 -11 -4 6 125.35 7.18 -11 -4 5 116.80 8.37 11 -4 -5 142.59 7.93 -11 -4 5 143.27 7.71 11 -4 -5 150.36 7.55 11 -4 -5 153.88 9.09 -11 -4 5 149.91 7.05 -11 -4 5 151.78 8.01 -11 -4 5 153.72 7.97 -11 -4 4 13.47 2.69 -11 -4 4 11.79 3.16 -11 -4 4 13.04 2.64 11 -4 -4 14.18 2.56 11 -4 -4 14.25 2.89 -11 -4 4 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86.36 6.20 -11 3 -7 82.42 5.59 -11 3 -8 57.25 4.84 -11 3 -8 66.35 5.28 -11 3 -8 56.07 4.92 -11 3 -8 51.77 4.47 -11 3 -8 47.86 4.11 -11 3 -9 122.22 6.34 -11 3 -9 110.99 6.30 -11 3 -9 109.89 6.20 -11 3 -9 116.95 6.00 -11 3 -10 20.89 2.43 -11 3 -10 19.06 2.36 -11 3 -10 18.76 2.48 -11 3 -11 99.96 4.05 11 3 11 110.19 4.33 -11 3 -11 98.44 4.36 -11 3 -11 106.88 4.66 -11 4 11 162.10 5.43 -11 4 11 153.15 5.37 -11 4 10 6.96 1.60 -11 4 10 7.32 1.78 -11 4 10 4.18 1.33 -11 4 9 -0.33 0.90 -11 4 9 3.13 1.51 -11 4 9 1.34 1.31 -11 4 9 1.55 1.18 -11 4 8 5.56 1.70 -11 4 8 8.46 2.12 -11 4 8 6.46 1.93 -11 4 8 5.83 2.22 -11 4 7 131.17 7.48 -11 4 7 140.35 7.09 -11 4 7 141.24 7.29 -11 4 7 133.65 7.96 -11 4 6 110.02 7.24 -11 4 6 112.29 6.76 -11 4 6 114.14 6.56 -11 4 6 114.49 6.73 -11 4 6 112.50 7.71 -11 4 5 146.74 8.64 -11 4 5 156.23 8.48 -11 4 5 155.20 7.64 -11 4 5 155.23 7.79 -11 4 5 160.14 9.16 -11 4 5 157.11 8.44 -11 4 4 13.51 2.93 -11 4 4 16.20 3.10 -11 4 4 10.27 2.85 -11 4 4 16.97 2.72 -11 4 4 12.09 2.37 -11 4 4 11.67 2.91 -11 4 4 12.83 2.60 -11 4 3 64.87 5.94 -11 4 3 74.86 6.37 -11 4 3 81.24 6.66 -11 4 3 75.00 5.18 -11 4 3 71.35 6.43 -11 4 3 78.35 5.40 -11 4 3 66.54 6.02 -11 4 3 76.29 6.02 -11 4 2 44.88 5.10 -11 4 2 47.88 5.31 -11 4 2 43.03 4.97 -11 4 2 57.81 6.01 -11 4 2 40.61 4.69 -11 4 2 48.71 5.25 -11 4 2 47.07 4.79 -11 4 1 29.15 4.29 -11 4 1 29.74 4.31 -11 4 1 32.00 4.39 -11 4 1 22.55 4.05 -11 4 1 34.80 4.46 -11 4 1 26.15 3.84 -11 4 1 29.47 4.04 -11 4 0 200.41 10.34 -11 4 0 202.12 10.55 -11 4 0 195.94 10.36 -11 4 0 198.61 11.36 -11 4 0 197.71 10.33 -11 4 0 200.22 9.92 -11 4 0 194.26 9.88 -11 4 -1 21.65 3.00 -11 4 -1 16.54 3.25 -11 4 -1 16.31 3.72 11 4 1 18.08 2.95 -11 4 -1 13.79 3.03 -11 4 -1 20.74 3.53 -11 4 -2 349.02 13.35 -11 4 -2 349.94 11.71 11 4 2 371.59 12.46 -11 4 -2 351.35 13.89 -11 4 -2 331.86 12.91 -11 4 -3 152.73 7.84 -11 4 -3 148.23 9.02 -11 4 -3 163.92 9.19 -11 4 -4 44.20 4.33 -11 4 -4 48.65 4.50 -11 4 -4 42.69 4.79 -11 4 -4 46.96 5.23 -11 4 -4 42.66 4.21 -11 4 -5 136.06 7.39 -11 4 -5 140.45 8.17 -11 4 -5 149.36 8.91 -11 4 -5 135.20 8.52 -11 4 -5 143.02 7.66 -11 4 -6 13.03 2.59 -11 4 -6 16.26 3.11 -11 4 -6 13.24 3.16 -11 4 -6 14.99 2.54 -11 4 -7 43.39 4.42 -11 4 -7 42.92 3.97 -11 4 -7 35.82 3.98 -11 4 -7 35.01 3.68 -11 4 -8 40.79 3.96 -11 4 -8 35.79 3.93 -11 4 -8 42.49 3.68 -11 4 -8 37.18 3.57 -11 4 -8 38.90 3.66 -11 4 -9 39.89 3.50 -11 4 -9 33.09 3.39 -11 4 -9 35.32 3.51 -11 4 -9 39.57 3.16 -11 4 -9 32.52 2.86 -11 4 -10 1.42 0.93 -11 4 -10 2.08 1.05 -11 4 -10 1.52 1.10 -11 4 -10 -0.79 0.45 11 4 11 18.11 1.58 -11 4 -11 20.36 1.92 -11 5 11 1.53 0.57 -11 5 11 1.77 0.78 -11 5 10 16.06 1.87 -11 5 10 17.16 2.03 -11 5 10 14.58 1.94 -11 5 9 8.81 1.62 -11 5 9 10.01 1.66 -11 5 9 9.70 1.74 -11 5 9 11.15 2.18 -11 5 8 56.98 4.51 -11 5 8 63.25 4.25 -11 5 8 61.28 4.43 -11 5 8 63.02 5.04 -11 5 7 30.86 3.23 -11 5 7 27.22 3.51 -11 5 7 32.74 3.23 -11 5 7 30.68 3.37 -11 5 7 29.00 3.97 -11 5 6 2.56 1.55 -11 5 6 2.84 1.69 -11 5 6 5.42 2.20 -11 5 6 1.32 1.05 -11 5 6 0.58 1.17 -11 5 6 -1.90 2.25 -11 5 5 24.84 3.56 -11 5 5 19.92 3.33 -11 5 5 20.61 3.58 -11 5 5 20.32 2.62 -11 5 5 21.15 2.83 -11 5 5 20.50 3.71 -11 5 5 19.67 2.98 -11 5 4 33.95 4.44 -11 5 4 31.35 4.24 -11 5 4 29.39 4.25 -11 5 4 33.69 3.38 -11 5 4 30.97 4.36 -11 5 4 30.70 3.91 -11 5 3 100.00 7.31 -11 5 3 109.75 7.70 -11 5 3 96.22 7.24 -11 5 3 110.55 8.04 -11 5 3 103.92 7.33 -11 5 3 106.20 7.14 -11 5 2 166.94 9.40 -11 5 2 170.13 9.65 -11 5 2 163.19 9.45 -11 5 2 184.48 10.72 -11 5 2 163.61 9.03 -11 5 2 162.76 9.10 -11 5 1 222.77 10.93 -11 5 1 204.93 10.67 -11 5 1 205.73 10.65 -11 5 1 208.15 11.64 -11 5 1 194.04 10.31 -11 5 1 201.67 9.90 -11 5 1 210.38 10.27 -11 5 0 71.89 6.31 -11 5 0 76.89 5.46 -11 5 0 76.45 6.73 -11 5 0 79.40 6.70 -11 5 0 83.84 7.49 -11 5 0 67.77 6.27 -11 5 0 71.94 5.95 -11 5 0 76.30 6.40 -11 5 -1 146.79 8.74 -11 5 -1 151.80 7.75 -11 5 -1 159.67 10.37 11 5 1 159.94 8.12 -11 5 -1 150.33 9.16 -11 5 -1 150.97 8.80 -11 5 -2 41.43 4.72 -11 5 -2 40.96 4.18 -11 5 -2 36.33 4.86 -11 5 -2 42.04 5.02 -11 5 -2 42.47 5.01 -11 5 -3 41.22 4.20 -11 5 -3 39.97 4.89 -11 5 -3 49.68 5.10 -11 5 -4 17.06 2.90 -11 5 -4 21.75 3.48 -11 5 -4 19.29 3.40 -11 5 -4 18.52 3.78 -11 5 -4 21.24 3.10 -11 5 -5 2.34 1.55 -11 5 -5 2.31 1.69 -11 5 -5 2.62 1.43 -11 5 -5 4.31 2.55 -11 5 -5 5.10 1.70 -11 5 -6 32.25 3.57 -11 5 -6 31.62 3.96 -11 5 -6 34.58 4.38 -11 5 -6 27.79 3.40 -11 5 -6 33.14 3.78 -11 5 -7 139.76 6.79 -11 5 -7 153.15 7.50 -11 5 -7 148.48 7.15 -11 5 -7 153.77 7.16 -11 5 -8 1.91 1.45 -11 5 -8 3.64 1.45 -11 5 -8 1.07 0.74 -11 5 -8 3.30 1.76 -11 5 -8 4.22 1.45 -11 5 -9 68.44 4.07 -11 5 -9 58.07 4.15 -11 5 -9 71.68 4.58 -11 5 -9 58.46 3.68 -11 5 -10 79.28 3.41 11 5 10 94.33 3.92 -11 5 -10 85.55 4.22 -11 5 -10 92.24 4.41 -11 6 10 8.62 1.19 -11 6 10 7.45 1.32 -11 6 9 12.11 1.79 -11 6 9 14.93 1.64 -11 6 9 15.49 1.84 -11 6 9 16.73 2.33 -11 6 8 16.79 2.49 -11 6 8 19.59 2.05 -11 6 8 19.33 2.31 -11 6 8 20.26 2.89 -11 6 7 60.30 4.90 -11 6 7 57.38 4.24 -11 6 7 55.30 4.26 -11 6 7 55.22 3.53 -11 6 7 56.84 3.94 -11 6 7 64.72 5.17 -11 6 6 122.52 7.31 -11 6 6 120.91 6.87 -11 6 6 119.92 6.88 -11 6 6 122.57 5.93 -11 6 6 124.71 7.43 -11 6 6 116.89 6.33 -11 6 5 13.28 2.91 -11 6 5 11.84 2.78 -11 6 5 11.73 3.00 -11 6 5 11.99 1.86 -11 6 5 10.58 2.82 -11 6 5 14.84 2.55 -11 6 4 68.73 6.00 -11 6 4 55.71 5.43 -11 6 4 64.80 5.85 -11 6 4 53.26 5.32 -11 6 4 55.08 5.29 -11 6 4 58.59 5.27 -11 6 3 63.45 5.88 -11 6 3 69.43 6.20 -11 6 3 62.94 5.87 -11 6 3 75.80 6.64 -11 6 3 59.62 5.34 -11 6 3 68.35 5.76 -11 6 2 25.93 4.24 -11 6 2 17.24 3.48 -11 6 2 18.25 3.43 -11 6 2 23.99 4.45 -11 6 2 24.05 3.65 -11 6 2 19.09 3.32 -11 6 1 100.80 7.27 -11 6 1 104.07 6.24 -11 6 1 101.31 7.50 -11 6 1 95.95 7.35 -11 6 1 103.14 8.25 -11 6 1 94.60 7.34 -11 6 1 102.08 6.84 -11 6 1 87.49 6.67 -11 6 0 97.61 7.17 -11 6 0 97.82 6.19 -11 6 0 97.66 7.42 -11 6 0 104.64 7.61 -11 6 0 96.65 8.14 -11 6 0 97.52 7.48 -11 6 0 93.06 6.94 -11 6 -1 60.89 5.67 -11 6 -1 63.96 5.09 -11 6 -1 59.74 6.43 -11 6 -1 53.39 5.65 -11 6 -1 64.18 5.85 -11 6 -2 25.38 3.36 -11 6 -2 26.47 3.81 -11 6 -2 22.08 4.36 -11 6 -2 25.55 4.15 -11 6 -2 27.60 4.64 -11 6 -3 3.92 1.71 -11 6 -3 3.74 1.95 -11 6 -3 5.39 2.25 -11 6 -3 6.11 2.76 -11 6 -4 3.24 1.65 -11 6 -4 4.04 1.84 -11 6 -4 -0.02 1.45 -11 6 -4 3.15 2.26 -11 6 -4 2.95 1.68 -11 6 -5 22.62 3.11 -11 6 -5 21.50 3.04 -11 6 -5 23.29 3.46 -11 6 -5 23.25 3.60 -11 6 -5 19.89 2.97 -11 6 -6 58.97 4.58 -11 6 -6 63.68 5.38 -11 6 -6 63.48 5.49 -11 6 -6 54.34 4.57 -11 6 -6 59.80 4.42 -11 6 -7 2.80 1.52 -11 6 -7 3.66 1.48 -11 6 -7 4.43 1.20 -11 6 -7 1.03 1.15 -11 6 -8 7.18 1.58 -11 6 -8 6.45 1.47 -11 6 -8 9.46 2.19 -11 6 -8 6.22 1.60 -11 6 -9 23.64 2.02 -11 6 -9 23.63 2.45 -11 6 -9 27.72 2.58 -11 6 -9 23.92 2.20 -11 7 9 17.50 1.86 -11 7 9 14.95 1.38 -11 7 8 0.35 0.38 -11 7 8 4.86 1.53 -11 7 8 4.35 0.95 -11 7 8 4.66 1.42 -11 7 7 39.47 3.77 -11 7 7 39.94 3.34 -11 7 7 35.98 3.25 -11 7 7 36.72 2.64 -11 7 7 38.29 3.67 -11 7 7 30.99 2.76 -11 7 6 59.82 4.92 -11 7 6 51.78 4.34 -11 7 6 55.35 4.55 -11 7 6 53.64 4.53 -11 7 6 56.17 4.22 -11 7 5 96.27 6.40 -11 7 5 90.15 6.17 -11 7 5 84.90 5.97 -11 7 5 87.10 5.81 -11 7 5 91.44 6.06 -11 7 5 85.39 5.69 -11 7 4 77.74 6.13 -11 7 4 75.08 5.98 -11 7 4 83.04 6.32 -11 7 4 93.28 6.71 -11 7 4 90.16 6.04 -11 7 4 76.87 5.73 -11 7 3 112.67 7.31 -11 7 3 112.09 7.38 -11 7 3 105.01 7.25 -11 7 3 114.22 7.94 -11 7 3 120.72 7.00 -11 7 3 103.07 6.84 -11 7 2 96.54 6.90 -11 7 2 102.59 7.40 -11 7 2 105.13 7.40 -11 7 2 96.97 7.65 -11 7 2 96.70 6.18 -11 7 2 99.70 6.84 -11 7 1 1.86 1.17 -11 7 1 1.74 2.54 -11 7 1 3.17 2.71 -11 7 1 0.16 1.78 -11 7 1 1.07 2.45 -11 7 1 0.73 1.91 -11 7 1 -1.20 1.21 -11 7 1 2.24 2.09 -11 7 0 98.99 6.84 -11 7 0 98.48 6.06 -11 7 0 105.85 7.46 -11 7 0 101.50 7.30 -11 7 0 95.65 7.78 -11 7 0 85.10 6.82 -11 7 0 96.61 6.88 -11 7 -1 100.19 6.70 -11 7 -1 95.27 6.08 -11 7 -1 100.35 8.11 -11 7 -1 93.86 7.27 -11 7 -1 94.03 6.86 -11 7 -2 25.80 3.33 -11 7 -2 28.79 3.64 -11 7 -2 25.10 4.44 -11 7 -2 30.03 4.37 -11 7 -2 29.29 4.16 -11 7 -3 11.63 2.34 -11 7 -3 11.83 2.59 -11 7 -3 4.38 2.02 -11 7 -3 4.61 2.49 -11 7 -4 65.45 4.85 -11 7 -4 60.23 5.25 -11 7 -4 63.13 5.71 -11 7 -4 58.07 4.89 -11 7 -4 60.87 4.66 -11 7 -5 10.51 2.30 -11 7 -5 8.53 1.88 -11 7 -5 5.37 1.85 -11 7 -5 4.13 2.16 -11 7 -5 7.60 2.00 -11 7 -6 34.81 3.36 -11 7 -6 35.17 3.71 -11 7 -6 41.59 4.15 -11 7 -6 36.37 3.63 -11 7 -6 33.32 2.80 -11 7 -7 22.70 2.60 -11 7 -7 20.23 2.31 -11 7 -7 19.64 2.52 -11 7 -8 -0.43 0.85 -11 7 -8 0.89 0.70 -11 7 -8 0.24 0.95 -11 7 -8 -0.30 0.74 -11 7 -9 84.72 3.54 -11 8 8 58.72 3.40 -11 8 8 63.81 3.51 -11 8 7 27.86 2.81 -11 8 7 22.14 2.23 -11 8 7 27.07 2.56 -11 8 7 27.41 2.72 -11 8 7 24.68 2.18 -11 8 6 22.53 2.87 -11 8 6 21.73 2.67 -11 8 6 23.03 2.82 -11 8 6 21.96 2.64 -11 8 6 20.16 2.35 -11 8 5 32.11 3.57 -11 8 5 33.56 3.55 -11 8 5 31.62 3.51 -11 8 5 29.32 3.11 -11 8 5 34.69 3.41 -11 8 5 34.64 3.40 -11 8 4 49.49 4.41 -11 8 4 54.60 4.77 -11 8 4 48.33 4.52 -11 8 4 55.97 4.90 -11 8 4 52.91 4.15 -11 8 4 55.14 4.50 -11 8 3 82.03 5.72 -11 8 3 84.17 6.09 -11 8 3 87.05 6.17 -11 8 3 76.22 6.10 -11 8 3 76.00 4.94 -11 8 3 77.02 5.60 -11 8 2 126.10 7.13 -11 8 2 123.32 6.09 -11 8 2 121.31 7.35 -11 8 2 122.47 7.42 -11 8 2 124.10 8.05 -11 8 2 115.10 7.30 -11 8 2 134.85 6.50 -11 8 2 117.46 6.99 -11 8 1 28.16 3.13 -11 8 1 29.16 4.12 -11 8 1 29.99 4.10 -11 8 1 24.56 3.36 -11 8 1 30.75 4.54 -11 8 1 28.49 3.98 -11 8 1 25.77 3.70 -11 8 0 27.56 3.51 -11 8 0 27.29 3.23 -11 8 0 31.75 4.22 -11 8 0 27.55 3.84 -11 8 0 26.47 4.21 -11 8 0 30.28 4.14 -11 8 0 28.86 3.87 -11 8 -1 27.48 3.22 -11 8 -1 25.79 4.23 -11 8 -1 30.01 4.18 -11 8 -1 26.98 3.70 -11 8 -1 31.73 3.55 -11 8 -2 7.14 1.95 -11 8 -2 9.31 2.01 -11 8 -2 3.30 2.61 -11 8 -2 7.35 1.99 -11 8 -2 5.25 2.31 -11 8 -2 8.20 2.32 -11 8 -3 50.14 4.12 -11 8 -3 49.82 4.56 -11 8 -3 48.57 4.76 -11 8 -3 45.19 3.74 -11 8 -4 11.24 2.17 -11 8 -4 9.82 1.56 -11 8 -4 6.27 1.90 -11 8 -4 8.80 2.18 -11 8 -4 6.92 1.92 -11 8 -5 10.61 2.00 -11 8 -5 6.17 1.83 -11 8 -5 9.44 2.21 -11 8 -5 8.00 1.91 -11 8 -6 25.99 2.60 -11 8 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4.47 -11 9 0 41.75 3.95 -11 9 0 42.87 3.58 -11 9 -1 30.42 3.11 -11 9 -1 23.60 3.48 -11 9 -1 25.44 3.36 -11 9 -1 28.25 3.26 -11 9 -1 34.61 3.10 -11 9 -2 4.44 1.42 -11 9 -2 5.45 1.19 -11 9 -2 4.90 2.03 -11 9 -2 2.49 1.05 -11 9 -2 4.66 1.85 -11 9 -3 1.53 1.13 -11 9 -3 1.04 0.92 -11 9 -4 13.19 2.00 -11 9 -4 11.29 1.96 -11 9 -4 13.25 2.19 -11 9 -4 11.14 1.99 -11 9 -5 2.70 1.08 -11 9 -5 3.88 1.03 -11 9 -5 2.17 0.97 -11 9 -5 2.79 1.18 -11 9 -5 2.50 1.09 -11 9 -6 54.56 3.01 -11 9 -6 57.73 3.27 -11 10 5 2.55 0.75 -11 10 5 3.14 0.86 -11 10 5 2.20 0.83 -11 10 5 0.41 0.50 -11 10 4 0.84 0.82 -11 10 4 0.77 0.81 -11 10 4 1.02 0.60 -11 10 4 1.14 0.69 -11 10 4 0.98 0.86 -11 10 4 0.55 0.77 -11 10 3 5.60 0.99 -11 10 3 4.62 1.31 -11 10 3 3.00 1.14 -11 10 3 3.40 0.99 -11 10 3 0.54 0.99 -11 10 3 3.28 1.17 -11 10 3 3.81 1.22 -11 10 2 26.81 2.26 -11 10 2 27.41 2.22 -11 10 2 28.14 2.98 -11 10 2 29.30 2.90 -11 10 2 26.51 2.58 -11 10 1 99.17 4.36 -11 10 1 105.82 5.73 -11 10 1 106.95 5.50 -11 10 1 110.38 5.16 -11 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3.34 -14 3 -2 54.91 3.70 -14 3 -2 62.58 4.21 -14 3 -2 59.58 4.28 -14 3 -3 40.21 3.15 -14 3 -3 42.90 3.27 -14 3 -3 49.19 3.78 -14 3 -4 12.20 1.76 -14 3 -4 11.95 1.97 -14 3 -4 10.25 1.46 -14 3 -5 31.59 2.55 -14 3 -5 36.10 2.84 -14 3 -6 9.01 1.26 -14 3 -6 9.85 1.36 14 4 -6 1.61 0.94 -14 4 6 1.53 0.71 14 4 -5 23.64 2.45 -14 4 5 16.01 1.63 14 4 -4 39.28 3.29 -14 4 4 30.40 2.56 14 4 -3 68.51 4.33 -14 4 3 65.49 4.05 14 4 -2 136.10 6.09 -14 4 2 124.53 5.80 -14 4 1 15.72 2.29 14 4 -1 13.68 2.05 -14 4 1 18.20 2.49 14 4 0 75.33 4.19 -14 4 0 78.79 4.72 -14 4 0 71.91 4.62 -14 4 -1 17.71 2.39 14 4 1 18.39 2.09 -14 4 -1 15.31 2.18 -14 4 -2 26.88 2.54 -14 4 -2 30.20 2.72 -14 4 -2 28.49 3.02 -14 4 -3 24.91 2.44 -14 4 -3 25.54 2.25 -14 4 -3 31.78 2.91 -14 4 -4 163.85 5.77 -14 4 -4 177.72 6.27 -14 4 -5 177.20 5.49 -14 4 -5 186.93 5.84 14 5 -5 0.21 0.63 14 5 -4 53.27 3.32 -14 5 4 44.14 2.87 -14 5 3 7.69 1.49 14 5 -3 7.96 1.46 14 5 -2 122.21 5.02 -14 5 2 123.94 5.58 -14 5 2 115.81 5.27 14 5 -1 16.23 1.82 -14 5 1 18.19 2.30 -14 5 1 18.21 2.32 -14 5 0 132.50 5.58 -14 5 0 139.35 5.96 -14 5 -1 165.72 5.89 -14 5 -1 175.89 6.63 -14 5 -2 28.98 2.50 -14 5 -2 24.02 2.03 -14 5 -2 31.05 2.81 -14 5 -3 21.07 2.09 -14 5 -3 23.25 2.34 -14 5 -4 88.96 3.86 -14 5 -4 97.49 4.12 -14 6 4 17.75 1.69 -14 6 3 18.23 1.87 -14 6 3 17.58 1.83 -14 6 2 76.99 3.77 -14 6 2 76.28 3.83 -14 6 1 145.08 5.09 -14 6 1 145.72 5.43 -14 6 0 15.46 1.63 -14 6 0 15.95 1.94 -14 6 -1 63.96 3.56 -14 6 -2 2.81 0.87 -14 6 -2 1.07 0.65 -14 6 -3 4.47 0.87 -14 6 -3 4.12 0.84 -15 -4 3 31.37 1.92 -15 -4 2 54.53 2.67 -15 -4 1 40.12 2.38 15 -4 -1 31.19 1.97 -15 -4 0 109.36 3.85 15 -4 0 102.87 3.69 -15 -4 -1 37.97 2.23 15 -4 1 33.14 2.11 15 -4 2 45.71 2.35 -15 -3 4 51.29 2.56 -15 -3 4 50.74 2.65 -15 -3 3 81.70 3.45 -15 -3 2 33.45 2.35 15 -3 -2 30.22 2.17 -15 -3 1 16.81 1.76 15 -3 -1 14.13 1.62 -15 -3 1 10.93 1.39 -15 -3 0 11.52 1.41 15 -3 0 11.66 1.51 -15 -3 0 10.97 1.48 -15 -3 -1 7.54 1.24 15 -3 1 5.81 1.10 -15 -3 -1 7.37 1.28 -15 -3 -2 68.29 3.12 15 -3 2 67.62 3.25 -15 -3 -2 66.41 3.44 15 -3 3 71.35 3.03 -15 -3 -3 82.59 3.56 -15 -2 5 79.95 3.21 -15 -2 4 5.84 1.04 -15 -2 4 8.12 1.26 -15 -2 3 4.51 0.94 -15 -2 3 5.26 1.10 -15 -2 2 74.23 3.59 -15 -2 2 62.96 3.33 -15 -2 2 70.62 3.51 -15 -2 1 41.01 2.76 -15 -2 1 39.62 2.89 -15 -2 0 7.95 1.37 -15 -2 0 10.71 1.72 -15 -2 -1 29.85 2.29 15 -2 1 32.53 2.57 -15 -2 -1 31.98 2.72 -15 -2 -2 16.48 1.68 15 -2 2 14.99 1.67 -15 -2 -2 19.16 2.05 15 -2 3 18.75 1.69 -15 -2 -3 23.60 2.15 -15 -2 -4 42.24 2.44 -15 -1 5 15.77 1.52 -15 -1 4 1.89 0.69 -15 -1 4 2.64 0.86 -15 -1 3 18.60 1.75 -15 -1 3 17.78 1.81 -15 -1 3 17.73 1.79 -15 -1 2 14.07 1.68 -15 -1 2 14.44 1.87 -15 -1 2 13.13 1.59 -15 -1 1 32.13 2.41 -15 -1 1 28.62 2.67 -15 -1 0 -0.92 0.81 -15 -1 0 -0.41 0.92 -15 -1 -1 57.09 3.10 -15 -1 -1 56.42 3.70 -15 -1 -2 65.81 3.17 15 -1 2 66.99 3.49 -15 -1 -2 69.15 3.90 15 -1 3 36.95 2.36 -15 -1 -3 41.49 2.86 -15 -1 -4 8.21 1.19 -15 0 5 21.87 1.73 -15 0 4 11.79 1.39 -15 0 4 11.33 1.37 -15 0 3 82.84 3.35 -15 0 3 90.41 4.22 -15 0 3 95.48 3.90 -15 0 2 7.15 1.13 -15 0 2 7.63 1.50 -15 0 2 6.37 1.06 -15 0 1 51.56 2.83 -15 0 1 50.89 3.58 -15 0 0 58.64 3.00 -15 0 0 65.79 4.13 -15 0 -1 23.32 1.88 -15 0 -1 28.22 2.75 -15 0 -2 54.75 3.52 -15 0 -2 44.08 2.63 15 0 3 44.48 2.50 -15 0 -3 39.57 2.42 -15 0 -4 75.18 3.28 15 1 -5 14.75 1.56 15 1 -4 0.85 0.74 -15 1 4 0.93 0.53 -15 1 4 1.58 0.58 15 1 -3 14.92 1.95 -15 1 3 14.28 1.75 -15 1 3 14.34 1.42 15 1 -2 13.96 1.97 -15 1 2 13.32 1.83 -15 1 1 34.72 3.00 -15 1 0 -0.67 0.62 -15 1 0 -0.55 0.92 -15 1 -1 61.63 3.83 -15 1 -1 52.25 3.06 -15 1 -2 70.77 3.89 -15 1 -2 62.91 3.33 -15 1 -3 43.70 2.80 -15 1 -3 37.89 2.52 -15 1 -4 9.15 1.19 15 2 -5 85.04 3.53 15 2 -4 8.23 1.32 -15 2 4 6.77 1.05 15 2 -3 3.02 1.06 -15 2 3 4.20 1.06 15 2 -2 77.53 4.11 -15 2 2 75.00 4.07 15 2 -1 43.84 3.12 -15 2 1 41.41 3.17 -15 2 0 8.60 1.34 -15 2 0 9.77 1.59 -15 2 -1 34.37 2.76 -15 2 -1 33.45 2.54 -15 2 -2 15.06 1.74 -15 2 -2 16.44 1.80 -15 2 -3 16.13 1.58 -15 2 -3 20.09 1.88 -15 2 -4 36.65 2.24 15 3 -4 50.34 2.80 -15 3 4 44.16 2.49 15 3 -3 84.33 3.82 -15 3 3 77.71 3.72 15 3 -2 37.81 2.64 -15 3 2 35.92 2.66 -15 3 1 16.97 1.96 -15 3 1 12.33 1.46 -15 3 0 11.57 1.49 -15 3 0 14.88 1.84 -15 3 -1 6.45 1.16 -15 3 -1 7.69 1.32 -15 3 -2 61.15 2.99 -15 3 -2 66.59 3.33 -15 3 -3 73.06 3.28 -15 4 3 29.88 2.05 -15 4 2 53.38 2.92 -15 4 1 46.21 2.78 -15 4 1 38.99 2.37 -15 4 0 108.99 4.05 -15 4 0 108.88 4.06 -15 4 -1 37.70 2.40 -15 4 -2 44.30 2.49 0 0 0 0.00 0.00 TITL TR_4-Cu in P2(1) REM P2(1) (#4 in standard setting) CELL 1.54184 12.471087 12.098626 13.764492 90.0000 91.7422 90.0000 ZERR 8.00 0.000157 0.000186 0.000166 0.0000 0.0011 0.0000 LATT -1 SYMM -x, y+1/2,-z SFAC C H O UNIT 48.00 96.00 48.00 TREF HKLF 4 END ; _shelx_hkl_checksum 24690 _shelx_res_file ; TITL I P 21 R 0.03 CELL 1.54184 12.47110 12.09860 13.76450 90.00000 91.74200 90.00000 ZERR 4 0.00020 0.00020 0.00020 0.00000 0.00100 0.00000 LATT -1 SYMM -X, Y+ 0.50000, -Z SFAC C H O UNIT 104 116 22 PLAN 30 FMAP 2 L.S. 9 BOND $H CONF ACTA HTAB EQIV $1 -X, Y-1/2, -Z+1 HTAB C13 O2B_$1 HTAB C18 O1 EQIV $2 -X+1, Y+1/2, -Z+1 HTAB C21 O1W_$2 HTAB C13B O4 HTAB C14B O3 EQIV $3 X, Y, Z-1 HTAB C18B O5_$3 HTAB C18B O1B HTAB O1W O3 HTAB O1W O4B HTAB O1W O1 HTAB O1W O3 DFIX 0.84 .02 O1W H1W O1W H2W WGHT 0.045400 0.392300 EXTI 0.001180 FVAR 0.67389 O1 3 0.417463 0.144194 0.438409 11.00000 0.02472 0.02381 = 0.02430 0.00301 0.01137 0.00628 O2 3 0.165982 0.068535 0.785678 11.00000 0.02549 0.01897 = 0.01518 0.00662 0.00450 0.00243 O3 3 0.250318 0.325230 0.458998 11.00000 0.01761 0.01751 = 0.01088 0.00342 0.00297 -0.00097 O4 3 0.075555 0.490605 0.551848 11.00000 0.01593 0.01822 = 0.01277 0.00511 0.00093 0.00435 O5 3 0.321073 0.730087 0.901006 11.00000 0.02875 0.02352 = 0.01663 -0.00186 0.00127 -0.00095 C1 1 0.374661 0.105203 0.509081 11.00000 0.01707 0.01441 = 0.01808 -0.00233 0.00254 0.00099 C2 1 0.428016 0.012231 0.563477 11.00000 0.01780 0.01931 = 0.02659 -0.00033 0.00273 0.00437 AFIX 43 H2 2 0.496492 -0.007294 0.544749 11.00000 -1.20000 AFIX 0 C3 1 0.386819 -0.045843 0.636689 11.00000 0.02064 0.01653 = 0.02509 0.00165 -0.00126 0.00469 AFIX 43 H3 2 0.425990 -0.103071 0.665632 11.00000 -1.20000 AFIX 0 C4 1 0.276956 -0.017779 0.671594 11.00000 0.02089 0.01472 = 0.01742 0.00277 0.00044 0.00053 C5 1 0.258419 -0.006864 0.781090 11.00000 0.02619 0.02073 = 0.01830 0.00695 0.00101 0.00403 AFIX 23 H5A 2 0.242126 -0.078047 0.809516 11.00000 -1.20000 H5B 2 0.320926 0.024129 0.814744 11.00000 -1.20000 AFIX 0 C6 1 0.168640 0.137114 0.705066 11.00000 0.01788 0.01527 = 0.01194 0.00197 0.00090 -0.00312 C7 1 0.106175 0.223414 0.684873 11.00000 0.01383 0.01821 = 0.01245 0.00225 0.00281 -0.00227 AFIX 43 H7 2 0.051307 0.241959 0.726144 11.00000 -1.20000 AFIX 0 C8 1 0.124420 0.292380 0.593722 11.00000 0.01207 0.01574 = 0.01168 0.00181 0.00220 0.00012 C9 1 0.233138 0.263026 0.545192 11.00000 0.01365 0.01342 = 0.01051 0.00189 0.00186 0.00079 C10 1 0.261198 0.139209 0.541237 11.00000 0.01471 0.01436 = 0.01178 -0.00144 0.00203 0.00056 C11 1 0.260424 0.103642 0.647099 11.00000 0.01625 0.01415 = 0.01142 0.00170 -0.00059 0.00027 AFIX 13 H11 2 0.322272 0.141257 0.677764 11.00000 -1.20000 AFIX 0 C12 1 0.127813 0.415224 0.621146 11.00000 0.01302 0.01594 = 0.01032 0.00296 0.00166 0.00214 C13 1 0.036222 0.482577 0.650141 11.00000 0.01380 0.01837 = 0.01392 0.00203 0.00320 0.00156 AFIX 13 H13 2 -0.033175 0.447733 0.661699 11.00000 -1.20000 AFIX 0 C14 1 0.075443 0.576672 0.713565 11.00000 0.01608 0.01732 = 0.01804 -0.00008 0.00373 0.00275 AFIX 23 H14A 2 0.067789 0.559555 0.781851 11.00000 -1.20000 H14B 2 0.036630 0.644258 0.698299 11.00000 -1.20000 AFIX 0 C15 1 0.194908 0.587109 0.688198 11.00000 0.01654 0.01469 = 0.01463 0.00218 0.00316 0.00133 AFIX 13 H15 2 0.198080 0.629657 0.627769 11.00000 -1.20000 AFIX 0 C16 1 0.230017 0.465929 0.664838 11.00000 0.01263 0.01432 = 0.01192 0.00142 0.00201 0.00064 C17 1 0.315963 0.459560 0.588062 11.00000 0.01154 0.01644 = 0.01384 0.00307 0.00274 0.00006 AFIX 23 H17A 2 0.300175 0.513536 0.537519 11.00000 -1.20000 H17B 2 0.385212 0.477824 0.617818 11.00000 -1.20000 AFIX 0 C18 1 0.321326 0.345734 0.543126 11.00000 0.01233 0.01679 = 0.01347 0.00321 0.00320 0.00082 AFIX 13 H18 2 0.393621 0.314705 0.538894 11.00000 -1.20000 AFIX 0 C19 1 0.263411 0.645881 0.763240 11.00000 0.01889 0.01287 = 0.01659 0.00344 0.00247 0.00180 C20 1 0.236891 0.677671 0.853809 11.00000 0.02108 0.01908 = 0.01737 0.00097 0.00265 -0.00058 AFIX 43 H20 2 0.170304 0.665552 0.880527 11.00000 -1.20000 AFIX 0 C21 1 0.403217 0.731389 0.836799 11.00000 0.02242 0.01842 = 0.02440 0.00040 0.00117 -0.00164 AFIX 43 H21 2 0.470499 0.762246 0.849459 11.00000 -1.20000 AFIX 0 C22 1 0.372551 0.681588 0.752753 11.00000 0.02064 0.01590 = 0.02010 -0.00031 0.00301 -0.00095 AFIX 43 H22 2 0.414055 0.672127 0.698369 11.00000 -1.20000 AFIX 0 C23 1 0.193034 -0.100117 0.629483 11.00000 0.02567 0.01566 = 0.02673 0.00146 0.00130 -0.00209 AFIX 137 H23A 2 0.206321 -0.113130 0.562109 11.00000 -1.50000 H23B 2 0.122426 -0.069795 0.635615 11.00000 -1.50000 H23C 2 0.198207 -0.168588 0.664556 11.00000 -1.50000 AFIX 0 C24 1 0.184631 0.078459 0.468695 11.00000 0.01955 0.01881 = 0.01548 -0.00230 -0.00106 -0.00061 AFIX 137 H24A 2 0.172018 0.123829 0.412280 11.00000 -1.50000 H24B 2 0.117776 0.063956 0.499042 11.00000 -1.50000 H24C 2 0.216565 0.009876 0.449725 11.00000 -1.50000 AFIX 0 C25 1 0.028106 0.273687 0.521408 11.00000 0.01383 0.02011 = 0.01573 -0.00006 -0.00057 0.00012 AFIX 137 H25A 2 0.044575 0.304156 0.459215 11.00000 -1.50000 H25B 2 -0.034432 0.309465 0.545528 11.00000 -1.50000 H25C 2 0.014639 0.195887 0.514783 11.00000 -1.50000 AFIX 0 C26 1 0.264915 0.404800 0.758413 11.00000 0.01679 0.01507 = 0.01327 0.00134 0.00012 -0.00073 AFIX 137 H26A 2 0.286767 0.331023 0.742664 11.00000 -1.50000 H26B 2 0.205918 0.401858 0.801544 11.00000 -1.50000 H26C 2 0.323861 0.443330 0.789493 11.00000 -1.50000 AFIX 0 O1B 3 0.537947 0.831492 0.056477 11.00000 0.01793 0.02654 = 0.03148 0.00107 0.01002 -0.00166 O2B 3 0.102890 0.937816 0.172270 11.00000 0.01873 0.02110 = 0.02302 0.00681 0.00663 0.00703 O3B 3 0.464951 0.665201 0.207855 11.00000 0.01367 0.01954 = 0.02004 0.00066 -0.00030 0.00397 O4B 3 0.293660 0.514144 0.333933 11.00000 0.01851 0.01774 = 0.01447 0.00369 -0.00092 0.00061 O5B 3 -0.005549 0.276527 0.021621 11.00000 0.03074 0.03392 = 0.02646 -0.00286 -0.00493 -0.01143 C1B 1 0.455390 0.879339 0.075582 11.00000 0.01639 0.01622 = 0.01823 -0.00124 0.00433 -0.00414 C2B 1 0.419096 0.975719 0.013889 11.00000 0.02305 0.02093 = 0.01962 0.00247 0.00629 -0.00438 AFIX 43 H2B 2 0.461209 0.993106 -0.038588 11.00000 -1.20000 AFIX 0 C3B 1 0.332157 1.039518 0.026508 11.00000 0.02926 0.01487 = 0.01690 0.00240 0.00389 -0.00280 AFIX 43 H3B 2 0.316987 1.097712 -0.015861 11.00000 -1.20000 AFIX 0 C4B 1 0.259647 1.016211 0.109498 11.00000 0.02256 0.01505 = 0.01518 -0.00026 0.00301 0.00161 C5B 1 0.136806 1.009792 0.093171 11.00000 0.02352 0.01829 = 0.02031 0.00585 0.00333 0.00525 AFIX 23 H5C 2 0.104291 1.082378 0.097616 11.00000 -1.20000 H5D 2 0.118139 0.977929 0.030238 11.00000 -1.20000 AFIX 0 C6B 1 0.186806 0.867861 0.196996 11.00000 0.01388 0.01587 = 0.01568 -0.00304 0.00211 0.00278 C7B 1 0.188917 0.787687 0.262388 11.00000 0.01595 0.01529 = 0.01466 -0.00168 0.00526 0.00162 AFIX 43 H7B 2 0.130485 0.777578 0.301840 11.00000 -1.20000 AFIX 0 C8B 1 0.286113 0.711557 0.273871 11.00000 0.01471 0.01500 = 0.01128 0.00007 0.00233 0.00128 C9B 1 0.371006 0.732451 0.193796 11.00000 0.01029 0.01530 = 0.01407 -0.00019 0.00076 0.00134 C10B 1 0.387508 0.854126 0.165504 11.00000 0.01462 0.01529 = 0.01489 -0.00065 0.00271 -0.00200 C11B 1 0.276476 0.893948 0.133310 11.00000 0.01719 0.01272 = 0.01126 -0.00013 0.00238 -0.00026 AFIX 13 H11B 2 0.259989 0.854704 0.072388 11.00000 -1.20000 AFIX 0 C12B 1 0.246442 0.592141 0.264707 11.00000 0.01372 0.01596 = 0.01123 0.00220 0.00043 0.00268 C13B 1 0.178888 0.534180 0.333882 11.00000 0.01918 0.01764 = 0.01210 0.00287 0.00214 0.00036 AFIX 13 H13B 2 0.147031 0.574508 0.387596 11.00000 -1.20000 AFIX 0 C14B 1 0.115928 0.444745 0.280648 11.00000 0.02101 0.01995 = 0.01390 0.00371 0.00329 -0.00341 AFIX 23 H14C 2 0.044291 0.469985 0.262392 11.00000 -1.20000 H14D 2 0.110654 0.378695 0.320162 11.00000 -1.20000 AFIX 0 C15B 1 0.182857 0.423106 0.190094 11.00000 0.01813 0.01407 = 0.01391 0.00188 0.00125 -0.00143 AFIX 13 H15B 2 0.243299 0.375908 0.210517 11.00000 -1.20000 AFIX 0 C16B 1 0.229784 0.539036 0.164507 11.00000 0.01521 0.01334 = 0.01133 0.00113 0.00245 0.00022 C17B 1 0.338792 0.534045 0.117147 11.00000 0.01825 0.01473 = 0.01727 -0.00068 0.00649 0.00086 AFIX 23 H17C 2 0.382876 0.478287 0.149512 11.00000 -1.20000 H17D 2 0.328889 0.512632 0.049558 11.00000 -1.20000 AFIX 0 C18B 1 0.395901 0.644614 0.122837 11.00000 0.01353 0.01479 = 0.01532 0.00043 0.00371 0.00163 AFIX 13 H18B 2 0.423868 0.671086 0.061268 11.00000 -1.20000 AFIX 0 C19B 1 0.123331 0.364559 0.109081 11.00000 0.02364 0.01340 = 0.01614 0.00305 0.00110 -0.00111 C20B 1 0.019693 0.332960 0.105547 11.00000 0.02672 0.02551 = 0.02183 -0.00161 0.00000 -0.00609 AFIX 43 H20B 2 -0.028675 0.347620 0.154017 11.00000 -1.20000 AFIX 0 C21B 1 0.087349 0.272497 -0.029055 11.00000 0.04027 0.02650 = 0.01650 -0.00188 0.00092 -0.00959 AFIX 43 H21B 2 0.093873 0.238839 -0.089331 11.00000 -1.20000 AFIX 0 C22B 1 0.167739 0.323787 0.020178 11.00000 0.03065 0.01979 = 0.01668 0.00065 0.00285 -0.00418 AFIX 43 H22B 2 0.238141 0.331512 0.000811 11.00000 -1.20000 AFIX 0 C23B 1 0.281986 1.100682 0.191174 11.00000 0.03788 0.01486 = 0.02182 -0.00366 0.00110 0.00283 AFIX 137 H23D 2 0.358042 1.109254 0.201233 11.00000 -1.50000 H23E 2 0.251093 1.074955 0.250074 11.00000 -1.50000 H23F 2 0.250762 1.170547 0.173178 11.00000 -1.50000 AFIX 0 C24B 1 0.444305 0.917177 0.249953 11.00000 0.02040 0.01964 = 0.01959 -0.00262 -0.00174 -0.00511 AFIX 137 H24D 2 0.475454 0.983835 0.225597 11.00000 -1.50000 H24E 2 0.499688 0.871524 0.278653 11.00000 -1.50000 H4F 2 0.393081 0.935369 0.298107 11.00000 -1.50000 AFIX 0 C25B 1 0.337291 0.727210 0.377118 11.00000 0.02410 0.01960 = 0.01279 -0.00041 -0.00091 -0.00104 AFIX 137 H25D 2 0.403559 0.686948 0.382147 11.00000 -1.50000 H25E 2 0.289042 0.700066 0.424634 11.00000 -1.50000 H25F 2 0.350935 0.804302 0.388451 11.00000 -1.50000 AFIX 0 C26B 1 0.148670 0.604588 0.101426 11.00000 0.01854 0.01622 = 0.01288 0.00167 -0.00026 0.00047 AFIX 137 H26D 2 0.178448 0.675409 0.086058 11.00000 -1.50000 H26E 2 0.083898 0.614713 0.136307 11.00000 -1.50000 H26F 2 0.132897 0.564670 0.042432 11.00000 -1.50000 AFIX 0 O1W 3 0.409481 0.315437 0.297448 11.00000 0.02487 0.02647 = 0.02690 0.00105 0.00393 0.00237 H1W 2 0.367332 0.373795 0.312342 11.00000 0.07005 H2W 2 0.401631 0.265296 0.346730 11.00000 0.05949 HKLF 4 REM I P 21 R 0.03 REM wR2 = 0.0797, GooF = S = 1.021, Restrained GooF = 1.022 for all data REM R1 = 0.0313 for 8067 Fo > 4sig(Fo) and 0.0331 for all 8304 data REM 585 parameters refined using 3 restraints END WGHT 0.0454 0.3926 REM Instructions for potential hydrogen bonds HTAB C13 O2B_$1 HTAB C18 O1 HTAB C21 O1W_$2 HTAB C13B O4 HTAB C14B O3 HTAB C18B O5_$3 HTAB C18B O1B HTAB O1W O3 HTAB O1W O4B HTAB O1W O1 HTAB O1W O3 REM Highest difference peak 0.239, deepest hole -0.237, 1-sigma level 0.039 Q1 1 0.4007 -0.0881 0.5482 11.00000 0.05 0.24 Q2 1 0.2307 0.5665 0.2128 11.00000 0.05 0.22 Q3 1 0.1848 0.4394 0.6436 11.00000 0.05 0.22 Q4 1 0.3325 0.8826 0.1562 11.00000 0.05 0.22 Q5 1 0.2015 0.4797 0.1739 11.00000 0.05 0.20 Q6 1 0.2550 0.1164 0.5897 11.00000 0.05 0.20 Q7 1 0.3157 0.1349 0.5289 11.00000 0.05 0.19 Q8 1 0.2474 0.2008 0.5327 11.00000 0.05 0.19 Q9 1 0.2681 0.6556 0.2671 11.00000 0.05 0.19 Q10 1 0.1476 0.2654 0.0029 11.00000 0.05 0.18 Q11 1 0.2202 0.5265 0.6845 11.00000 0.05 0.18 Q12 1 0.2748 1.0607 0.1477 11.00000 0.05 0.17 Q13 1 0.3069 0.7296 0.3192 11.00000 0.05 0.17 Q14 1 0.2073 0.1204 0.6623 11.00000 0.05 0.17 Q15 1 0.4088 0.8609 0.1245 11.00000 0.05 0.17 Q16 1 0.3632 0.6949 0.1472 11.00000 0.05 0.17 Q17 1 0.4035 0.0526 0.5422 11.00000 0.05 0.16 Q18 1 0.0566 0.5288 0.6842 11.00000 0.05 0.16 Q19 1 0.0826 0.2867 0.5564 11.00000 0.05 0.16 Q20 1 0.2374 0.7477 0.2665 11.00000 0.05 0.16 Q21 1 0.2446 0.4378 0.7042 11.00000 0.05 0.16 Q22 1 -0.0558 0.4662 0.6430 11.00000 0.05 0.16 Q23 1 0.1180 0.2633 0.6402 11.00000 0.05 0.16 Q24 1 0.2312 0.6137 0.7259 11.00000 0.05 0.16 Q25 1 0.1523 0.3985 0.1549 11.00000 0.05 0.16 Q26 1 0.1775 0.2801 0.5739 11.00000 0.05 0.16 Q27 1 0.2740 0.9594 0.1254 11.00000 0.05 0.15 Q28 1 0.1605 0.3476 0.0672 11.00000 0.05 0.15 Q29 1 0.2313 0.6721 0.8035 11.00000 0.05 0.15 Q30 1 0.2368 -0.0602 0.6483 11.00000 0.05 0.15 ; _shelx_res_checksum 92840 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy O O1 0.41746(12) 0.14419(15) 0.43841(11) 0.0241(3) Uani d 1 O O2 0.16598(12) 0.06854(13) 0.78568(10) 0.0198(3) Uani d 1 O O3 0.25032(11) 0.32523(13) 0.45900(9) 0.0153(3) Uani d 1 O O4 0.07555(11) 0.49060(13) 0.55185(9) 0.0156(3) Uani d 1 O O5 0.32107(13) 0.73009(14) 0.90101(10) 0.0230(3) Uani d 1 C C1 0.37466(15) 0.10520(18) 0.50908(14) 0.0165(4) Uani d 1 C C2 0.42802(16) 0.01223(19) 0.56348(16) 0.0212(4) Uani d 1 H H2 0.496492 -0.007294 0.544749 0.025 Uiso calc 1 C C3 0.38682(16) -0.04584(19) 0.63669(15) 0.0208(4) Uani d 1 H H3 0.425990 -0.103071 0.665632 0.025 Uiso calc 1 C C4 0.27696(16) -0.01778(18) 0.67159(14) 0.0177(4) Uani d 1 C C5 0.25842(17) -0.0069(2) 0.78109(15) 0.0217(4) Uani d 1 H H5A 0.242126 -0.078047 0.809516 0.026 Uiso calc 1 H H5B 0.320926 0.024129 0.814744 0.026 Uiso calc 1 C C6 0.16864(15) 0.13711(18) 0.70507(13) 0.0150(4) Uani d 1 C C7 0.10617(14) 0.22341(18) 0.68487(13) 0.0148(4) Uani d 1 H H7 0.051307 0.241959 0.726144 0.018 Uiso calc 1 C C8 0.12442(14) 0.29238(17) 0.59372(13) 0.0131(4) Uani d 1 C C9 0.23314(14) 0.26303(16) 0.54519(13) 0.0125(3) Uani d 1 C C10 0.26120(14) 0.13921(17) 0.54124(13) 0.0136(4) Uani d 1 C C11 0.26042(15) 0.10364(17) 0.64710(12) 0.0140(4) Uani d 1 H H11 0.322272 0.141257 0.677764 0.017 Uiso calc 1 C C12 0.12781(14) 0.41522(17) 0.62115(12) 0.0131(4) Uani d 1 C C13 0.03622(15) 0.48258(18) 0.65014(13) 0.0153(4) Uani d 1 H H13 -0.033175 0.447733 0.661699 0.018 Uiso calc 1 C C14 0.07544(15) 0.57667(18) 0.71357(14) 0.0171(4) Uani d 1 H H14A 0.067789 0.559555 0.781851 0.020 Uiso calc 1 H H14B 0.036630 0.644258 0.698299 0.020 Uiso calc 1 C C15 0.19491(15) 0.58711(17) 0.68820(13) 0.0152(4) Uani d 1 H H15 0.198080 0.629657 0.627769 0.018 Uiso calc 1 C C16 0.23002(14) 0.46593(17) 0.66484(13) 0.0129(3) Uani d 1 C C17 0.31596(14) 0.45956(17) 0.58806(13) 0.0139(4) Uani d 1 H H17A 0.300175 0.513536 0.537519 0.017 Uiso calc 1 H H17B 0.385212 0.477824 0.617818 0.017 Uiso calc 1 C C18 0.32133(14) 0.34573(17) 0.54313(13) 0.0141(4) Uani d 1 H H18 0.393621 0.314705 0.538894 0.017 Uiso calc 1 C C19 0.26341(15) 0.64588(18) 0.76324(14) 0.0161(4) Uani d 1 C C20 0.23689(17) 0.67767(19) 0.85381(15) 0.0191(4) Uani d 1 H H20 0.170304 0.665552 0.880527 0.023 Uiso calc 1 C C21 0.40322(17) 0.73139(19) 0.83680(16) 0.0217(4) Uani d 1 H H21 0.470499 0.762246 0.849459 0.026 Uiso calc 1 C C22 0.37255(16) 0.68159(18) 0.75275(15) 0.0188(4) Uani d 1 H H22 0.414055 0.672127 0.698369 0.023 Uiso calc 1 C C23 0.19303(17) -0.10012(19) 0.62948(16) 0.0227(4) Uani d 1 H H23A 0.206321 -0.113130 0.562109 0.034 Uiso calc 1 H H23B 0.122426 -0.069795 0.635615 0.034 Uiso calc 1 H H23C 0.198207 -0.168588 0.664556 0.034 Uiso calc 1 C C24 0.18463(16) 0.07846(18) 0.46869(14) 0.0180(4) Uani d 1 H H24A 0.172018 0.123829 0.412280 0.027 Uiso calc 1 H H24B 0.117776 0.063956 0.499042 0.027 Uiso calc 1 H H24C 0.216565 0.009876 0.449725 0.027 Uiso calc 1 C C25 0.02811(15) 0.27369(18) 0.52141(13) 0.0166(4) Uani d 1 H H25A 0.044575 0.304156 0.459215 0.025 Uiso calc 1 H H25B -0.034432 0.309465 0.545528 0.025 Uiso calc 1 H H25C 0.014639 0.195887 0.514783 0.025 Uiso calc 1 C C26 0.26491(15) 0.40480(18) 0.75841(13) 0.0150(4) Uani d 1 H H26A 0.286767 0.331023 0.742664 0.023 Uiso calc 1 H H26B 0.205918 0.401858 0.801544 0.023 Uiso calc 1 H H26C 0.323861 0.443330 0.789493 0.023 Uiso calc 1 O O1B 0.53795(12) 0.83149(15) 0.05648(12) 0.0251(3) Uani d 1 O O2B 0.10289(11) 0.93782(14) 0.17227(11) 0.0208(3) Uani d 1 O O3B 0.46495(11) 0.66520(13) 0.20786(10) 0.0178(3) Uani d 1 O O4B 0.29366(11) 0.51414(13) 0.33393(10) 0.0169(3) Uani d 1 O O5B -0.00555(14) 0.27653(17) 0.02162(12) 0.0305(4) Uani d 1 C C1B 0.45539(15) 0.87934(18) 0.07558(14) 0.0169(4) Uani d 1 C C2B 0.41910(17) 0.9757(2) 0.01389(15) 0.0211(4) Uani d 1 H H2B 0.461209 0.993106 -0.038588 0.025 Uiso calc 1 C C3B 0.33216(17) 1.03952(18) 0.02651(15) 0.0203(4) Uani d 1 H H3B 0.316987 1.097712 -0.015861 0.024 Uiso calc 1 C C4B 0.25965(16) 1.01621(18) 0.10950(14) 0.0175(4) Uani d 1 C C5B 0.13681(17) 1.00979(19) 0.09317(15) 0.0207(4) Uani d 1 H H5C 0.104291 1.082378 0.097616 0.025 Uiso calc 1 H H5D 0.118139 0.977929 0.030238 0.025 Uiso calc 1 C C6B 0.18681(14) 0.86786(18) 0.19700(13) 0.0151(4) Uani d 1 C C7B 0.18892(15) 0.78769(17) 0.26239(13) 0.0152(4) Uani d 1 H H7B 0.130485 0.777578 0.301840 0.018 Uiso calc 1 C C8B 0.28611(14) 0.71156(17) 0.27387(13) 0.0136(4) Uani d 1 C C9B 0.37101(14) 0.73245(17) 0.19380(13) 0.0132(4) Uani d 1 C C10B 0.38751(14) 0.85413(17) 0.16550(13) 0.0149(4) Uani d 1 C C11B 0.27648(15) 0.89395(17) 0.13331(13) 0.0137(4) Uani d 1 H H11B 0.259989 0.854704 0.072388 0.016 Uiso calc 1 C C12B 0.24644(15) 0.59214(17) 0.26471(13) 0.0136(4) Uani d 1 C C13B 0.17889(15) 0.53418(18) 0.33388(13) 0.0163(4) Uani d 1 H H13B 0.147031 0.574508 0.387596 0.020 Uiso calc 1 C C14B 0.11593(16) 0.44474(19) 0.28065(14) 0.0182(4) Uani d 1 H H14C 0.044291 0.469985 0.262392 0.022 Uiso calc 1 H H14D 0.110654 0.378695 0.320162 0.022 Uiso calc 1 C C15B 0.18286(15) 0.42311(17) 0.19009(13) 0.0154(4) Uani d 1 H H15B 0.243299 0.375908 0.210517 0.018 Uiso calc 1 C C16B 0.22978(14) 0.53904(17) 0.16451(13) 0.0133(4) Uani d 1 C C17B 0.33879(15) 0.53405(18) 0.11715(14) 0.0166(4) Uani d 1 H H17C 0.382876 0.478287 0.149512 0.020 Uiso calc 1 H H17D 0.328889 0.512632 0.049558 0.020 Uiso calc 1 C C18B 0.39590(14) 0.64461(17) 0.12284(13) 0.0145(3) Uani d 1 H H18B 0.423868 0.671086 0.061268 0.017 Uiso calc 1 C C19B 0.12333(16) 0.36456(18) 0.10908(14) 0.0177(4) Uani d 1 C C20B 0.01969(18) 0.3330(2) 0.10555(16) 0.0247(4) Uani d 1 H H20B -0.028675 0.347620 0.154017 0.030 Uiso calc 1 C C21B 0.0873(2) 0.2725(2) -0.02906(16) 0.0278(5) Uani d 1 H H21B 0.093873 0.238839 -0.089331 0.033 Uiso calc 1 C C22B 0.16774(18) 0.3238(2) 0.02018(15) 0.0223(4) Uani d 1 H H22B 0.238141 0.331512 0.000811 0.027 Uiso calc 1 C C23B 0.2820(2) 1.1007(2) 0.19117(16) 0.0248(4) Uani d 1 H H23D 0.358042 1.109254 0.201233 0.037 Uiso calc 1 H H23E 0.251093 1.074955 0.250074 0.037 Uiso calc 1 H H23F 0.250762 1.170547 0.173178 0.037 Uiso calc 1 C C24B 0.44431(16) 0.91718(19) 0.24995(15) 0.0199(4) Uani d 1 H H24D 0.475454 0.983835 0.225597 0.030 Uiso calc 1 H H24E 0.499688 0.871524 0.278653 0.030 Uiso calc 1 H H4F 0.393081 0.935369 0.298107 0.030 Uiso calc 1 C C25B 0.33729(16) 0.72721(19) 0.37712(13) 0.0189(4) Uani d 1 H H25D 0.403559 0.686948 0.382147 0.028 Uiso calc 1 H H25E 0.289042 0.700066 0.424634 0.028 Uiso calc 1 H H25F 0.350935 0.804302 0.388451 0.028 Uiso calc 1 C C26B 0.14867(15) 0.60459(18) 0.10143(13) 0.0159(4) Uani d 1 H H26D 0.178448 0.675409 0.086058 0.024 Uiso calc 1 H H26E 0.083898 0.614713 0.136307 0.024 Uiso calc 1 H H26F 0.132897 0.564670 0.042432 0.024 Uiso calc 1 O O1W 0.40948(13) 0.31544(15) 0.29745(12) 0.0260(3) Uani d 1 H H1W 0.367(3) 0.374(3) 0.312(3) 0.070(14) Uiso d 1 H H2W 0.402(3) 0.265(3) 0.347(3) 0.059(12) Uiso d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0247(7) 0.0238(8) 0.0243(7) 0.0063(6) 0.0114(6) 0.0030(6) O2 0.0255(7) 0.0190(8) 0.0152(6) 0.0024(6) 0.0045(5) 0.0066(5) O3 0.0176(6) 0.0175(7) 0.0109(6) -0.0010(5) 0.0030(5) 0.0034(5) O4 0.0159(6) 0.0182(7) 0.0128(6) 0.0043(5) 0.0009(5) 0.0051(5) O5 0.0288(8) 0.0235(9) 0.0166(7) -0.0010(6) 0.0013(6) -0.0019(6) C1 0.0171(9) 0.0144(10) 0.0181(8) 0.0010(7) 0.0025(7) -0.0023(7) C2 0.0178(9) 0.0193(12) 0.0266(10) 0.0044(8) 0.0027(7) -0.0003(8) C3 0.0206(9) 0.0165(10) 0.0251(10) 0.0047(8) -0.0013(7) 0.0017(8) C4 0.0209(9) 0.0147(10) 0.0174(9) 0.0005(7) 0.0004(7) 0.0028(7) C5 0.0262(10) 0.0207(11) 0.0183(9) 0.0040(8) 0.0010(7) 0.0070(8) C6 0.0179(8) 0.0153(10) 0.0119(8) -0.0031(7) 0.0009(6) 0.0020(7) C7 0.0138(8) 0.0182(10) 0.0124(8) -0.0023(7) 0.0028(6) 0.0022(7) C8 0.0121(7) 0.0157(10) 0.0117(8) 0.0001(6) 0.0022(6) 0.0018(7) C9 0.0137(8) 0.0134(10) 0.0105(7) 0.0008(7) 0.0019(6) 0.0019(6) C10 0.0147(8) 0.0144(10) 0.0118(8) 0.0006(7) 0.0020(6) -0.0014(7) C11 0.0162(8) 0.0142(9) 0.0114(8) 0.0003(7) -0.0006(6) 0.0017(7) C12 0.0130(8) 0.0159(10) 0.0103(7) 0.0021(7) 0.0017(6) 0.0030(7) C13 0.0138(8) 0.0184(10) 0.0139(8) 0.0016(7) 0.0032(6) 0.0020(7) C14 0.0161(9) 0.0173(10) 0.0180(8) 0.0027(7) 0.0037(7) -0.0001(7) C15 0.0165(9) 0.0147(10) 0.0146(8) 0.0013(7) 0.0032(6) 0.0022(7) C16 0.0126(8) 0.0143(10) 0.0119(8) 0.0006(6) 0.0020(6) 0.0014(6) C17 0.0115(7) 0.0164(10) 0.0138(8) 0.0001(6) 0.0027(6) 0.0031(7) C18 0.0123(8) 0.0168(10) 0.0135(8) 0.0008(7) 0.0032(6) 0.0032(7) C19 0.0189(9) 0.0129(10) 0.0166(8) 0.0018(7) 0.0025(7) 0.0034(7) C20 0.0211(9) 0.0191(10) 0.0174(9) -0.0006(7) 0.0026(7) 0.0010(7) C21 0.0224(9) 0.0184(11) 0.0244(10) -0.0016(8) 0.0012(8) 0.0004(8) C22 0.0206(9) 0.0159(10) 0.0201(9) -0.0010(7) 0.0030(7) -0.0003(7) C23 0.0257(10) 0.0157(11) 0.0267(10) -0.0021(8) 0.0013(8) 0.0015(8) C24 0.0195(9) 0.0188(11) 0.0155(8) -0.0006(7) -0.0011(7) -0.0023(7) C25 0.0138(8) 0.0201(10) 0.0157(8) 0.0001(7) -0.0006(6) -0.0001(7) C26 0.0168(8) 0.0151(10) 0.0133(8) -0.0007(7) 0.0001(6) 0.0013(7) O1B 0.0179(7) 0.0265(9) 0.0315(8) -0.0017(6) 0.0100(6) 0.0011(7) O2B 0.0187(7) 0.0211(8) 0.0230(7) 0.0070(6) 0.0066(5) 0.0068(6) O3B 0.0137(6) 0.0195(8) 0.0200(6) 0.0040(5) -0.0003(5) 0.0007(5) O4B 0.0185(6) 0.0177(8) 0.0145(6) 0.0006(5) -0.0009(5) 0.0037(5) O5B 0.0307(8) 0.0339(10) 0.0265(8) -0.0114(7) -0.0049(6) -0.0029(7) C1B 0.0164(8) 0.0162(10) 0.0182(9) -0.0041(7) 0.0043(7) -0.0012(7) C2B 0.0231(9) 0.0209(11) 0.0196(9) -0.0044(8) 0.0063(7) 0.0025(8) C3B 0.0293(10) 0.0149(10) 0.0169(9) -0.0028(8) 0.0039(7) 0.0024(7) C4B 0.0226(9) 0.0150(10) 0.0152(8) 0.0016(7) 0.0030(7) -0.0003(7) C5B 0.0235(10) 0.0183(11) 0.0203(9) 0.0052(8) 0.0033(7) 0.0058(8) C6B 0.0139(8) 0.0159(10) 0.0157(8) 0.0028(7) 0.0021(6) -0.0030(7) C7B 0.0160(8) 0.0153(10) 0.0147(8) 0.0016(7) 0.0053(6) -0.0017(7) C8B 0.0147(8) 0.0150(10) 0.0113(8) 0.0013(7) 0.0023(6) 0.0001(7) C9B 0.0103(8) 0.0153(10) 0.0141(8) 0.0013(7) 0.0008(6) -0.0002(7) C10B 0.0146(8) 0.0153(10) 0.0149(8) -0.0020(7) 0.0027(6) -0.0007(7) C11B 0.0172(8) 0.0127(10) 0.0113(7) -0.0003(7) 0.0024(6) -0.0001(7) C12B 0.0137(8) 0.0160(10) 0.0112(7) 0.0027(7) 0.0004(6) 0.0022(7) C13B 0.0192(9) 0.0176(10) 0.0121(8) 0.0004(7) 0.0021(6) 0.0029(7) C14B 0.0210(9) 0.0200(10) 0.0139(8) -0.0034(7) 0.0033(7) 0.0037(7) C15B 0.0181(8) 0.0141(10) 0.0139(8) -0.0014(7) 0.0013(7) 0.0019(7) C16B 0.0152(8) 0.0133(10) 0.0113(8) 0.0002(7) 0.0025(6) 0.0011(7) C17B 0.0183(9) 0.0147(10) 0.0173(8) 0.0009(7) 0.0065(7) -0.0007(7) C18B 0.0135(8) 0.0148(10) 0.0153(8) 0.0016(7) 0.0037(6) 0.0004(7) C19B 0.0236(9) 0.0134(10) 0.0161(9) -0.0011(7) 0.0011(7) 0.0031(7) C20B 0.0267(10) 0.0255(12) 0.0218(10) -0.0061(9) 0.0000(8) -0.0016(9) C21B 0.0403(12) 0.0265(13) 0.0165(9) -0.0096(10) 0.0009(8) -0.0019(8) C22B 0.0306(10) 0.0198(11) 0.0167(9) -0.0042(8) 0.0028(7) 0.0006(8) C23B 0.0379(12) 0.0149(11) 0.0218(9) 0.0028(8) 0.0011(8) -0.0037(8) C24B 0.0204(9) 0.0196(11) 0.0196(9) -0.0051(7) -0.0017(7) -0.0026(8) C25B 0.0241(9) 0.0196(11) 0.0128(8) -0.0010(8) -0.0009(7) -0.0004(7) C26B 0.0185(8) 0.0162(10) 0.0129(8) 0.0005(7) -0.0003(6) 0.0017(7) O1W 0.0249(7) 0.0265(9) 0.0269(8) 0.0024(6) 0.0039(6) 0.0011(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C6 O2 C5 107.37(15) C9 O3 C18 62.10(11) C13 O4 C12 60.48(11) C20 O5 C21 105.99(16) O1 C1 C2 119.44(18) O1 C1 C10 123.41(19) C2 C1 C10 116.90(17) C3 C2 C1 126.46(18) C3 C2 H2 116.8 C1 C2 H2 116.8 C2 C3 C4 119.62(19) C2 C3 H3 120.2 C4 C3 H3 120.2 C3 C4 C11 105.43(17) C3 C4 C5 119.87(17) C11 C4 C5 96.37(16) C3 C4 C23 110.35(18) C11 C4 C23 117.01(16) C5 C4 C23 107.63(17) O2 C5 C4 103.68(15) O2 C5 H5A 111.0 C4 C5 H5A 111.0 O2 C5 H5B 111.0 C4 C5 H5B 111.0 H5A C5 H5B 109.0 C7 C6 O2 127.60(18) C7 C6 C11 124.34(17) O2 C6 C11 107.88(16) C6 C7 C8 120.00(17) C6 C7 H7 120.0 C8 C7 H7 120.0 C7 C8 C12 109.30(15) C7 C8 C25 108.35(15) C12 C8 C25 108.29(16) C7 C8 C9 112.18(15) C12 C8 C9 107.83(15) C25 C8 C9 110.82(15) O3 C9 C18 59.97(11) O3 C9 C10 116.35(15) C18 C9 C10 119.00(15) O3 C9 C8 112.82(15) C18 C9 C8 120.29(16) C10 C9 C8 115.80(15) C11 C10 C9 103.50(15) C11 C10 C24 117.57(16) C9 C10 C24 110.41(15) C11 C10 C1 103.35(15) C9 C10 C1 118.59(16) C24 C10 C1 103.91(15) C6 C11 C10 118.01(16) C6 C11 C4 104.37(16) C10 C11 C4 118.79(17) C6 C11 H11 104.7 C10 C11 H11 104.7 C4 C11 H11 104.7 O4 C12 C13 59.67(11) O4 C12 C16 111.01(16) C13 C12 C16 108.54(16) O4 C12 C8 115.88(15) C13 C12 C8 126.08(17) C16 C12 C8 120.29(16) O4 C13 C12 59.85(11) O4 C13 C14 112.04(16) C12 C13 C14 109.59(16) O4 C13 H13 120.2 C12 C13 H13 120.2 C14 C13 H13 120.2 C13 C14 C15 103.23(15) C13 C14 H14A 111.1 C15 C14 H14A 111.1 C13 C14 H14B 111.1 C15 C14 H14B 111.1 H14A C14 H14B 109.1 C19 C15 C14 114.58(16) C19 C15 C16 115.36(16) C14 C15 C16 104.32(16) C19 C15 H15 107.4 C14 C15 H15 107.4 C16 C15 H15 107.4 C12 C16 C17 107.62(15) C12 C16 C26 110.47(15) C17 C16 C26 111.61(15) C12 C16 C15 102.85(15) C17 C16 C15 113.27(16) C26 C16 C15 110.63(15) C18 C17 C16 111.66(16) C18 C17 H17A 109.3 C16 C17 H17A 109.3 C18 C17 H17B 109.3 C16 C17 H17B 109.3 H17A C17 H17B 107.9 O3 C18 C9 57.93(11) O3 C18 C17 116.53(15) C9 C18 C17 124.25(15) O3 C18 H18 115.2 C9 C18 H18 115.2 C17 C18 H18 115.2 C20 C19 C22 105.37(18) C20 C19 C15 128.20(18) C22 C19 C15 126.43(17) C19 C20 O5 111.22(18) C19 C20 H20 124.4 O5 C20 H20 124.4 C22 C21 O5 110.43(19) C22 C21 H21 124.8 O5 C21 H21 124.8 C21 C22 C19 106.99(18) C21 C22 H22 126.5 C19 C22 H22 126.5 C4 C23 H23A 109.5 C4 C23 H23B 109.5 H23A C23 H23B 109.5 C4 C23 H23C 109.5 H23A C23 H23C 109.5 H23B C23 H23C 109.5 C10 C24 H24A 109.5 C10 C24 H24B 109.5 H24A C24 H24B 109.5 C10 C24 H24C 109.5 H24A C24 H24C 109.5 H24B C24 H24C 109.5 C8 C25 H25A 109.5 C8 C25 H25B 109.5 H25A C25 H25B 109.5 C8 C25 H25C 109.5 H25A C25 H25C 109.5 H25B C25 H25C 109.5 C16 C26 H26A 109.5 C16 C26 H26B 109.5 H26A C26 H26B 109.5 C16 C26 H26C 109.5 H26A C26 H26C 109.5 H26B C26 H26C 109.5 C6B O2B C5B 108.27(15) C9B O3B C18B 61.78(12) C13B O4B C12B 60.74(12) C20B O5B C21B 105.70(18) O1B C1B C2B 119.27(18) O1B C1B C10B 124.39(19) C2B C1B C10B 116.16(17) C3B C2B C1B 126.96(19) C3B C2B H2B 116.5 C1B C2B H2B 116.5 C2B C3B C4B 119.69(19) C2B C3B H3B 120.2 C4B C3B H3B 120.2 C3B C4B C11B 105.21(16) C3B C4B C23B 109.30(18) C11B C4B C23B 117.75(17) C3B C4B C5B 121.03(17) C11B C4B C5B 96.42(16) C23B C4B C5B 107.26(17) O2B C5B C4B 103.25(15) O2B C5B H5C 111.1 C4B C5B H5C 111.1 O2B C5B H5D 111.1 C4B C5B H5D 111.1 H5C C5B H5D 109.1 C7B C6B O2B 128.06(17) C7B C6B C11B 124.13(18) O2B C6B C11B 107.75(17) C6B C7B C8B 120.80(16) C6B C7B H7B 119.6 C8B C7B H7B 119.6 C7B C8B C12B 107.89(15) C7B C8B C25B 108.93(16) C12B C8B C25B 108.27(16) C7B C8B C9B 112.33(15) C12B C8B C9B 108.47(15) C25B C8B C9B 110.83(15) O3B C9B C18B 59.73(12) O3B C9B C10B 117.51(15) C18B C9B C10B 119.14(15) O3B C9B C8B 112.27(15) C18B C9B C8B 120.38(17) C10B C9B C8B 115.44(15) C11B C10B C9B 104.45(15) C11B C10B C24B 117.13(17) C9B C10B C24B 110.12(16) C11B C10B C1B 102.69(15) C9B C10B C1B 118.08(16) C24B C10B C1B 104.75(15) C6B C11B C10B 117.34(16) C6B C11B C4B 103.46(16) C10B C11B C4B 119.18(16) C6B C11B H11B 105.2 C10B C11B H11B 105.2 C4B C11B H11B 105.2 O4B C12B C13B 59.59(12) O4B C12B C16B 111.08(16) C13B C12B C16B 108.61(16) O4B C12B C8B 115.81(15) C13B C12B C8B 125.98(17) C16B C12B C8B 120.35(15) O4B C13B C12B 59.67(11) O4B C13B C14B 112.21(17) C12B C13B C14B 109.08(15) O4B C13B H13B 120.3 C12B C13B H13B 120.3 C14B C13B H13B 120.3 C13B C14B C15B 103.12(15) C13B C14B H14C 111.1 C15B C14B H14C 111.1 C13B C14B H14D 111.1 C15B C14B H14D 111.1 H14C C14B H14D 109.1 C19B C15B C14B 114.41(16) C19B C15B C16B 115.89(16) C14B C15B C16B 104.18(16) C19B C15B H15B 107.3 C14B C15B H15B 107.3 C16B C15B H15B 107.3 C17B C16B C12B 107.65(15) C17B C16B C26B 111.05(15) C12B C16B C26B 111.24(16) C17B C16B C15B 113.88(16) C12B C16B C15B 102.42(14) C26B C16B C15B 110.26(15) C18B C17B C16B 111.47(16) C18B C17B H17C 109.3 C16B C17B H17C 109.3 C18B C17B H17D 109.3 C16B C17B H17D 109.3 H17C C17B H17D 108.0 O3B C18B C9B 58.50(11) O3B C18B C17B 117.30(16) C9B C18B C17B 123.98(16) O3B C18B H18B 115.0 C9B C18B H18B 115.0 C17B C18B H18B 115.0 C20B C19B C22B 105.34(19) C20B C19B C15B 127.87(19) C22B C19B C15B 126.69(18) C19B C20B O5B 111.6(2) C19B C20B H20B 124.2 O5B C20B H20B 124.2 C22B C21B O5B 110.8(2) C22B C21B H21B 124.6 O5B C21B H21B 124.6 C21B C22B C19B 106.6(2) C21B C22B H22B 126.7 C19B C22B H22B 126.7 C4B C23B H23D 109.5 C4B C23B H23E 109.5 H23D C23B H23E 109.5 C4B C23B H23F 109.5 H23D C23B H23F 109.5 H23E C23B H23F 109.5 C10B C24B H24D 109.5 C10B C24B H24E 109.5 H24D C24B H24E 109.5 C10B C24B H4F 109.5 H24D C24B H4F 109.5 H24E C24B H4F 109.5 C8B C25B H25D 109.5 C8B C25B H25E 109.5 H25D C25B H25E 109.5 C8B C25B H25F 109.5 H25D C25B H25F 109.5 H25E C25B H25F 109.5 C16B C26B H26D 109.5 C16B C26B H26E 109.5 H26D C26B H26E 109.5 C16B C26B H26F 109.5 H26D C26B H26F 109.5 H26E C26B H26F 109.5 H1W O1W H2W 106(4) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C1 1.219(3) O2 C6 1.387(2) O2 C5 1.473(3) O3 C9 1.427(2) O3 C18 1.457(2) O4 C13 1.456(2) O4 C12 1.459(2) O5 C20 1.373(3) O5 C21 1.373(3) C1 C2 1.496(3) C1 C10 1.551(2) C2 C3 1.343(3) C2 H2 0.9300 C3 C4 1.504(3) C3 H3 0.9300 C4 C11 1.520(3) C4 C5 1.537(3) C4 C23 1.545(3) C5 H5A 0.9700 C5 H5B 0.9700 C6 C7 1.327(3) C6 C11 1.472(2) C7 C8 1.530(2) C7 H7 0.9300 C8 C12 1.534(3) C8 C25 1.553(2) C8 C9 1.570(2) C9 C18 1.488(3) C9 C10 1.540(3) C10 C11 1.520(2) C10 C24 1.546(3) C11 H11 0.9800 C12 C13 1.468(3) C12 C16 1.522(3) C13 C14 1.507(3) C13 H13 0.9800 C14 C15 1.546(3) C14 H14A 0.9700 C14 H14B 0.9700 C15 C19 1.500(3) C15 C16 1.566(3) C15 H15 0.9800 C16 C17 1.530(2) C16 C26 1.537(2) C17 C18 1.512(3) C17 H17A 0.9700 C17 H17B 0.9700 C18 H18 0.9800 C19 C20 1.355(3) C19 C22 1.439(3) C20 H20 0.9300 C21 C22 1.349(3) C21 H21 0.9300 C22 H22 0.9300 C23 H23A 0.9600 C23 H23B 0.9600 C23 H23C 0.9600 C24 H24A 0.9600 C24 H24B 0.9600 C24 H24C 0.9600 C25 H25A 0.9600 C25 H25B 0.9600 C25 H25C 0.9600 C26 H26A 0.9600 C26 H26B 0.9600 C26 H26C 0.9600 O1B C1B 1.217(3) O2B C6B 1.380(2) O2B C5B 1.466(2) O3B C9B 1.435(2) O3B C18B 1.453(2) O4B C13B 1.452(2) O4B C12B 1.453(2) O5B C20B 1.370(3) O5B C21B 1.371(3) C1B C2B 1.504(3) C1B C10B 1.551(2) C2B C3B 1.346(3) C2B H2B 0.9300 C3B C4B 1.505(3) C3B H3B 0.9300 C4B C11B 1.528(3) C4B C23B 1.538(3) C4B C5B 1.544(3) C5B H5C 0.9700 C5B H5D 0.9700 C6B C7B 1.323(3) C6B C11B 1.476(2) C7B C8B 1.527(3) C7B H7B 0.9300 C8B C12B 1.531(3) C8B C25B 1.552(2) C8B C9B 1.572(2) C9B C18B 1.483(3) C9B C10B 1.538(3) C10B C11B 1.519(3) C10B C24B 1.544(3) C11B H11B 0.9800 C12B C13B 1.469(3) C12B C16B 1.530(2) C13B C14B 1.513(3) C13B H13B 0.9800 C14B C15B 1.543(3) C14B H14C 0.9700 C14B H14D 0.9700 C15B C19B 1.499(3) C15B C16B 1.564(3) C15B H15B 0.9800 C16B C17B 1.527(2) C16B C26B 1.534(2) C17B C18B 1.516(3) C17B H17C 0.9700 C17B H17D 0.9700 C18B H18B 0.9800 C19B C20B 1.347(3) C19B C22B 1.445(3) C20B H20B 0.9300 C21B C22B 1.345(3) C21B H21B 0.9300 C22B H22B 0.9300 C23B H23D 0.9600 C23B H23E 0.9600 C23B H23F 0.9600 C24B H24D 0.9600 C24B H24E 0.9600 C24B H4F 0.9600 C25B H25D 0.9600 C25B H25E 0.9600 C25B H25F 0.9600 C26B H26D 0.9600 C26B H26E 0.9600 C26B H26F 0.9600 O1W H1W 0.91(3) O1W H2W 0.92(2) loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O1W H1W O4B . 0.91(4) 1.95(4) 2.857(2) 171(4) yes O1W H2W O1 . 0.92(4) 1.93(4) 2.838(2) 166(3) yes C15B H15B O1W . 0.98 2.47 3.408(3) 160 yes C3 H3 O1W 2_646 0.93 2.32 3.155(3) 149 yes C13 H13 O2B 2_546 0.98 2.47 3.088(2) 121 yes C5 H5A Cg1 1_545 0.97 2.93 3.744(3) 142 yes C5B H5C Cg2 1_565 0.97 2.91 3.806(3) 154 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion O1 C1 C2 C3 -173.5(2) C10 C1 C2 C3 1.0(3) C1 C2 C3 C4 -0.8(3) C2 C3 C4 C11 -26.3(3) C2 C3 C4 C5 -133.3(2) C2 C3 C4 C23 100.9(2) C6 O2 C5 C4 -28.9(2) C3 C4 C5 O2 153.99(19) C11 C4 C5 O2 42.11(19) C23 C4 C5 O2 -78.9(2) C5 O2 C6 C7 -173.6(2) C5 O2 C6 C11 1.8(2) O2 C6 C7 C8 177.46(18) C11 C6 C7 C8 2.8(3) C6 C7 C8 C12 -130.80(19) C6 C7 C8 C25 111.4(2) C6 C7 C8 C9 -11.3(3) C18 O3 C9 C10 -109.79(18) C18 O3 C9 C8 112.88(17) C7 C8 C9 O3 178.88(15) C12 C8 C9 O3 -60.73(18) C25 C8 C9 O3 57.6(2) C7 C8 C9 C18 -113.64(19) C12 C8 C9 C18 6.7(2) C25 C8 C9 C18 125.11(18) C7 C8 C9 C10 41.3(2) C12 C8 C9 C10 161.69(14) C25 C8 C9 C10 -80.0(2) O3 C9 C10 C11 166.89(15) C18 C9 C10 C11 98.23(18) C8 C9 C10 C11 -57.04(19) O3 C9 C10 C24 -66.45(19) C18 C9 C10 C24 -135.10(16) C8 C9 C10 C24 69.62(19) O3 C9 C10 C1 53.2(2) C18 C9 C10 C1 -15.4(2) C8 C9 C10 C1 -170.71(15) O1 C1 C10 C11 -160.1(2) C2 C1 C10 C11 25.8(2) O1 C1 C10 C9 -46.3(3) C2 C1 C10 C9 139.50(18) O1 C1 C10 C24 76.7(2) C2 C1 C10 C24 -97.54(19) C7 C6 C11 C10 -23.6(3) O2 C6 C11 C10 160.80(17) C7 C6 C11 C4 -158.03(19) O2 C6 C11 C4 26.4(2) C9 C10 C11 C6 47.7(2) C24 C10 C11 C6 -74.3(2) C1 C10 C11 C6 171.94(17) C9 C10 C11 C4 175.50(16) C24 C10 C11 C4 53.5(2) C1 C10 C11 C4 -60.2(2) C3 C4 C11 C6 -164.54(15) C5 C4 C11 C6 -41.12(18) C23 C4 C11 C6 72.4(2) C3 C4 C11 C10 61.5(2) C5 C4 C11 C10 -175.07(16) C23 C4 C11 C10 -61.5(2) C13 O4 C12 C16 -99.79(17) C13 O4 C12 C8 118.32(18) C7 C8 C12 O4 -140.84(15) C25 C8 C12 O4 -23.0(2) C9 C8 C12 O4 96.97(17) C7 C8 C12 C13 -70.8(2) C25 C8 C12 C13 47.1(2) C9 C8 C12 C13 167.03(16) C7 C8 C12 C16 81.02(19) C25 C8 C12 C16 -161.14(15) C9 C8 C12 C16 -41.2(2) C12 O4 C13 C14 100.55(18) C16 C12 C13 O4 104.00(16) C8 C12 C13 O4 -101.50(19) O4 C12 C13 C14 -104.71(17) C16 C12 C13 C14 -0.7(2) C8 C12 C13 C14 153.79(17) O4 C13 C14 C15 -43.4(2) C12 C13 C14 C15 21.0(2) C13 C14 C15 C19 -159.66(16) C13 C14 C15 C16 -32.58(18) O4 C12 C16 C17 -75.67(19) C13 C12 C16 C17 -139.46(16) C8 C12 C16 C17 64.3(2) O4 C12 C16 C26 162.26(15) C13 C12 C16 C26 98.48(18) C8 C12 C16 C26 -57.8(2) O4 C12 C16 C15 44.17(18) C13 C12 C16 C15 -19.61(19) C8 C12 C16 C15 -175.85(14) C19 C15 C16 C12 158.70(15) C14 C15 C16 C12 32.11(17) C19 C15 C16 C17 -85.44(19) C14 C15 C16 C17 147.97(15) C19 C15 C16 C26 40.7(2) C14 C15 C16 C26 -85.86(17) C12 C16 C17 C18 -47.9(2) C26 C16 C17 C18 73.44(19) C15 C16 C17 C18 -160.92(15) C9 O3 C18 C17 -115.44(17) C10 C9 C18 O3 105.41(17) C8 C9 C18 O3 -100.44(17) O3 C9 C18 C17 102.18(19) C10 C9 C18 C17 -152.41(17) C8 C9 C18 C17 1.7(3) C16 C17 C18 O3 88.00(18) C16 C17 C18 C9 20.2(2) C14 C15 C19 C20 9.1(3) C16 C15 C19 C20 -112.1(2) C14 C15 C19 C22 -170.2(2) C16 C15 C19 C22 68.6(3) C22 C19 C20 O5 -0.3(2) C15 C19 C20 O5 -179.66(19) C21 O5 C20 C19 0.3(2) C20 O5 C21 C22 -0.2(3) O5 C21 C22 C19 0.1(3) C20 C19 C22 C21 0.1(2) C15 C19 C22 C21 179.5(2) O1B C1B C2B C3B -177.9(2) C10B C1B C2B C3B -2.6(3) C1B C2B C3B C4B -0.3(3) C2B C3B C4B C11B -24.5(3) C2B C3B C4B C23B 102.9(2) C2B C3B C4B C5B -131.8(2) C6B O2B C5B C4B -27.7(2) C3B C4B C5B O2B 154.08(19) C11B C4B C5B O2B 42.01(18) C23B C4B C5B O2B -79.7(2) C5B O2B C6B C7B -177.5(2) C5B O2B C6B C11B -0.2(2) O2B C6B C7B C8B 174.55(18) C11B C6B C7B C8B -2.4(3) C6B C7B C8B C12B -125.86(19) C6B C7B C8B C25B 116.8(2) C6B C7B C8B C9B -6.3(3) C18B O3B C9B C10B -109.37(18) C18B O3B C9B C8B 113.19(18) C7B C8B C9B O3B 176.75(15) C12B C8B C9B O3B -64.09(19) C25B C8B C9B O3B 54.6(2) C7B C8B C9B C18B -116.30(19) C12B C8B C9B C18B 2.9(2) C25B C8B C9B C18B 121.60(19) C7B C8B C9B C10B 38.4(2) C12B C8B C9B C10B 157.54(15) C25B C8B C9B C10B -83.7(2) O3B C9B C10B C11B 167.09(15) C18B C9B C10B C11B 98.22(17) C8B C9B C10B C11B -56.79(18) O3B C9B C10B C24B -66.33(19) C18B C9B C10B C24B -135.21(17) C8B C9B C10B C24B 69.79(19) O3B C9B C10B C1B 53.9(2) C18B C9B C10B C1B -15.0(2) C8B C9B C10B C1B -170.02(15) O1B C1B C10B C11B -155.6(2) C2B C1B C10B C11B 29.4(2) O1B C1B C10B C9B -41.4(3) C2B C1B C10B C9B 143.56(18) O1B C1B C10B C24B 81.5(2) C2B C1B C10B C24B -93.5(2) C7B C6B C11B C10B -20.7(3) O2B C6B C11B C10B 161.79(16) C7B C6B C11B C4B -154.20(19) O2B C6B C11B C4B 28.3(2) C9B C10B C11B C6B 47.7(2) C24B C10B C11B C6B -74.4(2) C1B C10B C11B C6B 171.47(17) C9B C10B C11B C4B 173.74(15) C24B C10B C11B C4B 51.7(2) C1B C10B C11B C4B -62.5(2) C3B C4B C11B C6B -166.74(15) C23B C4B C11B C6B 71.2(2) C5B C4B C11B C6B -42.12(17) C3B C4B C11B C10B 60.8(2) C23B C4B C11B C10B -61.2(2) C5B C4B C11B C10B -174.53(15) C13B O4B C12B C16B -99.80(17) C13B O4B C12B C8B 118.22(19) C7B C8B C12B O4B -137.40(15) C25B C8B C12B O4B -19.7(2) C9B C8B C12B O4B 100.68(17) C7B C8B C12B C13B -67.5(2) C25B C8B C12B C13B 50.2(2) C9B C8B C12B C13B 170.56(17) C7B C8B C12B C16B 84.35(19) C25B C8B C12B C16B -157.90(16) C9B C8B C12B C16B -37.6(2) C12B O4B C13B C14B 99.81(17) C16B C12B C13B O4B 104.03(16) C8B C12B C13B O4B -101.40(19) O4B C12B C13B C14B -105.13(18) C16B C12B C13B C14B -1.1(2) C8B C12B C13B C14B 153.47(17) O4B C13B C14B C15B -41.9(2) C12B C13B C14B C15B 22.3(2) C13B C14B C15B C19B -161.82(17) C13B C14B C15B C16B -34.29(19) O4B C12B C16B C17B -76.79(19) C13B C12B C16B C17B -140.52(17) C8B C12B C16B C17B 63.2(2) O4B C12B C16B C26B 161.32(15) C13B C12B C16B C26B 97.60(19) C8B C12B C16B C26B -58.7(2) O4B C12B C16B C15B 43.55(18) C13B C12B C16B C15B -20.18(19) C8B C12B C16B C15B -176.43(15) C19B C15B C16B C17B -84.0(2) C14B C15B C16B C17B 149.37(16) C19B C15B C16B C12B 160.06(16) C14B C15B C16B C12B 33.45(18) C19B C15B C16B C26B 41.6(2) C14B C15B C16B C26B -85.02(17) C12B C16B C17B C18B -49.3(2) C26B C16B C17B C18B 72.7(2) C15B C16B C17B C18B -162.08(15) C9B O3B C18B C17B -114.92(18) C10B C9B C18B O3B 106.67(17) C8B C9B C18B O3B -99.58(17) O3B C9B C18B C17B 103.6(2) C10B C9B C18B C17B -149.69(18) C8B C9B C18B C17B 4.1(3) C16B C17B C18B O3B 89.66(19) C16B C17B C18B C9B 20.8(3) C14B C15B C19B C20B 2.4(3) C16B C15B C19B C20B -118.9(2) C14B C15B C19B C22B -173.4(2) C16B C15B C19B C22B 65.3(3) C22B C19B C20B O5B -0.5(3) C15B C19B C20B O5B -177.0(2) C21B O5B C20B C19B 0.3(3) C20B O5B C21B C22B 0.0(3) O5B C21B C22B C19B -0.3(3) C20B C19B C22B C21B 0.5(3) C15B C19B C22B C21B 177.0(2) _cod_database_fobs_code 2243188