#------------------------------------------------------------------------------ #$Date: 2016-10-10 12:58:24 +0300 (Mon, 10 Oct 2016) $ #$Revision: 187235 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/00/00/3000023.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3000023 _cell_angle_alpha 90.000 _cell_angle_beta 111.980 _cell_angle_gamma 90.000 _cell_length_a 14.8305 _cell_length_b 8.5741 _cell_length_c 17.6175 _exptl_crystal_F_000 1000.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file Compound6.fcf _[local]_cod_data_source_block an205 _shelx_title ' AN410 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 250.32 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4983.00 5064.03 211.92 o 4 0 0 37232.45 38659.12 1582.89 o 6 0 0 4267.18 4423.01 157.72 o 8 0 0 1929.70 1880.32 78.70 o 10 0 0 243.72 257.05 31.52 o 12 0 0 1577.83 1603.67 122.77 o 14 0 0 38.86 31.45 17.38 o 16 0 0 194.46 183.25 32.39 o 2 1 0 1367.99 1402.64 52.31 o 3 1 0 18.15 23.58 4.42 o 4 1 0 3372.53 3185.62 88.64 o 5 1 0 590.61 593.26 23.35 o 6 1 0 946.34 1106.96 43.00 o 7 1 0 8172.67 9065.65 249.20 o 8 1 0 2489.41 2572.68 79.85 o 9 1 0 541.20 535.76 30.85 o 10 1 0 228.45 208.12 19.63 o 11 1 0 886.79 897.89 40.35 o 12 1 0 275.70 266.66 22.49 o 13 1 0 478.18 482.04 40.59 o 14 1 0 105.84 99.19 16.32 o 15 1 0 490.78 465.33 39.94 o 16 1 0 9.20 13.42 13.90 o 0 2 0 146.33 140.44 30.32 o 1 2 0 2125.59 2275.57 108.85 o 3 2 0 12226.09 13186.54 446.55 o 4 2 0 1098.48 1209.97 51.20 o 5 2 0 0.07 1.03 5.64 o 6 2 0 10844.75 11540.60 339.61 o 7 2 0 215.99 253.72 29.25 o 8 2 0 1863.36 2011.18 66.14 o 9 2 0 1.53 1.56 6.57 o 10 2 0 2239.13 2187.62 83.42 o 11 2 0 503.28 520.78 33.74 o 12 2 0 132.44 135.50 20.84 o 13 2 0 0.05 8.60 16.09 o 14 2 0 552.62 578.90 54.44 o 15 2 0 3.67 6.24 13.63 o 16 2 0 45.01 41.44 18.04 o 1 3 0 6237.03 6282.06 188.80 o 2 3 0 14978.58 16201.66 547.68 o 4 3 0 1736.07 2033.45 99.79 o 5 3 0 1372.47 1381.66 79.02 o 6 3 0 240.87 272.60 25.57 o 7 3 0 644.66 670.07 43.18 o 8 3 0 416.74 495.40 38.37 o 9 3 0 191.70 223.48 27.46 o 10 3 0 18.09 48.40 18.04 o 11 3 0 106.72 112.91 22.69 o 12 3 0 37.71 19.12 16.06 o 13 3 0 3.85 8.29 15.82 o 14 3 0 23.42 29.86 20.44 o 15 3 0 122.83 138.08 54.72 o 0 4 0 1535.05 1398.51 71.18 o 1 4 0 27.68 30.05 6.69 o 2 4 0 118.97 108.70 14.02 o 3 4 0 91.50 142.24 16.44 o 4 4 0 4276.76 4163.08 207.07 o 6 4 0 110.33 148.44 20.14 o 7 4 0 337.51 268.21 27.83 o 8 4 0 2672.69 2688.55 125.50 o 9 4 0 2.62 4.62 11.90 o 10 4 0 2.28 29.08 16.39 o 11 4 0 95.83 96.23 22.16 o 12 4 0 233.43 279.86 36.84 o 13 4 0 61.93 74.21 23.13 o 14 4 0 8.21 16.92 21.52 o 15 4 0 0.32 -5.49 21.33 o 1 5 0 283.06 302.56 21.44 o 2 5 0 322.27 368.37 24.06 o 3 5 0 1758.95 1917.99 80.97 o 4 5 0 300.67 220.72 26.61 o 5 5 0 1360.79 1282.55 70.99 o 6 5 0 222.66 191.38 29.78 o 7 5 0 146.38 112.35 47.90 o 8 5 0 21.38 13.21 12.57 o 9 5 0 170.51 163.39 25.47 o 10 5 0 862.72 826.40 60.10 o 11 5 0 71.05 57.39 19.16 o 12 5 0 0.94 24.06 17.36 o 13 5 0 98.67 135.62 31.38 o 14 5 0 5.62 37.00 23.68 o 0 6 0 46.84 37.16 13.18 o 1 6 0 156.14 195.66 29.29 o 2 6 0 2121.07 2131.84 99.87 o 3 6 0 1029.29 1091.09 71.08 o 4 6 0 71.85 81.89 21.55 o 5 6 0 0.44 -9.98 9.98 o 6 6 0 194.44 164.32 23.88 o 7 6 0 1460.13 1358.38 109.92 o 8 6 0 196.99 100.79 60.25 o 9 6 0 1.44 -2.15 14.10 o 10 6 0 370.06 408.36 42.58 o 11 6 0 13.89 30.50 20.19 o 12 6 0 105.73 129.92 29.10 o 13 6 0 22.20 42.02 41.75 o 1 7 0 31.33 40.08 19.18 o 2 7 0 44.65 71.42 21.58 o 3 7 0 586.52 667.77 47.76 o 4 7 0 193.73 151.94 24.05 o 5 7 0 11.07 10.74 18.69 o 6 7 0 39.66 45.41 19.34 o 7 7 0 2.17 -0.59 18.36 o 8 7 0 107.16 157.18 35.20 o 9 7 0 199.23 258.01 44.81 o 10 7 0 126.03 44.89 44.04 o 11 7 0 512.36 475.34 75.58 o 0 8 0 18.69 3.65 22.85 o 1 8 0 230.46 269.57 39.71 o 2 8 0 257.43 248.52 80.11 o 3 8 0 331.33 257.73 80.38 o 4 8 0 569.86 728.06 68.97 o 5 8 0 4.82 3.38 17.56 o 6 8 0 19.16 16.40 21.07 o 7 8 0 48.47 52.74 25.62 o 8 8 0 67.40 41.35 27.30 o 9 8 0 4.44 11.95 26.90 o 10 8 0 10.53 2.85 26.14 o 1 9 0 133.90 166.01 36.34 o 2 9 0 7.83 13.04 19.52 o 3 9 0 71.27 89.91 27.77 o 4 9 0 1.91 20.08 21.37 o 5 9 0 230.03 249.43 43.96 o 6 9 0 41.52 38.52 41.30 o 7 9 0 48.30 24.08 26.87 o 0 10 0 2.38 -24.88 32.92 o 1 10 0 18.27 44.98 27.43 o 2 10 0 10.93 3.49 25.02 o 3 10 0 42.21 50.17 27.60 o -15 0 1 804.90 759.61 61.73 o -13 0 1 1.90 4.45 13.04 o -11 0 1 17.71 20.15 17.62 o -9 0 1 1917.04 1820.57 78.93 o -7 0 1 7947.14 8301.70 508.69 o -5 0 1 161.28 242.46 24.35 o -3 0 1 19753.36 22012.47 903.06 o 3 0 1 341.79 310.38 14.06 o 5 0 1 74.54 84.02 10.33 o 7 0 1 4375.47 4801.52 213.63 o 9 0 1 3698.14 3808.29 172.02 o 11 0 1 1147.58 1124.32 89.04 o 13 0 1 226.28 298.36 35.56 o 15 0 1 5.98 13.62 17.80 o -16 1 1 501.80 497.97 39.40 o -15 1 1 12.66 21.23 14.29 o -14 1 1 799.46 775.86 42.22 o -13 1 1 400.82 364.13 27.08 o -12 1 1 1139.61 1033.15 47.60 o -11 1 1 0.01 0.59 8.21 o -10 1 1 12.75 6.76 7.87 o -9 1 1 810.00 744.84 36.67 o -8 1 1 2780.48 2672.56 82.32 o -7 1 1 32.49 25.15 6.41 o -6 1 1 1861.48 1930.73 59.74 o -5 1 1 3199.87 3386.12 94.93 o -4 1 1 593.73 538.82 22.64 o -3 1 1 1771.52 1789.96 49.98 o -2 1 1 1823.56 1932.59 58.68 o -1 1 1 272.31 297.44 15.38 o 0 1 1 9478.49 9907.83 287.95 o 1 1 1 13874.81 15571.76 403.63 o 2 1 1 20932.50 22061.32 571.39 o 4 1 1 1481.14 1480.65 37.55 o 5 1 1 2200.06 2384.35 62.99 o 6 1 1 3172.31 2952.67 86.63 o 7 1 1 1.08 10.04 5.31 o 8 1 1 2119.06 2238.02 71.63 o 9 1 1 37.04 39.62 17.28 o 10 1 1 1118.01 963.26 39.14 o 11 1 1 314.12 306.97 22.72 o 12 1 1 59.42 49.41 11.30 o 13 1 1 1.18 -9.43 9.88 o 14 1 1 38.37 25.84 12.61 o 15 1 1 439.05 415.58 32.00 o -16 2 1 13.60 25.58 16.34 o -15 2 1 73.94 71.71 18.17 o -14 2 1 110.34 130.23 33.74 o -13 2 1 1521.75 1514.70 121.52 o -12 2 1 4.15 16.32 12.70 o -11 2 1 8.81 14.57 11.29 o -10 2 1 89.99 85.32 15.66 o -9 2 1 2945.86 2900.58 101.03 o -8 2 1 821.18 842.67 41.34 o -7 2 1 37.21 75.38 11.28 o -6 2 1 9.21 22.96 6.57 o -5 2 1 5348.51 5540.78 167.31 o -4 2 1 7158.76 8306.14 351.74 o -3 2 1 15578.49 16526.37 556.36 o -2 2 1 20448.63 21691.18 725.90 o -1 2 1 6611.59 6795.22 179.80 o 0 2 1 3394.74 3691.52 100.01 o 1 2 1 7066.62 7838.21 231.78 o 2 2 1 62658.73 64874.14 1868.34 o 3 2 1 24764.22 26639.58 893.53 o 4 2 1 230.72 262.88 17.94 o 5 2 1 1912.72 1963.96 68.56 o 6 2 1 632.33 824.81 51.46 o 7 2 1 6952.38 7293.92 199.18 o 8 2 1 29.97 26.48 7.81 o 9 2 1 1452.86 1395.53 51.78 o 10 2 1 0.10 -1.44 7.99 o 11 2 1 371.97 356.02 27.77 o 12 2 1 10.08 19.86 13.45 o 13 2 1 695.06 631.67 36.26 o 14 2 1 40.56 13.44 12.92 o 15 2 1 43.57 52.78 17.71 o -15 3 1 3.92 43.80 22.34 o -14 3 1 326.90 300.44 39.44 o -13 3 1 214.27 225.79 33.86 o -12 3 1 908.23 977.71 66.70 o -11 3 1 66.32 88.86 30.44 o -10 3 1 794.33 849.57 62.33 o -9 3 1 403.50 391.57 35.34 o -8 3 1 3007.40 2997.76 120.84 o -7 3 1 171.49 169.51 20.42 o -6 3 1 4565.41 4664.01 171.86 o -5 3 1 145.93 122.39 46.68 o -4 3 1 6282.29 6720.09 236.30 o -3 3 1 136.79 159.23 15.65 o -2 3 1 171.69 170.20 15.19 o -1 3 1 2096.15 2165.64 143.99 o 0 3 1 2974.58 2720.77 175.96 o 1 3 1 3985.61 3976.02 174.87 o 2 3 1 3968.78 4358.69 156.06 o 3 3 1 398.77 534.86 30.25 o 4 3 1 19.12 3.47 5.96 o 5 3 1 1391.07 1350.78 72.86 o 6 3 1 2045.17 2280.76 93.70 o 7 3 1 299.25 269.46 26.47 o 8 3 1 730.63 755.94 48.80 o 9 3 1 1896.98 1918.70 132.06 o 10 3 1 2.66 -3.08 12.30 o 11 3 1 2.65 5.50 14.86 o 12 3 1 192.14 192.16 30.25 o 13 3 1 603.56 548.09 50.56 o 14 3 1 4.00 10.50 25.64 o 15 3 1 5.09 21.57 18.10 o -15 4 1 361.80 367.05 45.99 o -14 4 1 147.82 153.71 30.99 o -13 4 1 53.21 19.32 20.22 o -12 4 1 377.42 458.14 47.66 o -11 4 1 870.19 958.19 65.46 o -10 4 1 424.06 324.07 36.22 o -9 4 1 27.71 18.39 13.50 o -8 4 1 170.89 176.43 22.93 o -7 4 1 1213.61 1120.81 73.78 o -6 4 1 3989.01 3836.00 320.46 o -5 4 1 20.45 32.48 9.81 o -4 4 1 96.42 116.67 14.99 o -3 4 1 2824.43 2712.15 166.18 o -2 4 1 493.42 476.54 28.65 o -1 4 1 1555.18 1479.33 76.96 o 0 4 1 81.49 102.90 10.93 o 1 4 1 12457.41 12776.46 436.95 o 2 4 1 43.98 20.48 12.06 o 3 4 1 3091.77 3454.15 160.07 o 4 4 1 6127.00 6310.37 226.12 o 5 4 1 15677.18 16550.42 567.92 o 6 4 1 1187.43 1292.86 62.20 o 7 4 1 700.91 671.51 45.96 o 8 4 1 88.23 54.71 15.14 o 9 4 1 457.26 518.75 44.08 o 10 4 1 59.37 83.34 20.65 o 11 4 1 268.12 293.56 35.45 o 12 4 1 35.46 80.51 22.84 o 13 4 1 6.35 23.37 20.01 o 14 4 1 5.88 10.71 20.70 o -14 5 1 200.91 222.81 38.04 o -13 5 1 0.60 -8.32 19.63 o -12 5 1 54.25 25.64 19.46 o -11 5 1 29.81 46.43 17.82 o -10 5 1 791.30 936.42 63.02 o -9 5 1 53.35 49.79 16.16 o -8 5 1 350.68 312.67 41.56 o -7 5 1 102.22 134.12 20.78 o -6 5 1 1146.86 1331.11 64.01 o -5 5 1 2682.05 2811.85 113.06 o -4 5 1 39.56 37.08 11.51 o -3 5 1 1.25 5.42 6.51 o -2 5 1 6913.66 7285.08 223.58 o -1 5 1 270.96 295.71 21.15 o 0 5 1 134.46 120.70 13.49 o 1 5 1 54.95 50.53 9.40 o 2 5 1 1550.89 1485.96 56.03 o 3 5 1 311.77 287.69 27.11 o 5 5 1 60.77 63.93 22.11 o 6 5 1 571.70 618.05 44.73 o 7 5 1 0.05 -9.13 11.00 o 8 5 1 338.06 315.38 33.53 o 9 5 1 166.82 202.79 28.45 o 10 5 1 513.84 467.60 44.32 o 11 5 1 4.47 19.98 17.23 o 12 5 1 23.99 20.31 19.15 o 13 5 1 93.50 107.31 28.08 o -13 6 1 225.86 274.80 70.95 o -12 6 1 8.75 43.98 25.19 o -11 6 1 34.46 15.60 16.41 o -10 6 1 265.64 119.70 76.12 o -9 6 1 222.67 292.78 48.60 o -8 6 1 344.33 371.11 37.92 o -7 6 1 106.52 129.25 33.48 o -6 6 1 410.28 397.54 35.60 o -5 6 1 939.35 909.12 110.35 o -4 6 1 198.05 195.53 36.39 o -3 6 1 1762.11 2034.11 74.88 o -2 6 1 325.75 380.13 26.82 o -1 6 1 1094.57 1073.74 46.07 o 0 6 1 21.97 19.23 9.60 o 1 6 1 251.20 245.44 22.33 o 2 6 1 397.66 502.51 31.18 o 3 6 1 90.03 99.75 14.23 o 4 6 1 4.00 3.34 10.04 o 5 6 1 188.82 174.48 23.15 o 6 6 1 79.66 41.25 29.19 o 7 6 1 20.64 24.93 14.89 o 8 6 1 330.97 420.31 41.75 o 9 6 1 511.25 559.62 50.58 o 10 6 1 8.76 12.48 16.62 o 11 6 1 170.19 241.43 36.15 o 12 6 1 12.85 28.60 23.63 o -12 7 1 196.73 250.81 47.48 o -11 7 1 0.34 3.90 23.48 o -10 7 1 13.90 -4.84 28.90 o -9 7 1 117.64 182.39 37.33 o -8 7 1 122.00 132.56 31.67 o -7 7 1 33.28 24.72 25.01 o -6 7 1 16.39 7.68 40.36 o -5 7 1 226.52 249.94 29.75 o -4 7 1 724.42 765.80 52.11 o -3 7 1 19.55 30.03 14.53 o -2 7 1 56.06 42.90 17.68 o -1 7 1 275.90 328.44 46.74 o 0 7 1 1094.48 1189.24 61.96 o 1 7 1 172.39 167.20 22.34 o 2 7 1 2.02 1.96 9.98 o 3 7 1 10.86 18.52 13.48 o 4 7 1 962.96 921.87 58.10 o 5 7 1 178.94 218.49 29.02 o 6 7 1 250.24 203.22 28.28 o 7 7 1 4.54 4.69 13.68 o 8 7 1 1280.93 1218.40 95.47 o 9 7 1 0.56 -20.79 20.79 o 10 7 1 48.92 25.73 26.71 o 11 7 1 67.73 57.27 30.66 o -10 8 1 91.35 77.77 32.98 o -9 8 1 63.44 99.00 51.95 o -8 8 1 4.41 32.08 21.53 o -7 8 1 55.63 70.98 25.52 o -6 8 1 133.35 109.86 54.65 o -5 8 1 328.42 321.68 45.29 o -4 8 1 68.69 122.87 28.92 o -3 8 1 367.39 392.85 49.09 o -2 8 1 33.15 55.09 22.75 o -1 8 1 204.18 212.90 40.53 o 0 8 1 711.97 681.80 64.30 o 1 8 1 531.01 480.76 105.79 o 2 8 1 59.38 27.10 19.16 o 3 8 1 146.50 156.37 32.10 o 4 8 1 31.72 36.71 20.10 o 5 8 1 2.10 -11.57 17.49 o 6 8 1 55.11 19.87 29.17 o 7 8 1 8.68 37.15 23.96 o 8 8 1 34.27 52.92 28.40 o 9 8 1 21.87 10.98 25.85 o -7 9 1 15.49 -17.98 36.94 o -6 9 1 26.18 15.26 36.10 o -5 9 1 106.77 164.69 35.19 o -4 9 1 33.15 67.53 27.96 o -3 9 1 19.88 27.78 39.11 o -2 9 1 203.97 196.70 44.41 o -1 9 1 3.88 -0.31 17.66 o 0 9 1 38.32 27.64 29.58 o 1 9 1 5.87 4.92 20.48 o 2 9 1 459.65 511.63 59.62 o 3 9 1 222.68 240.77 42.21 o 4 9 1 107.00 151.39 33.39 o 5 9 1 81.91 110.23 31.35 o 6 9 1 260.60 413.45 57.62 o 7 9 1 3.47 16.85 23.99 o -3 10 1 60.56 73.87 30.51 o -2 10 1 25.45 0.99 36.61 o -1 10 1 26.20 12.85 34.78 o 0 10 1 10.39 -8.11 24.52 o 1 10 1 26.78 42.47 27.60 o 2 10 1 0.84 -6.32 23.52 o -16 0 2 172.75 150.35 29.75 o -14 0 2 458.25 409.40 43.01 o -12 0 2 307.06 313.48 38.87 o -10 0 2 1162.79 1004.82 57.40 o -8 0 2 422.94 415.91 46.31 o -6 0 2 11229.78 12982.03 544.95 o -4 0 2 3753.19 4044.03 175.69 o -2 0 2 16569.14 18897.80 1091.81 o 0 0 2 773.39 790.85 51.51 o 2 0 2 1536.83 1694.91 155.12 o 4 0 2 772.81 722.96 27.62 o 6 0 2 2063.91 1905.71 64.55 o 8 0 2 2312.73 2401.20 96.39 o 10 0 2 28.67 13.09 10.62 o 12 0 2 700.88 683.56 51.23 o 14 0 2 1.66 4.50 14.89 o -16 1 2 98.40 76.01 19.22 o -15 1 2 230.91 261.81 27.53 o -14 1 2 0.81 -4.85 11.40 o -13 1 2 928.94 878.89 68.17 o -12 1 2 377.91 391.24 33.20 o -11 1 2 63.62 62.08 14.73 o -10 1 2 76.28 97.82 14.50 o -9 1 2 1673.97 1599.18 55.93 o -8 1 2 25.93 15.73 6.70 o -7 1 2 2285.72 2321.97 79.46 o -6 1 2 191.77 159.12 14.33 o -5 1 2 7844.39 8258.63 216.74 o -4 1 2 2482.01 2684.63 74.18 o -3 1 2 5173.54 5526.05 161.55 o -2 1 2 5926.75 6532.36 169.34 o -1 1 2 1169.92 1206.71 38.59 o 0 1 2 11207.21 12437.43 361.12 o 1 1 2 1596.30 1751.04 49.10 o 2 1 2 2694.57 2757.39 76.18 o 3 1 2 1412.27 1574.97 61.79 o 4 1 2 2187.30 2329.45 56.21 o 5 1 2 863.40 769.76 23.11 o 6 1 2 26.09 59.32 6.50 o 7 1 2 718.53 676.65 25.99 o 8 1 2 368.39 418.49 29.27 o 9 1 2 348.16 347.25 21.55 o 10 1 2 10.65 15.61 8.30 o 11 1 2 159.02 147.88 18.93 o 12 1 2 85.01 107.73 15.65 o 13 1 2 57.12 80.56 15.09 o 14 1 2 19.40 18.66 13.48 o 15 1 2 7.58 3.20 12.75 o -16 2 2 324.89 353.05 32.17 o -15 2 2 10.28 -7.19 12.91 o -14 2 2 619.27 614.48 46.58 o -13 2 2 4.89 14.43 13.44 o -12 2 2 1080.75 1044.23 57.09 o -11 2 2 75.64 56.12 14.51 o -10 2 2 453.28 476.74 34.29 o -9 2 2 610.77 616.26 37.22 o -8 2 2 493.97 486.50 31.03 o -7 2 2 638.04 746.99 40.42 o -6 2 2 648.36 651.44 31.36 o -5 2 2 595.76 722.63 28.61 o -4 2 2 4342.94 4515.16 137.62 o -3 2 2 982.09 1079.98 37.67 o -2 2 2 2032.05 2005.74 63.57 o -1 2 2 618.19 591.88 22.87 o 0 2 2 880.43 967.98 34.21 o 1 2 2 9.48 7.28 3.67 o 2 2 2 599.64 652.69 26.19 o 3 2 2 6547.50 6733.60 181.39 o 4 2 2 388.73 354.02 19.07 o 5 2 2 73.41 82.80 11.49 o 6 2 2 1161.42 976.28 41.30 o 7 2 2 8.44 10.78 6.86 o 8 2 2 2.92 2.76 7.82 o 9 2 2 585.42 627.27 39.82 o 10 2 2 2452.10 2317.58 88.88 o 11 2 2 16.23 23.58 14.74 o 12 2 2 379.94 392.73 44.02 o 13 2 2 171.13 146.15 20.43 o 14 2 2 480.27 425.25 34.34 o 15 2 2 0.08 25.26 16.05 o -16 3 2 50.17 30.67 44.62 o -15 3 2 296.92 312.92 42.14 o -14 3 2 423.12 447.93 46.95 o -13 3 2 412.73 448.49 45.44 o -12 3 2 58.48 89.95 21.35 o -11 3 2 2940.58 2836.35 121.77 o -10 3 2 996.79 1013.41 77.76 o -9 3 2 294.62 268.68 28.71 o -8 3 2 2389.47 2304.58 96.74 o -7 3 2 3221.42 3240.77 252.25 o -6 3 2 296.95 227.73 44.55 o -5 3 2 987.42 910.19 43.25 o -4 3 2 137.61 119.12 13.58 o -3 3 2 19.31 17.52 5.25 o -2 3 2 1035.25 1120.20 38.11 o -1 3 2 3506.19 3689.65 114.06 o 0 3 2 2573.70 2717.21 77.48 o 1 3 2 3350.79 3277.12 104.25 o 2 3 2 2792.92 2704.31 88.49 o 3 3 2 290.06 318.79 30.48 o 4 3 2 18.51 41.25 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