#------------------------------------------------------------------------------ #$Date: 2025-09-04 17:44:29 +0300 (Thu, 04 Sep 2025) $ #$Revision: 302010 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/95/4519501.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519501 _cell_angle_alpha 90.000 _cell_angle_beta 94.322 _cell_angle_gamma 90.000 _cell_length_a 18.1007 _cell_length_b 4.0084 _cell_length_c 11.4184 _exptl_crystal_F_000 390.96 _reflns_d_resolution_high 0.7499 _cod_data_source_file 06-1c_1d_047RZ1F_053TZ_jw27471.fcf _cod_data_source_block jw27471 _shelx_title ' jw27471_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 85.91 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 533.66 527.17 30.11 o 3 0 0 707.10 673.89 38.49 o 4 0 0 1209.27 1131.66 64.72 o 5 0 0 99.74 95.24 2.09 o 6 0 0 1.11 4.38 0.15 o 7 0 0 5107.12 4402.89 249.43 o 8 0 0 157.82 187.74 3.40 o 9 0 0 1951.13 1843.74 86.94 o 10 0 0 388.62 534.50 10.11 o 11 0 0 629.15 597.80 11.46 o 12 0 0 44.38 51.33 1.21 o 13 0 0 180.65 157.93 3.33 o 14 0 0 1297.39 1285.92 27.55 o 15 0 0 241.73 213.08 5.17 o 16 0 0 1.55 2.74 0.25 o 17 0 0 8.11 11.06 1.15 o 18 0 0 29.87 33.12 1.10 o 19 0 0 117.74 99.73 3.40 o 20 0 0 25.21 26.83 0.95 o 21 0 0 163.26 166.90 4.81 o 22 0 0 152.45 172.09 6.27 o 23 0 0 12.19 16.11 0.73 o 24 0 0 7.95 9.01 0.48 o 1 1 0 2172.29 2125.45 85.04 o 3 1 0 2964.63 2840.00 92.75 o 4 1 0 509.67 467.16 8.84 o 5 1 0 128.98 117.79 2.48 o 6 1 0 1876.82 1776.09 50.30 o 7 1 0 1.60 1.79 0.13 o 8 1 0 392.30 374.33 5.50 o 9 1 0 251.36 218.30 2.88 o 10 1 0 38.81 36.18 0.47 o 11 1 0 107.75 100.03 1.37 o 12 1 0 26.27 21.35 0.32 o 13 1 0 998.66 915.42 12.97 o 14 1 0 33.70 31.97 0.47 o 15 1 0 294.57 273.05 3.99 o 16 1 0 722.13 628.79 9.49 o 17 1 0 133.23 130.32 2.61 o 18 1 0 5.89 6.33 0.46 o 19 1 0 19.13 21.42 0.42 o 20 1 0 151.46 166.08 4.51 o 21 1 0 0.19 0.08 0.11 o 22 1 0 6.98 8.70 0.27 o 23 1 0 18.33 13.62 0.53 o 0 2 0 154.46 122.03 3.55 o 1 2 0 947.17 916.83 15.61 o 2 2 0 0.76 0.94 0.09 o 3 2 0 7.54 6.92 0.18 o 4 2 0 441.21 459.24 6.50 o 5 2 0 48.79 43.24 0.62 o 6 2 0 352.90 308.53 3.95 o 7 2 0 320.29 315.54 3.94 o 8 2 0 428.99 421.15 5.12 o 9 2 0 5.92 6.23 0.17 o 10 2 0 229.49 227.84 2.70 o 11 2 0 57.97 50.60 0.75 o 12 2 0 250.93 243.23 3.24 o 13 2 0 662.13 640.55 8.37 o 14 2 0 903.49 884.76 12.15 o 15 2 0 89.18 82.56 1.23 o 16 2 0 66.02 64.31 0.95 o 17 2 0 65.22 61.44 0.94 o 18 2 0 47.01 43.52 0.71 o 19 2 0 19.86 19.71 0.46 o 20 2 0 11.21 11.23 0.36 o 21 2 0 15.40 16.93 0.57 o 22 2 0 11.09 12.88 0.63 o 1 3 0 5.05 5.13 0.17 o 2 3 0 33.82 36.01 0.59 o 3 3 0 16.32 16.47 0.33 o 4 3 0 0.05 0.34 0.10 o 5 3 0 51.84 52.34 0.76 o 6 3 0 13.74 11.15 0.24 o 7 3 0 0.92 1.06 0.09 o 8 3 0 41.63 43.35 0.64 o 9 3 0 35.19 35.49 0.53 o 10 3 0 0.97 1.03 0.09 o 11 3 0 7.68 7.02 0.22 o 12 3 0 37.40 39.04 0.61 o 13 3 0 0.12 0.35 0.09 o 14 3 0 0.13 0.25 0.08 o 15 3 0 0.20 0.16 0.10 o 16 3 0 17.04 18.05 0.42 o 17 3 0 17.60 16.94 0.50 o 18 3 0 3.53 3.48 0.30 o 19 3 0 5.61 5.79 0.34 o 0 4 0 7.09 7.22 0.51 o 1 4 0 2.99 2.69 0.28 o 2 4 0 39.95 42.80 0.82 o 3 4 0 1.55 6.02 1.15 o 4 4 0 39.50 40.07 0.74 o 5 4 0 10.40 11.39 0.32 o 6 4 0 15.57 15.54 0.39 o 7 4 0 1.64 1.53 0.13 o 8 4 0 1.19 1.17 0.12 o 9 4 0 3.56 2.86 0.19 o 10 4 0 3.69 3.36 0.23 o 11 4 0 16.35 17.36 0.62 o 12 4 0 77.15 79.67 1.78 o 13 4 0 17.33 17.12 0.51 o 14 4 0 39.93 39.20 0.99 o 15 4 0 2.97 1.91 0.20 o 1 5 0 11.29 11.61 0.62 o 2 5 0 11.42 13.20 0.65 o 3 5 0 2.41 2.60 0.38 o 4 5 0 3.18 2.84 0.27 o 5 5 0 1.83 2.06 0.25 o 6 5 0 1.27 1.24 0.23 o 7 5 0 0.03 0.00 0.22 o 8 5 0 2.53 2.49 0.30 o -23 1 1 2.17 3.14 0.19 o -22 1 1 11.68 13.09 0.36 o -21 1 1 11.83 12.14 0.34 o -20 1 1 8.01 6.27 0.48 o -19 1 1 60.21 55.95 2.60 o -18 1 1 30.20 24.63 0.63 o -17 1 1 187.44 162.34 2.52 o -16 1 1 4.25 3.26 0.12 o -15 1 1 8.53 7.20 0.19 o -14 1 1 100.44 99.66 1.46 o -13 1 1 145.20 146.85 2.04 o -12 1 1 10.65 10.29 0.22 o -11 1 1 1.75 0.77 0.12 o -10 1 1 799.03 835.51 12.70 o -9 1 1 1603.04 1495.21 28.21 o -8 1 1 200.05 206.21 3.09 o -7 1 1 52.34 64.63 1.35 o -6 1 1 455.98 473.51 8.54 o -5 1 1 752.73 695.46 14.66 o -4 1 1 106.62 112.85 2.33 o -3 1 1 111.52 107.15 1.97 o -2 1 1 136.61 119.02 2.71 o -1 1 1 497.54 509.23 10.16 o 1 1 1 111.74 131.10 2.80 o 2 1 1 2671.04 2553.55 102.20 o 3 1 1 228.63 205.51 3.13 o 4 1 1 707.87 703.76 16.32 o 5 1 1 1059.52 987.19 28.10 o 6 1 1 48.36 46.87 0.92 o 7 1 1 5.70 4.39 0.17 o 8 1 1 763.21 833.34 13.62 o 9 1 1 226.29 226.18 3.07 o 10 1 1 604.17 658.48 8.60 o 11 1 1 13.14 11.98 0.29 o 12 1 1 836.29 792.37 11.94 o 13 1 1 2.94 1.93 0.25 o 14 1 1 81.46 80.09 1.06 o 15 1 1 1.89 1.54 0.95 o 16 1 1 137.75 128.93 1.78 o 17 1 1 3.56 2.16 0.15 o 18 1 1 20.19 16.62 0.33 o 19 1 1 32.59 30.44 0.49 o 20 1 1 11.77 10.67 0.29 o 21 1 1 7.16 8.73 0.39 o 22 1 1 0.69 1.39 0.14 o 23 1 1 53.24 65.91 2.21 o -22 2 1 55.70 58.82 3.62 o -21 2 1 7.38 6.82 0.31 o -20 2 1 0.93 1.26 0.12 o -19 2 1 46.99 43.89 0.75 o -18 2 1 81.02 81.43 1.31 o -17 2 1 1.29 0.89 0.09 o -16 2 1 12.94 12.24 0.26 o -15 2 1 59.23 61.64 1.00 o -14 2 1 10.43 11.28 0.32 o -13 2 1 29.39 28.07 0.54 o -12 2 1 200.73 192.14 2.80 o -11 2 1 301.01 293.74 4.12 o -10 2 1 35.41 33.18 0.51 o -9 2 1 1.13 1.54 0.10 o -8 2 1 936.55 895.57 11.94 o -7 2 1 211.73 207.49 2.82 o -6 2 1 259.74 238.71 3.05 o -5 2 1 275.17 250.71 3.38 o -4 2 1 967.11 944.63 11.93 o -3 2 1 630.90 601.71 7.62 o -2 2 1 6.90 8.78 0.24 o -1 2 1 427.23 380.86 6.46 o 0 2 1 123.76 151.53 3.93 o 1 2 1 166.55 153.44 3.35 o 2 2 1 9.33 13.10 0.29 o 3 2 1 126.45 120.98 2.46 o 4 2 1 855.45 862.01 10.88 o 5 2 1 20.88 22.05 0.39 o 6 2 1 447.55 450.69 5.47 o 7 2 1 247.58 251.01 3.15 o 8 2 1 264.18 256.69 3.23 o 9 2 1 192.35 190.43 2.35 o 10 2 1 627.85 642.89 7.78 o 11 2 1 290.69 285.78 3.66 o 12 2 1 75.88 75.45 1.03 o 13 2 1 8.55 7.32 0.20 o 14 2 1 1.88 1.77 0.12 o 15 2 1 228.43 228.05 3.19 o 16 2 1 36.05 35.08 0.63 o 17 2 1 62.81 62.95 0.96 o 18 2 1 164.55 162.83 2.46 o 19 2 1 0.98 0.72 0.12 o 20 2 1 7.27 6.16 0.26 o 21 2 1 65.03 76.38 3.14 o 22 2 1 34.20 39.82 1.67 o -19 3 1 55.02 52.05 1.93 o -18 3 1 0.16 -0.09 0.11 o -17 3 1 24.23 23.71 0.64 o -16 3 1 45.78 47.42 0.90 o -15 3 1 10.57 9.92 0.24 o -14 3 1 41.10 43.57 0.72 o -13 3 1 75.54 80.21 1.26 o -12 3 1 432.27 462.36 7.01 o -11 3 1 7.53 7.57 0.21 o -10 3 1 193.70 205.28 2.88 o -9 3 1 299.79 317.62 4.54 o -8 3 1 43.78 44.05 0.67 o -7 3 1 71.17 74.29 1.16 o -6 3 1 349.20 367.21 5.08 o -5 3 1 532.08 541.61 7.69 o -4 3 1 240.26 245.32 3.51 o -3 3 1 285.28 283.10 4.31 o -2 3 1 80.39 75.69 1.16 o -1 3 1 109.95 106.28 1.66 o 0 3 1 4.17 4.44 0.20 o 1 3 1 146.54 142.55 2.46 o 2 3 1 355.90 347.16 5.26 o 3 3 1 2.30 1.93 0.10 o 4 3 1 889.43 904.05 14.14 o 5 3 1 386.55 405.09 6.93 o 6 3 1 45.18 41.85 0.81 o 7 3 1 0.99 0.92 0.09 o 8 3 1 232.68 249.22 3.67 o 9 3 1 229.24 240.49 3.33 o 10 3 1 143.80 152.88 2.14 o 11 3 1 21.90 22.68 0.41 o 12 3 1 15.67 16.60 0.32 o 13 3 1 229.36 241.11 3.44 o 14 3 1 245.43 253.45 3.51 o 15 3 1 42.38 43.61 0.68 o 16 3 1 7.47 8.38 0.29 o 17 3 1 40.24 40.17 1.50 o 18 3 1 0.70 0.55 0.26 o 19 3 1 35.04 31.14 2.04 o -16 4 1 2.00 1.58 0.43 o -15 4 1 14.08 14.23 0.58 o -14 4 1 19.66 20.34 0.58 o -13 4 1 0.18 -0.05 0.15 o -12 4 1 42.52 44.29 1.09 o -11 4 1 55.04 59.81 1.62 o -10 4 1 13.80 14.59 0.40 o -9 4 1 10.22 10.43 0.35 o -8 4 1 70.90 76.00 1.52 o -7 4 1 61.71 67.00 1.42 o -6 4 1 12.88 13.58 0.36 o -5 4 1 45.00 50.08 1.05 o -4 4 1 143.22 146.46 2.68 o -3 4 1 160.74 168.88 3.57 o -1 4 1 44.48 49.08 0.90 o 0 4 1 15.29 18.62 0.61 o 1 4 1 9.61 11.39 0.54 o 2 4 1 12.03 13.14 0.41 o 3 4 1 63.74 69.31 1.37 o 4 4 1 151.57 161.15 3.28 o 5 4 1 0.09 0.00 0.12 o 6 4 1 80.30 87.02 1.71 o 7 4 1 117.04 124.84 2.30 o 8 4 1 55.83 61.87 1.12 o 9 4 1 25.93 28.08 0.58 o 10 4 1 162.25 173.30 3.32 o 11 4 1 103.10 111.66 2.46 o 12 4 1 0.01 0.20 0.12 o 13 4 1 0.50 0.42 0.13 o 14 4 1 3.94 4.29 0.29 o 15 4 1 21.44 20.41 0.77 o -8 5 1 0.74 0.19 0.22 o -7 5 1 4.68 4.49 0.40 o -6 5 1 16.57 17.11 0.70 o -5 5 1 18.34 20.23 0.74 o -4 5 1 9.02 8.85 0.57 o -2 5 1 20.39 25.69 1.24 o -1 5 1 13.36 27.53 1.86 o 0 5 1 31.80 38.60 1.41 o 1 5 1 4.59 21.72 1.58 o 2 5 1 19.02 22.96 0.79 o 5 5 1 19.97 23.04 0.71 o 6 5 1 7.79 8.18 0.44 o 7 5 1 0.29 0.13 0.20 o 8 5 1 26.20 28.70 0.92 o -24 0 2 15.30 17.99 1.15 o -23 0 2 50.88 44.65 5.02 o -22 0 2 24.69 25.66 1.23 o -21 0 2 129.58 148.03 3.86 o -20 0 2 18.62 24.67 0.64 o -19 0 2 39.87 52.34 1.26 o -18 0 2 125.48 124.54 3.67 o -17 0 2 353.69 297.64 7.15 o -16 0 2 926.71 839.67 22.71 o -15 0 2 1052.67 949.62 26.46 o -14 0 2 916.82 830.92 17.71 o -13 0 2 9.30 5.23 0.16 o -12 0 2 362.99 339.26 7.76 o -11 0 2 363.15 304.26 6.57 o -10 0 2 1789.17 1694.64 42.80 o -9 0 2 416.01 473.71 10.18 o -8 0 2 1913.81 1715.25 68.85 o -7 0 2 3227.34 2819.53 160.27 o -6 0 2 18.05 15.14 0.57 o -5 0 2 18.93 25.55 0.66 o -4 0 2 955.43 902.58 46.52 o -3 0 2 492.74 453.31 14.73 o 0 0 2 1259.42 1512.69 85.94 o 1 0 2 3296.48 3633.24 205.56 o 4 0 2 124.53 128.17 3.45 o 5 0 2 66.90 76.12 3.27 o 6 0 2 2252.09 2395.14 136.68 o 7 0 2 3026.11 3231.08 184.06 o 8 0 2 349.86 431.08 8.69 o 9 0 2 129.15 165.86 3.42 o 10 0 2 2400.70 2426.32 98.36 o 11 0 2 48.94 53.04 1.15 o 12 0 2 536.31 545.75 11.15 o 13 0 2 560.39 528.98 10.07 o 14 0 2 2209.90 1966.52 63.93 o 15 0 2 2.28 1.14 6.81 o 16 0 2 61.05 48.50 1.10 o 17 0 2 488.79 435.15 8.71 o 18 0 2 238.32 203.13 5.67 o 19 0 2 28.59 25.65 2.52 o 20 0 2 70.87 72.72 2.37 o 21 0 2 104.36 113.53 3.75 o 22 0 2 4.76 3.35 0.25 o 23 0 2 18.17 28.96 1.72 o -23 1 2 18.42 21.51 1.29 o -22 1 2 0.67 0.82 0.14 o -21 1 2 60.60 65.21 1.55 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o 17 1 2 55.08 52.27 0.78 o 18 1 2 2.01 1.45 0.18 o 19 1 2 162.51 150.98 2.70 o 20 1 2 53.04 49.81 1.62 o 21 1 2 0.47 0.25 0.15 o 22 1 2 31.62 31.86 1.37 o 23 1 2 148.55 178.39 7.15 o -22 2 2 33.61 35.46 3.62 o -21 2 2 65.31 72.33 2.62 o -20 2 2 0.01 0.16 0.10 o -19 2 2 9.65 9.63 0.25 o -18 2 2 23.23 23.78 0.40 o -17 2 2 31.54 30.35 0.52 o -16 2 2 39.33 37.37 0.91 o -15 2 2 259.26 249.97 4.45 o -14 2 2 13.85 13.13 0.40 o -13 2 2 366.04 353.46 4.92 o -12 2 2 9.18 10.42 0.23 o -11 2 2 95.72 88.15 1.31 o -10 2 2 8.81 6.67 0.17 o -9 2 2 118.20 120.94 1.91 o -8 2 2 199.69 175.35 2.46 o -7 2 2 333.18 314.08 4.22 o -6 2 2 1.29 2.97 0.11 o -5 2 2 1.38 0.80 0.09 o -4 2 2 1140.82 1101.51 16.04 o -3 2 2 184.26 177.81 2.28 o -2 2 2 187.92 195.68 3.87 o -1 2 2 188.45 192.85 3.16 o 0 2 2 2170.55 2399.68 81.12 o 1 2 2 439.49 473.42 10.12 o 2 2 2 362.42 385.36 6.92 o 3 2 2 423.03 410.75 6.01 o 4 2 2 1269.32 1356.46 18.01 o 5 2 2 41.84 50.37 0.68 o 6 2 2 488.61 496.86 6.48 o 7 2 2 194.77 185.41 2.41 o 8 2 2 29.87 24.54 0.35 o 9 2 2 63.08 60.00 0.80 o 10 2 2 30.60 37.21 0.50 o 11 2 2 30.46 29.16 0.47 o 12 2 2 53.88 49.24 0.70 o 13 2 2 100.28 92.71 1.23 o 14 2 2 35.10 34.13 0.50 o 15 2 2 50.64 50.91 0.72 o 16 2 2 139.39 129.71 1.91 o 17 2 2 66.58 64.09 0.98 o 18 2 2 8.91 8.91 0.45 o 19 2 2 7.32 6.62 0.33 o 20 2 2 34.93 43.77 1.50 o 21 2 2 27.82 31.58 2.11 o -19 3 2 4.92 5.21 0.40 o -18 3 2 1.15 1.01 0.15 o -17 3 2 0.35 0.60 0.14 o -16 3 2 0.09 0.14 0.10 o -15 3 2 1.39 1.26 0.10 o -14 3 2 10.28 10.28 0.30 o -13 3 2 39.49 39.34 0.62 o -12 3 2 64.19 63.96 0.98 o -11 3 2 0.49 0.94 0.10 o -10 3 2 4.71 4.40 0.16 o -9 3 2 19.39 20.27 0.37 o -8 3 2 10.47 11.88 0.27 o -7 3 2 55.75 60.84 0.96 o -6 3 2 71.53 69.25 1.12 o -5 3 2 107.81 110.60 1.54 o -4 3 2 2.66 3.34 0.13 o -3 3 2 1.52 1.60 0.09 o -2 3 2 1.46 1.51 0.09 o -1 3 2 7.77 10.58 0.22 o 0 3 2 32.84 29.75 0.48 o 1 3 2 61.69 69.74 1.08 o 2 3 2 262.45 275.47 3.93 o 3 3 2 14.63 15.62 0.32 o 4 3 2 0.75 0.66 0.11 o 5 3 2 7.30 7.00 0.20 o 6 3 2 0.51 0.63 0.12 o 7 3 2 15.46 15.58 0.36 o 8 3 2 34.28 36.53 0.72 o 9 3 2 70.48 72.35 1.24 o 10 3 2 1.95 1.75 0.14 o 11 3 2 3.33 4.09 0.16 o 12 3 2 2.13 2.14 0.12 o 13 3 2 0.27 0.47 0.09 o 14 3 2 4.46 3.56 0.21 o 15 3 2 38.41 38.29 0.84 o 16 3 2 37.21 37.74 0.82 o 17 3 2 2.44 2.48 0.14 o 18 3 2 0.45 0.22 0.19 o 19 3 2 3.35 3.12 0.30 o -15 4 2 15.41 14.57 0.90 o -14 4 2 13.36 12.27 0.52 o -13 4 2 122.72 125.58 4.32 o -12 4 2 7.07 5.96 0.38 o -11 4 2 17.67 14.61 0.58 o -10 4 2 0.08 -0.13 0.15 o -9 4 2 0.12 0.03 0.12 o -8 4 2 1.78 1.21 0.13 o -7 4 2 0.02 0.01 0.11 o -6 4 2 0.03 0.11 0.12 o -5 4 2 5.14 4.81 0.26 o -4 4 2 50.48 52.85 1.07 o -3 4 2 29.32 29.45 0.72 o -2 4 2 6.94 6.26 0.30 o -1 4 2 3.15 2.22 0.21 o 0 4 2 46.52 49.87 0.98 o 2 4 2 3.71 3.17 0.23 o 3 4 2 0.12 0.26 0.14 o 4 4 2 30.55 31.81 0.61 o 5 4 2 5.98 6.75 0.33 o 6 4 2 0.34 0.48 0.11 o 7 4 2 0.36 0.20 0.11 o 8 4 2 0.42 0.23 0.11 o 9 4 2 1.00 0.55 0.12 o 10 4 2 14.25 13.63 0.37 o 11 4 2 0.06 0.02 0.11 o 12 4 2 5.10 4.64 0.22 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