#------------------------------------------------------------------------------ #$Date: 2025-03-14 05:12:06 +0200 (Fri, 14 Mar 2025) $ #$Revision: 298435 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/27/2312783.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312783 _cell_angle_alpha 90.000 _cell_angle_beta 105.480 _cell_angle_gamma 90.000 _cell_length_a 7.8054 _cell_length_b 16.8220 _cell_length_c 10.5506 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high 0.7975 _cod_data_source_file jx3091zy_241017_2_100k_autosup2.hkl _cod_data_source_block zy_241017_2_100k_auto _shelx_title ' zy_241017_2_100k_auto_a.res in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 133.58 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -20 0 3.28 3.80 0.78 o 2 -20 0 86.99 79.50 2.88 o 1 -19 0 100.92 89.53 3.84 o 2 -19 0 80.59 79.08 3.58 o 3 -19 0 57.61 61.13 2.83 o 0 -18 0 324.47 310.98 5.95 o 1 -18 0 191.73 175.85 4.27 o 2 -18 0 65.76 62.00 1.73 o 3 -18 0 128.28 132.29 3.29 o 4 -18 0 67.17 67.82 1.76 o 1 -17 0 642.02 603.97 7.86 o 2 -17 0 116.65 117.09 2.61 o 3 -17 0 40.09 37.84 1.16 o 4 -17 0 12.84 11.29 0.63 o 5 -17 0 98.56 95.05 2.04 o 0 -16 0 218.75 228.81 5.07 o 1 -16 0 42.66 39.33 1.25 o 2 -16 0 539.77 529.73 6.35 o 3 -16 0 98.00 101.89 2.01 o 4 -16 0 248.78 252.70 2.84 o 5 -16 0 270.98 291.23 4.45 o 6 -16 0 79.85 76.51 3.12 o 1 -15 0 104.41 109.09 1.92 o 2 -15 0 97.13 93.69 1.94 o 3 -15 0 77.46 77.89 1.31 o 4 -15 0 41.83 36.67 1.04 o 5 -15 0 113.79 108.48 1.91 o 6 -15 0 218.58 221.56 3.52 o 0 -14 0 699.93 651.06 16.95 o 1 -14 0 208.72 191.13 2.42 o 2 -14 0 1369.29 1300.24 16.27 o 3 -14 0 156.88 144.83 1.75 o 4 -14 0 197.32 189.54 2.48 o 5 -14 0 210.09 223.40 3.24 o 6 -14 0 195.94 202.18 4.60 o 1 -13 0 205.42 205.10 2.85 o 2 -13 0 159.14 158.65 2.20 o 3 -13 0 131.81 130.69 1.79 o 4 -13 0 2.72 4.35 0.45 o 5 -13 0 489.53 470.28 5.74 o 6 -13 0 147.71 142.72 4.10 o 7 -13 0 141.95 137.94 3.77 o 0 -12 0 390.56 389.11 7.11 o 1 -12 0 282.33 255.31 2.22 o 2 -12 0 344.73 321.70 2.80 o 3 -12 0 775.82 761.96 4.99 o 4 -12 0 257.35 267.95 2.92 o 5 -12 0 231.90 249.28 3.69 o 6 -12 0 3.28 2.36 1.16 o 7 -12 0 131.03 135.82 4.19 o 1 -11 0 1022.91 989.85 9.51 o 2 -11 0 1083.47 1051.18 7.35 o 3 -11 0 131.13 124.91 1.58 o 4 -11 0 237.40 240.42 2.58 o 5 -11 0 913.13 882.46 7.50 o 6 -11 0 152.25 149.56 6.87 o 7 -11 0 447.05 426.58 7.21 o 0 -10 0 677.56 680.95 8.13 o 1 -10 0 9.66 10.58 0.43 o 2 -10 0 1170.57 1163.38 12.45 o 3 -10 0 147.29 147.79 1.66 o 4 -10 0 183.69 172.76 2.00 o 5 -10 0 661.02 665.12 6.86 o 6 -10 0 376.99 364.72 6.21 o 7 -10 0 206.04 190.88 4.68 o 1 -9 0 306.41 302.35 1.84 o 2 -9 0 523.67 495.20 5.51 o 3 -9 0 681.39 680.81 5.69 o 4 -9 0 97.37 96.12 1.30 o 5 -9 0 661.93 631.25 8.61 o 6 -9 0 416.26 408.20 8.00 o 7 -9 0 153.17 151.28 7.91 o 8 -9 0 584.39 572.94 10.98 o 0 -8 0 1184.87 1244.55 12.62 o 1 -8 0 1079.83 1038.41 6.68 o 2 -8 0 63.60 69.46 0.80 o 3 -8 0 377.88 380.42 3.43 o 4 -8 0 596.86 567.86 3.51 o 5 -8 0 220.67 220.12 3.42 o 6 -8 0 177.50 158.34 4.68 o 7 -8 0 205.96 199.00 4.93 o 8 -8 0 171.75 160.39 5.14 o 1 -7 0 943.61 938.00 4.98 o 2 -7 0 64.64 66.06 1.45 o 3 -7 0 573.83 573.99 3.20 o 4 -7 0 1236.05 1218.44 7.59 o 5 -7 0 634.09 589.73 5.62 o 6 -7 0 893.55 861.11 10.72 o 7 -7 0 50.78 49.84 3.50 o 8 -7 0 200.92 197.93 4.22 o 0 -6 0 4953.95 4620.54 54.31 o 1 -6 0 100.44 103.72 1.18 o 2 -6 0 177.93 173.85 1.24 o 3 -6 0 399.91 440.12 2.42 o 4 -6 0 37.09 39.95 0.78 o 5 -6 0 249.16 256.48 3.24 o 6 -6 0 972.36 988.74 13.98 o 7 -6 0 290.79 280.62 8.98 o 8 -6 0 10.32 9.66 1.07 o 1 -5 0 731.21 668.20 3.21 o 2 -5 0 1029.98 937.76 5.44 o 3 -5 0 161.51 166.06 1.11 o 4 -5 0 1267.09 1244.79 7.99 o 5 -5 0 201.28 193.39 2.97 o 6 -5 0 117.86 117.94 2.90 o 7 -5 0 358.08 345.72 10.23 o 8 -5 0 86.81 84.21 2.91 o 0 -4 0 2140.81 1918.53 22.73 o 1 -4 0 913.68 854.84 3.60 o 2 -4 0 469.18 426.65 1.99 o 3 -4 0 1715.56 1755.99 7.36 o 4 -4 0 128.54 136.77 1.35 o 5 -4 0 164.87 167.08 3.02 o 6 -4 0 943.54 934.85 8.94 o 7 -4 0 1059.54 1027.09 15.08 o 8 -4 0 182.61 178.01 6.65 o 1 -3 0 7981.68 8044.68 26.92 o 2 -3 0 639.66 602.42 3.76 o 3 -3 0 2550.70 2403.62 9.76 o 4 -3 0 763.93 741.72 6.40 o 5 -3 0 721.95 727.04 9.99 o 6 -3 0 46.97 42.34 1.62 o 7 -3 0 152.12 153.81 4.05 o 8 -3 0 151.16 150.80 6.38 o 0 -2 0 1568.38 1525.12 8.38 o 1 -2 0 5314.35 5206.40 25.66 o 2 -2 0 3333.47 3242.80 18.19 o 3 -2 0 4.17 2.70 0.27 o 4 -2 0 190.72 181.79 1.51 o 5 -2 0 320.90 324.08 4.36 o 6 -2 0 839.43 836.11 12.84 o 7 -2 0 785.76 787.19 7.79 o 8 -2 0 63.43 63.40 2.94 o 1 -1 0 1298.88 1227.63 4.63 o 2 -1 0 6656.71 6534.37 30.62 o 3 -1 0 145.83 110.22 0.88 o 4 -1 0 311.64 287.35 3.42 o 5 -1 0 6.65 9.01 0.71 o 6 -1 0 138.46 131.80 3.51 o 7 -1 0 411.34 410.45 4.80 o 8 -1 0 21.54 22.02 2.06 o 9 -1 0 91.63 89.45 3.53 o 1 0 0 6.24 11.57 0.24 o 2 0 0 8658.58 8824.29 39.57 o 3 0 0 63.77 80.58 0.76 o 4 0 0 7.19 6.81 0.30 o 5 0 0 439.97 425.77 5.13 o 6 0 0 373.01 369.36 6.07 o 7 0 0 149.56 145.78 2.56 o 8 0 0 7.81 7.84 0.90 o 1 1 0 1258.75 1225.70 7.89 o 2 1 0 6665.89 6784.90 30.54 o 3 1 0 166.03 133.72 1.25 o 4 1 0 276.00 249.44 2.93 o 5 1 0 7.47 11.83 1.00 o 6 1 0 139.87 139.45 2.49 o 7 1 0 419.61 412.82 5.86 o 8 1 0 16.92 16.40 1.09 o 9 1 0 99.39 76.63 4.24 o 0 2 0 1404.67 1430.87 13.48 o 1 2 0 5442.39 5489.95 26.50 o 2 2 0 3323.69 3407.08 15.46 o 3 2 0 5.33 3.89 0.31 o 4 2 0 185.10 178.85 1.71 o 5 2 0 326.55 320.41 3.32 o 6 2 0 757.35 766.67 9.79 o 7 2 0 878.54 881.89 7.92 o 8 2 0 53.31 52.16 1.88 o 9 2 0 27.18 21.99 1.48 o 1 3 0 8206.72 8570.94 28.77 o 2 3 0 681.34 683.94 3.72 o 3 3 0 2452.16 2430.27 9.91 o 4 3 0 875.23 882.61 8.50 o 5 3 0 746.55 764.01 7.71 o 6 3 0 38.34 34.71 1.02 o 7 3 0 144.83 150.49 2.57 o 8 3 0 140.42 139.27 2.55 o 9 3 0 47.65 38.81 1.94 o 0 4 0 2231.70 2124.72 12.72 o 1 4 0 788.17 773.87 3.52 o 2 4 0 456.02 434.24 2.30 o 3 4 0 1750.30 1886.37 8.67 o 4 4 0 108.12 120.01 1.30 o 5 4 0 194.30 200.75 2.35 o 6 4 0 1045.98 1045.21 9.29 o 7 4 0 984.83 987.15 7.51 o 8 4 0 153.23 149.63 2.75 o 9 4 0 24.14 19.40 1.50 o 1 5 0 678.97 653.88 3.27 o 2 5 0 981.76 941.98 4.87 o 3 5 0 101.22 113.32 0.89 o 4 5 0 1388.33 1415.94 10.20 o 5 5 0 184.79 179.82 1.90 o 6 5 0 147.02 153.56 1.79 o 7 5 0 371.14 353.53 4.13 o 8 5 0 86.02 86.44 2.62 o 9 5 0 28.59 18.58 2.16 o 0 6 0 5076.77 5165.91 39.38 o 1 6 0 73.52 79.93 0.61 o 2 6 0 227.38 237.94 1.36 o 3 6 0 437.57 501.35 2.19 o 4 6 0 24.08 29.21 0.99 o 5 6 0 284.90 295.29 2.36 o 6 6 0 915.18 907.48 5.24 o 7 6 0 278.73 284.06 3.69 o 8 6 0 18.24 17.08 1.23 o 1 7 0 856.87 909.78 4.84 o 2 7 0 76.15 83.25 0.73 o 3 7 0 611.80 653.68 2.77 o 4 7 0 1203.63 1242.80 6.68 o 5 7 0 628.70 609.98 3.84 o 6 7 0 921.12 933.33 6.09 o 7 7 0 50.82 52.37 1.50 o 8 7 0 215.61 217.61 3.19 o 0 8 0 1046.81 1170.07 10.10 o 1 8 0 1049.52 1071.82 7.12 o 2 8 0 100.07 113.72 0.89 o 3 8 0 404.61 438.97 2.44 o 4 8 0 585.97 588.45 3.11 o 5 8 0 201.44 211.08 1.94 o 6 8 0 167.63 160.42 2.31 o 7 8 0 225.06 221.77 3.50 o 8 8 0 197.33 188.41 4.18 o 1 9 0 272.79 284.42 1.89 o 2 9 0 508.15 510.41 2.67 o 3 9 0 634.47 685.15 3.53 o 4 9 0 124.13 132.22 1.24 o 5 9 0 644.16 634.46 4.76 o 6 9 0 406.83 416.04 4.32 o 7 9 0 147.69 156.23 3.10 o 8 9 0 581.80 583.18 7.72 o 0 10 0 666.13 701.58 9.39 o 1 10 0 19.10 22.16 0.75 o 2 10 0 1119.57 1165.10 7.21 o 3 10 0 121.48 135.62 1.43 o 4 10 0 168.84 166.35 1.68 o 5 10 0 715.08 745.08 5.40 o 6 10 0 407.21 416.79 6.74 o 7 10 0 211.98 209.98 4.21 o 8 10 0 109.34 105.64 4.28 o 1 11 0 1035.37 1049.63 6.54 o 2 11 0 979.11 1017.87 8.14 o 3 11 0 122.73 125.10 1.40 o 4 11 0 225.66 242.46 2.19 o 5 11 0 927.63 941.80 6.62 o 6 11 0 171.38 169.48 3.80 o 7 11 0 454.68 444.21 8.33 o 8 11 0 96.66 90.68 3.18 o 0 12 0 415.62 432.41 6.50 o 1 12 0 307.06 296.30 2.79 o 2 12 0 321.73 318.18 2.46 o 3 12 0 755.34 780.71 5.67 o 4 12 0 230.17 248.86 2.32 o 5 12 0 262.35 282.67 3.58 o 6 12 0 2.06 2.17 0.92 o 7 12 0 131.78 135.46 6.08 o 1 13 0 167.28 176.95 2.03 o 2 13 0 178.56 186.21 2.17 o 3 13 0 127.98 136.88 2.06 o 4 13 0 4.36 7.45 0.63 o 5 13 0 483.26 476.28 10.22 o 6 13 0 144.74 141.35 7.23 o 0 14 0 711.12 686.70 7.20 o 1 14 0 217.11 216.07 3.07 o 2 14 0 1408.60 1416.35 11.66 o 3 14 0 174.37 168.85 3.07 o 4 14 0 231.72 222.47 3.76 o 5 14 0 182.52 190.61 5.81 o 6 14 0 183.57 179.10 7.42 o 1 15 0 100.32 112.88 1.92 o 2 15 0 70.47 71.85 1.98 o 3 15 0 83.14 87.01 1.93 o 4 15 0 34.64 33.69 1.54 o 5 15 0 129.99 120.21 3.92 o 0 16 0 213.46 229.52 3.63 o 1 16 0 50.20 48.68 1.25 o 2 16 0 519.01 529.86 5.15 o 3 16 0 89.80 96.61 2.21 o 4 16 0 229.64 242.12 3.55 o 5 16 0 279.46 299.50 9.70 o 1 17 0 693.37 673.03 6.65 o 2 17 0 111.08 121.61 2.14 o 3 17 0 49.70 46.71 1.25 o 4 17 0 12.11 11.33 1.01 o 0 18 0 306.95 322.92 3.70 o 1 18 0 196.64 195.20 2.41 o 2 18 0 53.26 54.62 1.30 o 3 18 0 121.48 133.41 2.07 o 4 18 0 75.19 82.19 3.64 o 1 19 0 92.44 92.74 1.47 o 2 19 0 90.20 91.84 1.61 o 3 19 0 52.86 58.89 2.09 o 4 19 0 220.42 251.56 5.68 o 0 20 0 39.96 39.40 2.37 o 1 20 0 6.53 6.31 0.63 o 2 20 0 92.49 92.65 2.81 o -3 -19 1 55.66 52.40 2.41 o -2 -19 1 102.39 101.51 4.05 o -1 -19 1 19.90 20.79 1.93 o 0 -19 1 0.20 0.26 0.66 o 1 -19 1 55.28 49.36 1.96 o 2 -19 1 28.23 29.91 1.51 o 3 -19 1 168.37 149.21 11.88 o -4 -18 1 10.39 12.24 0.86 o -3 -18 1 57.79 52.53 1.74 o -2 -18 1 261.60 259.02 4.51 o -1 -18 1 93.52 83.87 2.36 o 0 -18 1 153.39 140.77 2.75 o 1 -18 1 263.78 239.49 4.24 o 2 -18 1 79.08 84.24 2.00 o 3 -18 1 157.65 158.17 3.04 o 4 -18 1 17.45 18.04 1.15 o -5 -17 1 149.98 143.82 2.63 o -4 -17 1 19.35 18.45 0.73 o -3 -17 1 158.88 147.15 2.56 o -2 -17 1 340.50 326.12 4.59 o -1 -17 1 282.96 269.22 5.81 o 0 -17 1 56.13 49.91 2.36 o 1 -17 1 98.27 92.23 2.29 o 2 -17 1 77.86 77.21 1.85 o 3 -17 1 37.29 35.63 1.20 o 4 -17 1 34.19 32.60 1.15 o 5 -17 1 38.29 35.12 2.26 o -6 -16 1 70.03 74.05 4.29 o -5 -16 1 108.13 113.53 2.27 o -4 -16 1 226.22 229.92 2.43 o -3 -16 1 48.21 43.74 1.42 o -2 -16 1 98.08 94.04 1.91 o -1 -16 1 194.49 183.22 2.96 o 0 -16 1 899.03 830.74 8.88 o 1 -16 1 29.97 29.17 1.01 o 2 -16 1 179.55 171.55 2.74 o 3 -16 1 313.55 304.38 3.36 o 4 -16 1 4.93 5.41 0.57 o 5 -16 1 131.90 139.03 2.77 o -6 -15 1 2.50 3.17 0.74 o -5 -15 1 131.48 127.94 2.40 o -4 -15 1 119.78 106.85 2.44 o -3 -15 1 63.53 54.76 1.22 o -2 -15 1 485.13 451.97 5.18 o -1 -15 1 545.53 507.56 4.93 o 0 -15 1 28.99 31.59 1.05 o 1 -15 1 235.43 219.24 2.82 o 2 -15 1 39.58 46.14 1.19 o 3 -15 1 3.01 4.25 0.49 o 4 -15 1 112.31 109.65 1.75 o 5 -15 1 217.25 222.19 3.77 o 6 -15 1 21.76 20.95 1.24 o -7 -14 1 14.45 12.89 1.42 o -6 -14 1 46.88 46.57 2.24 o -5 -14 1 209.94 233.21 3.09 o -4 -14 1 121.17 121.06 1.69 o -3 -14 1 34.61 35.75 1.01 o -2 -14 1 713.31 673.02 8.17 o -1 -14 1 471.41 451.93 4.48 o 0 -14 1 87.50 73.13 1.65 o 1 -14 1 600.85 566.54 6.19 o 2 -14 1 568.14 554.25 4.83 o 3 -14 1 253.03 256.77 2.75 o 4 -14 1 85.31 88.80 1.75 o 5 -14 1 79.31 80.70 2.35 o 6 -14 1 260.09 263.73 7.59 o -7 -13 1 19.22 22.27 2.06 o -6 -13 1 183.64 185.31 4.00 o -5 -13 1 249.18 239.46 2.99 o -4 -13 1 56.45 50.56 1.07 o -3 -13 1 31.14 33.87 0.92 o -2 -13 1 290.35 275.97 3.04 o -1 -13 1 896.03 830.81 6.13 o 0 -13 1 7.55 8.20 0.50 o 1 -13 1 441.86 425.79 4.42 o 2 -13 1 274.96 272.52 2.66 o 3 -13 1 345.10 346.97 3.43 o 4 -13 1 249.04 242.19 2.57 o 5 -13 1 45.55 40.64 1.50 o 6 -13 1 56.55 57.94 2.00 o -7 -12 1 28.85 27.59 1.62 o -6 -12 1 164.21 164.51 3.57 o -5 -12 1 89.58 90.52 1.69 o -4 -12 1 135.10 129.75 1.97 o -3 -12 1 86.09 84.67 1.24 o -2 -12 1 830.61 804.05 7.53 o -1 -12 1 398.71 373.22 4.08 o 0 -12 1 15.99 14.30 0.50 o 1 -12 1 38.67 39.72 0.96 o 2 -12 1 1071.54 1017.37 8.01 o 3 -12 1 117.85 115.87 1.59 o 4 -12 1 114.31 111.75 1.64 o 5 -12 1 109.58 115.27 2.40 o 6 -12 1 253.13 272.27 5.98 o 7 -12 1 20.29 20.74 1.74 o -7 -11 1 64.48 62.71 2.03 o -6 -11 1 127.68 128.63 4.20 o -5 -11 1 305.04 278.81 3.62 o -4 -11 1 102.21 97.23 1.51 o -3 -11 1 650.64 646.48 5.00 o -2 -11 1 717.45 744.75 4.24 o -1 -11 1 150.47 150.46 3.01 o 0 -11 1 30.73 28.26 0.68 o 1 -11 1 406.04 404.62 4.71 o 2 -11 1 113.32 105.98 1.32 o 3 -11 1 1061.61 1030.56 6.46 o 4 -11 1 485.08 467.90 5.13 o 5 -11 1 138.18 125.43 2.55 o 6 -11 1 256.48 257.49 8.16 o 7 -11 1 207.65 213.45 6.32 o -7 -10 1 50.35 48.95 1.91 o -6 -10 1 6.34 9.72 0.91 o -5 -10 1 240.52 248.91 5.30 o -4 -10 1 758.38 776.48 5.53 o -3 -10 1 73.48 66.49 1.04 o -2 -10 1 104.35 89.95 1.24 o -1 -10 1 100.90 89.82 1.52 o 0 -10 1 202.85 222.14 2.10 o 1 -10 1 810.64 824.48 7.47 o 2 -10 1 436.08 406.64 4.55 o 3 -10 1 308.00 295.76 2.60 o 4 -10 1 1482.08 1434.78 11.92 o 5 -10 1 590.63 602.87 6.31 o 6 -10 1 489.26 480.85 10.99 o 7 -10 1 23.21 23.42 2.24 o -8 -9 1 55.97 57.88 2.82 o -7 -9 1 37.35 34.59 1.97 o -6 -9 1 396.94 400.54 6.62 o -5 -9 1 1122.55 1071.80 7.85 o -4 -9 1 276.73 275.57 2.42 o -3 -9 1 656.29 684.98 4.86 o -2 -9 1 1676.33 1664.41 11.79 o -1 -9 1 18.09 20.88 0.56 o 0 -9 1 125.24 131.30 1.67 o 1 -9 1 96.39 91.42 1.00 o 2 -9 1 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156.86 164.33 3.31 o -2 9 8 109.94 108.61 3.65 o -1 9 8 182.55 187.43 4.74 o 0 9 8 404.59 410.39 4.69 o 1 9 8 6.52 7.52 1.16 o 2 9 8 75.41 75.76 2.31 o 3 9 8 26.68 19.01 1.02 o 4 9 8 272.21 254.77 6.08 o -7 10 8 28.60 27.78 1.21 o -6 10 8 54.75 57.77 1.84 o -5 10 8 108.92 114.92 2.23 o -4 10 8 334.67 349.31 14.20 o -3 10 8 60.15 65.24 3.03 o -2 10 8 584.17 586.82 7.03 o -1 10 8 48.34 48.43 1.53 o 0 10 8 242.38 250.66 6.78 o 1 10 8 27.03 24.31 1.67 o 2 10 8 105.77 103.62 2.51 o 3 10 8 0.52 1.91 0.57 o 4 10 8 262.52 281.68 18.43 o -7 11 8 114.70 113.20 3.85 o -6 11 8 179.33 177.14 3.93 o -5 11 8 86.53 88.25 3.02 o -4 11 8 233.81 241.79 5.90 o -3 11 8 376.38 406.46 7.43 o -2 11 8 156.41 149.52 3.48 o -1 11 8 123.12 121.35 2.97 o 0 11 8 24.35 26.19 1.24 o 1 11 8 249.91 299.49 5.83 o 2 11 8 88.25 99.23 2.66 o 3 11 8 21.89 26.75 1.31 o 4 11 8 40.46 37.59 2.78 o -6 12 8 382.11 392.21 6.75 o -5 12 8 103.29 98.43 2.04 o -4 12 8 25.00 28.73 1.48 o -3 12 8 566.04 615.76 9.03 o -2 12 8 103.06 104.05 1.97 o -1 12 8 145.52 134.92 2.30 o 0 12 8 9.55 10.80 0.96 o 1 12 8 68.60 74.76 2.96 o 2 12 8 0.91 0.88 0.53 o 3 12 8 170.20 172.02 6.92 o -5 13 8 64.46 68.43 2.05 o -4 13 8 7.99 10.14 1.01 o -3 13 8 16.50 19.26 1.15 o -2 13 8 39.05 36.47 1.41 o -1 13 8 50.35 49.87 1.44 o 0 13 8 157.94 169.59 4.02 o 1 13 8 98.22 92.68 2.11 o 2 13 8 93.41 88.00 2.08 o 3 13 8 27.51 25.73 2.25 o -5 14 8 35.66 34.19 2.50 o -4 14 8 68.79 73.63 2.16 o -3 14 8 72.40 74.52 4.32 o -2 14 8 171.17 190.03 8.39 o -1 14 8 14.13 17.52 0.99 o 0 14 8 46.43 49.18 1.83 o 1 14 8 150.83 161.33 3.17 o -4 15 8 2.84 3.35 0.89 o -3 15 8 65.13 74.01 2.62 o -2 15 8 0.96 2.03 1.32 o -1 15 8 89.36 90.81 2.78 o 0 15 8 141.65 146.33 6.63 o -3 16 8 55.02 55.67 2.42 o -2 16 8 63.35 59.32 2.55 o -4 -14 9 39.70 41.51 2.13 o -3 -14 9 117.42 117.09 2.02 o -2 -14 9 82.25 76.70 1.47 o -1 -14 9 161.73 161.58 2.46 o 0 -14 9 25.13 22.06 1.71 o -5 -13 9 334.15 301.79 6.54 o -4 -13 9 8.18 9.08 0.56 o -3 -13 9 101.87 100.79 1.56 o -2 -13 9 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442.95 3.44 o -4 -9 9 96.39 90.27 1.30 o -3 -9 9 187.49 182.08 1.92 o -2 -9 9 72.80 69.22 1.18 o -1 -9 9 352.86 359.61 4.18 o 0 -9 9 49.71 41.56 1.03 o 1 -9 9 400.07 399.72 7.08 o 2 -9 9 72.08 68.07 3.57 o 3 -9 9 7.12 6.27 1.14 o -7 -8 9 160.12 153.25 3.57 o -6 -8 9 141.55 142.75 2.30 o -5 -8 9 179.10 177.15 2.17 o -4 -8 9 69.99 65.63 1.10 o -3 -8 9 124.89 128.42 1.77 o -2 -8 9 137.85 131.20 2.05 o -1 -8 9 277.62 252.11 3.94 o 0 -8 9 58.02 64.40 1.28 o 1 -8 9 48.06 45.62 1.35 o 2 -8 9 55.78 54.05 1.69 o 3 -8 9 351.16 315.57 12.87 o -7 -7 9 80.57 82.38 2.69 o -6 -7 9 154.01 147.56 2.07 o -5 -7 9 264.99 270.12 3.66 o -4 -7 9 192.30 188.29 2.03 o -3 -7 9 289.95 282.79 3.38 o -2 -7 9 314.79 302.84 2.48 o -1 -7 9 178.32 167.42 1.82 o 0 -7 9 70.26 75.50 1.70 o 1 -7 9 46.62 55.87 1.40 o 2 -7 9 21.72 23.19 1.11 o 3 -7 9 15.36 17.83 1.16 o 4 -7 9 17.36 15.79 1.41 o -7 -6 9 267.41 261.32 3.93 o -6 -6 9 59.47 62.85 1.51 o -5 -6 9 128.19 129.99 1.98 o -4 -6 9 663.50 647.04 4.65 o -3 -6 9 51.72 51.66 0.97 o -2 -6 9 849.40 826.79 6.25 o -1 -6 9 167.44 156.13 1.85 o 0 -6 9 392.27 373.29 4.32 o 1 -6 9 54.11 52.00 1.39 o 2 -6 9 27.40 28.53 1.38 o 3 -6 9 165.93 164.26 3.58 o 4 -6 9 297.43 288.37 6.91 o -8 -5 9 70.11 72.40 2.99 o -7 -5 9 91.28 94.74 1.94 o -6 -5 9 121.31 124.39 2.34 o -5 -5 9 33.41 34.33 0.96 o -4 -5 9 237.26 219.10 2.10 o -3 -5 9 160.62 158.07 1.57 o -2 -5 9 394.94 393.70 3.53 o -1 -5 9 906.74 929.55 5.81 o 0 -5 9 339.01 320.47 2.72 o 1 -5 9 151.12 152.41 2.70 o 2 -5 9 56.07 52.79 1.98 o 3 -5 9 163.67 162.43 3.04 o 4 -5 9 67.30 61.91 1.92 o -8 -4 9 33.71 34.18 1.59 o -7 -4 9 52.64 51.01 1.23 o -6 -4 9 296.04 301.61 3.58 o -5 -4 9 32.94 31.08 1.01 o -4 -4 9 296.25 293.36 2.29 o -3 -4 9 553.21 563.60 3.79 o -2 -4 9 361.71 343.00 2.66 o -1 -4 9 28.14 28.71 0.81 o 0 -4 9 452.97 457.23 4.68 o 1 -4 9 31.69 32.81 1.29 o 2 -4 9 567.28 552.82 6.92 o 3 -4 9 250.80 250.68 3.67 o 4 -4 9 97.79 89.99 2.93 o -8 -3 9 202.64 215.98 8.76 o -7 -3 9 539.95 526.86 8.05 o -6 -3 9 12.58 13.01 0.76 o -5 -3 9 162.79 155.04 2.44 o -4 -3 9 59.75 58.45 1.01 o -3 -3 9 653.81 652.25 4.32 o -2 -3 9 60.30 54.90 1.00 o -1 -3 9 1581.94 1621.93 15.31 o 0 -3 9 323.66 317.21 3.23 o 1 -3 9 4.75 4.66 0.56 o 2 -3 9 136.42 136.30 2.40 o 3 -3 9 256.09 258.81 3.79 o 4 -3 9 86.91 85.45 3.21 o -8 -2 9 70.46 71.43 2.44 o -7 -2 9 163.23 166.87 2.82 o -6 -2 9 2.39 3.19 0.45 o -5 -2 9 495.08 500.11 4.61 o -4 -2 9 521.96 515.36 3.66 o -3 -2 9 94.67 92.33 1.53 o -2 -2 9 33.27 30.63 0.78 o -1 -2 9 142.32 146.60 1.84 o 0 -2 9 375.52 379.00 3.68 o 1 -2 9 383.03 378.48 4.37 o 2 -2 9 8.58 9.21 0.62 o 3 -2 9 182.52 188.89 3.29 o 4 -2 9 100.32 89.90 2.17 o -8 -1 9 185.32 200.73 3.39 o -7 -1 9 80.96 84.89 1.61 o -6 -1 9 31.44 31.98 1.12 o -5 -1 9 158.93 154.78 2.05 o -4 -1 9 779.33 766.79 5.35 o -3 -1 9 94.37 90.66 1.45 o -2 -1 9 111.15 103.09 1.50 o -1 -1 9 1372.58 1365.51 11.42 o 0 -1 9 390.09 362.40 6.54 o 1 -1 9 321.37 312.45 4.18 o 2 -1 9 126.43 133.61 2.06 o 3 -1 9 67.48 71.40 1.66 o 4 -1 9 36.58 37.62 1.35 o 5 -1 9 70.20 73.71 3.97 o -8 0 9 188.74 194.77 4.86 o -7 0 9 14.64 18.00 0.83 o -6 0 9 72.74 75.07 1.66 o -5 0 9 172.18 170.00 2.26 o -4 0 9 255.90 265.79 3.14 o -3 0 9 457.46 422.64 3.47 o -2 0 9 2.06 2.03 0.45 o -1 0 9 12.84 12.01 0.76 o 0 0 9 17.52 22.38 0.92 o 1 0 9 22.99 23.14 0.92 o 2 0 9 824.90 844.99 12.65 o 3 0 9 56.42 63.57 1.75 o 4 0 9 16.62 19.98 1.05 o -8 1 9 166.03 177.85 2.78 o -7 1 9 83.11 89.80 2.18 o -6 1 9 36.25 35.31 1.27 o -5 1 9 156.86 155.08 2.42 o -4 1 9 783.16 781.54 7.33 o -3 1 9 108.41 107.50 1.91 o -2 1 9 126.86 119.49 2.04 o -1 1 9 1346.12 1335.30 12.83 o 0 1 9 364.49 342.01 3.48 o 1 1 9 331.73 320.52 3.31 o 2 1 9 122.02 133.35 2.23 o 3 1 9 74.70 79.67 1.87 o 4 1 9 34.29 37.50 1.12 o -8 2 9 73.95 72.14 2.29 o -7 2 9 137.96 140.18 2.65 o -6 2 9 3.69 3.66 0.56 o -5 2 9 516.69 532.07 5.11 o -4 2 9 514.87 519.38 4.75 o -3 2 9 101.43 99.44 1.95 o -2 2 9 33.80 32.71 1.13 o -1 2 9 131.96 136.37 2.31 o 0 2 9 400.50 411.48 4.61 o 1 2 9 371.82 372.51 4.33 o 2 2 9 3.46 2.86 0.50 o 3 2 9 172.89 190.94 2.90 o 4 2 9 100.49 99.04 1.78 o -8 3 9 188.71 194.91 3.30 o -7 3 9 560.01 572.63 8.03 o -6 3 9 16.94 18.80 1.02 o -5 3 9 151.99 158.15 3.39 o -4 3 9 48.79 47.77 1.53 o -3 3 9 639.37 632.70 10.06 o -2 3 9 52.89 44.24 1.39 o -1 3 9 1549.10 1608.24 13.68 o 0 3 9 284.24 275.81 3.82 o 1 3 9 2.46 3.22 0.46 o 2 3 9 139.39 142.99 2.04 o 3 3 9 259.09 277.24 3.52 o 4 3 9 93.52 95.65 2.18 o -8 4 9 33.91 35.47 1.32 o -7 4 9 46.59 45.11 1.86 o -6 4 9 288.58 302.69 6.13 o -5 4 9 20.35 21.09 1.18 o -4 4 9 309.52 310.28 4.01 o -3 4 9 555.45 570.14 7.97 o -2 4 9 393.00 387.78 6.44 o -1 4 9 30.26 31.80 1.20 o 0 4 9 500.23 508.68 6.18 o 1 4 9 25.79 29.83 0.94 o 2 4 9 565.04 567.69 6.00 o 3 4 9 273.93 299.09 3.99 o 4 4 9 100.96 103.47 3.15 o -8 5 9 72.75 73.83 1.57 o -7 5 9 77.86 83.81 2.45 o -6 5 9 118.73 125.06 4.64 o -5 5 9 39.01 41.15 1.50 o -4 5 9 257.40 242.72 5.55 o -3 5 9 168.75 170.92 4.33 o -2 5 9 381.39 384.11 7.89 o -1 5 9 915.63 920.17 17.85 o 0 5 9 401.66 378.86 4.59 o 1 5 9 146.07 152.80 2.67 o 2 5 9 45.66 48.41 1.47 o 3 5 9 141.08 153.04 3.19 o 4 5 9 72.65 71.92 3.53 o -8 6 9 176.71 184.95 3.84 o -7 6 9 290.33 288.11 5.37 o -6 6 9 65.29 73.41 2.50 o -5 6 9 145.71 144.78 3.76 o -4 6 9 588.64 593.68 6.80 o -3 6 9 45.36 46.38 1.97 o -2 6 9 886.28 896.16 15.25 o -1 6 9 181.75 170.55 5.26 o 0 6 9 365.89 354.26 3.75 o 1 6 9 47.93 47.77 1.75 o 2 6 9 27.51 32.35 1.08 o 3 6 9 169.50 173.76 2.73 o 4 6 9 298.08 310.88 5.96 o -7 7 9 61.80 63.11 1.69 o -6 7 9 175.23 184.71 5.45 o -5 7 9 257.40 270.31 4.77 o -4 7 9 183.53 184.31 3.61 o -3 7 9 278.75 272.53 5.94 o -2 7 9 300.88 291.28 6.62 o -1 7 9 189.84 191.64 6.06 o 0 7 9 66.74 70.81 2.59 o 1 7 9 44.92 55.49 2.60 o 2 7 9 13.34 17.96 0.92 o 3 7 9 20.89 22.48 1.32 o 4 7 9 16.63 13.53 1.25 o -7 8 9 169.01 155.05 4.36 o -6 8 9 132.16 137.39 3.53 o -5 8 9 156.57 151.78 4.20 o -4 8 9 68.66 66.44 2.62 o -3 8 9 118.30 129.32 3.41 o -2 8 9 119.43 120.41 5.62 o -1 8 9 256.54 229.28 5.88 o 0 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22.48 1.41 o 0 2 12 102.68 104.50 13.33 o -6 3 12 297.26 286.78 4.59 o -5 3 12 1.21 1.96 0.61 o -4 3 12 68.90 70.83 2.10 o -3 3 12 94.54 97.32 2.41 o -2 3 12 105.68 104.74 7.44 o -1 3 12 21.94 24.33 1.64 o 0 3 12 211.41 169.68 4.75 o -5 4 12 84.56 81.85 2.19 o -4 4 12 104.65 109.27 3.42 o -3 4 12 22.53 20.73 1.56 o -2 4 12 111.55 116.87 5.51 o -1 4 12 22.44 24.68 2.19 o 0 4 12 109.16 97.80 3.43 o -5 5 12 63.15 61.46 2.00 o -4 5 12 10.37 11.50 1.23 o -3 5 12 31.06 32.07 2.32 o -2 5 12 85.43 81.42 3.85 o -1 5 12 84.67 83.79 12.73 o 0 5 12 308.25 270.02 5.84 o -3 6 12 322.01 346.05 7.64 o -2 6 12 59.11 61.37 4.14 o -1 6 12 64.17 71.22 2.98 o 0 6 12 145.36 140.04 5.31 o -2 7 12 15.09 17.55 1.55 o -1 7 12 53.81 54.44 3.54 o -1 8 12 180.76 200.31 6.40 o -3 -3 13 102.38 93.33 2.27 o -2 -3 13 129.15 123.00 13.53 o -4 -2 13 86.68 83.90 3.10 o -3 -2 13 25.00 20.06 1.10 o -2 -2 13 10.77 9.20 0.78 o -4 -1 13 22.36 18.89 1.08 o -3 -1 13 40.14 41.86 1.53 o -2 -1 13 33.18 28.61 1.75 o -4 0 13 17.25 17.31 1.52 o -3 0 13 47.03 38.17 1.98 o -2 0 13 45.76 43.26 2.17 o -4 1 13 21.18 18.87 1.51 o -3 1 13 38.50 41.35 1.99 o -2 1 13 42.63 40.60 2.07 o