#------------------------------------------------------------------------------ #$Date: 2025-02-21 04:59:40 +0200 (Fri, 21 Feb 2025) $ #$Revision: 297816 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/27/2312759.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312759 _cell_angle_alpha 90.000 _cell_angle_beta 91.835 _cell_angle_gamma 90.000 _cell_length_a 4.9567 _cell_length_b 15.9757 _cell_length_c 8.7693 _exptl_crystal_F_000 388.00 _reflns_d_resolution_high 0.7934 _cod_data_source_file dg3069Isup2.hkl _cod_data_source_block I _shelx_title ' exp_1876_auto in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 117.84 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2826.18 2704.59 74.76 o 4 0 0 156.55 157.25 6.41 o 6 0 0 747.33 793.84 34.13 o 1 1 0 835.63 758.62 11.83 o 2 1 0 16.26 8.33 0.86 o 3 1 0 128.89 104.26 2.32 o 4 1 0 18.62 15.09 0.88 o 5 1 0 17.93 19.53 1.18 o 6 1 0 107.22 103.60 6.68 o 0 2 0 3243.73 3115.83 61.48 o 1 2 0 625.78 570.72 6.54 o 2 2 0 769.50 745.19 11.17 o 3 2 0 446.99 435.13 6.45 o 4 2 0 91.58 88.10 1.91 o 5 2 0 11.40 10.69 0.78 o 6 2 0 128.54 140.58 4.50 o 1 3 0 1400.24 1305.86 14.88 o 2 3 0 29.40 46.44 1.52 o 3 3 0 17.59 17.15 0.92 o 4 3 0 69.79 70.56 1.69 o 5 3 0 200.55 207.43 3.90 o 6 3 0 178.11 156.09 4.67 o 0 4 0 17.82 20.76 1.42 o 1 4 0 1983.88 1810.11 19.46 o 2 4 0 1999.67 2083.69 27.09 o 3 4 0 389.75 383.10 5.03 o 4 4 0 636.84 616.71 7.62 o 5 4 0 81.09 79.71 2.20 o 6 4 0 109.77 101.74 4.92 o 1 5 0 10460.99 9953.56 121.96 o 2 5 0 95.68 91.85 2.38 o 3 5 0 50.93 46.99 1.23 o 4 5 0 52.44 55.91 1.57 o 5 5 0 168.32 166.28 4.37 o 0 6 0 9786.46 10172.48 163.28 o 1 6 0 338.83 399.61 5.64 o 2 6 0 1245.84 1246.98 13.57 o 3 6 0 3.49 3.39 0.58 o 4 6 0 225.61 213.30 3.82 o 5 6 0 3.38 2.39 0.61 o 1 7 0 5057.74 4941.22 48.87 o 2 7 0 186.79 195.04 2.81 o 3 7 0 98.04 93.60 1.84 o 4 7 0 9.13 8.69 0.75 o 5 7 0 234.74 243.91 13.29 o 0 8 0 30.95 36.19 1.20 o 1 8 0 216.58 223.28 3.01 o 2 8 0 12.20 12.65 0.63 o 3 8 0 811.12 779.80 9.07 o 4 8 0 142.96 153.28 3.74 o 5 8 0 13.14 12.64 1.11 o 1 9 0 172.78 173.36 2.41 o 2 9 0 5.57 7.08 0.48 o 3 9 0 62.87 55.03 1.64 o 4 9 0 41.83 41.27 1.95 o 5 9 0 242.40 264.17 6.98 o 0 10 0 451.42 446.62 5.67 o 1 10 0 400.46 369.73 3.91 o 2 10 0 94.38 100.14 2.19 o 3 10 0 230.88 228.82 3.56 o 4 10 0 70.46 72.76 2.95 o 5 10 0 22.02 21.73 1.45 o 1 11 0 2191.06 2159.93 16.83 o 2 11 0 155.93 158.60 2.43 o 3 11 0 22.01 15.71 0.88 o 4 11 0 302.90 315.77 8.83 o 5 11 0 393.07 362.18 11.87 o 0 12 0 521.99 494.21 6.21 o 1 12 0 492.62 480.72 4.61 o 2 12 0 81.00 88.78 1.86 o 3 12 0 8.07 10.58 0.77 o 4 12 0 0.54 0.51 0.59 o 1 13 0 714.48 721.50 6.50 o 2 13 0 0.70 1.37 0.34 o 3 13 0 154.57 161.50 3.50 o 4 13 0 17.17 17.08 1.02 o 0 14 0 495.47 514.52 7.37 o 1 14 0 164.61 150.88 2.21 o 2 14 0 10.42 7.61 0.57 o 3 14 0 160.40 180.87 3.86 o 4 14 0 44.31 48.36 1.83 o 1 15 0 177.97 184.44 3.20 o 2 15 0 405.39 403.85 5.66 o 3 15 0 6.95 7.73 0.57 o 4 15 0 98.21 102.01 3.94 o 0 16 0 523.49 580.78 8.55 o 1 16 0 0.06 0.20 0.32 o 2 16 0 63.71 62.56 1.50 o 3 16 0 129.03 135.55 4.34 o 1 17 0 113.33 111.11 2.14 o 2 17 0 267.61 278.82 4.11 o 0 18 0 130.73 130.93 4.05 o 1 18 0 18.97 15.58 0.76 o 2 18 0 129.58 133.84 2.55 o 1 19 0 34.13 34.15 1.55 o 0 20 0 17.47 13.57 1.78 o -5 0 1 394.62 379.86 9.76 o -3 0 1 327.61 306.23 8.78 o -1 0 1 29.09 35.05 1.52 o 1 0 1 5692.83 5489.34 116.16 o 3 0 1 695.91 724.96 11.84 o 5 0 1 94.32 92.14 5.94 o -6 1 1 51.37 57.64 4.52 o -5 1 1 0.16 0.69 0.44 o -4 1 1 0.46 0.60 0.28 o -3 1 1 758.64 741.10 12.44 o -2 1 1 129.33 128.07 4.47 o -1 1 1 9410.99 8748.63 102.36 o 0 1 1 83.63 82.57 1.93 o 1 1 1 4617.85 4364.65 64.02 o 2 1 1 10.17 9.92 0.69 o 3 1 1 2.95 3.35 0.40 o 4 1 1 4.92 4.64 0.51 o 5 1 1 2.72 3.62 0.58 o 6 1 1 101.00 116.84 7.21 o -6 2 1 33.42 30.99 2.40 o -5 2 1 489.91 504.43 11.63 o -4 2 1 4.56 2.94 0.48 o -3 2 1 179.99 201.99 4.73 o -2 2 1 164.39 146.09 3.63 o -1 2 1 5448.04 5204.73 86.27 o 0 2 1 191.66 184.17 4.04 o 1 2 1 7013.31 6930.69 89.37 o 2 2 1 32.58 29.23 1.63 o 3 2 1 200.95 223.43 3.12 o 4 2 1 412.61 416.67 6.56 o 5 2 1 951.55 1024.61 19.38 o 6 2 1 9.55 7.76 1.09 o -5 3 1 319.15 313.39 6.40 o -4 3 1 59.53 51.84 1.54 o -3 3 1 6.27 8.67 0.66 o -2 3 1 112.53 116.43 3.55 o -1 3 1 180.25 189.67 3.08 o 0 3 1 669.22 647.99 11.26 o 1 3 1 3093.50 3068.82 31.20 o 2 3 1 102.86 102.67 2.35 o 3 3 1 347.41 322.70 4.13 o 4 3 1 72.73 74.94 1.91 o 5 3 1 0.91 3.52 0.76 o 6 3 1 252.76 213.52 10.78 o -5 4 1 124.54 130.52 3.02 o -4 4 1 4.41 4.82 0.50 o -3 4 1 2.35 3.28 0.38 o -2 4 1 3380.59 3295.84 44.47 o -1 4 1 1231.31 1212.35 14.05 o 0 4 1 911.20 914.83 11.95 o 1 4 1 386.59 372.74 4.69 o 2 4 1 0.82 1.79 0.33 o 3 4 1 3.63 2.71 0.30 o 4 4 1 101.43 99.04 2.19 o 5 4 1 433.19 467.43 8.65 o 6 4 1 43.29 39.58 2.96 o -5 5 1 119.95 114.90 3.15 o -4 5 1 78.78 71.01 1.76 o -3 5 1 515.94 509.56 5.81 o -2 5 1 105.41 111.06 2.46 o -1 5 1 991.77 1056.74 17.39 o 0 5 1 5873.70 5519.95 80.32 o 1 5 1 312.85 276.80 3.81 o 2 5 1 1369.46 1449.45 15.96 o 3 5 1 799.56 802.20 7.85 o 4 5 1 7.14 4.54 0.50 o 5 5 1 96.67 96.41 2.80 o -5 6 1 215.56 210.56 6.54 o -4 6 1 545.54 554.00 8.10 o -3 6 1 826.83 804.20 8.56 o -2 6 1 4440.34 4232.86 42.49 o -1 6 1 552.02 533.42 11.61 o 0 6 1 847.07 826.85 16.44 o 1 6 1 3275.98 3366.74 42.19 o 2 6 1 1394.45 1327.20 14.64 o 3 6 1 81.24 76.76 1.56 o 4 6 1 46.13 45.92 1.46 o 5 6 1 5.99 6.50 0.80 o -5 7 1 28.75 30.91 1.79 o -4 7 1 208.69 193.59 4.33 o -3 7 1 139.01 120.35 2.27 o -2 7 1 214.81 207.18 3.30 o -1 7 1 1110.59 1091.36 13.04 o 0 7 1 96.97 113.45 3.07 o 1 7 1 110.10 124.18 2.76 o 2 7 1 1756.07 1764.20 14.65 o 3 7 1 4.81 4.91 0.44 o 4 7 1 142.36 130.40 2.95 o 5 7 1 6.95 5.74 0.80 o -5 8 1 117.56 115.48 4.98 o -4 8 1 32.20 29.27 1.45 o -3 8 1 11.34 11.89 0.78 o -2 8 1 13.70 10.70 0.68 o -1 8 1 618.47 654.82 6.07 o 0 8 1 101.55 96.77 2.22 o 1 8 1 1100.40 1097.39 10.13 o 2 8 1 4.30 3.50 0.32 o 3 8 1 80.59 80.58 1.75 o 4 8 1 105.64 108.43 4.66 o 5 8 1 0.99 0.46 0.60 o -5 9 1 15.48 21.51 2.26 o -4 9 1 215.97 220.06 4.81 o -3 9 1 1578.47 1590.17 17.68 o -2 9 1 1230.35 1220.82 11.53 o -1 9 1 488.70 475.10 4.82 o 0 9 1 1223.84 1131.90 9.09 o 1 9 1 76.70 71.25 1.30 o 2 9 1 257.82 255.56 4.21 o 3 9 1 296.43 304.71 4.22 o 4 9 1 779.12 808.66 16.80 o 5 9 1 25.68 26.78 1.34 o -5 10 1 17.86 21.61 1.66 o -4 10 1 28.38 29.67 1.66 o -3 10 1 48.26 45.14 1.49 o -2 10 1 1450.30 1400.92 13.87 o -1 10 1 114.59 111.99 1.64 o 0 10 1 17.42 16.65 0.55 o 1 10 1 191.24 194.57 2.32 o 2 10 1 397.54 367.16 3.97 o 3 10 1 0.05 0.03 0.34 o 4 10 1 214.65 237.27 6.24 o 5 10 1 11.48 10.34 1.12 o -5 11 1 0.09 0.43 0.51 o -4 11 1 304.44 306.94 7.41 o -3 11 1 264.67 280.06 4.99 o -2 11 1 70.75 61.82 1.55 o -1 11 1 1104.96 1084.36 9.13 o 0 11 1 2907.76 2849.32 20.16 o 1 11 1 643.56 660.89 6.14 o 2 11 1 244.92 247.89 3.15 o 3 11 1 50.21 42.92 1.25 o 4 11 1 1.25 1.35 0.54 o 5 11 1 5.42 6.84 1.46 o -5 12 1 1.44 1.85 0.73 o -4 12 1 297.06 333.39 6.59 o -3 12 1 130.76 128.58 2.87 o -2 12 1 314.18 315.96 4.12 o -1 12 1 37.60 29.51 0.84 o 0 12 1 12.47 11.63 0.48 o 1 12 1 2.80 4.03 0.38 o 2 12 1 366.63 354.76 4.33 o 3 12 1 0.27 1.71 0.37 o 4 12 1 120.72 130.88 3.89 o -4 13 1 57.69 59.72 1.99 o -3 13 1 140.02 156.03 3.05 o -2 13 1 116.59 103.14 1.97 o -1 13 1 505.56 494.33 5.14 o 0 13 1 632.38 629.50 5.55 o 1 13 1 103.34 92.36 1.62 o 2 13 1 80.19 91.29 1.89 o 3 13 1 140.25 157.03 2.96 o 4 13 1 19.09 17.95 1.08 o -4 14 1 0.12 0.24 0.35 o -3 14 1 24.44 24.87 1.07 o -2 14 1 34.60 34.44 1.14 o -1 14 1 226.45 221.40 2.92 o 0 14 1 174.88 173.32 2.37 o 1 14 1 64.93 59.40 1.28 o 2 14 1 17.61 15.42 0.77 o 3 14 1 26.65 25.28 1.01 o 4 14 1 122.53 119.08 4.54 o -4 15 1 275.68 292.04 7.75 o -3 15 1 273.82 295.92 6.91 o -2 15 1 242.10 262.21 3.86 o -1 15 1 486.25 498.68 5.65 o 0 15 1 520.75 506.97 5.01 o 1 15 1 149.77 152.45 2.61 o 2 15 1 78.19 81.58 1.69 o 3 15 1 169.50 165.12 3.42 o 4 15 1 167.39 181.72 19.26 o -3 16 1 6.19 3.31 0.44 o -2 16 1 2.60 2.76 0.44 o -1 16 1 247.24 255.06 3.53 o 0 16 1 154.25 160.52 2.45 o 1 16 1 180.77 193.37 2.84 o 2 16 1 97.54 90.82 1.99 o 3 16 1 7.02 4.57 0.50 o -3 17 1 352.16 397.97 12.67 o -2 17 1 5.81 4.80 0.53 o -1 17 1 273.84 294.42 3.76 o 0 17 1 50.87 50.24 1.30 o 1 17 1 23.92 25.81 0.94 o 2 17 1 29.55 29.60 1.02 o 3 17 1 188.23 175.86 8.73 o -2 18 1 45.05 45.47 1.52 o -1 18 1 46.51 49.97 1.32 o 0 18 1 93.53 87.86 2.02 o 1 18 1 390.38 441.25 6.71 o 2 18 1 30.86 26.00 1.10 o -1 19 1 83.94 79.72 2.71 o 0 19 1 10.13 13.70 0.78 o 1 19 1 5.34 5.23 0.68 o 0 20 1 22.67 17.66 1.97 o -4 0 2 1019.12 993.19 16.20 o -2 0 2 322.03 350.23 10.55 o 0 0 2 13887.31 15725.01 306.21 o 2 0 2 1500.35 1551.08 50.49 o 4 0 2 61.05 53.38 2.57 o 6 0 2 246.88 259.38 12.79 o -5 1 2 94.11 95.79 2.78 o -4 1 2 154.12 158.00 3.45 o -3 1 2 417.19 383.55 5.80 o -2 1 2 2149.44 2046.01 29.72 o -1 1 2 13.18 8.07 0.52 o 0 1 2 5982.88 6227.97 99.87 o 1 1 2 209.69 225.31 3.78 o 2 1 2 79.27 65.77 3.25 o 3 1 2 13.93 9.55 0.60 o 4 1 2 558.01 568.15 7.17 o 5 1 2 153.97 159.74 5.25 o 6 1 2 4.36 4.31 0.79 o -6 2 2 60.33 58.29 4.02 o -5 2 2 74.18 69.59 2.42 o -4 2 2 832.27 829.78 9.96 o -3 2 2 38.85 40.83 1.29 o -2 2 2 639.37 676.35 10.39 o -1 2 2 75.41 76.05 1.64 o 0 2 2 1010.46 938.14 14.16 o 1 2 2 2.60 2.26 0.40 o 2 2 2 972.35 873.06 10.40 o 3 2 2 184.94 190.05 2.60 o 4 2 2 0.13 1.41 0.42 o 5 2 2 218.30 237.95 5.61 o 6 2 2 162.50 152.77 5.72 o -5 3 2 204.61 204.83 4.32 o -4 3 2 56.43 54.61 1.46 o -3 3 2 342.93 352.58 4.72 o -2 3 2 252.73 290.58 5.21 o -1 3 2 902.41 861.37 10.45 o 0 3 2 1873.14 1925.03 26.33 o 1 3 2 894.35 836.21 11.37 o 2 3 2 948.69 994.58 10.61 o 3 3 2 124.31 128.29 2.09 o 4 3 2 975.59 986.06 12.74 o 5 3 2 151.18 155.28 3.81 o 6 3 2 13.67 11.11 1.52 o -5 4 2 15.93 16.03 1.35 o -4 4 2 959.93 941.08 10.77 o -3 4 2 332.10 316.12 4.39 o -2 4 2 286.76 296.37 5.06 o -1 4 2 3027.56 2920.18 32.60 o 0 4 2 559.46 552.16 8.32 o 1 4 2 489.56 456.25 6.98 o 2 4 2 4844.96 4855.67 43.44 o 3 4 2 219.11 207.41 2.84 o 4 4 2 61.78 59.15 1.68 o 5 4 2 245.46 256.29 5.73 o -5 5 2 530.52 549.13 11.31 o -4 5 2 1.16 2.08 0.45 o -3 5 2 713.67 695.91 7.47 o -2 5 2 1811.92 1780.83 19.34 o -1 5 2 335.51 349.52 5.18 o 0 5 2 238.94 250.19 4.32 o 1 5 2 26.17 14.86 0.93 o 2 5 2 383.68 385.52 4.23 o 3 5 2 617.30 605.72 6.15 o 4 5 2 292.33 280.17 4.82 o 5 5 2 7.74 7.56 0.82 o -5 6 2 10.64 9.40 0.86 o -4 6 2 424.83 405.41 7.30 o -3 6 2 497.10 466.19 9.15 o -2 6 2 221.28 232.43 3.59 o -1 6 2 2247.19 2156.92 26.02 o 0 6 2 405.39 419.67 7.47 o 1 6 2 3492.60 3493.35 34.29 o 2 6 2 2.65 5.14 0.34 o 3 6 2 313.10 308.65 3.98 o 4 6 2 42.12 41.35 1.45 o 5 6 2 71.42 81.59 2.44 o -5 7 2 159.45 164.66 7.00 o -4 7 2 17.24 15.35 0.99 o -3 7 2 93.29 83.23 2.05 o -2 7 2 6.30 5.76 0.53 o -1 7 2 1.38 1.15 0.27 o 0 7 2 1.66 4.36 0.42 o 1 7 2 722.99 688.10 6.61 o 2 7 2 68.86 75.13 1.34 o 3 7 2 45.04 39.81 1.16 o 4 7 2 174.88 170.80 3.49 o 5 7 2 246.29 242.63 8.96 o -5 8 2 4.90 2.77 0.82 o -4 8 2 22.77 17.26 1.23 o -3 8 2 1032.92 1051.92 13.14 o -2 8 2 1407.89 1398.49 13.74 o -1 8 2 90.74 77.66 1.37 o 0 8 2 28.20 27.65 0.81 o 1 8 2 279.27 294.92 3.12 o 2 8 2 584.59 596.99 5.67 o 3 8 2 1946.84 1907.08 19.52 o 4 8 2 285.41 309.90 6.49 o 5 8 2 227.61 222.01 9.05 o -5 9 2 224.46 247.55 6.75 o -4 9 2 2.19 2.54 0.70 o -3 9 2 909.30 873.75 11.19 o -2 9 2 446.74 456.82 5.20 o -1 9 2 591.25 569.37 5.73 o 0 9 2 456.06 482.36 4.82 o 1 9 2 1414.82 1355.60 10.82 o 2 9 2 85.68 88.81 1.57 o 3 9 2 399.50 390.23 5.60 o 4 9 2 0.29 0.99 0.51 o 5 9 2 212.31 202.40 8.01 o -5 10 2 26.25 26.94 1.36 o -4 10 2 127.68 127.87 3.49 o -3 10 2 230.74 243.18 4.03 o -2 10 2 13.17 17.37 0.78 o -1 10 2 210.07 196.43 2.48 o 0 10 2 185.64 198.54 2.67 o 1 10 2 946.36 926.67 7.60 o 2 10 2 229.04 200.09 2.58 o 3 10 2 392.86 369.30 5.20 o 4 10 2 167.25 165.70 6.23 o 5 10 2 92.40 90.85 4.06 o -5 11 2 268.46 223.79 19.10 o -4 11 2 136.07 134.59 3.35 o -3 11 2 89.02 81.58 2.06 o -2 11 2 139.15 142.04 2.88 o -1 11 2 414.37 433.68 4.73 o 0 11 2 1379.57 1376.72 10.67 o 1 11 2 248.38 249.75 2.82 o 2 11 2 0.13 0.49 0.32 o 3 11 2 3.45 1.42 0.40 o 4 11 2 112.06 131.62 3.31 o 5 11 2 109.54 84.70 5.19 o -4 12 2 22.39 22.75 1.10 o -3 12 2 89.50 89.06 2.34 o -2 12 2 99.20 98.13 2.00 o -1 12 2 2412.73 2350.10 18.85 o 0 12 2 15.54 14.18 0.56 o 1 12 2 27.18 27.08 0.90 o 2 12 2 0.44 0.77 0.33 o 3 12 2 34.72 38.53 1.29 o 4 12 2 48.00 56.62 2.12 o -4 13 2 94.22 97.93 2.78 o -3 13 2 50.94 52.50 1.69 o -2 13 2 402.18 409.07 5.16 o -1 13 2 108.28 104.63 1.83 o 0 13 2 495.81 483.58 4.56 o 1 13 2 728.25 729.22 7.51 o 2 13 2 0.59 3.35 0.42 o 3 13 2 185.75 193.10 3.41 o 4 13 2 258.04 261.99 10.45 o -4 14 2 3.53 4.16 0.55 o -3 14 2 8.24 11.59 0.78 o -2 14 2 1.86 3.32 0.47 o -1 14 2 8.73 10.45 0.58 o 0 14 2 425.60 439.19 4.43 o 1 14 2 196.97 181.62 2.29 o 2 14 2 75.52 73.96 1.71 o 3 14 2 48.88 51.26 1.39 o 4 14 2 80.29 68.63 3.34 o -4 15 2 57.98 51.15 2.78 o -3 15 2 135.37 146.04 3.36 o -2 15 2 868.49 913.89 11.86 o -1 15 2 2.77 2.86 0.41 o 0 15 2 7.95 9.35 0.60 o 1 15 2 292.50 287.51 3.67 o 2 15 2 125.99 128.34 2.25 o 3 15 2 252.01 262.80 4.57 o -3 16 2 89.36 98.17 2.03 o -2 16 2 1.31 1.38 0.36 o -1 16 2 150.38 155.91 2.49 o 0 16 2 342.22 365.19 4.71 o 1 16 2 173.06 180.85 2.74 o 2 16 2 143.47 152.67 2.62 o 3 16 2 120.90 111.83 4.43 o -3 17 2 0.13 0.15 0.38 o -2 17 2 386.80 395.54 5.95 o -1 17 2 254.57 257.07 3.99 o 0 17 2 406.29 425.33 7.29 o 1 17 2 76.83 75.60 1.74 o 2 17 2 51.15 53.65 1.37 o 3 17 2 32.18 30.41 2.31 o -2 18 2 5.79 4.70 0.60 o -1 18 2 3.46 2.08 0.35 o 0 18 2 2.23 2.02 0.37 o 1 18 2 15.62 12.31 0.63 o 2 18 2 126.83 93.25 5.67 o -1 19 2 113.09 112.39 6.41 o 0 19 2 117.05 120.16 5.22 o 1 19 2 0.09 0.77 0.54 o -5 0 3 1084.62 1121.16 29.68 o -3 0 3 2986.29 2976.32 47.24 o -1 0 3 1313.68 1467.93 28.53 o 1 0 3 1446.62 1411.64 30.75 o 3 0 3 121.30 104.58 2.62 o 5 0 3 127.35 148.52 7.55 o 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