#------------------------------------------------------------------------------ #$Date: 2019-11-12 10:30:17 +0200 (Tue, 12 Nov 2019) $ #$Revision: 227656 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/31/2243188.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243188 _cell_angle_alpha 90.000 _cell_angle_beta 91.742 _cell_angle_gamma 90.000 _cell_length_a 12.4711 _cell_length_b 12.0986 _cell_length_c 13.7645 _exptl_crystal_F_000 916.00 _reflns_d_resolution_high 0.7928 _cod_data_source_file su5448Isup2.hkl _cod_data_source_block I _shelx_title ' tr_4-cu in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 154.99 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -14 0 95.63 99.11 7.16 o 1 -14 0 376.06 119.31 183.48 o 2 -14 0 133.73 146.71 5.88 o 3 -14 0 97.15 93.54 3.83 o 4 -14 0 430.12 406.04 7.90 o 5 -14 0 52.41 49.31 2.55 o 6 -14 0 0.69 0.32 1.26 o 1 -13 0 31.08 42.85 3.32 o 2 -13 0 155.28 155.30 7.57 o 3 -13 0 21.39 17.86 3.46 o 4 -13 0 249.81 259.90 7.49 o 5 -13 0 146.44 148.14 4.81 o 6 -13 0 98.63 98.02 4.38 o 7 -13 0 42.67 38.08 2.56 o 8 -13 0 23.04 18.72 1.98 o 0 -12 0 212.81 176.35 8.63 o 1 -12 0 127.85 142.67 5.79 o 2 -12 0 10.56 15.54 1.86 o 3 -12 0 83.90 104.50 5.04 o 4 -12 0 176.28 171.20 6.32 o 5 -12 0 21.56 21.50 2.81 o 6 -12 0 210.98 200.54 7.19 o 7 -12 0 23.48 25.79 2.39 o 8 -12 0 155.28 153.16 4.59 o 9 -12 0 199.45 198.29 6.48 o 1 -11 0 151.98 144.99 4.77 o 2 -11 0 151.75 146.41 5.46 o 3 -11 0 537.20 480.11 11.12 o 4 -11 0 452.64 449.16 10.81 o 5 -11 0 73.05 93.17 5.96 o 6 -11 0 60.34 71.81 4.25 o 7 -11 0 491.82 530.75 11.65 o 8 -11 0 93.78 96.60 5.19 o 9 -11 0 66.50 64.28 3.72 o 10 -11 0 209.08 195.17 5.28 o 0 -10 0 115.94 103.36 6.86 o 1 -10 0 586.06 563.13 13.03 o 2 -10 0 433.32 437.94 9.24 o 3 -10 0 148.38 159.88 10.42 o 4 -10 0 539.13 505.51 13.66 o 5 -10 0 214.37 203.97 7.20 o 6 -10 0 104.46 103.06 5.20 o 7 -10 0 344.55 365.06 9.33 o 8 -10 0 6.34 4.90 2.66 o 9 -10 0 242.89 259.33 6.75 o 10 -10 0 38.38 34.96 2.33 o 11 -10 0 203.19 48.01 92.58 o 1 -9 0 408.09 412.13 53.08 o 2 -9 0 280.22 243.33 40.98 o 3 -9 0 288.64 320.94 10.76 o 4 -9 0 895.14 938.64 21.10 o 5 -9 0 758.08 726.71 23.78 o 6 -9 0 112.61 122.37 6.42 o 7 -9 0 18.90 23.39 3.22 o 8 -9 0 282.93 291.19 8.04 o 9 -9 0 130.33 136.99 5.32 o 10 -9 0 290.89 297.85 7.22 o 11 -9 0 100.17 92.78 4.06 o 12 -9 0 84.94 94.37 5.65 o 0 -8 0 259.44 305.52 39.11 o 1 -8 0 113.57 145.38 36.03 o 2 -8 0 83.61 54.72 18.69 o 3 -8 0 918.18 871.64 76.81 o 4 -8 0 366.75 343.88 50.55 o 5 -8 0 165.23 165.77 11.71 o 6 -8 0 149.93 134.96 6.33 o 7 -8 0 240.14 237.27 7.49 o 8 -8 0 13.51 19.44 2.21 o 9 -8 0 205.89 201.92 6.61 o 10 -8 0 41.19 41.66 2.73 o 11 -8 0 63.82 60.36 3.14 o 12 -8 0 2.42 -0.03 0.82 o 13 -8 0 129.26 128.85 6.36 o 1 -7 0 699.48 723.57 55.13 o 2 -7 0 301.73 290.45 23.80 o 3 -7 0 141.75 154.30 29.76 o 4 -7 0 131.06 133.75 16.34 o 5 -7 0 0.79 -3.04 4.97 o 6 -7 0 23.04 27.44 9.60 o 7 -7 0 833.00 790.30 17.27 o 8 -7 0 176.87 159.30 4.48 o 9 -7 0 40.56 38.40 2.45 o 10 -7 0 233.80 236.41 5.91 o 11 -7 0 218.81 203.37 6.74 o 12 -7 0 40.59 36.62 2.87 o 13 -7 0 25.38 26.13 1.98 o 0 -6 0 856.18 797.45 52.88 o 1 -6 0 3048.91 3019.43 113.83 o 2 -6 0 1110.94 1061.41 40.85 o 3 -6 0 261.35 308.72 20.00 o 4 -6 0 756.65 819.97 35.78 o 5 -6 0 378.29 334.47 25.10 o 6 -6 0 1286.69 1198.59 51.23 o 7 -6 0 397.05 349.35 29.56 o 8 -6 0 329.90 348.17 10.13 o 9 -6 0 148.67 151.68 5.34 o 10 -6 0 162.03 152.02 5.07 o 11 -6 0 218.26 215.42 8.33 o 12 -6 0 49.95 52.99 3.34 o 13 -6 0 50.43 51.56 2.76 o 14 -6 0 32.89 33.35 3.42 o 1 -5 0 4910.45 4967.05 99.70 o 2 -5 0 3647.40 3697.83 55.75 o 3 -5 0 164.45 177.99 10.99 o 4 -5 0 182.37 226.92 18.31 o 5 -5 0 275.39 296.97 22.79 o 6 -5 0 166.08 163.09 18.48 o 7 -5 0 377.74 379.77 29.74 o 8 -5 0 39.92 35.36 4.65 o 9 -5 0 116.99 105.63 3.86 o 10 -5 0 223.78 203.84 5.88 o 11 -5 0 161.54 164.23 7.55 o 12 -5 0 22.24 24.69 3.16 o 13 -5 0 17.51 20.33 2.11 o 14 -5 0 275.81 276.84 10.09 o 0 -4 0 447.62 391.60 28.82 o 1 -4 0 2876.28 2854.50 40.09 o 2 -4 0 705.91 715.61 21.05 o 3 -4 0 5120.82 5445.08 75.63 o 4 -4 0 432.86 447.28 32.79 o 5 -4 0 1447.63 1515.51 48.81 o 6 -4 0 988.90 999.96 43.09 o 7 -4 0 140.81 160.85 18.73 o 8 -4 0 107.95 109.32 16.79 o 9 -4 0 483.72 457.88 8.93 o 10 -4 0 213.73 198.45 5.30 o 11 -4 0 467.36 451.05 10.84 o 12 -4 0 334.77 333.64 10.19 o 13 -4 0 22.57 24.26 2.91 o 14 -4 0 158.36 157.81 5.37 o 15 -4 0 232.93 235.20 7.20 o 1 -3 0 4043.56 3709.52 85.19 o 2 -3 0 4079.23 3982.30 38.15 o 3 -3 0 1736.89 1764.45 44.57 o 4 -3 0 1067.07 984.91 33.86 o 5 -3 0 2986.88 3062.88 65.37 o 6 -3 0 1237.63 1370.51 47.64 o 7 -3 0 979.23 990.73 43.60 o 8 -3 0 352.31 377.10 39.33 o 9 -3 0 1138.94 1221.03 16.69 o 10 -3 0 74.37 72.31 3.62 o 11 -3 0 26.56 17.16 2.19 o 12 -3 0 24.63 26.26 2.93 o 13 -3 0 74.40 65.51 4.41 o 14 -3 0 141.02 134.98 4.52 o 15 -3 0 26.99 25.26 1.88 o 0 -2 0 3078.32 3085.85 149.72 o 1 -2 0 1239.83 1248.04 14.85 o 2 -2 0 7883.19 7395.57 45.91 o 3 -2 0 1535.76 1443.07 66.72 o 4 -2 0 17.72 10.33 4.65 o 5 -2 0 1258.44 1196.27 38.45 o 6 -2 0 311.70 401.33 26.51 o 7 -2 0 75.90 95.78 18.81 o 8 -2 0 406.93 454.88 42.06 o 9 -2 0 892.16 836.10 61.44 o 10 -2 0 282.88 291.70 9.55 o 11 -2 0 5.05 6.42 1.71 o 12 -2 0 330.46 350.67 9.30 o 13 -2 0 129.81 143.25 5.64 o 14 -2 0 142.58 144.79 4.78 o 15 -2 0 19.38 20.45 3.06 o 1 -1 0 365.44 363.21 6.05 o 2 -1 0 9207.08 9161.41 98.36 o 3 -1 0 100.09 90.69 12.44 o 4 -1 0 3188.52 3139.58 58.24 o 5 -1 0 259.38 227.54 15.72 o 6 -1 0 753.04 882.11 57.61 o 7 -1 0 616.05 689.94 46.79 o 8 -1 0 826.26 829.23 55.63 o 9 -1 0 168.12 192.79 28.65 o 10 -1 0 719.37 694.10 11.38 o 11 -1 0 121.07 109.33 4.77 o 12 -1 0 758.76 809.50 12.50 o 13 -1 0 156.03 160.50 5.29 o 14 -1 0 47.26 46.44 3.94 o 15 -1 0 0.23 -1.35 1.35 o 1 0 0 0.09 4.24 1.18 o 2 0 0 22198.55 20594.65 636.09 o 3 0 0 77.54 85.19 5.72 o 4 0 0 57.23 41.18 4.76 o 5 0 0 373.45 381.06 15.00 o 6 0 0 1613.29 1815.56 47.26 o 7 0 0 1789.58 1904.96 53.56 o 8 0 0 132.80 162.20 24.50 o 9 0 0 63.28 93.57 20.04 o 10 0 0 0.06 -1.14 1.14 o 11 0 0 430.64 408.11 8.83 o 12 0 0 138.95 139.34 6.08 o 13 0 0 50.40 53.89 3.71 o 14 0 0 1087.58 1147.66 22.84 o 15 0 0 126.16 135.92 7.93 o 1 1 0 368.24 360.28 7.65 o 2 1 0 9222.05 8679.72 34.75 o 3 1 0 100.26 83.83 4.40 o 4 1 0 3160.01 3060.57 32.64 o 5 1 0 254.30 253.44 11.08 o 6 1 0 750.48 851.42 32.83 o 7 1 0 614.44 659.67 32.09 o 8 1 0 821.37 871.39 44.41 o 9 1 0 167.42 211.31 29.20 o 10 1 0 722.88 672.97 11.10 o 11 1 0 120.28 112.02 5.34 o 12 1 0 760.17 778.96 29.19 o 13 1 0 158.13 164.38 6.11 o 14 1 0 46.35 48.39 2.98 o 15 1 0 0.25 -1.14 1.14 o 0 2 0 3083.51 3025.05 109.30 o 1 2 0 1231.00 1211.14 16.96 o 2 2 0 7891.83 7337.67 53.73 o 3 2 0 1530.84 1449.17 30.55 o 4 2 0 18.40 12.38 3.77 o 5 2 0 1259.59 1208.80 30.59 o 6 2 0 315.41 394.76 22.89 o 7 2 0 76.82 106.37 12.84 o 8 2 0 403.22 432.38 27.97 o 9 2 0 898.93 879.05 42.90 o 10 2 0 281.15 279.54 6.15 o 11 2 0 5.45 5.52 2.09 o 12 2 0 328.96 314.08 13.75 o 13 2 0 129.66 154.01 10.00 o 14 2 0 143.83 157.11 6.25 o 15 2 0 20.75 20.23 2.27 o 1 3 0 4041.76 3559.07 42.37 o 2 3 0 4086.03 3826.45 68.88 o 3 3 0 1737.11 1656.27 30.84 o 4 3 0 1059.21 995.16 18.93 o 5 3 0 2983.69 3090.17 49.42 o 6 3 0 1242.16 1376.32 36.46 o 7 3 0 988.51 1087.77 40.67 o 8 3 0 346.77 388.55 26.25 o 9 3 0 1142.02 1157.60 19.85 o 10 3 0 74.28 70.29 3.62 o 11 3 0 25.79 20.27 2.47 o 12 3 0 23.96 21.99 3.19 o 13 3 0 74.26 69.99 5.91 o 14 3 0 142.11 137.32 4.66 o 15 3 0 28.75 29.01 3.67 o 0 4 0 449.72 445.37 42.83 o 1 4 0 2895.87 2864.23 33.48 o 2 4 0 711.81 692.53 15.63 o 3 4 0 5116.79 5162.32 75.07 o 4 4 0 435.20 506.88 14.83 o 5 4 0 1452.36 1514.53 35.00 o 6 4 0 993.48 1046.95 44.16 o 7 4 0 143.84 131.53 22.55 o 8 4 0 109.27 123.46 23.66 o 9 4 0 488.33 465.37 8.72 o 10 4 0 212.60 198.67 6.47 o 11 4 0 467.55 440.01 8.68 o 12 4 0 335.10 332.85 9.21 o 13 4 0 23.16 27.80 2.95 o 14 4 0 158.32 167.17 5.75 o 15 4 0 233.20 241.54 6.36 o 1 5 0 4900.49 4931.39 36.41 o 2 5 0 3635.93 3599.57 57.67 o 3 5 0 163.88 160.11 10.51 o 4 5 0 181.44 216.20 14.51 o 5 5 0 271.64 302.65 23.49 o 6 5 0 168.94 165.23 26.46 o 7 5 0 381.81 341.75 37.94 o 8 5 0 39.44 34.75 3.86 o 9 5 0 117.74 106.90 4.41 o 10 5 0 227.74 212.68 6.80 o 11 5 0 161.58 167.25 4.97 o 12 5 0 21.70 24.42 2.83 o 13 5 0 17.66 20.06 3.22 o 14 5 0 277.00 301.08 9.03 o 0 6 0 852.53 870.80 38.38 o 1 6 0 3055.73 3192.29 40.95 o 2 6 0 1111.23 1118.69 23.47 o 3 6 0 260.74 282.25 20.99 o 4 6 0 755.75 784.01 37.53 o 5 6 0 380.88 362.63 27.79 o 6 6 0 1279.66 1188.97 52.65 o 7 6 0 397.90 379.27 40.67 o 8 6 0 331.96 357.38 8.95 o 9 6 0 146.76 150.96 5.39 o 10 6 0 160.97 145.71 5.62 o 11 6 0 217.83 216.93 6.04 o 12 6 0 51.44 59.10 3.04 o 13 6 0 49.84 51.40 7.47 o 14 6 0 32.81 34.74 2.77 o 1 7 0 693.12 817.44 25.83 o 2 7 0 299.98 279.42 19.99 o 3 7 0 141.74 145.18 16.33 o 4 7 0 131.05 108.72 15.14 o 5 7 0 0.66 -3.29 6.30 o 6 7 0 22.04 42.00 10.90 o 7 7 0 828.69 791.72 24.44 o 8 7 0 176.15 163.19 7.49 o 9 7 0 41.09 37.55 2.88 o 10 7 0 239.01 245.83 7.13 o 11 7 0 216.85 216.48 5.83 o 12 7 0 40.91 34.69 2.63 o 13 7 0 25.82 24.73 2.31 o 0 8 0 260.72 242.60 35.32 o 1 8 0 113.92 111.38 18.77 o 2 8 0 85.02 81.40 12.02 o 3 8 0 908.76 899.99 36.07 o 4 8 0 365.89 380.53 29.52 o 5 8 0 165.38 121.56 33.86 o 6 8 0 150.34 120.48 10.60 o 7 8 0 237.58 226.47 11.97 o 8 8 0 13.78 11.72 3.11 o 9 8 0 205.69 203.40 7.26 o 10 8 0 40.79 44.02 3.40 o 11 8 0 62.88 63.12 3.19 o 12 8 0 2.35 1.33 1.15 o 13 8 0 128.50 131.70 5.20 o 1 9 0 413.16 473.13 55.17 o 2 9 0 277.37 269.33 57.88 o 3 9 0 291.62 285.32 45.72 o 4 9 0 891.60 811.02 53.38 o 5 9 0 761.00 664.36 39.67 o 7 9 0 19.23 16.04 3.07 o 8 9 0 283.85 297.97 8.46 o 9 9 0 131.04 135.58 5.85 o 10 9 0 290.61 310.64 7.36 o 11 9 0 99.32 97.34 3.96 o 12 9 0 84.40 94.67 4.80 o 0 10 0 113.87 163.55 34.43 o 1 10 0 586.25 627.35 40.71 o 2 10 0 431.84 421.09 34.00 o 6 10 0 101.14 79.96 10.40 o 7 10 0 342.30 359.28 12.07 o 8 10 0 6.25 4.37 1.84 o 9 10 0 243.83 270.27 6.59 o 10 10 0 38.67 43.27 2.17 o 11 10 0 206.05 212.68 5.45 o 5 11 0 70.45 86.59 9.91 o 6 11 0 60.88 63.53 4.90 o 7 11 0 487.14 523.48 12.98 o 8 11 0 93.07 88.66 4.21 o 9 11 0 66.70 68.46 3.37 o 10 11 0 209.56 221.93 5.51 o 5 12 0 22.57 22.22 4.83 o 6 12 0 211.23 210.30 10.11 o 7 12 0 23.65 25.85 2.18 o 8 12 0 154.01 165.61 5.12 o 9 12 0 200.03 206.70 4.98 o 6 13 0 100.14 102.26 9.80 o 7 13 0 41.83 40.08 3.65 o 8 13 0 24.59 21.94 3.31 o -6 -14 1 90.08 88.43 2.93 o -5 -14 1 23.45 26.80 1.99 o -4 -14 1 72.37 67.86 3.26 o -3 -14 1 23.10 18.36 1.88 o -2 -14 1 83.48 86.54 4.58 o -1 -14 1 376.25 389.92 9.34 o 0 -14 1 82.21 38.01 41.20 o 1 -14 1 132.87 151.51 9.73 o 2 -14 1 126.00 109.16 8.49 o 3 -14 1 14.08 20.00 2.28 o 4 -14 1 20.43 24.35 3.33 o 5 -14 1 141.54 136.51 4.55 o 6 -14 1 147.05 146.59 7.12 o -8 -13 1 82.88 87.97 3.03 o -7 -13 1 98.45 89.22 3.74 o -6 -13 1 370.11 365.24 8.29 o -5 -13 1 187.11 182.65 7.66 o -4 -13 1 152.56 160.77 6.35 o -3 -13 1 12.15 11.83 2.19 o -2 -13 1 208.38 216.13 7.45 o -1 -13 1 18.47 14.00 1.84 o 0 -13 1 96.73 107.62 5.14 o 1 -13 1 36.87 44.83 2.79 o 2 -13 1 180.30 186.89 5.72 o 3 -13 1 73.07 79.00 3.82 o 4 -13 1 83.13 89.21 3.94 o 5 -13 1 59.99 62.35 3.39 o 6 -13 1 1.83 1.47 1.22 o 7 -13 1 41.02 35.58 2.02 o 8 -13 1 21.07 24.11 2.09 o -9 -12 1 1.59 2.33 0.89 o -8 -12 1 195.39 177.14 7.79 o -7 -12 1 28.98 25.56 2.06 o -6 -12 1 201.77 201.79 5.39 o -5 -12 1 50.33 56.76 3.70 o -4 -12 1 21.15 29.30 3.63 o -3 -12 1 181.03 156.23 7.18 o -2 -12 1 526.39 509.18 10.98 o -1 -12 1 1709.28 1688.29 17.58 o 0 -12 1 82.07 85.34 4.47 o 1 -12 1 176.80 164.13 5.31 o 2 -12 1 734.39 698.47 10.86 o 3 -12 1 61.82 55.42 3.77 o 4 -12 1 10.30 11.96 2.16 o 5 -12 1 31.51 29.01 4.58 o 6 -12 1 135.28 126.53 5.07 o 7 -12 1 47.33 43.07 2.91 o 8 -12 1 29.44 25.51 2.04 o 9 -12 1 163.83 151.63 7.56 o -10 -11 1 1.60 0.14 1.04 o -9 -11 1 73.15 76.72 4.03 o -8 -11 1 43.72 47.22 3.58 o -7 -11 1 405.83 420.32 9.39 o -6 -11 1 81.59 85.87 4.63 o -5 -11 1 127.06 147.54 6.03 o -4 -11 1 636.93 646.50 17.81 o -3 -11 1 176.97 155.96 5.66 o -2 -11 1 173.70 162.23 5.79 o -1 -11 1 219.23 196.88 6.37 o 0 -11 1 207.03 205.22 5.68 o 1 -11 1 162.06 163.64 5.08 o 2 -11 1 68.82 67.84 3.66 o 3 -11 1 393.59 394.63 10.11 o 4 -11 1 34.90 30.94 3.16 o 5 -11 1 27.57 27.12 3.05 o 6 -11 1 22.64 17.98 3.98 o 7 -11 1 835.30 827.10 15.27 o 8 -11 1 189.09 194.19 11.09 o 9 -11 1 21.94 22.60 2.07 o 10 -11 1 64.97 58.64 3.06 o -11 -10 1 239.96 69.83 107.83 o -10 -10 1 104.14 96.49 3.65 o -9 -10 1 36.48 38.40 2.50 o -8 -10 1 106.13 103.70 4.95 o -7 -10 1 500.04 485.89 12.21 o -6 -10 1 720.71 707.07 14.96 o -5 -10 1 4.91 4.74 1.87 o -4 -10 1 243.11 230.53 7.93 o -3 -10 1 276.12 248.34 7.23 o -2 -10 1 332.72 319.41 8.00 o -1 -10 1 922.05 862.71 13.13 o 0 -10 1 154.71 147.33 4.81 o 1 -10 1 271.30 232.57 5.98 o 2 -10 1 4.69 2.57 1.38 o 3 -10 1 245.26 234.88 9.22 o 4 -10 1 105.89 121.31 6.79 o 5 -10 1 12.11 6.74 3.09 o 6 -10 1 87.17 91.65 4.89 o 7 -10 1 72.96 82.34 5.08 o 8 -10 1 303.90 302.26 9.46 o 9 -10 1 9.11 7.45 1.65 o 10 -10 1 7.50 11.24 1.65 o 11 -10 1 2.06 -1.40 2.00 o -12 -9 1 44.00 34.94 5.94 o -11 -9 1 99.85 93.69 5.24 o -10 -9 1 61.27 56.16 3.23 o -9 -9 1 315.85 331.02 9.25 o -8 -9 1 424.48 438.76 9.86 o -7 -9 1 970.68 921.76 27.27 o -6 -9 1 115.03 113.78 6.19 o -5 -9 1 108.31 85.64 6.73 o -4 -9 1 46.81 52.39 4.52 o -3 -9 1 399.40 417.09 11.33 o -2 -9 1 279.19 305.33 14.80 o -1 -9 1 143.46 117.21 26.98 o 0 -9 1 277.14 246.18 30.74 o 1 -9 1 69.87 66.47 21.46 o 2 -9 1 636.09 656.46 44.07 o 3 -9 1 187.50 175.44 9.44 o 4 -9 1 247.49 243.73 9.06 o 5 -9 1 2140.12 2080.07 31.46 o 6 -9 1 616.69 583.97 12.09 o 7 -9 1 417.25 397.76 8.72 o 8 -9 1 318.45 316.60 7.34 o 9 -9 1 303.19 287.91 6.83 o 10 -9 1 178.94 189.05 5.06 o 11 -9 1 59.08 61.74 3.98 o 12 -9 1 21.44 20.62 2.64 o -13 -8 1 317.97 354.24 10.58 o -12 -8 1 300.58 296.14 8.70 o -11 -8 1 64.24 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