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Information card for entry 4087351
Preview
| Coordinates | 4087351.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | (DME)potassium 2,3,4,5-tetraethylarsolide |
|---|---|
| Formula | C44 H80 As3 K3 O4 |
| Calculated formula | C44 H80 As3 K3 O4 |
| Title of publication | Synthesis and Spectroscopic and Structural Investigations of the 2,3,4,5-Tetraethylarsolides and -stibolides of the Alkali Metals Sodium, Potassium, Rubidium, and Cesium |
| Authors of publication | Westerhausen, Matthias; Ossberger, Manfred W.; Mayer, Peter; Piotrowski, Holger; Nöth, Heinrich |
| Journal of publication | Organometallics |
| Year of publication | 2004 |
| Journal volume | 23 |
| Journal issue | 14 |
| Pages of publication | 3417 - 3424 |
| a | 9.835 ± 0.0009 Å |
| b | 16.6544 ± 0.0013 Å |
| c | 32.621 ± 0.004 Å |
| α | 90° |
| β | 102.767 ± 0.012° |
| γ | 90° |
| Cell volume | 5211.1 ± 0.9 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0871 |
| Residual factor for significantly intense reflections | 0.0467 |
| Weighted residual factors for significantly intense reflections | 0.1002 |
| Weighted residual factors for all reflections included in the refinement | 0.1119 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.894 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 209875 (current) | 2018-08-17 | cif/ Adding structures of 4087351 via cif-deposit CGI script. |
4087351.cif |
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