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Information card for entry 4517164
Preview
| Coordinates | 4517164.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C25 H29 N S |
|---|---|
| Calculated formula | C25 H29 N S |
| Title of publication | Diastereo- and Enantioselective CuH-Catalyzed Hydroamination of Strained Trisubstituted Alkenes |
| Authors of publication | Feng, Sheng; Hao, Hua; Liu, Peng; Buchwald, Stephen L. |
| Journal of publication | ACS Catalysis |
| Year of publication | 2019 |
| Pages of publication | 282 |
| a | 13.0414 ± 0.0011 Å |
| b | 5.7208 ± 0.0004 Å |
| c | 14.1145 ± 0.0012 Å |
| α | 90° |
| β | 93.997 ± 0.004° |
| γ | 90° |
| Cell volume | 1050.48 ± 0.15 Å3 |
| Cell temperature | 99 ± 2 K |
| Ambient diffraction temperature | 99 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0454 |
| Residual factor for significantly intense reflections | 0.044 |
| Weighted residual factors for significantly intense reflections | 0.1092 |
| Weighted residual factors for all reflections included in the refinement | 0.1098 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.125 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 245061 (current) | 2019-12-14 | cif/ Adding structures of 4517164 via cif-deposit CGI script. |
4517164.cif |
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