#------------------------------------------------------------------------------ #$Date: 2023-07-05 11:47:04 +0300 (Wed, 05 Jul 2023) $ #$Revision: 284837 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/13/17/7131724.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7131724 loop_ _publ_author_name 'Yang, Zhongzhen' 'Tam, Jerry K. F.' 'Wootton, Jack M.' 'Lynam, Jason M.' 'Unsworth, William P.' _publ_section_title ; Ring expansion reactions of PO-containing molecules. ; _journal_issue 51 _journal_name_full 'Chemical communications (Cambridge, England)' _journal_page_first 7927 _journal_page_last 7930 _journal_paper_doi 10.1039/d3cc02087h _journal_volume 59 _journal_year 2023 _chemical_formula_moiety 'C20 H18 N O4 P' _chemical_formula_sum 'C20 H18 N O4 P' _chemical_formula_weight 367.32 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary dual _audit_creation_date 2023-05-02 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2023-05-02 deposited with the CCDC. 2023-05-30 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 93.0143(14) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.34363(18) _cell_length_b 9.78579(15) _cell_length_c 15.6829(2) _cell_measurement_reflns_used 6431 _cell_measurement_temperature 110.00(10) _cell_measurement_theta_max 75.7680 _cell_measurement_theta_min 4.6850 _cell_volume 1738.49(4) _computing_cell_refinement 'CrysAlisPro 1.171.42.73a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.73a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.73a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 110.00(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -63.00 -7.00 0.50 0.15 -- -47.17 59.00-111.00 112 2 \w -118.00 -31.00 0.50 0.15 -- -47.17 -59.00 108.00 174 3 \w -6.00 20.00 0.50 0.15 -- -47.17 59.00-111.00 52 4 \w 93.00 178.00 0.50 0.60 -- 107.75 59.00-111.00 170 5 \w 37.00 121.00 0.50 0.60 -- 107.75 -59.00 108.00 168 6 \w 9.00 39.00 0.50 0.15 -- 47.17 -59.00 108.00 60 7 \w 63.00 116.00 0.50 0.15 -- 47.17 178.00 30.00 106 8 \w 67.00 92.00 0.50 0.15 -- 47.17 178.00-180.00 50 9 \w 65.00 120.00 0.50 0.15 -- 47.17 178.00 150.00 110 10 \w 38.00 120.00 0.50 0.60 -- 107.75 -37.00-120.00 164 11 \w 42.00 72.00 0.50 0.60 -- 107.75 -99.00-120.00 60 12 \w 56.00 112.00 0.50 0.60 -- 107.75-125.00 120.00 112 13 \w 76.00 112.00 0.50 0.60 -- 107.75 -19.00 -60.00 72 14 \w 43.00 71.00 0.50 0.60 -- 107.75 -19.00 -60.00 56 15 \w 97.00 168.00 0.50 0.60 -- 107.75 19.00-150.00 142 16 \w 58.00 83.00 0.50 0.60 -- 107.75 -99.00-180.00 50 17 \w 63.00 108.00 0.50 0.60 -- 107.75-125.00 0.00 90 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0152477000 _diffrn_orient_matrix_UB_12 0.1101106000 _diffrn_orient_matrix_UB_13 -0.0698099000 _diffrn_orient_matrix_UB_21 -0.1345948000 _diffrn_orient_matrix_UB_22 -0.0020181000 _diffrn_orient_matrix_UB_23 0.0088198000 _diffrn_orient_matrix_UB_31 0.0121395000 _diffrn_orient_matrix_UB_32 0.1125083000 _diffrn_orient_matrix_UB_33 0.0687347000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0321 _diffrn_reflns_av_unetI/netI 0.0308 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -4 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 9824 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 67.049 _diffrn_reflns_theta_max 67.049 _diffrn_reflns_theta_min 4.696 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 1.629 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.684 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.73a (Rigaku Oxford Diffraction, 2022) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.403 _exptl_crystal_description irregular _exptl_crystal_F_000 768 _exptl_crystal_recrystallization_method 'evaporation of an ethyl acetate solution' _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.146 _exptl_crystal_size_min 0.084 _refine_diff_density_max 0.312 _refine_diff_density_min -0.417 _refine_diff_density_rms 0.055 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.042 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 307 _refine_ls_number_reflns 3108 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.042 _refine_ls_R_factor_all 0.0333 _refine_ls_R_factor_gt 0.0305 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0367P)^2^+0.6828P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0763 _refine_ls_wR_factor_ref 0.0780 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2842 _reflns_number_total 3108 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d3cc02087h2.cif _cod_data_source_block wpu23008 _cod_depositor_comments 'Adding full bibliography for 7131724.cif.' _cod_original_cell_volume 1738.49(5) _cod_database_code 7131724 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C20 H18 N1 O4 P1' _chemical_oxdiff_usercomment 'Zhongzhen Yang YZZ0306-R1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.881 _shelx_estimated_absorpt_t_min 0.758 _olex2_refinement_description ; ; _shelx_res_file ; TITL wpu23008_a.res in P2(1)/n wpu23008.res created by SHELXL-2018/3 at 12:46:51 on 02-May-2023 REM Old TITL wpu23008 in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.089, Rweak 0.006, Alpha 0.018 REM 0.314 for 206 systematic absences, Orientation as input REM Formula found by SHELXT: C20 N O4 P CELL 1.54184 11.343625 9.785794 15.682859 90 93.0143 90 ZERR 4 0.000179 0.00015 0.000224 0 0.0014 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H N O P UNIT 80 72 4 16 4 EQIV $1 -X,1-Y,1-Z L.S. 8 PLAN 5 SIZE 0.08 0.15 0.18 TEMP -163 CONF HTAB N1 O4_$1 BOND list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.036700 0.682800 FVAR 3.76459 C1 1 0.122819 0.776862 0.512079 11.00000 0.01403 0.01395 = 0.02055 -0.00203 -0.00162 0.00090 C2 1 0.148009 0.857619 0.440371 11.00000 0.01369 0.01692 = 0.02090 -0.00024 -0.00147 0.00275 C3 1 0.154609 0.802634 0.356721 11.00000 0.02482 0.01800 = 0.02129 0.00047 0.00115 0.00242 H3 2 0.148391 0.707126 0.349560 11.00000 0.01980 C4 1 0.179691 0.885964 0.289341 11.00000 0.03457 0.02556 = 0.02053 0.00133 0.00075 -0.00183 H4 2 0.185273 0.849035 0.232715 11.00000 0.02832 C5 1 0.193655 1.028568 0.301864 11.00000 0.03193 0.02221 = 0.02853 0.00706 0.00623 0.00231 H5 2 0.212430 1.084913 0.252931 11.00000 0.02635 C6 1 0.191704 1.083383 0.382001 11.00000 0.02164 0.01560 = 0.03094 0.00217 -0.00118 -0.00005 H6 2 0.200645 1.178118 0.391199 11.00000 0.03252 C7 1 0.165814 0.999916 0.453021 11.00000 0.01354 0.01699 = 0.02537 -0.00019 -0.00084 0.00150 C8 1 0.156011 1.055819 0.535793 11.00000 0.01850 0.01615 = 0.02875 -0.00452 -0.00065 0.00026 H8 2 0.167084 1.150991 0.543531 11.00000 0.02547 C9 1 0.130972 0.974745 0.602774 11.00000 0.01859 0.02063 = 0.02155 -0.00723 -0.00014 0.00138 H9 2 0.123086 1.011034 0.658506 11.00000 0.02819 C10 1 0.112798 0.831985 0.592036 11.00000 0.01362 0.01969 = 0.02005 -0.00239 -0.00082 0.00051 C11 1 0.092367 0.748544 0.670255 11.00000 0.01756 0.02079 = 0.01804 -0.00528 0.00174 0.00158 C12 1 -0.006850 0.552642 0.729781 11.00000 0.02220 0.02629 = 0.01826 -0.00080 0.00370 -0.00395 H12A 2 -0.018482 0.598235 0.785610 11.00000 0.02509 H12B 2 -0.079498 0.504061 0.713868 11.00000 0.02046 C13 1 0.096335 0.452413 0.737253 11.00000 0.02600 0.02870 = 0.01605 0.00417 -0.00088 -0.00165 H13A 2 0.161354 0.493309 0.768261 11.00000 0.02364 H13B 2 0.074785 0.374108 0.770716 11.00000 0.02934 C14 1 0.135801 0.398182 0.652969 11.00000 0.02177 0.01981 = 0.02007 0.00444 -0.00067 -0.00123 H14A 2 0.068941 0.382191 0.611776 11.00000 0.01856 H14B 2 0.183864 0.313926 0.662167 11.00000 0.02247 C15 1 0.346471 0.612269 0.501732 11.00000 0.01819 0.01674 = 0.01975 0.00154 -0.00078 0.00235 C16 1 0.402176 0.588856 0.426135 11.00000 0.02272 0.02480 = 0.01953 0.00352 0.00010 0.00525 H16 2 0.371814 0.517132 0.388803 11.00000 0.02973 C17 1 0.501624 0.663384 0.407923 11.00000 0.02399 0.03759 = 0.02957 0.01382 0.00752 0.00752 H17 2 0.536889 0.646868 0.357083 11.00000 0.03376 C18 1 0.545019 0.760992 0.464885 11.00000 0.02001 0.03442 = 0.05297 0.01152 0.00309 -0.00468 H18 2 0.610657 0.812092 0.450558 11.00000 0.04159 C19 1 0.491478 0.782845 0.541203 11.00000 0.02501 0.03174 = 0.04915 -0.00740 -0.00096 -0.00659 H19 2 0.519953 0.854034 0.578493 11.00000 0.04815 C20 1 0.392490 0.708805 0.560099 11.00000 0.02028 0.02656 = 0.03047 -0.00671 0.00028 -0.00056 H20 2 0.352251 0.721568 0.612799 11.00000 0.02450 N1 3 0.006763 0.655041 0.663658 11.00000 0.01756 0.02200 = 0.01649 -0.00149 -0.00057 -0.00088 H1 2 -0.034420 0.646129 0.616398 11.00000 0.02058 O1 4 0.107852 0.636344 0.497230 11.00000 0.01807 0.01365 = 0.01652 -0.00083 -0.00153 0.00042 O2 4 0.153615 0.768300 0.736335 11.00000 0.02636 0.03391 = 0.01688 -0.00359 -0.00184 -0.00723 O3 4 0.215553 0.498088 0.615553 11.00000 0.01807 0.02095 = 0.01599 0.00146 -0.00071 -0.00073 O4 4 0.184811 0.406640 0.461826 11.00000 0.02215 0.01641 = 0.01994 -0.00250 -0.00214 0.00085 P1 5 0.211246 0.525353 0.517130 11.00000 0.01655 0.01420 = 0.01397 -0.00095 -0.00098 0.00066 HKLF 4 REM wpu23008_a.res in P2(1)/n REM wR2 = 0.0780, GooF = S = 1.042, Restrained GooF = 1.042 for all data REM R1 = 0.0305 for 2842 Fo > 4sig(Fo) and 0.0333 for all 3108 data REM 307 parameters refined using 0 restraints END WGHT 0.0367 0.6828 REM Highest difference peak 0.312, deepest hole -0.417, 1-sigma level 0.055 Q1 1 0.2961 0.5634 0.5153 11.00000 0.05 0.31 Q2 1 0.1089 0.7929 0.6241 11.00000 0.05 0.25 Q3 1 0.1816 1.0401 0.4211 11.00000 0.05 0.24 Q4 1 0.1360 0.9315 0.4432 11.00000 0.05 0.23 Q5 1 0.1449 0.7997 0.5592 11.00000 0.05 0.22 ; _shelx_res_checksum 99085 _shelx_hkl_file ; 0 0 2 290766. 7527.84 1 0 0 3 45.9416 40.6917 1 0 0 4 115854. 3143.25 1 0 0 5-11.5478 44.9654 1 0 0 6 2941.50 243.868 6 0 0 6 3344.32 247.842 1 0 0 7 38.9678 67.8564 6 0 0 7-17.3874 55.2789 1 0 0 8 42326.1 1449.02 1 0 0 9 24.5334 69.7662 1 0 0 10 63.8660 48.1922 5 0 0 10 143.389 135.246 1 0 0 11 36.5803 48.6595 5 0 0 11 32.9304 81.1006 1 0 0 12 2639.75 342.671 1 0 0 12 2524.00 185.085 5 0 0 13-22.3441 63.5403 5 0 0 14 361.696 92.8263 5 0 0 15 11.5470 56.8730 5 0 0 16 969.921 118.810 5 0 0 17 9.34294 53.1358 5 0 0 18 3623.40 197.484 5 0 0 18 3446.74 193.273 16 0 1 0 23.7878 18.6108 7 0 -1 1 76038.1 2021.69 6 0 1 1 78876.3 2021.30 6 0 1 1 78033.7 2057.58 7 0 1 1 77888.4 2020.00 1 0 -1 1 75811.9 2018.79 1 0 1 2 6389.78 253.624 9 0 -1 2 6398.60 235.037 1 0 1 2 5824.61 230.065 1 0 1 2 6193.88 235.358 6 0 -1 2 6511.60 238.363 6 0 1 3 41304.9 1168.44 9 0 -1 3 38929.8 1148.34 1 0 1 3 40397.2 1153.06 1 0 1 3 40436.7 1158.01 6 0 -1 3 39206.7 1156.04 6 0 1 4 44.7786 47.7317 9 0 -1 4 164.385 62.3160 6 0 1 4 57.7012 49.3850 6 0 -1 4 234.547 60.9087 1 0 1 4 135.753 55.4217 1 0 1 5 28348.3 963.137 6 0 -1 5 29813.8 974.446 6 0 -1 5 29026.3 950.744 1 0 1 5 28459.9 946.432 1 0 1 6 7683.35 407.049 6 0 -1 6 7957.02 415.340 6 0 -1 6 6661.63 375.848 1 0 -1 7 71681.5 2154.38 6 0 1 7 65813.8 2127.81 6 0 -1 7 71037.4 2114.89 1 0 -1 8 145.789 88.9137 1 0 -1 9 18900.7 852.853 1 0 -1 10 1408.63 119.836 5 0 1 10 989.405 104.866 5 0 1 10 1352.24 220.565 1 0 -1 10 1437.10 229.625 1 0 -1 11 4246.13 236.742 5 0 1 11 4371.67 238.202 5 0 -1 11 4282.82 416.898 1 0 1 11 5078.14 446.517 1 0 1 12 2768.54 194.209 5 0 -1 12 2867.73 196.800 5 0 1 12 2413.65 331.292 1 0 -1 12 3153.74 374.427 1 0 1 12 2870.75 170.412 11 0 1 13 19793.1 640.427 11 0 -1 13 19719.6 702.187 5 0 1 13 19978.5 704.580 5 0 1 14 4089.12 254.243 5 0 -1 14 4157.99 255.871 5 0 -1 15 398.748 90.0249 5 0 1 15 352.134 85.2923 5 0 1 -15 508.902 170.842 2 0 -1 -15 423.364 159.577 2 0 -1 16 6339.13 314.478 5 0 1 16 5926.44 306.606 5 0 1 17 2461.53 176.254 5 0 -1 17 2713.63 179.926 5 0 1 17 2747.29 185.509 16 0 -1 18 3318.70 180.403 5 0 1 18 2793.73 169.128 5 0 1 18 2773.67 168.281 16 0 2 0 32439.9 971.425 9 0 2 0 33535.6 948.783 7 0 2 -1 1261.73 97.7077 9 0 2 1 1290.10 107.015 7 0 2 1 1412.46 64.7398 1 0 -2 1 1185.09 60.8598 1 0 2 2 2341.10 123.549 6 0 -2 2 2065.43 118.920 6 0 2 2 2313.02 160.551 7 0 2 2 2281.41 119.830 1 0 -2 2 2230.11 118.787 1 0 2 3 6808.60 287.251 6 0 -2 3 6946.12 291.044 6 0 -2 3 6630.58 279.710 1 0 2 3 7059.61 286.072 1 0 2 4 5771.46 322.476 7 0 -2 4 6356.13 294.240 1 0 2 4 5970.79 287.921 1 0 2 4 5687.69 316.377 9 0 -2 4 5993.39 296.337 6 0 2 4 5900.50 292.823 6 0 2 5 18262.3 656.364 1 0 -2 5 17016.8 644.566 1 0 2 5 17396.0 684.728 9 0 2 5 17512.1 666.189 6 0 -2 5 17578.5 669.606 6 0 2 6 906.619 131.573 1 0 -2 6 683.985 115.313 1 0 2 6 971.336 141.619 6 0 -2 7 84574.8 2516.26 1 0 2 7 85812.7 2521.83 1 0 -2 8 14871.1 695.329 1 0 2 8 15151.6 704.320 1 0 2 9 12479.7 658.782 1 0 -2 9 12271.7 658.365 1 0 2 10 19138.6 628.328 5 0 -2 10 18413.2 624.517 5 0 2 10 19009.9 903.707 1 0 -2 10 18850.2 899.864 1 0 2 10 18870.6 625.010 12 0 2 11 813.495 96.4511 12 0 -2 11 858.186 103.785 5 0 2 11 708.032 97.4010 5 0 2 11 759.962 90.9606 11 0 -2 11 1122.47 218.585 1 0 2 11 694.625 177.126 1 0 2 12 9150.34 359.106 11 0 2 12 9081.62 385.897 12 0 -2 12 10100.6 411.792 5 0 2 12 9329.62 398.362 5 0 -2 13 2546.15 196.715 5 0 2 13 3343.18 216.708 5 0 2 13 2985.89 178.774 11 0 2 13 3088.06 198.065 12 0 2 14 1441.37 145.606 5 0 -2 14 1483.48 147.707 5 0 2 14 1359.00 127.621 12 0 2 15 10.7827 53.1104 5 0 -2 15 32.5346 57.6960 5 0 2 16 52.4715 60.6089 16 0 2 16 9.85860 49.5578 5 0 -2 16-19.8131 54.5518 5 0 2 17 606.604 85.3301 5 0 -2 17 493.292 78.5374 5 0 2 -17 395.580 66.3356 15 0 2 17 579.718 89.6577 16 0 2 18 234.508 56.3961 5 0 -2 18 130.913 49.1943 5 0 2 18 232.508 59.5634 16 0 3 0 121.823 51.6774 7 0 3 0 40.9799 44.9385 9 0 3 -1 1003.64 107.189 9 0 3 -1 970.016 96.5840 7 0 3 1 1071.28 115.689 7 0 3 -2 4255.29 224.588 9 0 3 2 4053.56 246.861 7 0 3 3 4257.63 271.636 7 0 3 -3 4160.27 215.914 9 0 3 3 4257.27 278.310 9 0 3 3 3964.07 198.887 1 0 -3 3 4418.18 205.767 1 0 3 4 1353.01 162.146 7 0 3 4 1283.65 158.470 9 0 3 -4 1234.65 106.044 9 0 3 4 1315.20 122.308 1 0 -3 4 1143.45 116.229 1 0 3 5 255.019 93.4636 7 0 3 5 147.815 83.1686 9 0 -3 5 118.122 58.3120 1 0 3 5 155.224 60.1517 1 0 3 6 6756.79 423.844 9 0 -3 6 6649.13 367.313 1 0 3 6 6735.45 372.468 1 0 -3 7 143.349 84.5520 1 0 3 7 108.252 57.4410 1 0 3 8 3327.11 293.013 1 0 -3 8 3499.99 301.564 1 0 3 9 24752.6 769.208 17 0 3 9 24872.9 1023.33 1 0 -3 9 22372.0 989.865 1 0 3 9 23872.3 766.321 12 0 3 10 9711.78 391.985 12 0 3 10 9558.54 376.280 5 0 -3 10 9732.05 380.446 5 0 3 10 9658.65 393.721 17 0 3 10 9151.14 358.813 11 0 3 10 10128.9 614.620 1 0 -3 10 10056.8 612.419 1 0 3 11 4939.06 259.056 12 0 3 11 4704.60 233.134 11 0 3 11 4526.06 243.466 5 0 -3 11 5036.42 256.907 5 0 3 12 13420.8 509.288 12 0 3 12 12419.9 461.939 11 0 -3 12 14179.1 510.208 5 0 3 12 12052.7 484.992 5 0 3 13 93.6203 58.2356 12 0 3 13 20.4775 55.4410 5 0 -3 13 20.6768 54.0162 5 0 3 13 22.4023 54.6634 11 0 3 14 420.310 84.5966 12 0 3 -14 541.064 165.062 2 0 -3 -14 500.505 164.435 2 0 3 14 411.379 83.1442 5 0 -3 14 187.027 69.0148 5 0 3 14 287.062 67.8504 11 0 -3 15 285.425 73.0004 5 0 3 15 224.127 68.1823 5 0 -3 16 877.869 105.009 5 0 3 16 851.846 101.820 5 0 3 17 47.5845 41.5754 5 0 -3 17 20.6736 40.9920 5 0 3 -17 6.80416 38.7012 15 0 3 -18 157.205 35.2410 15 0 3 18 220.373 44.5731 5 0 -3 18 221.482 45.2437 5 0 4 0 21280.5 744.784 7 0 4 0 22006.0 800.312 9 0 4 -1 6940.92 321.037 7 0 4 1 6885.30 350.781 7 0 4 -1 6513.45 349.670 9 0 4 1 6323.63 367.830 9 0 4 2 477.985 97.1113 7 0 4 -2 328.230 76.0025 9 0 4 -2 399.483 69.0360 7 0 -4 -3 73.4325 31.1446 2 0 4 -3 10.0410 27.2004 2 0 4 -3 8.72144 35.0877 7 0 4 3 16.6989 55.6905 7 0 4 4 8614.99 490.553 9 0 4 -4 8045.73 363.769 9 0 4 4 8152.62 462.675 7 0 4 -5 42627.0 1296.26 9 0 4 5 47213.5 1567.95 9 0 4 5 45519.4 1526.29 7 0 4 6 619.325 142.980 9 0 4 7 7172.82 506.250 9 0 4 8 5538.03 259.655 12 0 4 8 5076.91 253.359 17 0 4 8 4993.34 248.436 16 0 4 9 6472.24 303.534 16 0 4 9 6926.90 311.945 17 0 4 -9 6410.03 283.146 10 0 4 9 6434.80 284.923 11 0 4 9 6825.73 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515.896 12 -1 3 8 6012.52 432.079 9 -1 3 7 1568.42 194.607 6 -1 -3 7 1947.52 218.324 6 -1 3 7 1649.22 207.546 9 -1 -3 6 9099.15 466.492 6 -1 3 6 9255.24 465.088 6 -1 3 6 9065.19 501.689 9 -1 -3 5 459.359 94.0892 6 -1 3 5 492.734 94.7866 6 -1 3 5 470.957 105.316 9 -1 3 4 9995.76 412.235 6 -1 -3 4 10712.4 424.548 6 1 -3 -4 10593.9 419.712 2 -1 3 4 10754.3 500.636 9 1 3 -4 9398.15 321.142 9 -1 -3 3 1028.38 96.2799 6 -1 3 3 796.895 86.6530 6 -1 3 3 851.168 123.943 9 1 3 -3 951.435 82.6182 9 1 3 -3 937.110 94.6407 2 1 -3 -3 970.587 95.1247 2 1 3 -2 35.9049 33.8694 9 -1 3 2 26.9770 40.6884 9 -1 -3 2 33.6888 25.6122 6 -1 3 2 9.68824 24.3602 6 1 -3 -2 20.1788 25.8701 2 1 3 -2 44.5643 29.8768 2 1 -3 -1 2026.74 99.1582 2 1 3 -1 2398.33 102.580 2 -1 -3 1 2263.25 99.0281 6 -1 3 1 2041.52 148.630 7 -1 3 1 2482.11 185.754 8 1 3 -1 2266.20 157.841 9 1 3 0 4821.02 258.188 7 -1 3 0 4265.87 198.030 7 1 -3 0 4664.31 141.022 3 1 3 0 4560.88 245.814 9 -1 3 0 4461.35 241.942 8 -1 3 0 4161.05 252.876 9 1 3 1 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627.890 11 1 -3 11 19861.3 971.598 1 1 3 11 18005.9 930.958 1 1 -3 11 19119.0 647.646 5 1 3 11 19009.0 642.934 5 1 3 11 18660.1 659.315 12 1 3 12 13318.0 486.856 11 1 -3 12 11927.1 756.828 1 1 3 12 14098.0 813.395 1 1 3 12 12829.2 512.045 12 1 3 12 13615.0 505.756 5 1 -3 12 12623.6 498.127 5 1 3 13 8.49436 61.5825 11 1 -3 13-31.4482 59.6176 5 1 3 13 10.3644 58.0163 5 1 3 13 32.3713 53.1459 12 1 -3 14 1376.30 137.240 5 1 3 14 1245.32 131.183 5 1 3 14 1359.12 148.667 16 1 3 14 1446.82 127.700 11 1 3 15 6351.49 313.473 16 1 -3 15 5403.53 284.170 5 1 3 15 5850.32 290.682 5 1 3 15 5491.24 250.684 11 -1 3 -15 5409.82 293.195 15 1 3 16 818.614 109.583 16 1 -3 16 845.919 101.352 5 1 3 16 707.714 93.3067 5 -1 3 -16 714.952 95.6187 15 1 3 17 97.4915 47.1441 5 1 -3 17 39.6580 42.5768 5 1 3 17 38.7453 49.9076 16 -1 3 -17 62.1015 37.4917 15 -1 -4 17 4140.93 181.401 5 -1 4 17 4179.45 179.353 5 1 4 -17 4420.35 212.505 15 -1 4 17 4483.39 209.894 16 -1 4 16 148.612 58.2548 16 -1 -4 16 138.524 51.5406 5 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471.765 2 -1 4 7 1528.45 228.226 9 1 4 -7 2150.29 224.638 2 1 -4 -7 1740.55 194.307 2 -1 4 6 3007.55 296.092 9 1 4 -6 3228.07 244.122 2 1 -4 -6 2630.08 222.940 2 -1 4 5 27653.0 1083.21 9 1 -4 -5 27151.4 908.938 2 1 4 -5 26958.6 910.381 2 -1 4 4 4647.25 343.924 9 1 4 -4 3815.79 205.066 9 1 -4 -4 4358.13 232.518 2 1 4 -4 4296.08 230.844 2 -1 4 3 2008.90 217.385 9 1 4 -3 1862.12 147.510 9 1 -4 -3 1904.25 123.204 2 1 4 -3 1906.52 123.773 2 -1 4 2 16020.6 567.136 7 1 4 -2 16643.3 541.327 9 -1 4 1 22530.6 766.623 7 1 4 -1 21737.0 800.441 7 1 4 -1 22048.5 787.691 9 -1 4 1 23598.4 863.530 9 1 4 0 36593.1 1170.56 7 -1 4 0 35258.4 1075.11 7 1 4 0 34188.3 1156.13 9 -1 4 0 36818.5 1202.57 9 1 4 1 54972.7 1683.55 7 -1 4 -1 54123.8 1524.96 7 1 4 1 55193.0 1698.43 9 -1 4 -1 54595.2 1679.17 9 -1 4 -2 533.284 55.9224 7 1 4 2 708.896 126.954 7 1 4 2 497.921 44.1001 1 -1 4 -2 562.521 102.409 9 1 4 2 577.662 114.857 9 1 4 3 28275.0 1023.21 7 1 4 3 27474.9 820.589 1 1 -4 3 26958.1 815.695 1 -1 4 -3 28033.5 957.991 9 1 4 4 20887.3 845.718 7 1 4 4 20482.4 677.932 1 1 -4 4 19042.3 664.829 1 1 4 5 30422.5 1151.71 7 1 -4 5 28756.8 968.961 1 1 4 5 30079.9 977.332 1 1 4 5 29371.0 1166.28 9 1 4 6 30999.3 1072.23 1 1 -4 6 31894.3 1079.95 1 1 4 6 32361.5 1246.81 7 1 -4 7 982.460 155.709 1 1 4 7 771.518 139.966 1 1 4 8 2921.81 185.554 16 1 -4 8 2739.34 267.355 1 1 4 8 3089.24 282.462 1 1 4 8 2996.57 187.014 12 1 4 8 3378.60 186.360 11 1 4 8 3049.20 185.970 17 1 4 9 1322.36 122.287 17 1 4 9 1164.36 123.921 16 1 4 9 1131.12 101.444 5 1 4 9 1114.86 119.328 12 -1 4 -9 1212.49 112.540 10 1 4 9 1060.45 110.432 11 1 -4 9 1100.72 187.199 1 1 4 9 1259.84 200.075 1 1 4 10 8645.27 378.625 17 1 4 10 9045.74 392.254 16 1 4 10 8500.00 348.366 5 1 4 10 9351.56 396.099 12 -1 4 -10 8982.00 360.879 10 1 4 10 8474.07 361.849 11 1 -4 10 8507.09 556.857 1 1 4 10 9219.64 578.022 1 1 4 11 6805.80 328.415 17 1 4 11 6647.01 333.582 16 1 -4 11 6663.75 307.410 5 1 4 11 6824.60 305.680 5 1 4 11 7036.37 316.413 11 1 4 11 6603.50 334.752 12 1 4 12 766.694 101.047 5 1 -4 12 845.194 103.157 5 1 4 12 978.441 129.794 16 1 4 12 965.890 118.650 17 1 4 12 949.138 120.023 12 1 4 12 960.130 112.913 11 1 4 13 4071.56 230.538 5 1 -4 13 3843.82 227.069 5 1 4 13 4100.12 225.553 11 1 4 13 4177.22 254.929 12 1 4 14 1778.34 144.325 5 1 -4 14 1879.18 150.409 5 1 4 15 1733.54 131.827 5 1 -4 15 1509.24 127.148 5 -1 4 -15 1428.29 142.971 15 1 -4 16 1092.73 96.4715 5 1 4 16 891.715 89.5235 5 -1 4 -16 992.109 108.091 15 1 4 17 515.751 56.1677 5 1 -4 17 479.868 58.3284 5 -1 4 -17 506.086 69.4404 15 -1 5 16 2404.59 147.235 16 1 5 -16 2168.58 155.639 15 -1 5 15 1753.43 139.444 16 -1 5 15 1770.95 140.487 12 -1 5 14 303.725 75.4342 16 -1 5 14 228.146 67.2325 12 -1 5 13 1716.78 151.079 16 -1 5 13 1398.14 142.339 12 -1 5 12 1729.29 157.553 16 -1 5 12 1880.01 165.672 12 -1 5 11 93.1243 65.0184 16 -1 5 11 113.420 64.5582 12 -1 5 10 7044.73 324.346 16 -1 5 10 6858.65 332.324 12 1 5 -10 6140.42 296.536 10 1 5 -9 42.8491 48.0025 10 -1 5 9 153.522 61.6026 16 -1 5 9 20.4178 45.9336 12 -1 5 9 104.040 57.3173 17 -1 5 8 12876.2 487.674 12 -1 5 8 11854.3 758.639 9 1 5 -8 12579.0 470.713 10 -1 5 8 12875.7 490.918 17 -1 5 8 13339.9 474.630 16 1 5 -7 1604.00 130.133 10 -1 5 7 1840.20 143.720 17 -1 5 7 1558.39 254.001 9 -1 5 6 9396.47 370.752 12 -1 5 6 9229.61 605.094 9 -1 5 6 9519.37 375.050 17 -1 5 5 2952.27 314.604 9 -1 5 4 29460.8 1184.39 9 1 5 -4 28553.1 932.802 9 1 5 -3 4717.21 286.412 9 1 5 -3 4726.52 306.485 7 1 5 -2 6436.17 370.549 9 1 5 -2 6683.03 384.259 7 1 5 -1 3657.67 275.642 9 -1 5 1 3582.02 305.215 9 1 5 -1 4065.79 289.025 7 -1 5 0 6689.64 425.677 9 1 5 0 6236.54 389.904 9 1 5 0 6586.41 394.979 7 -1 5 0 6620.75 330.635 7 -1 5 -1 586.491 120.277 9 1 5 1 512.378 117.301 9 1 5 1 450.778 115.614 7 1 5 2 5735.12 399.150 9 -1 5 -2 5299.64 354.840 9 1 5 2 4892.17 357.033 7 -1 5 -3 767.686 132.082 9 1 5 3 666.673 139.550 9 1 5 3 833.371 151.435 7 -1 5 -4 10655.8 529.035 9 1 5 4 12172.3 635.017 7 -1 5 -5 8236.76 435.078 9 1 5 5 9357.52 576.399 7 1 5 6 5336.44 439.449 7 1 5 6 4660.04 232.773 12 -1 5 -6 4970.24 238.884 10 1 5 7 8003.05 343.220 11 1 5 7 8335.31 355.505 12 1 5 7 8735.95 354.647 16 -1 5 -7 8665.25 354.098 10 1 5 8 16165.5 566.589 11 1 5 8 15989.2 578.645 17 1 5 8 16084.3 575.849 16 -1 5 -8 16430.2 574.428 10 1 5 9 3778.97 238.616 12 1 5 9 3887.73 225.971 11 1 5 9 4151.37 239.747 17 1 5 9 3859.14 234.805 16 -1 5 -9 4202.37 232.635 10 1 5 10 1689.14 158.613 12 1 5 10 1325.66 135.742 11 1 5 10 1710.83 155.056 16 1 5 10 1521.92 144.929 17 -1 5 -10 1585.51 141.384 10 1 5 11 4659.96 277.939 12 1 5 11 4758.30 271.579 17 1 5 11 4624.27 273.495 16 -1 5 -11 5132.16 259.418 10 1 5 12 4724.03 275.464 12 1 5 12 4800.59 271.547 17 1 5 12 4894.71 278.652 16 1 5 13 630.322 105.044 16 1 5 13 681.440 108.416 12 1 5 14 60.8579 55.8871 16 -1 5 -14 91.3874 57.4563 15 1 5 15 735.104 98.0530 16 -1 5 -15 515.395 89.9206 15 -1 5 -16 90.5493 48.0357 15 1 6 -16 3573.41 185.058 15 1 6 -15 2497.95 172.530 15 -1 6 15 2650.77 163.054 12 -1 6 14 434.557 76.9591 12 -1 6 13 2284.60 177.591 12 -1 6 12 5113.14 267.353 16 -1 6 12 5284.27 288.224 12 -1 6 11 18261.9 661.795 12 -1 6 11 18570.9 633.606 16 1 6 -11 16954.2 612.280 10 -1 6 10 1609.91 154.683 12 1 6 -10 1383.42 133.360 10 -1 6 10 1607.89 157.951 17 -1 6 10 1368.36 134.800 16 -1 6 9 328.889 75.4594 16 -1 6 9 226.602 71.4303 17 1 6 -9 216.876 66.0597 10 1 6 -8 20463.8 712.999 10 -1 6 8 21629.7 736.645 17 -1 6 8 21333.4 698.824 16 -1 6 7 2162.82 163.194 12 -1 6 7 1684.12 292.085 9 1 6 -7 1860.13 152.972 10 -1 6 7 1844.73 157.422 17 1 6 -6 3492.94 206.380 10 -1 6 6 3457.04 388.595 9 -1 6 6 2866.60 190.455 17 -1 6 6 3158.30 195.607 12 1 6 -5 17.3848 41.9233 10 -1 6 5 35.7661 80.4110 9 -1 6 5 41.1853 40.5826 12 -1 6 5 77.4116 49.6862 17 1 6 -4 2676.99 175.355 10 -1 6 4 2997.33 179.065 17 -1 6 4 2938.69 172.194 12 -1 6 3 33974.1 1334.36 9 1 6 -3 30697.7 1104.65 9 -1 6 2 11953.5 685.125 9 1 6 -2 11829.7 579.257 9 1 6 -2 11263.9 557.050 7 -1 6 1 11172.7 632.363 9 1 6 -1 11124.8 577.106 9 1 6 -1 9874.75 532.303 7 -1 6 0 8183.24 509.294 9 1 6 0 6911.21 467.280 9 1 6 0 7407.99 451.382 7 1 6 1 7187.16 484.960 9 -1 6 -1 7165.73 472.081 9 1 6 1 6612.17 439.890 7 1 6 2 703.908 153.481 9 -1 6 -2 721.510 145.344 9 1 6 2 667.526 146.028 7 1 6 3 5034.78 426.532 9 -1 6 -3 4177.58 337.725 9 1 6 3 5635.77 425.239 7 -1 6 -3 4877.34 238.881 10 1 6 4 1136.99 102.401 12 1 6 4 1059.04 204.277 9 -1 6 -4 1147.55 163.275 9 1 6 4 1161.36 204.933 7 1 6 4 982.942 106.563 17 1 6 5 332.434 63.1790 12 -1 6 -5 315.470 87.9125 9 1 6 5 276.087 65.3124 17 1 6 5 161.904 98.0271 7 -1 6 -6 972.542 109.889 10 1 6 6 905.879 104.637 12 1 6 6 854.282 105.425 17 -1 6 -7 3336.63 211.604 10 1 6 7 3264.06 209.067 12 1 6 7 3191.43 210.743 17 1 6 8 1234.08 131.306 12 -1 6 -8 1233.61 133.539 10 -1 6 -9 1019.79 124.208 10 1 6 10 805.601 113.934 17 -1 6 -10 754.735 107.857 10 -1 6 -11 7157.24 330.814 10 1 6 11 7478.22 361.671 12 1 6 11 6651.78 340.391 17 -1 6 -12 3075.40 190.798 10 1 6 12 3347.29 218.547 17 1 6 12 3098.56 221.800 12 -1 6 -13 2160.95 178.079 15 1 6 13 2003.98 169.518 12 -1 6 -14 10.1005 58.3573 15 -1 6 -14 109.469 43.4592 14 -1 6 -15 130.759 56.4272 15 1 7 -14 2251.28 158.032 15 -1 7 14 2144.00 147.850 12 -1 7 13 1631.86 139.606 12 -1 7 12 7229.92 336.224 12 1 7 -12 6748.67 294.618 10 1 7 -11 1014.00 111.690 10 -1 7 10 8543.77 389.132 17 1 7 -10 7915.22 361.445 10 -1 7 9 1880.20 170.627 12 -1 7 9 2182.62 179.655 17 1 7 -9 2165.21 172.612 10 -1 7 8 11142.3 461.825 12 1 7 -8 11156.5 460.562 10 -1 7 8 10827.3 468.229 17 -1 7 7 17381.3 638.376 12 -1 7 7 17406.0 1023.27 9 1 7 -7 18505.8 650.813 10 -1 7 7 17743.8 648.003 17 -1 7 6 36328.2 1112.40 12 -1 7 6 36775.7 1611.64 9 1 7 -6 35946.3 1123.80 10 -1 7 6 35875.5 1121.78 17 1 7 -5-10.2954 51.7585 10 -1 7 5 39.5008 44.4061 17 -1 7 5 46.1940 45.5093 12 -1 7 4 7479.94 594.948 9 -1 7 4 6767.28 307.086 12 -1 7 4 7182.21 322.655 17 1 7 -3 3634.45 216.130 10 -1 7 3 3504.89 194.906 12 -1 7 3 4100.44 419.316 9 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4294.99 2 -2 3 0 165411. 4402.31 8 2 -3 1 55488.2 1582.04 3 2 3 1 60324.5 1597.04 3 2 3 1 55656.2 1724.44 7 -2 3 -1 54996.8 1643.64 8 2 3 2 3124.97 193.506 3 2 -3 2 2997.52 190.268 3 -2 3 -2 2968.37 186.718 8 2 3 2 3183.66 246.191 7 2 3 3 250.001 64.3518 1 2 -3 3 190.991 58.6497 1 -2 3 -3 252.258 53.9237 8 2 3 3 134.572 65.7221 7 2 3 4 23609.4 797.670 1 2 -3 4 23204.2 793.309 1 -2 3 -4 21667.3 667.739 8 2 3 4 24456.3 904.815 7 2 -3 5 8084.21 414.755 1 2 3 5 8588.54 423.383 1 2 3 5 8883.58 496.872 7 2 3 6 1653.80 185.409 1 2 -3 6 1628.49 185.308 1 2 3 7 21138.3 847.663 1 2 -3 7 19141.8 823.656 1 2 3 8 20536.1 885.278 1 2 -3 8 19956.3 880.641 1 2 3 9 11418.9 647.344 1 2 -3 9 12215.6 667.443 1 2 3 9 11529.2 445.006 16 2 3 9 11602.3 448.178 12 2 3 9 11875.2 425.929 5 2 -3 9 11204.2 422.340 5 2 3 9 11485.1 427.600 17 2 3 9 11168.4 427.378 11 2 3 10 6778.95 306.076 17 2 3 10 6876.15 509.081 1 2 -3 10 6699.68 501.930 1 2 -3 10 6644.06 307.423 5 2 3 10 6969.43 309.746 5 2 3 10 7547.89 338.312 16 2 3 10 6809.17 323.071 12 2 3 10 7127.36 316.200 11 2 3 11 19952.8 675.217 17 2 3 11 20305.2 709.672 16 2 -3 11 20841.4 689.103 5 2 3 11 19588.6 677.912 5 2 3 11 20517.8 1004.82 1 2 -3 11 19331.9 981.302 1 2 3 11 19689.5 677.068 11 2 3 11 20009.8 706.340 12 2 3 12 10330.3 450.669 16 2 -3 12 10409.2 432.443 5 2 3 12 9917.51 423.294 5 2 3 12 10459.1 691.936 1 2 -3 12 9917.44 681.440 1 2 3 12 10440.5 423.342 11 2 3 12 10900.2 453.836 12 2 3 13 10389.3 696.641 1 2 -3 13 10252.2 696.395 1 2 3 13 9720.61 434.891 16 2 3 13 9650.79 414.642 5 2 -3 13 10188.5 424.435 5 2 3 13 9149.46 396.193 11 2 3 14 1457.71 135.412 11 -2 3 -14 1621.56 152.144 15 2 3 14 1567.50 156.000 16 2 -3 14 1304.70 137.066 5 2 3 14 1524.97 144.992 5 2 3 15 104.514 57.2652 11 2 3 15 122.908 65.9460 5 2 -3 15 288.192 72.9993 5 -2 3 -15 80.1985 49.4979 15 2 3 15 170.763 67.9517 16 2 3 16 119.055 56.5059 5 2 -3 16 113.138 51.4744 5 -2 3 -16 135.555 50.1556 15 2 3 16 100.774 59.7676 16 -2 3 -17 2338.17 134.022 15 2 3 17 2565.57 159.989 16 2 3 17 2485.46 146.071 5 2 -3 17 2468.32 145.579 5 -2 4 17 22.6532 39.0498 16 -2 -4 17 55.7124 32.5480 5 -2 4 17 45.7526 33.9901 5 -2 -4 16 734.000 80.0974 5 -2 4 16 681.441 89.7447 16 -2 4 16 594.373 74.5577 5 -2 4 15 2682.96 173.807 12 -2 4 15 2539.94 177.753 16 -2 -4 15 2530.43 163.665 5 -2 4 15 2496.68 163.210 5 -2 4 14 4142.63 238.654 12 -2 4 14 4188.33 246.120 16 -2 -4 14 4523.14 234.778 5 -2 4 14 4206.44 228.129 5 -2 4 13 1523.83 146.617 16 -2 -4 13 1379.43 129.345 5 -2 4 13 1543.95 135.597 5 -2 4 13 1551.90 144.085 12 2 4 -13 1507.61 236.921 2 -2 4 12 541.254 90.9408 12 -2 4 12 806.499 110.299 16 2 4 -12 996.496 202.184 2 2 -4 -12 791.164 190.212 2 -2 -4 12 715.845 96.6809 5 -2 4 12 603.065 92.5850 5 -2 -4 11 154.766 56.0448 5 -2 4 11 34.1477 50.0721 5 2 -4 -11 32.3980 92.1416 2 -2 4 11 10.3408 46.5225 12 -2 4 10 719.258 87.7058 5 2 4 -10 853.818 183.397 2 2 -4 -10 473.220 143.793 2 -2 4 10 811.640 104.287 12 -2 4 9 5586.43 247.029 5 -2 4 9 5158.21 272.765 17 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753.182 75.0486 6 -2 4 1 3680.50 275.647 8 2 -4 -1 3562.10 169.443 2 2 4 -1 3757.94 164.190 2 -2 4 0 21877.8 851.461 9 2 4 0 21594.5 795.489 9 -2 4 0 20623.5 788.017 8 2 -4 0 20771.7 624.620 3 2 4 0 21422.9 632.866 3 2 4 0 22336.7 842.753 7 2 -4 1 22017.9 647.876 1 2 4 1 20794.6 647.680 1 2 4 1 22272.5 862.134 7 -2 4 -1 23506.9 799.149 8 2 4 2 6996.74 291.218 1 2 -4 2 7745.07 297.218 1 2 4 2 6994.49 427.041 7 2 4 3 124.588 80.8759 7 2 4 3 78.7021 39.3648 1 2 -4 3 60.3508 40.7017 1 2 4 4 3378.32 220.873 1 2 -4 4 3547.35 224.730 1 2 4 4 3041.67 289.831 7 2 4 5 1368.64 152.148 1 2 -4 5 1395.59 155.600 1 2 4 5 1104.92 183.395 7 2 4 6 6105.18 368.452 1 2 -4 6 5749.78 359.123 1 2 4 6 6732.80 481.525 7 2 4 7 11509.5 579.225 1 2 -4 7 11455.8 579.545 1 2 4 7 12389.6 709.749 7 2 4 8 8032.15 491.337 1 2 -4 8 7882.07 487.261 1 -2 4 -8 7560.60 324.024 10 2 4 8 7971.71 331.440 11 2 4 8 7969.82 332.979 17 2 4 8 7430.08 338.286 12 2 4 9 5094.21 401.786 1 2 -4 9 5139.41 408.033 1 -2 4 -9 5356.82 260.027 10 2 4 9 5173.56 260.781 11 2 4 9 5206.08 241.801 5 2 4 9 5124.56 260.371 17 2 4 9 4624.14 262.028 12 2 4 10 36119.4 1401.62 1 2 -4 10 35729.2 1394.96 1 -2 4 -10 35163.8 1078.79 10 2 4 10 35485.6 1089.40 11 2 4 10 37063.1 1126.67 12 2 4 10 35264.7 1066.22 5 2 -4 10 34775.7 1069.54 5 2 4 10 36454.3 1098.17 17 2 -4 11 866.266 186.462 1 2 4 11 548.286 156.892 1 2 -4 11 752.230 97.8025 5 2 4 11 826.460 100.058 5 2 4 11 1012.44 115.463 17 2 4 11 785.577 110.098 11 2 4 11 837.658 117.791 12 2 4 12 16085.1 583.183 17 2 4 12 15856.7 566.031 5 2 -4 12 15784.2 568.431 5 2 4 12 15275.9 568.936 11 2 4 12 15900.3 612.583 12 2 -4 13 5920.50 287.921 5 2 4 13 5545.53 279.115 5 2 4 13 5378.30 303.487 16 -2 4 -13 5982.32 322.906 15 2 4 13 5840.20 288.034 11 2 4 14 3592.17 232.286 16 2 4 14 3437.72 206.369 11 2 4 14 3790.31 212.647 5 2 -4 14 3548.31 209.855 5 -2 4 -14 4204.78 251.361 15 2 4 15 393.171 80.8864 16 2 -4 15 415.444 71.9193 5 2 4 15 374.556 69.1809 5 -2 4 -15 357.936 78.0555 15 2 4 16 178.763 62.9201 16 -2 4 -16 225.193 62.1394 15 2 4 16 163.331 48.2703 5 2 -4 16 174.786 49.9186 5 -2 4 -17 1753.10 112.686 15 2 4 17 1587.94 90.2930 5 -2 5 16 937.341 86.5879 16 -2 5 15 393.695 68.3399 16 -2 5 15 403.223 76.0928 12 -2 5 14 8.63330 49.8619 16 -2 5 14 18.9791 47.7038 12 -2 5 13 1997.09 158.628 16 -2 5 13 2001.42 164.961 12 -2 5 12 5314.62 281.667 16 -2 5 12 5502.69 294.036 12 -2 5 11 3048.07 213.274 12 -2 5 11 2857.86 195.868 16 -2 5 10 2380.81 170.744 16 2 5 -10 2738.49 173.209 10 -2 5 10 2427.58 188.495 17 -2 5 9 16.9446 47.4349 16 2 5 -9 59.3584 52.5624 10 -2 5 9 71.6032 55.3892 12 -2 5 9 21.1917 55.3618 17 -2 5 9 37.5463 92.4680 9 -2 5 8 18823.0 628.647 16 -2 5 8 19283.9 661.358 12 -2 5 8 18676.2 663.636 17 -2 5 8 19221.6 987.630 9 2 5 -8 20158.2 650.355 10 -2 5 7 1477.51 129.384 17 2 5 -7 1475.67 123.519 10 -2 5 7 1226.57 222.426 9 -2 5 6 16661.8 561.934 12 2 5 -6 15859.6 551.035 10 -2 5 6 17014.9 863.398 9 -2 5 6 16226.8 561.911 17 -2 5 5 505.930 137.722 9 -2 5 4 166.265 83.6868 9 -2 5 3 1150.27 188.163 9 2 5 -2 421.724 114.720 7 -2 5 1 29743.8 1130.88 9 2 5 -1 26779.7 1054.49 7 -2 5 0 6719.79 450.836 9 2 5 0 8134.47 470.290 7 2 5 1 265.483 102.278 7 -2 5 -1 399.493 104.999 9 -2 5 -2 12198.0 608.104 9 2 5 2 10878.3 603.171 7 -2 5 -3 1483.10 193.743 9 2 5 3 1789.35 231.716 7 -2 5 -4 103.853 66.0806 9 2 5 4 82.1558 87.0991 7 -2 5 -5 101.426 64.4925 9 2 5 5-29.9571 73.7738 7 2 5 6 33.0622 74.3498 7 2 5 6 65.1901 47.0998 16 2 5 6 65.2608 43.4382 12 2 5 6 43.0121 49.7178 17 -2 5 -6 108.884 46.9217 10 -2 5 -6 117.041 62.0455 9 2 5 7 27057.0 1240.84 7 2 5 7 28437.1 888.576 17 2 5 7 28854.2 886.969 16 2 5 7 27585.7 885.138 12 2 5 7 28093.3 876.492 11 -2 5 -7 27058.9 877.249 10 -2 5 -8 754.972 99.1278 10 2 5 8 918.624 113.311 11 2 5 8 849.171 104.908 17 2 5 8 872.572 111.088 16 2 5 9 36020.1 1113.28 17 2 5 9 36127.1 1118.29 16 2 5 9 35844.9 1100.85 11 -2 5 -9 35510.5 1104.28 10 2 5 10 998.494 116.380 17 2 5 10 1122.56 133.092 12 2 5 10 978.862 127.140 16 2 5 10 929.388 122.409 11 -2 5 -10 998.021 115.708 10 2 5 11 10034.5 428.413 16 2 5 11 9596.64 410.953 17 2 5 11 9356.14 427.689 12 2 5 11 9582.49 401.419 11 -2 5 -11 8311.37 380.146 10 2 5 12 286.581 84.3555 12 2 5 12 220.860 70.5211 17 -2 5 -12 410.191 94.9863 15 -2 5 -13 221.728 60.3715 14 -2 5 -13 219.624 80.6372 15 -2 5 -14 4869.52 278.003 15 -2 5 -15 228.673 64.6374 15 -2 5 -16 4225.45 210.682 15 -2 6 15 3354.79 182.107 12 -2 6 14 60.4820 49.9250 12 -2 6 13 401.434 79.4697 12 -2 6 12 15215.0 540.535 16 -2 6 12 15567.4 582.965 12 2 6 -11 1094.47 115.227 10 -2 6 11 1041.42 111.774 16 -2 6 11 1134.24 132.739 12 2 6 -10 1403.43 133.408 10 -2 6 10 1698.80 157.548 12 -2 6 10 1607.59 159.507 17 -2 6 10 1957.56 149.594 16 2 6 -9 706.497 98.2574 10 -2 6 9 709.758 93.5407 16 -2 6 9 545.505 101.012 17 -2 6 9 647.482 105.427 12 2 6 -8 3703.14 218.743 10 -2 6 8 3298.24 400.919 9 -2 6 8 3305.15 190.371 16 -2 6 8 3176.36 214.775 17 2 6 -7 3590.90 217.750 10 -2 6 7 3349.40 395.819 9 -2 6 7 3731.61 225.487 17 -2 6 7 3585.00 222.388 12 2 6 -6 6306.41 301.822 10 -2 6 6 7097.84 564.716 9 -2 6 6 6319.17 302.090 17 -2 6 6 6542.35 304.973 12 2 6 -5 1505.96 133.282 10 -2 6 5 1673.52 136.340 12 -2 6 5 1533.09 267.667 9 -2 6 5 1546.05 131.896 17 2 6 -4 90.1370 71.6705 7 -2 6 4 63.2670 43.5953 12 -2 6 4 68.8396 77.4044 9 -2 6 4 78.4579 44.6665 17 2 6 -4 100.469 51.2408 10 2 6 -3 6157.41 421.031 7 2 6 -2 3941.38 331.345 7 -2 6 2 3973.94 379.503 9 2 6 -2 3801.15 205.317 10 2 6 -1 1349.07 195.328 7 -2 6 1 1356.57 218.603 9 2 6 0 1782.98 233.783 7 -2 6 0 2775.54 300.974 9 2 6 1 2583.98 282.860 7 -2 6 -1 2433.36 279.579 9 -2 6 -2 2962.40 177.940 10 2 6 2 3445.30 334.130 7 -2 6 -2 3144.95 319.657 9 -2 6 -3 1494.72 127.095 10 -2 6 -3 1402.30 208.844 9 -2 6 -4 12437.1 459.989 15 -2 6 -4 11756.4 639.850 9 2 6 4 12258.8 444.241 12 2 6 4 12655.1 730.852 7 2 6 5 2494.28 312.357 7 2 6 5 2153.43 153.111 12 -2 6 -5 2012.34 236.127 9 -2 6 -5 1768.09 149.125 15 2 6 5 2356.51 170.560 17 -2 6 -5 1941.83 153.462 10 -2 6 -6 1358.74 135.133 15 -2 6 -6 1287.59 127.212 10 2 6 6 1385.19 131.801 12 2 6 6 1585.96 262.581 7 -2 6 -7 6206.32 327.025 15 2 6 7 7091.78 331.373 12 -2 6 -7 6880.52 330.103 10 2 6 8 346.503 83.5452 12 -2 6 -8 516.431 92.9902 10 2 6 8 413.982 84.0470 17 -2 6 -8 350.547 87.7292 15 2 6 9 19257.6 720.066 12 -2 6 -9 20374.3 719.631 10 2 6 9 20733.5 728.830 17 -2 6 -10 5034.75 280.667 10 2 6 10 5347.58 290.669 17 2 6 11 617.238 98.7812 17 -2 6 -11 745.115 101.385 10 2 6 12 3956.44 256.078 12 -2 6 -12 4586.37 276.591 15 2 6 12 4393.77 249.187 17 -2 6 -13 14259.3 545.330 15 -2 6 -13 13419.1 490.512 14 -2 6 -14-9.60568 52.0064 15 -2 6 -15 613.355 82.4341 15 2 7 -14 3759.78 205.514 15 -2 7 14 3532.62 191.519 12 -2 7 13 778.913 96.2030 12 2 7 -12 8524.92 338.257 10 -2 7 12 9083.89 384.300 12 2 7 -11 566.055 84.7513 10 -2 7 11 769.920 110.245 12 2 7 -10 2049.47 162.374 10 -2 7 9 1608.07 157.000 17 2 7 -9 1873.61 159.828 10 -2 7 8 2821.10 203.459 12 -2 7 8 3122.42 213.867 17 2 7 -8 3247.58 213.045 10 -2 7 8 2882.47 387.215 9 -2 7 7 2571.78 190.046 12 -2 7 7 2542.02 362.071 9 -2 7 7 2445.88 186.311 17 2 7 -7 2434.18 186.470 10 2 7 -6 3392.72 224.439 10 -2 7 6 3630.52 437.603 9 -2 7 6 4149.22 238.872 17 -2 7 6 3794.18 228.054 12 2 7 -5 21777.1 742.850 10 -2 7 5 20809.9 1126.68 9 -2 7 5 21716.5 725.347 12 -2 7 5 21539.2 725.813 17 2 7 -4 7404.32 342.010 10 -2 7 4 7561.96 328.769 12 -2 7 4 7262.72 325.932 17 -2 7 3 1174.63 227.803 9 -2 7 3 1026.93 105.098 17 -2 7 3 1109.47 107.766 12 2 7 -2 16770.1 584.803 10 -2 7 2 15981.4 543.529 10 -2 7 2 15978.6 904.204 9 -2 7 2 16536.2 555.134 12 -2 7 1 672.655 79.8141 12 -2 7 1 686.621 86.3266 10 2 7 -1 631.740 90.1903 10 -2 7 1 602.001 77.6247 14 2 7 -1 644.209 151.165 7 -2 7 1 675.785 175.963 9 -2 7 0 2239.13 295.845 9 2 7 0 2699.74 294.997 7 -2 7 0 2348.28 161.051 10 2 7 0 2407.42 165.449 10 2 7 1 392.574 129.409 7 -2 7 -1 388.984 126.833 9 -2 7 -1 478.171 81.0751 10 2 7 1 576.253 83.0010 10 -2 7 -2 19819.5 938.683 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5 3 3 9 469.517 144.820 1 3 -3 9 175.472 93.4269 1 3 3 9 428.140 82.6181 16 3 3 9 337.306 80.2169 11 3 3 9 334.676 70.5825 12 3 3 9 353.929 63.9743 17 3 3 10 4973.85 272.322 16 3 3 10 4771.94 261.506 11 3 3 10 5094.72 276.016 12 3 3 10 4759.70 244.910 17 3 3 10 5143.50 445.419 1 3 -3 10 4604.81 424.270 1 3 -3 10 5170.61 262.583 5 3 3 10 5149.70 261.734 5 -3 3 -11 3231.39 219.925 15 3 3 11 3008.98 210.548 16 3 3 11 2309.05 316.679 1 3 -3 11 2762.98 340.936 1 3 3 11 2860.93 184.747 17 3 3 11 2915.42 202.385 11 3 -3 11 3339.92 208.557 5 3 3 11 3084.26 201.107 5 -3 3 -12 673.141 109.973 15 3 -3 12 789.363 107.002 5 3 3 12 528.668 89.8494 5 3 3 12 772.848 115.319 16 3 3 12 491.368 100.559 11 3 -3 12 601.064 181.826 1 3 3 12 489.550 161.411 1 3 -3 13 2560.42 335.696 1 3 3 13 1723.11 281.142 1 3 3 13 2012.89 171.124 11 3 3 13 2163.61 173.092 5 3 -3 13 2717.55 191.024 5 -3 3 -13 2575.03 197.484 15 3 3 13 2333.54 190.861 16 3 3 14 1155.46 126.133 11 3 -3 14 1296.92 132.346 5 3 3 14 1155.99 126.385 5 -3 3 -14 1282.21 136.880 15 3 3 14 1389.30 145.753 16 3 3 15 3168.76 188.600 11 3 3 15 3102.64 194.455 5 3 -3 15 3404.51 204.467 5 -3 3 -15 2736.93 187.580 15 3 3 15 3062.13 203.266 16 3 -3 16 169.802 54.6225 5 3 3 16 57.7492 45.9945 5 3 3 16 149.943 55.0142 11 -3 3 -16 68.6399 46.3861 15 3 3 16 190.523 61.8331 16 3 -3 17 1837.52 116.796 5 3 3 17 1547.95 108.220 5 3 -3 17 1517.71 92.0342 11 -3 4 17 1832.81 100.320 5 -3 4 17 1806.37 115.227 16 -3 -4 16 5.77758 35.8127 5 -3 4 16 17.1337 38.0932 5 -3 4 16 43.6777 33.3950 12 -3 4 16 38.9329 42.7835 16 -3 4 15 261.614 58.6923 5 -3 -4 15 146.189 52.7515 5 -3 4 15 225.673 64.5373 16 -3 4 15 220.237 58.3927 12 -3 -4 14 5273.83 257.745 5 -3 4 14 5170.16 253.710 5 -3 4 14 5153.93 262.004 12 -3 4 14 4787.62 259.854 16 -3 4 13 428.076 82.5423 16 3 4 -13 530.239 138.063 2 -3 -4 13 457.824 80.9378 5 -3 4 13 376.964 74.6429 5 -3 4 13 391.858 80.2668 12 -3 -4 12 3810.94 217.988 5 -3 4 12 3393.05 204.995 5 3 4 -12 3405.67 376.382 2 -3 4 12 3612.57 225.200 12 -3 4 12 3544.66 218.547 16 3 4 -11 14385.1 803.120 2 3 -4 -11 13698.3 794.887 2 -3 -4 11 14144.4 514.950 5 -3 4 11 14458.1 513.968 5 -3 4 11 13677.6 531.081 12 3 -4 -10 187.790 109.038 2 3 4 -10 62.0858 82.6193 2 -3 4 10 108.378 51.5450 12 -3 -4 10 72.6851 50.7820 5 -3 4 10 153.111 56.1990 5 -3 4 9 10983.6 420.012 4 3 4 -9 11841.7 662.846 2 3 -4 -9 10238.3 629.121 2 -3 4 9 11610.5 449.596 12 -3 4 9 10824.9 672.452 9 -3 4 9 12410.6 688.498 6 -3 -4 9 11771.2 679.588 6 -3 4 8 878.103 176.016 9 3 4 -8 948.068 178.488 2 3 -4 -8 682.454 161.958 2 -3 -4 8 966.344 173.340 6 -3 4 8 649.793 139.713 6 -3 4 8 833.314 97.0898 12 3 4 -8 659.626 80.5695 10 -3 4 8 897.408 103.836 17 -3 4 7 2553.14 167.487 17 3 4 -7 2280.37 248.031 2 3 -4 -7 2740.52 268.171 2 -3 4 7 2960.76 270.667 6 -3 -4 7 1993.86 231.916 6 -3 4 7 2930.39 308.204 9 3 4 -6 7525.52 443.520 2 3 -4 -6 7403.36 443.750 2 -3 -4 6 7060.51 425.126 6 -3 4 6 7787.95 444.591 6 -3 4 6 7828.11 507.244 9 -3 4 6 8785.27 560.678 8 3 -4 -5 2222.03 215.815 2 3 4 -5 2347.16 218.653 2 -3 4 5 2355.04 216.712 6 -3 -4 5 2633.85 225.901 6 -3 4 5 2576.00 273.327 9 -3 4 5 2703.98 287.864 8 -3 4 4 5028.86 386.059 9 3 -4 -4 4922.52 306.101 2 3 4 -4 4854.26 301.851 2 3 4 -3 8760.91 405.732 2 3 -4 -3 9161.97 414.301 2 -3 4 3 8297.36 512.383 9 -3 4 2 7597.88 444.444 8 3 4 -2 6401.36 322.406 2 3 -4 -2 6874.36 334.097 2 -3 4 2 7188.71 447.523 9 3 4 -1 16797.6 588.234 2 3 -4 -1 15810.9 587.829 2 -3 4 1 16988.6 719.098 8 -3 4 0 6745.34 393.043 8 3 4 0 5993.43 411.776 7 -3 4 -1 22252.6 763.355 8 3 4 1 21486.7 842.804 7 -3 4 -2 885.578 122.028 8 3 4 2 831.256 116.730 3 3 -4 2 971.798 123.255 3 3 4 2 1193.93 175.592 7 3 4 3 1028.41 170.712 7 3 -4 3 1113.90 130.033 1 3 4 3 1100.17 127.192 1 -3 4 -3 1177.18 129.689 8 3 -4 4 46139.9 1432.06 1 3 4 4 45619.4 1430.53 1 3 4 4 46976.5 1628.06 7 -3 4 -4 44848.1 1338.09 8 3 4 5 24151.5 1059.87 7 3 4 5 24801.3 915.022 1 3 -4 5 24678.2 912.090 1 3 4 6 34898.2 1407.00 7 3 4 6 36187.6 1257.06 1 3 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12 5333.56 300.717 16 3 4 12 5579.83 277.958 17 -3 4 -12 6086.17 323.125 15 3 4 12 5322.04 289.469 11 3 4 12 5029.41 439.639 1 3 -4 12 5576.97 278.135 5 3 4 12 5091.15 265.948 5 3 4 13 435.003 81.6571 5 3 -4 13 418.736 81.1476 5 -3 4 -13 360.179 85.2923 15 3 4 13 634.773 105.237 11 3 4 13 513.468 100.028 16 3 4 14 2659.96 196.777 16 -3 4 -14 2481.36 191.823 15 3 4 14 2658.34 179.686 11 3 4 14 2647.24 170.891 5 3 -4 14 2939.59 181.106 5 -3 4 -15 4858.82 254.186 15 3 4 15 4573.46 248.659 16 3 4 15 4902.22 227.458 5 3 -4 15 4713.85 227.355 5 -3 4 -16 981.678 96.1204 15 3 -4 16 1026.74 85.0171 5 3 4 16 974.564 83.0817 5 -3 5 16 3103.00 155.314 12 -3 5 15 999.824 99.2176 12 -3 5 15 1015.16 92.3183 16 -3 5 14 6773.47 290.264 16 -3 5 14 6478.68 305.490 12 -3 5 13 41.4164 46.3787 16 -3 5 13 40.5972 52.0398 12 -3 5 12 15197.5 543.558 16 -3 5 12 15216.9 573.131 12 -3 5 11 165.620 63.9150 16 -3 5 11 132.180 65.6267 12 3 5 -10 52288.7 1523.71 10 -3 5 10 54265.8 1530.56 16 -3 5 10 53395.3 1575.88 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71.1391 94.6169 7 3 5 7 7338.50 588.943 7 -3 5 -7 8510.10 372.821 15 -3 5 -7 7962.65 354.715 10 3 5 7 7737.60 356.781 12 3 5 7 8178.52 354.701 17 3 5 8 293.280 76.3916 12 3 5 8 411.012 154.836 7 -3 5 -8 272.754 75.0957 10 3 5 8 392.254 76.8198 17 3 5 9 7113.92 344.695 17 -3 5 -9 7792.72 376.487 15 -3 5 -9 8062.98 360.648 10 3 5 10 878.494 125.225 12 3 5 10 830.572 109.143 17 -3 5 -10 1248.49 143.229 15 3 5 10 926.892 119.979 11 -3 5 -11 1359.25 149.225 15 3 5 11 861.785 123.775 11 3 5 11 1078.32 119.414 17 -3 5 -11 1289.82 128.572 14 3 5 12 4555.24 272.917 16 3 5 12 4819.20 258.841 17 -3 5 -12 4600.46 283.099 15 -3 5 -12 4711.57 250.284 14 3 5 12 4987.70 269.467 11 -3 5 -13 9404.52 423.114 15 -3 5 -14 561.571 92.9321 15 -3 5 -15 780.036 94.7869 15 -3 5 -16 1107.49 94.2841 15 -3 6 15 1539.65 113.067 12 -3 6 14 1431.24 125.371 12 -3 6 13 2570.89 180.930 12 -3 6 12 63.4744 56.3030 12 3 6 -11 18792.0 640.095 10 -3 6 11 19941.8 695.280 12 3 6 -10 5249.19 270.617 10 -3 6 10 5767.81 303.766 12 -3 6 9 32705.6 1028.08 12 -3 6 9 32830.0 1460.07 9 3 6 -9 31189.0 993.934 10 3 6 -8 203.622 67.7767 10 -3 6 8 247.761 73.6722 17 -3 6 8 209.060 133.052 9 3 6 -7 2261.18 174.231 10 -3 6 7 2986.70 378.060 9 -3 6 7 2755.19 190.823 17 -3 6 6 26107.7 838.426 12 3 6 -6 26398.3 834.761 10 -3 6 6 24719.9 1207.47 9 -3 6 6 24892.4 824.753 17 -3 6 5 3774.14 221.747 12 3 6 -5 4503.42 238.379 10 -3 6 5 4179.57 224.684 17 -3 6 5 3842.84 410.933 9 3 6 -4 20294.9 960.128 7 3 6 -4 20570.6 701.234 10 -3 6 4 22411.5 696.329 17 -3 6 4 21711.6 1062.44 9 3 6 -3 5583.41 265.865 10 3 6 -3 4997.31 419.138 7 3 6 -2 8449.79 552.421 7 3 6 -1 15218.3 784.168 7 -3 6 1 15556.1 833.367 9 3 6 -1 14945.0 524.332 10 -3 6 0 26741.4 818.477 14 -3 6 0 28074.6 1190.83 9 3 6 0 26123.3 1130.26 7 3 6 0 25738.5 815.608 10 3 6 1 61.1561 86.9600 7 -3 6 -1 30.7669 61.8755 9 3 6 1 73.0999 44.7194 10 -3 6 -1 31.0118 46.1286 10 -3 6 -2 1925.41 147.207 10 3 6 2 2136.59 288.220 7 3 6 2 2270.78 147.296 10 -3 6 -2 2104.71 274.015 9 3 6 3 980.520 95.8972 10 3 6 3 1309.10 228.410 7 -3 6 -3 882.520 180.033 9 -3 6 -3 1265.54 120.444 10 -3 6 -3 1375.55 120.704 15 3 6 3 1329.07 110.087 12 -3 6 -4 21793.7 714.074 15 3 6 4 23411.8 1090.34 7 3 6 4 21051.2 691.309 12 3 6 4 20725.3 664.236 10 -3 6 -4 21817.5 993.660 9 3 6 5 3643.11 401.613 7 -3 6 -5 3972.49 232.032 15 -3 6 -5 3827.24 227.426 10 3 6 5 4152.85 226.447 12 -3 6 -5 3357.72 335.630 9 -3 6 -6 26.3085 52.8995 9 3 6 6-10.4942 51.6870 17 3 6 6-9.56907 47.1303 12 3 6 6-81.3766 122.720 7 -3 6 -6 20.8821 54.5445 10 -3 6 -6-10.5862 51.0420 15 -3 6 -7 7251.96 353.588 15 3 6 7 7489.04 616.672 7 -3 6 -7 7037.40 345.114 10 3 6 7 7338.40 348.137 17 3 6 7 7193.29 345.272 12 -3 6 -8 57683.1 1681.04 10 -3 6 -8 58731.8 1700.35 15 3 6 8 57961.9 1677.12 17 3 6 8 54132.7 1674.30 12 -3 6 -9 2611.90 199.069 10 3 6 9 2732.32 199.772 17 3 6 9 2644.77 206.189 12 -3 6 -9 2845.72 219.063 15 3 6 10 7889.11 365.727 17 3 6 11 145.433 62.7126 17 -3 6 -11 61.9734 54.0161 14 3 6 12 11189.5 447.188 17 -3 6 -12 11900.5 489.076 15 -3 6 -12 11317.1 443.127 14 -3 6 -13 593.535 80.5775 14 -3 6 -13 806.322 109.722 15 -3 6 -14 4524.25 241.282 15 -3 6 -15 3227.62 177.542 15 -3 7 14 129.918 44.4183 12 -3 7 13 373.008 69.3530 12 -3 7 12 803.354 103.514 12 3 7 -11 4292.58 221.943 10 -3 7 11 3905.51 237.723 12 3 7 -10 4775.69 253.225 10 3 7 -9 3803.26 229.793 10 3 7 -8 14743.2 568.636 10 -3 7 8 15637.6 585.112 17 -3 7 8 16122.7 963.389 9 -3 7 8 15682.4 586.118 12 3 7 -7 395.553 87.3512 10 -3 7 7 370.110 81.7125 17 -3 7 7 499.179 164.866 9 -3 7 7 524.979 91.3407 12 3 7 -6 42.6144 54.6160 10 -3 7 6 40.1192 52.3976 17 -3 7 6-44.9046 110.584 9 -3 7 6 10.4965 52.7657 12 3 7 -5 16630.5 605.273 10 -3 7 5 16584.7 586.633 17 -3 7 5 16452.4 972.371 9 -3 7 5 16152.4 591.990 12 -3 7 4 2957.97 194.946 12 -3 7 4 2976.23 187.255 17 3 7 -4 3102.69 207.314 10 -3 7 3 7707.27 336.617 12 3 7 -2 6303.48 491.442 7 -3 7 2 6715.11 288.139 14 -3 7 2 7643.40 589.538 9 -3 7 2 6583.97 285.385 10 3 7 -2 6654.69 317.917 10 -3 7 2 6697.78 298.106 12 -3 7 1 10009.7 385.557 14 3 7 -1 9821.59 404.249 10 -3 7 1 9303.54 375.577 10 3 7 -1 9932.29 638.800 7 -3 7 1 9637.83 672.074 9 -3 7 0 8472.36 362.773 14 3 7 0 9270.89 377.679 10 -3 7 0 9150.97 368.384 10 3 7 0 8664.41 601.034 7 -3 7 0 8424.28 623.075 9 -3 7 -1 2177.61 162.184 14 3 7 1 2185.92 158.519 10 -3 7 -1 2383.06 167.870 10 3 7 1 2064.20 292.685 7 -3 7 -1 1708.71 273.582 9 -3 7 -2-8.07026 47.3099 15 -3 7 -2-34.3703 77.2668 9 3 7 2-8.10954 39.1007 10 -3 7 -2 9.62005 50.2555 10 3 7 2 36.0380 62.7546 7 3 7 3 10004.6 382.951 10 -3 7 -3 9804.06 414.907 10 -3 7 -3 9783.47 642.576 9 -3 7 -3 9695.91 397.397 15 3 7 3 10589.4 704.437 7 3 7 4 1353.76 256.260 7 3 7 4 1389.69 115.811 10 -3 7 -4 1567.17 148.009 10 3 7 4 1659.01 145.213 12 -3 7 -4 1763.29 147.362 15 -3 7 -4 1538.01 235.259 9 -3 7 -5 6181.42 472.505 9 3 7 5 6687.14 578.602 7 -3 7 -5 7020.16 329.318 15 3 7 5 6422.50 333.933 17 3 7 5 6717.84 314.657 12 -3 7 -6 231.360 73.6151 15 3 7 6 149.452 58.5886 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8890.20 364.900 11 4 5 5 8721.84 626.934 7 4 5 6 345.209 75.9086 12 4 5 6 408.914 79.6662 17 4 5 6 568.179 92.2862 11 -4 5 -6 569.561 95.5393 15 4 5 6 309.227 135.104 7 -4 5 -6 483.762 95.3745 10 -4 5 -7 37158.0 1164.82 10 4 5 7 38031.0 1156.65 11 4 5 7 36694.4 1595.43 7 4 5 7 38778.1 1162.02 17 -4 5 -8 25236.5 824.258 14 4 5 8 24415.9 809.762 17 4 5 8 24152.0 813.811 11 -4 5 -9 24593.6 821.747 14 -4 5 -9 25481.2 858.413 15 4 5 9 23919.2 809.655 17 -4 5 -10 813.316 121.212 15 -4 5 -10 684.364 98.3572 14 4 5 10 664.929 96.8876 17 4 5 11 11038.5 436.176 17 -4 5 -11 11139.5 439.810 14 -4 5 -11 10114.1 465.251 15 4 5 12 3235.74 210.255 11 4 5 12 3084.86 188.824 17 -4 5 -12 2755.39 181.989 14 -4 5 -12 2690.95 209.288 15 -4 5 -13 9058.50 400.857 15 -4 5 -14 100.362 54.3274 15 -4 5 -15 246.173 58.6502 15 -4 6 15 1593.58 107.192 12 -4 6 14 629.150 79.6111 12 -4 6 13 5640.33 274.570 12 -4 6 12 339.479 77.5931 12 -4 6 11 6813.52 327.736 12 4 6 -11 6146.39 280.736 10 4 6 -10 2416.04 166.600 10 -4 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5426.93 235.169 5 -7 -3 15 1537.78 108.698 5 -7 3 15 1336.04 103.313 5 -7 -3 14 85.4319 50.1769 5 -7 3 14 128.331 50.7569 5 -7 3 13 3025.05 189.445 4 -7 -3 13 2975.12 191.148 4 -7 3 12 486.629 73.6645 12 -7 -3 12 604.842 92.5452 4 -7 3 12 506.863 85.9677 4 -7 3 11 2506.66 174.883 12 -7 3 11 3102.15 200.963 4 -7 -3 11 2931.75 197.976 4 -7 -3 10 234.832 118.092 6 -7 3 10 78.5999 79.0902 6 -7 3 10 163.539 123.356 8 -7 3 10 158.054 56.9520 12 7 3 -10 124.211 124.921 2 7 -3 -10 292.875 139.549 2 -7 3 10 60.2747 62.3457 4 -7 -3 10 120.828 64.9024 4 -7 3 9 586.261 180.184 8 -7 3 9 976.840 115.564 4 -7 -3 9 992.133 218.310 6 -7 3 9 1265.80 235.767 6 7 3 -9 1064.03 230.304 2 7 -3 -9 828.398 217.674 2 -7 -3 9 910.166 114.136 4 -7 3 8 960.127 234.729 8 -7 3 8 784.090 104.144 4 7 -3 -8 927.964 219.568 2 7 3 -8 676.496 205.209 2 -7 -3 8 995.635 114.023 4 -7 3 7 2308.08 169.925 4 -7 -3 7 2484.66 175.486 4 -7 3 7 2031.46 267.222 9 -7 3 7 2165.36 324.309 8 7 3 -7 2913.47 364.933 2 7 -3 -7 2873.72 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82.6976 4 -7 -3 0 13637.9 482.757 4 -7 3 0 13579.4 483.998 4 7 -3 0 12360.2 736.838 2 7 3 0 13650.1 759.176 2 7 3 1 2188.64 305.361 7 7 3 2 8164.04 600.313 7 -7 3 -2 7254.28 338.422 15 7 3 2 7960.46 562.762 3 7 -3 2 8136.17 570.660 3 7 3 3 2396.45 323.893 7 7 3 3 2987.89 337.015 3 7 -3 3 2481.38 320.409 3 -7 3 -3 2692.88 189.077 15 7 -3 4 1986.61 148.875 5 7 3 4 1833.56 281.132 7 -7 3 -4 1993.33 164.574 15 7 3 4 1958.60 147.395 11 7 3 4 2207.46 320.132 3 7 -3 4 2268.63 320.552 3 -7 3 -5 85.8250 60.0673 15 7 3 5 38.0542 85.5591 7 7 3 5-78.5814 142.431 3 7 -3 5 78.1622 96.2519 3 7 3 5 43.2337 49.9565 5 7 -3 5 79.0862 53.7551 5 7 3 5 65.6496 63.3856 11 7 3 6 18281.7 631.192 5 7 -3 6 17571.9 627.425 5 7 3 6 17818.6 949.190 1 7 -3 6 17332.7 936.606 1 -7 3 -6 18379.5 660.195 15 7 3 6 19053.4 1002.95 7 7 3 6 17991.8 625.167 11 7 -3 7 935.486 111.808 5 7 3 7 1007.13 210.230 1 7 -3 7 966.474 212.819 1 -7 3 -7 1019.61 125.919 15 7 3 7 844.017 108.858 5 7 3 7 983.351 118.463 11 7 3 7 1223.74 245.871 7 7 3 8 8954.36 385.925 5 7 -3 8 9037.38 388.051 5 7 3 8 10396.6 694.577 1 7 -3 8 7980.70 620.985 1 7 3 8 8286.41 397.457 11 -7 3 -8 8758.01 403.011 15 7 3 8 8956.08 657.382 7 7 3 9 4669.37 458.172 1 7 -3 9 4380.73 451.561 1 7 3 9 4485.24 252.266 5 7 -3 9 4075.51 244.968 5 -7 3 -9 4385.06 264.845 15 7 3 9 4486.45 262.028 11 -7 3 -10 591.178 103.018 15 7 3 10 407.886 95.5519 11 7 3 10 547.211 93.6986 5 7 -3 10 527.881 89.9512 5 -7 3 -11 103.233 63.1919 15 7 3 11 70.3671 71.5164 11 7 3 11 56.7539 60.9549 5 7 -3 11 222.467 71.5128 5 -7 3 -12 45.0242 52.0074 15 7 3 12 46.2866 65.8111 11 7 3 12-8.57812 53.8588 5 7 -3 12-8.79470 47.6162 5 -7 3 -13-7.17454 40.1616 15 7 3 13 24.2097 62.8452 11 7 3 13 36.5746 49.3342 5 7 -3 13 7.53621 46.7065 5 7 3 14 10283.8 373.715 11 -7 3 -14 9525.71 338.085 15 7 3 14 9846.46 355.514 5 7 -3 14 10274.8 362.754 5 -7 4 15 19.2501 27.9386 5 -7 -4 14 1204.19 91.4096 5 -7 4 14 1291.87 94.2209 5 -7 4 13 72.0811 40.1076 12 -7 -4 13 64.2972 42.4213 5 -7 4 13 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190.645 3 7 -4 3 872.076 197.569 3 -7 4 -3 798.993 106.444 14 7 4 3 582.752 192.739 7 7 4 4 1978.83 317.201 7 7 -4 4 1878.59 284.260 3 7 4 4 1861.68 282.496 3 7 4 4 1559.36 136.357 11 -7 4 -4 1838.89 156.900 14 -7 4 -4 1952.93 169.580 15 -7 4 -5 5573.65 303.313 15 7 4 5 5922.14 280.901 11 7 4 5 5999.89 548.222 7 7 4 5 5694.11 468.271 1 7 -4 5 4921.10 442.707 1 -7 4 -5 5396.62 289.893 14 7 4 6 431.637 162.755 7 -7 4 -6 517.249 91.3622 14 7 4 6 368.035 150.845 1 7 -4 6 531.681 157.098 1 -7 4 -6 427.740 92.4334 15 7 4 6 318.177 84.3676 11 7 4 6 483.673 79.4430 17 7 4 7 565.588 181.946 7 -7 4 -7 991.924 119.348 14 -7 4 -7 920.888 127.712 15 7 4 7 1103.01 214.975 1 7 -4 7 855.784 183.693 1 7 4 7 951.744 108.529 5 7 -4 7 1012.36 111.609 5 7 4 7 958.583 122.440 11 7 4 8 2086.78 326.772 7 7 4 8 2045.55 159.963 5 7 -4 8 2737.09 181.154 5 -7 4 -8 2470.21 198.468 15 7 4 8 2710.39 329.513 1 7 4 8 2247.68 181.521 11 7 4 9 123.622 75.4330 11 -7 4 -9 107.262 63.4409 15 7 4 9 43.4598 53.2005 5 7 -4 9 98.4771 59.0614 5 7 4 10 40.2452 69.3472 11 7 4 10-8.29923 52.1071 5 7 -4 10-17.1530 47.2279 5 -7 4 -10 45.2603 55.7301 15 -7 4 -11 2919.55 198.830 15 7 4 11 2710.73 190.871 11 7 4 11 2719.81 170.300 5 7 -4 11 2741.01 174.112 5 -7 4 -12 1866.01 149.440 15 7 4 12 1985.55 154.621 11 7 4 12 1805.30 129.441 5 7 -4 12 1878.16 134.286 5 -7 4 -13 175.759 54.5522 15 7 4 13 263.335 70.3103 11 -7 4 -14 1208.69 89.4217 15 -7 5 14 518.061 58.1835 12 -7 5 13 14186.2 475.329 12 -7 5 12 476.581 73.9189 12 -7 5 11 6738.05 309.499 12 -7 5 10 48.9982 45.1659 12 7 5 -9 7591.31 315.403 10 -7 5 9 6735.11 336.639 12 7 5 -8 983.398 108.812 10 7 5 -7 17010.2 603.727 10 -7 5 7 17254.9 949.382 9 -7 5 7 17053.4 1014.66 8 7 5 -6 19.1595 50.9646 10 -7 5 6-39.1924 88.1078 9 -7 5 6 24.3182 48.2148 13 -7 5 5 1596.12 291.239 8 7 5 -5 1302.01 133.198 10 -7 5 5 1807.96 288.008 9 -7 5 5 1488.82 132.581 13 -7 5 4 2019.69 324.720 8 -7 5 4 2101.88 157.239 13 7 5 -4 2081.92 167.094 10 -7 5 4 1878.46 300.723 9 -7 5 3 11508.2 454.094 13 -7 5 3 11922.5 462.204 15 -7 5 3 11615.1 794.146 9 -7 5 3 12378.0 807.142 8 -7 5 2 290.561 73.9122 15 7 5 -2 458.045 166.213 7 -7 5 2 333.205 74.5318 13 -7 5 2 249.047 144.761 9 -7 5 2 197.318 112.479 8 -7 5 1 753.846 104.361 15 7 5 -1 364.354 159.716 7 -7 5 1 722.908 100.462 13 -7 5 1 878.279 219.283 9 7 5 0 31209.7 1452.05 7 -7 5 0 30629.9 1327.40 8 -7 5 0 29597.6 958.039 15 -7 5 -1 2092.76 289.747 8 -7 5 -1 1857.00 162.238 15 7 5 1 2351.35 355.719 7 -7 5 -2 2624.95 195.903 15 -7 5 -2 3012.20 329.717 8 -7 5 -3 1953.83 168.548 15 -7 5 -3 1919.28 162.867 14 -7 5 -4 423.746 86.7067 14 -7 5 -4 363.944 91.9853 15 -7 5 -5 247.304 75.2618 14 7 5 5 184.710 131.480 7 7 5 5 301.950 77.8001 11 7 5 6 422.025 89.9479 11 -7 5 -6 335.764 82.4877 14 7 5 6 554.109 88.0389 17 -7 5 -7 10587.2 447.505 14 -7 5 -7 10896.8 466.976 15 7 5 7 10319.8 763.511 7 7 5 7 10663.6 435.368 11 7 5 7 10119.7 413.254 17 -7 5 -8 20713.8 723.619 14 -7 5 -8 21667.7 757.250 15 7 5 8 22436.8 729.694 11 7 5 8 19864.5 680.362 17 7 5 9 1123.15 129.316 11 -7 5 -9 1245.97 139.333 15 7 5 10 1703.03 149.916 11 -7 5 -10 1837.72 160.566 15 -7 5 -11 1498.54 137.395 15 -7 5 -11 1392.65 110.021 13 -7 5 -12 1893.07 142.772 15 -7 5 -13 413.604 66.8175 15 -7 6 13 66.8678 33.9535 12 -7 6 12 4947.85 228.586 12 -7 6 11 313.029 64.0419 12 -7 6 10 5411.20 273.802 12 7 6 -10 5122.28 233.496 10 -7 6 9 2141.78 167.671 12 7 6 -9 2059.66 147.301 10 -7 6 8 2558.01 187.249 12 7 6 -8 2323.51 165.827 10 7 6 -7 263.368 72.3329 10 7 6 -6 1645.66 146.842 10 -7 6 6 1119.94 249.725 9 7 6 -5 5948.05 300.076 10 7 6 -5 5524.97 554.905 7 -7 6 5 5594.17 539.269 9 -7 6 5 5191.39 261.963 13 7 6 -4 14871.8 564.956 10 -7 6 4 14803.6 534.913 13 -7 6 4 16653.6 962.764 8 -7 6 4 15390.7 932.999 9 7 6 -4 13744.3 926.695 7 7 6 -3 6508.93 329.805 10 -7 6 3 6421.49 304.790 15 -7 6 3 7230.38 322.229 13 -7 6 3 7332.55 609.561 8 -7 6 3 7147.29 613.587 9 7 6 -3 6500.56 607.741 7 -7 6 2 1075.95 243.899 9 7 6 -2 934.379 120.316 10 -7 6 2 925.197 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59.6277 14 7 6 8 281.972 62.9417 17 7 6 9 14869.5 503.298 17 -7 6 -9 15034.7 564.310 15 -7 6 -10 1197.84 127.617 15 -7 6 -11 799.891 97.9068 15 -7 6 -11 813.641 79.0241 13 -7 6 -12 5500.96 244.938 15 -7 7 11 3120.01 170.996 12 -7 7 10 368.427 68.3028 12 7 7 -10 337.648 55.8428 10 -7 7 9 578.407 87.0469 12 7 7 -9 522.180 74.4246 10 -7 7 8 224.774 65.4423 12 7 7 -8 185.266 60.8251 10 7 7 -7 11740.4 453.121 10 -7 7 6 14763.0 568.739 12 7 7 -6 16105.0 569.112 10 7 7 -5 4818.53 264.235 10 -7 7 4 2426.17 161.664 13 7 7 -4 2499.81 188.954 10 -7 7 3 506.349 83.3737 13 7 7 -3 538.184 99.2793 10 -7 7 2 2108.71 151.794 15 -7 7 2 2063.31 158.401 13 -7 7 1 48.8887 49.1595 13 -7 7 1 26.4815 40.6783 15 -7 7 0 6558.79 305.791 15 7 7 0 7028.58 632.010 7 7 7 0 5967.37 315.720 10 -7 7 0 6001.57 580.871 9 7 7 1 4412.30 254.929 10 -7 7 -1 4414.72 248.561 15 7 7 2 12062.7 481.803 10 -7 7 -2 12350.2 482.565 15 7 7 3 3533.41 216.685 10 -7 7 -3 3789.86 232.098 15 7 7 4 571.714 88.1058 10 -7 7 -4 718.081 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240.029 3 8 -3 1 1055.34 229.304 3 -8 3 -1 1250.91 132.184 15 -8 3 -1 1112.73 117.444 4 -8 -3 -1 1223.12 122.448 4 -8 3 -1 1161.67 124.644 13 -8 3 -2 25254.1 841.421 4 -8 3 -2 26301.5 856.460 13 8 3 2 27604.0 1237.99 3 8 -3 2 27057.0 1228.99 3 -8 3 -2 26325.0 869.387 15 8 3 2 26876.4 1282.23 7 -8 3 -3 9417.95 408.689 13 8 3 3 10401.4 714.280 3 8 -3 3 9831.66 702.769 3 -8 3 -3 9784.73 427.464 15 8 3 3 10354.3 719.654 7 -8 3 -4 39727.2 1021.32 13 8 3 4 36059.7 1477.32 7 -8 3 -4 37769.4 1038.23 15 -8 3 -5 440.114 90.1600 15 8 3 5 568.398 182.896 7 8 3 5 431.068 85.3445 11 -8 3 -5 435.005 85.2460 13 8 3 6 13523.0 835.342 1 8 -3 6 15282.5 875.799 1 8 3 6 13437.9 848.930 7 -8 3 -6 14527.5 563.815 15 -8 3 -6 14352.5 535.898 13 8 3 6 14122.4 520.738 11 8 3 7 1325.40 135.807 11 8 3 7 1417.76 261.263 1 8 -3 7 1293.79 254.063 1 8 3 7 1012.41 121.712 5 8 -3 7 1079.80 121.625 5 8 3 7 1508.82 254.146 7 -8 3 -7 1160.47 134.428 15 -8 3 -7 997.652 116.185 13 -8 3 -8 31453.3 987.560 13 -8 3 -8 32683.2 1037.16 15 8 3 8 31393.6 1413.08 1 8 -3 8 31327.1 1407.65 1 8 3 8 32132.1 1007.43 5 8 -3 8 31753.1 1007.39 5 8 3 8 32695.3 1007.12 11 -8 3 -9 1629.21 154.760 15 8 3 9 1750.73 150.074 5 8 -3 9 1965.16 160.162 5 -8 3 -9 1852.36 141.336 13 8 3 9 1705.23 156.126 11 8 3 10 1568.60 139.678 5 8 -3 10 1588.59 141.901 5 -8 3 -10 1743.86 151.003 15 8 3 10 1526.97 148.315 11 8 3 11 187.038 63.7081 5 8 -3 11 317.611 72.6179 5 8 3 11 243.186 75.9375 11 -8 3 -11 366.326 75.2418 15 -8 3 -12 914.499 95.3467 15 8 3 12 955.943 106.434 11 -8 3 -13 717.851 70.7638 15 8 3 13 683.305 84.8697 11 -8 4 14 3715.41 151.712 5 -8 4 13 52.6768 33.0134 12 -8 -4 13 4.94406 34.8007 5 -8 4 13 19.9957 31.3931 5 -8 4 12 17415.2 563.372 12 -8 -4 12 16955.9 561.419 4 -8 4 11 6140.33 284.039 12 -8 4 11 6281.22 279.689 4 -8 -4 11 6570.79 285.857 4 -8 4 10 6317.23 297.632 12 -8 4 10 6111.66 284.965 4 -8 -4 10 6369.21 289.465 4 -8 4 9 8.60178 46.5759 4 -8 -4 9 51.8847 50.6983 4 8 4 -8 11594.1 435.123 10 -8 4 8 11985.9 816.293 8 8 4 -8 11623.5 750.837 2 -8 4 8 11374.2 443.968 4 -8 -4 8 11765.5 448.174 4 8 4 -7 980.850 107.792 10 -8 4 7 1066.85 114.496 4 -8 -4 7 947.263 108.924 4 8 4 -7 1036.75 202.317 2 8 4 -6 3009.58 373.385 2 8 -4 -6 3109.24 382.454 2 -8 4 6 3952.20 224.648 13 -8 4 6 3172.67 379.715 9 -8 4 6 4133.32 222.742 4 -8 -4 6 3414.13 207.464 4 -8 4 6 3752.15 441.326 8 8 4 -6 3795.40 220.059 10 8 4 -5 1649.02 270.702 2 8 -4 -5 1913.48 304.293 2 -8 4 5 1806.36 151.490 13 -8 4 5 2021.29 149.770 4 -8 -4 5 1845.89 149.194 4 -8 4 5 1852.34 290.907 9 -8 4 4 118.880 50.5377 4 -8 -4 4 59.6827 48.5231 4 -8 4 4 39.6218 53.6590 13 8 -4 -4 74.9835 99.7424 2 8 4 -4-36.7088 110.732 2 -8 4 4 38.9945 87.6807 9 -8 4 4 218.389 131.749 8 -8 4 3 336.378 70.4553 4 -8 -4 3 160.247 57.1602 4 -8 4 3 255.382 154.392 8 -8 4 3 190.820 64.8983 13 -8 4 3 219.983 70.8729 15 8 -4 -3 147.669 128.695 2 8 4 -3 253.457 131.372 2 -8 4 3 279.742 133.373 9 -8 4 2 7585.78 620.504 8 -8 4 2 6588.71 332.839 15 8 -4 -2 6101.33 532.120 2 8 4 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454.205 136.268 1 8 4 6 3615.41 213.328 11 8 4 6 2845.33 388.418 7 -8 4 -6 3494.44 236.760 15 8 4 6 2960.29 348.970 1 -8 4 -7 9402.88 426.077 15 8 4 7 9413.43 394.088 11 -8 4 -7 9390.43 401.258 13 8 4 7 9449.64 638.107 1 -8 4 -8 13372.0 532.425 15 8 4 8 13360.8 502.637 11 -8 4 -8 13014.7 495.807 13 -8 4 -9 2208.03 180.926 15 8 4 9 2386.20 175.593 11 -8 4 -9 2444.56 165.839 13 -8 4 -10 4590.56 252.612 15 8 4 10 4365.37 236.268 11 -8 4 -10 4264.63 211.451 13 8 4 11 764.104 97.3224 11 -8 4 -11 638.458 88.2454 15 8 4 12 868.921 96.6178 11 -8 4 -12 1003.99 96.5360 15 -8 4 -13 143.964 38.9576 15 -8 5 13 7232.27 264.856 12 -8 5 12 1114.25 96.1467 12 -8 5 11 10041.6 385.426 12 -8 5 10 95.1198 51.4899 12 8 5 -9 10851.5 407.206 10 -8 5 9 11664.4 452.062 12 8 5 -8 3749.52 211.509 10 8 5 -7 1115.48 116.145 10 -8 5 6 7476.95 323.647 13 8 5 -6 7473.11 339.566 10 -8 5 5 9.23489 55.7235 13 -8 5 5 121.257 90.8746 9 8 5 -5 99.2762 54.6848 10 -8 5 5 91.1630 129.623 8 -8 5 4 2321.95 174.958 13 -8 5 4 2466.45 354.765 8 -8 5 4 2390.55 348.190 9 8 5 -4 2589.34 189.397 10 -8 5 3 1930.69 160.359 13 -8 5 3 2449.72 354.876 9 8 5 -3 2036.97 357.020 7 -8 5 3 2179.90 337.862 8 -8 5 2 1765.35 153.961 13 -8 5 2 2086.84 166.271 15 -8 5 2 1313.64 264.556 9 8 5 -2 1387.92 290.024 7 -8 5 2 2316.45 341.919 8 -8 5 1 4226.57 478.904 9 -8 5 1 4413.44 259.017 15 -8 5 1 4564.01 464.851 8 8 5 -1 4545.65 514.748 7 -8 5 1 4638.98 260.366 13 -8 5 0 608.153 99.2010 15 8 5 0 831.421 236.497 7 -8 5 0 796.890 107.054 13 -8 5 0 690.025 197.344 8 -8 5 -1 1426.41 144.321 15 -8 5 -1 1289.96 246.912 8 -8 5 -2 5406.87 300.620 15 -8 5 -2 5651.10 297.743 13 8 5 3 238.920 152.068 7 -8 5 -3 272.484 86.1550 15 8 5 4 2498.04 378.551 7 8 5 5 1020.21 243.438 7 8 5 5 921.330 107.503 17 -8 5 -6 5091.32 289.398 15 8 5 6 4672.19 242.691 17 -8 5 -7 5311.43 299.549 15 8 5 7 5729.30 254.982 17 -8 5 -8 255.369 79.2480 15 -8 5 -8 292.771 69.8044 13 -8 5 -9 2425.97 180.999 15 -8 5 -9 2191.51 154.740 13 -8 5 -10 1498.01 132.446 15 -8 5 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118.005 15 8 6 1 687.141 216.434 7 8 6 2 3781.69 233.685 10 -8 6 -2 4100.61 246.382 15 8 6 2 3548.24 456.182 7 8 6 3 750.304 103.450 10 -8 6 -3 485.924 94.9647 15 8 6 4 36.4958 46.7863 10 -8 6 -4 56.8919 62.6664 15 8 6 5 612.117 89.1828 10 -8 6 -5 826.032 112.699 15 8 6 5 579.224 90.6446 17 8 6 6 1134.88 113.010 17 8 6 6 1132.65 107.285 10 8 6 7 2158.21 144.363 17 8 6 7 1898.79 126.576 10 8 6 8 83.6306 38.0694 17 -8 6 -8 108.490 50.3807 13 -8 6 -8 29.4470 54.9810 15 -8 6 -9 3373.76 186.242 13 -8 6 -9 3377.37 203.888 15 -8 6 -10 8527.43 313.834 13 -8 6 -10 8575.54 345.287 15 -8 6 -11 899.997 87.3611 15 -8 7 10-6.10011 32.4523 12 8 7 -9 1404.91 101.393 10 -8 7 9 1655.79 123.587 12 -8 7 8 119.867 50.9905 12 8 7 -8 218.231 53.7719 10 8 7 -7 866.324 96.9675 10 8 7 -6 4888.78 249.428 10 -8 7 5 13126.6 454.372 13 8 7 -5 14002.6 508.428 10 -8 7 4 5785.03 267.973 13 8 7 -4 6595.81 307.524 10 -8 7 3 16.5206 46.9792 13 8 7 -3 9.83780 53.2636 10 -8 7 2 11557.6 441.995 13 8 7 -2 11023.9 454.495 10 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5192.49 250.259 10 -8 8 4 4831.29 241.342 12 -8 8 3 2087.24 150.036 12 -8 8 3 1950.72 129.019 13 -8 8 2 694.292 86.2994 12 -8 8 2 681.670 82.1224 13 -8 8 1 9000.22 353.507 13 8 8 -1 8748.32 366.286 10 -8 8 0 1073.06 107.871 13 8 8 0 1160.46 112.952 10 -8 8 -1 1776.56 127.651 15 -8 8 -1 1729.98 139.601 13 8 8 1 2113.41 147.092 10 -8 8 -2 2457.03 157.491 15 8 8 2 2959.32 172.552 10 -8 8 -2 2437.10 166.988 13 -8 8 -3 15478.1 539.247 15 8 8 3 16055.5 532.943 10 -8 8 -3 17129.0 565.511 13 8 8 3 15791.6 565.455 17 8 8 4 839.102 95.4040 17 8 8 4 769.401 78.4618 10 -8 8 -4 869.390 93.9173 15 8 8 5 599.447 75.9755 17 -8 8 -5 579.566 77.5753 15 -8 8 -5 655.215 86.1360 13 8 8 5 453.371 53.9322 10 -8 8 -6 5165.14 237.178 13 -8 8 -6 5243.17 233.798 15 8 8 6 5137.31 224.635 17 -8 8 -7 4767.55 210.654 13 8 8 7 4311.07 184.036 17 -8 8 -7 4267.32 200.418 15 8 9 -5 280.372 52.3332 10 -8 9 5 199.898 43.7382 12 8 9 -4 1359.59 106.843 10 -8 9 4 1514.12 98.5413 12 -8 9 3 424.584 55.3835 12 8 9 -2 10511.4 359.951 10 -8 9 2 8724.60 314.238 12 -8 9 1 282.828 47.4216 13 -8 9 1 223.003 39.1926 12 -8 9 0 5230.68 218.251 13 8 9 0 5270.83 229.859 10 -8 9 -1 601.438 70.8767 13 8 9 1 648.389 73.1149 10 8 9 1 598.526 81.6323 17 -8 9 -2 1876.85 119.976 13 8 9 2 1565.72 103.834 10 8 9 2 1614.47 123.618 17 -8 9 -3 110.988 44.3481 13 8 9 3 48.5561 38.6671 17 8 9 3 117.760 34.3932 10 -9 0 14-6.73308 43.8698 4 -9 0 13 2528.51 169.748 4 -9 0 12-18.5288 55.8868 4 -9 0 11 24563.3 813.445 4 -9 0 10 10.6569 55.6726 4 -9 0 9 17812.9 643.135 4 9 0 -9 16473.3 1024.86 2 9 0 -8 47.8585 136.113 2 -9 0 8 111.053 70.6570 4 -9 0 7 31861.1 1021.60 4 9 0 -7 31226.5 1507.88 2 9 0 -6-47.7887 127.116 2 -9 0 6-10.9577 59.3272 4 9 0 -5 17874.8 1059.02 2 -9 0 5 17595.2 642.206 4 9 0 -4 139.848 140.600 2 -9 0 4 10.6721 61.6383 4 9 0 -3 5078.85 529.723 2 -9 0 3 4107.00 246.670 4 9 0 -2 45.2078 143.727 2 -9 0 2 10.4454 51.4476 4 -9 0 2 10.5526 55.1279 13 9 0 -1 18311.7 1054.60 2 -9 0 1 17715.6 636.803 13 -9 0 1 17223.2 634.145 4 -9 0 0 20.4581 55.3892 13 9 0 0 44.6390 118.741 2 -9 0 0 63.2898 58.0936 4 -9 0 -1 563.477 93.0664 13 -9 0 -1 655.189 96.4755 15 9 0 1 440.832 149.047 7 -9 0 -1 361.876 85.2445 4 9 0 2-44.7344 118.992 3 -9 0 -2 9.87093 50.6030 13 -9 0 -2-19.9514 54.0097 15 9 0 3 88.1216 132.929 3 -9 0 -3 173.223 68.4852 13 -9 0 -3 98.8064 51.7120 15 9 0 4 47.1774 142.292 3 -9 0 -4 9.27986 47.5730 13 -9 0 -4 9.74741 46.9986 15 -9 0 -5 9582.45 398.444 13 -9 0 -5 10334.6 416.354 15 -9 0 -6 36.7688 48.9107 15 9 0 7 32443.2 1499.52 1 9 0 8-10.9844 66.2609 5 9 0 9 30472.7 978.711 5 9 0 10-19.8075 58.9080 5 9 0 11 12874.0 488.593 5 9 0 11 13225.9 477.193 11 9 0 12 55.0892 55.8336 11 9 0 13 6766.61 268.689 11 -9 -1 14 334.923 61.8187 5 -9 1 13 1873.25 143.952 4 -9 -1 13 2225.75 153.614 4 -9 -1 12 9436.33 389.685 4 -9 -1 11 799.977 107.516 4 -9 1 10 7594.81 360.801 4 -9 -1 10 8498.12 373.447 4 -9 1 9 4815.42 277.515 4 -9 -1 9 5136.86 279.973 4 9 1 -9 4089.10 485.688 2 9 -1 -9 4856.50 516.463 2 -9 1 8 18462.0 672.801 4 -9 -1 8 18715.3 675.826 4 9 1 -8 20138.8 1126.54 2 9 -1 -8 18423.9 1089.58 2 -9 1 8 19032.5 1039.93 8 9 1 -7 380.004 178.758 2 9 -1 -7 95.4607 127.064 2 -9 1 7 208.527 74.1963 4 -9 -1 7 197.756 78.2717 4 9 1 -6 8329.29 687.956 2 9 -1 -6 7894.60 665.768 2 -9 -1 6 8049.14 369.844 4 -9 1 6 7672.54 365.550 4 -9 1 5 3980.75 243.957 4 -9 -1 5 3860.36 241.509 4 9 1 -5 4178.38 478.143 2 9 -1 -5 4151.28 475.631 2 -9 1 4 17937.1 651.326 4 -9 -1 4 17973.0 653.861 4 9 1 -4 19645.3 1098.82 2 9 -1 -4 17691.8 1058.58 2 -9 1 3 439.667 91.6158 4 -9 -1 3 314.272 80.7444 4 9 1 -3 363.202 158.387 2 9 -1 -3 319.245 159.104 2 -9 1 2 852.938 113.355 13 9 1 -2 494.953 187.389 2 9 -1 -2 406.821 182.673 2 -9 -1 2 842.336 114.041 4 -9 1 2 633.925 99.1093 4 -9 1 1 253.518 76.0204 13 9 -1 -1 89.5651 156.051 2 9 1 -1 133.907 142.004 2 -9 1 1 176.952 73.4389 4 -9 -1 1 229.137 75.6885 4 9 -1 0 40599.3 1733.01 2 9 1 0 38441.2 1700.14 2 -9 1 0 39734.4 1221.91 4 -9 -1 0 38746.5 1216.89 4 -9 1 0 40350.0 1224.07 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537.213 95.3461 13 -9 2 -3 1080.12 131.052 15 9 2 3 584.510 185.564 7 -9 2 -3 1137.88 125.974 13 9 2 3 1287.16 272.659 3 9 -2 3 839.826 223.692 3 9 2 4 565.805 166.426 7 -9 2 -4 942.631 114.945 13 9 2 4 572.675 204.472 3 9 -2 4 855.565 239.712 3 -9 2 -4 699.061 108.671 15 -9 2 -5 7067.84 335.104 13 9 2 5 6101.69 536.373 7 9 2 5 9044.47 714.559 3 9 -2 5 7980.59 678.827 3 -9 2 -5 7374.68 354.872 15 -9 2 -6 47.3565 49.4889 13 9 2 6-42.4953 104.655 1 9 -2 6 127.110 134.709 1 9 2 6 57.5268 59.0128 11 -9 2 -6 22.1010 56.6583 15 -9 2 -7 104.635 55.5136 13 -9 2 -7 117.489 62.6756 15 9 2 7 146.248 69.7861 11 9 2 7 42.2632 85.0258 1 9 -2 7 126.402 119.845 1 9 2 8-26.2064 65.7211 11 -9 2 -8 20.0567 58.7887 15 9 2 9 27870.6 866.764 11 -9 2 -9 26850.0 867.965 15 -9 2 -10 216.272 60.3263 15 9 2 10 129.417 70.1045 11 -9 2 -11 239.354 52.4527 15 9 2 11 233.998 68.8403 11 9 2 12 24.9607 51.7378 11 -9 -3 13 2956.21 155.563 5 -9 3 13 3229.32 161.417 5 -9 3 12 2331.63 150.031 4 -9 -3 12 2289.08 149.551 4 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9 3 4 2454.81 368.326 3 9 -3 4 2758.35 382.778 3 9 3 4 1636.63 292.015 7 9 3 5 5109.22 491.628 1 9 -3 5 5478.17 502.005 1 -9 3 -5 5859.14 308.389 15 -9 3 -5 5489.01 286.572 13 9 3 5 4590.75 468.667 7 9 3 6 1429.64 258.724 1 9 -3 6 1342.63 251.105 1 -9 3 -6 1774.90 151.681 13 9 3 6 1355.43 126.458 11 -9 3 -6 1784.17 161.111 15 -9 3 -7 9.11594 50.2023 13 9 3 7 16.6719 59.8537 11 -9 3 -7 66.5986 63.1302 15 -9 3 -8 2829.94 178.138 13 -9 3 -8 2787.71 199.198 15 9 3 8 2946.06 189.085 11 9 3 9 8.06556 60.1369 11 -9 3 -9-9.41163 50.9552 15 -9 3 -10 3404.98 200.803 15 9 3 10 4009.72 209.553 11 9 3 11 541.069 78.2711 11 -9 3 -11 295.391 60.3336 15 9 3 12 60.3492 47.4594 11 -9 3 -12 30.2973 34.5538 15 -9 4 13 4928.11 178.796 5 -9 4 12 124.054 36.5609 12 -9 -4 12 192.167 41.8313 5 -9 4 12 127.615 39.5915 5 -9 4 11 18.7596 35.5658 12 -9 4 11-11.9798 39.4914 4 -9 -4 11 61.0102 43.8058 4 -9 4 10 3760.26 202.099 12 -9 4 10 3582.19 191.739 4 -9 -4 10 3525.08 191.130 4 -9 4 9 8.64544 42.5830 12 -9 4 9 15.2628 47.9156 4 -9 -4 9 23.1189 43.1390 4 9 4 -8 6.97367 47.0436 10 -9 -4 8 89.9363 52.6436 4 -9 4 8 56.7492 48.9145 4 9 4 -7 1156.08 112.569 10 -9 4 7 1148.24 114.750 4 -9 -4 7 1106.45 115.617 4 -9 4 6 457.822 80.6362 4 -9 -4 6 538.866 86.5840 4 9 4 -6 525.134 85.8687 10 9 4 -5 1063.14 117.813 10 -9 4 5 901.647 106.896 4 -9 -4 5 1021.69 113.549 4 -9 4 5 819.210 177.246 9 9 4 -5 1126.48 232.297 2 -9 4 5 821.078 109.240 13 9 4 -4 271.677 103.269 2 -9 4 4 114.298 54.5540 4 -9 -4 4 79.5366 50.3303 4 -9 4 4 45.1708 111.271 8 -9 4 4 78.8089 56.0883 9 -9 4 4 115.297 64.1541 13 9 4 -3 231.447 122.770 2 -9 4 3 82.2494 109.538 9 -9 4 3 215.509 69.5998 13 -9 4 3 401.613 161.857 8 -9 4 3 203.064 63.0220 4 -9 -4 3 274.979 70.4497 4 -9 4 2 35.4747 51.2246 4 -9 -4 2 62.3481 49.0516 4 -9 4 2 43.6554 76.0222 8 -9 4 2 42.5193 74.0440 9 -9 4 2 10.9321 59.1913 13 -9 4 2-11.3094 62.2805 15 -9 4 1 465.980 170.736 8 9 4 -1 544.581 193.106 7 -9 4 1 397.472 92.2386 13 9 4 -1 547.454 171.742 3 -9 4 1 435.110 79.1600 4 -9 -4 1 392.434 77.9702 4 -9 4 1 528.206 96.5673 15 9 4 0-48.7617 138.660 7 9 4 0-37.8557 142.404 3 -9 4 0 35.6843 49.9389 4 -9 -4 0 53.7210 52.4894 4 -9 4 0 122.352 100.437 8 -9 4 0 23.2743 58.4995 15 9 4 1 6081.42 589.565 7 -9 4 -1 5753.67 517.236 8 -9 4 -1 5809.59 284.533 4 -9 -4 -1 5788.12 286.646 4 9 4 1 5952.40 519.716 3 -9 4 -1 6357.94 318.330 13 -9 4 -2 800.618 172.279 8 9 4 2 642.427 198.340 3 -9 4 -2 470.466 85.7087 4 -9 -4 -2 562.467 88.7914 4 -9 4 -2 635.466 102.012 13 9 4 3 873.803 223.749 7 9 4 3 1079.96 215.024 3 -9 4 -3 1184.39 132.246 13 -9 4 -3 1232.31 122.994 4 -9 -4 -3 1207.77 123.952 4 -9 4 -3 1167.87 134.075 15 -9 4 -4 4873.31 287.881 15 9 4 4 5043.06 516.791 7 -9 4 -4 4778.90 259.528 4 -9 -4 -4 5481.00 271.130 4 -9 4 -4 5426.13 287.568 13 9 4 4 5735.97 484.003 1 -9 4 -5 2370.29 188.709 15 -9 4 -5 2060.68 161.681 4 -9 -4 -5 2207.51 165.128 4 -9 4 -5 2177.86 176.072 13 9 4 6 492.601 87.2073 11 -9 4 -6 632.278 105.516 15 -9 4 -6 544.780 85.7878 4 -9 -4 -6 413.116 79.6818 4 -9 4 -6 617.746 97.5289 13 9 4 7 2591.05 169.245 11 -9 4 -7 2689.26 195.859 15 -9 4 -7 2216.66 168.144 13 9 4 8 321.709 74.2235 11 -9 4 -8 249.480 65.6381 13 -9 4 -8 295.635 77.7218 15 -9 4 -9 8072.71 324.221 13 -9 4 -9 8478.32 363.126 15 9 4 9 8799.95 343.191 11 -9 4 -10 1609.75 128.171 15 -9 4 -11 635.336 65.2242 4 -9 -4 -11 499.189 59.7559 4 -9 4 -11 626.813 76.0970 15 -9 5 12 4601.75 186.563 12 -9 5 11 5001.01 220.420 12 -9 5 10 5347.49 247.526 12 -9 5 9 137.652 52.2444 12 9 5 -8 833.540 89.0407 10 9 5 -7 4853.59 245.066 10 9 5 -6 2177.85 161.070 10 -9 5 5 1236.05 122.356 13 9 5 -5 1272.67 130.794 10 -9 5 4 1948.16 158.647 13 9 5 -4 1808.42 156.403 10 -9 5 3 1377.18 136.040 13 9 5 -3 1221.74 134.726 10 -9 5 2 328.090 79.9484 13 9 5 -2 150.878 133.969 7 -9 5 1 64.8152 54.3357 13 -9 5 1 133.781 77.6763 9 -9 5 1 11.0197 54.3083 15 -9 5 0 2310.80 355.970 9 -9 5 0 2443.96 190.623 15 -9 5 0 2759.52 199.493 13 -9 5 -1 6776.56 342.317 15 -9 5 -2 6828.79 344.529 15 -9 5 -2 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-3 2 145.671 60.7724 4 -11 3 1 222.367 74.7558 13 -11 -3 1 147.175 59.5110 4 -11 3 0 3307.66 216.721 13 -11 3 0 3247.68 202.664 4 -11 -3 0 3191.77 202.319 4 -11 3 -1 1238.40 133.954 13 -11 3 -1 1064.31 117.716 4 -11 -3 -1 1398.15 129.463 4 -11 3 -2 11589.7 462.470 13 -11 3 -2 11480.4 469.137 15 -11 3 -2 11237.0 443.306 4 -11 -3 -2 11391.0 445.623 4 -11 3 -3 5350.24 276.246 13 -11 3 -3 5525.83 284.945 15 -11 3 -3 5387.50 266.595 4 -11 -3 -3 4938.18 262.205 4 -11 3 -4 5171.69 260.255 13 -11 3 -4 5314.14 273.187 15 -11 3 -4 4804.63 249.803 4 -11 -3 -4 4963.89 252.979 4 -11 3 -5 3874.42 212.335 13 -11 3 -5 3645.82 218.897 15 -11 3 -5 3942.98 213.930 4 -11 -3 -5 4001.62 213.791 4 -11 3 -6 9030.59 351.908 13 -11 3 -6 8972.78 368.336 15 -11 3 -6 9534.25 362.729 4 -11 -3 -6 8958.59 357.917 4 -11 3 -7 2149.54 131.350 13 -11 3 -7 2411.75 153.812 15 -11 3 -7 2646.88 153.655 4 -11 -3 -7 2215.53 145.310 4 -11 3 -8 2071.39 129.324 15 -11 3 -8 2074.16 127.023 4 -11 -3 -8 1706.90 119.296 4 -11 3 -9 1413.89 94.0403 4 -11 -3 -9 1372.93 93.5278 4 -11 4 9 181.718 39.7430 12 -11 4 9 158.218 37.7685 4 -11 -4 9 120.321 36.0703 4 -11 4 8 801.957 80.9735 12 -11 4 8 814.409 73.6773 4 -11 -4 8 733.123 72.6900 4 11 4 -7 4.74329 29.7857 10 -11 4 7 10.6978 38.0291 4 -11 -4 7 65.5728 39.2368 4 11 4 -6 302.135 59.8881 10 -11 4 6 375.337 61.1539 4 -11 -4 6 376.022 61.6299 4 -11 4 5-6.42816 40.3599 4 -11 -4 5-13.0544 39.3739 4 11 4 -5 56.1793 45.2072 10 -11 4 4 67.7980 43.6781 4 -11 -4 4 75.6733 46.9396 4 11 4 -4 54.6435 49.6650 10 -11 4 3 795.469 103.700 13 11 4 -3 795.437 96.4630 10 -11 4 3 676.930 84.9201 4 -11 -4 3 792.254 90.5712 4 -11 -4 2 1261.21 114.197 4 -11 4 2 1556.77 123.039 4 -11 4 2 1508.84 139.430 13 -11 4 1 1941.88 139.382 4 -11 -4 1 1809.06 135.403 4 -11 4 0 7.32244 42.9271 4 -11 -4 0-29.5734 42.0487 4 -11 4 0-9.86374 53.4039 13 -11 4 -1 2362.48 156.763 4 -11 -4 -1 2574.30 164.023 4 -11 4 -1 2298.49 173.739 13 -11 4 -2 1623.60 126.861 4 -11 -4 -2 1581.49 126.281 4 -11 4 -2 1805.63 149.918 13 -11 4 -2 1651.72 148.040 15 -11 4 -3 11697.3 428.926 4 -11 -4 -3 12061.5 432.505 4 -11 4 -3 12387.2 468.294 13 -11 4 -3 12488.5 476.955 15 -11 4 -4 225.886 63.6652 13 -11 -4 -4 121.947 50.1899 4 -11 4 -4 197.374 56.7161 4 -11 4 -4 198.608 64.3391 15 -11 4 -5 2650.46 150.386 4 -11 4 -5 3068.18 177.729 13 -11 4 -5 2853.30 178.847 15 -11 4 -6 179.970 53.8188 13 -11 -4 -6 123.323 42.4650 4 -11 4 -6 229.137 47.6339 4 -11 4 -6 90.7925 47.0522 15 -11 -4 -7 7469.29 266.785 4 -11 4 -7 6970.54 262.499 4 -11 4 -7 7707.62 282.986 13 -11 4 -8 37.1212 34.5650 15 -11 5 8 4.92622 31.3236 12 11 5 -7 1084.86 81.8304 10 -11 5 7 1432.33 106.687 12 11 5 -6 426.144 59.1948 10 11 5 -5 3679.04 188.166 10 11 5 -4 1370.54 115.383 10 -11 5 3 14786.0 525.439 13 11 5 -3 15344.9 524.240 10 -11 5 2 3129.57 189.152 13 11 5 -2 2865.24 178.959 10 -11 5 1 4677.46 242.049 13 11 5 -1 4323.85 229.610 10 11 5 0 105.186 52.1565 10 -11 5 -1 1833.27 147.201 13 -11 5 -2 3762.36 214.495 13 -11 5 -3 1183.19 115.204 13 11 5 3 1250.71 112.516 10 -11 5 -4 3100.11 182.897 15 11 5 4 2931.46 166.578 10 -11 5 -4 2865.45 173.981 13 -11 5 -5 110.685 47.8798 13 11 5 5 184.472 49.0093 10 -11 5 -6 2306.69 144.584 15 -11 5 -6 2228.64 132.949 13 11 5 6 2284.56 120.873 10 -11 6 6 1701.58 114.704 12 11 6 -6 1657.50 99.9279 10 11 6 -5 2980.72 151.077 10 11 6 -4 79.4622 41.5924 10 11 6 -3 3160.17 170.741 10 11 6 -2 703.525 82.5445 10 -11 6 2 733.097 86.5142 13 11 6 -1 19.9700 39.0362 10 -11 6 1 68.0528 46.9160 13 -11 6 0 642.625 81.1346 13 11 6 1 9337.16 336.289 17 11 6 1 11597.4 386.511 10 -11 6 -2-13.5546 42.5537 13 11 6 2 47.9371 42.1724 10 -11 6 -3 6277.27 262.741 13 11 6 3 5898.22 245.651 10 -11 6 -4 1460.03 107.976 13 11 6 4 1270.54 94.3084 10 -12 0 9-17.9549 39.9155 4 -12 0 8 7344.31 301.084 4 -12 0 7 60.3649 51.4746 4 -12 0 6 9288.30 373.636 4 -12 0 5-69.1180 55.6464 4 -12 0 4 638.843 91.0312 4 -12 0 3 46.4010 51.9608 4 -12 0 2 16633.6 594.388 4 -12 0 1 67.0733 57.0173 4 -12 0 0 554.945 91.3480 4 -12 0 -1-9.47656 49.5065 4 -12 0 -2 7034.29 323.646 4 -12 0 -3-44.9155 59.9180 4 -12 0 -4 25.6987 54.4723 4 -12 0 -5 8.03486 47.7904 4 -12 0 -6 571.633 80.3549 4 -12 0 -7 6.49886 41.3233 4 -12 1 9 810.249 81.7232 4 -12 -1 9 739.983 81.3181 4 -12 1 8 333.863 63.7498 4 -12 -1 8 361.624 65.3742 4 -12 1 7 6756.34 297.513 4 -12 -1 7 7599.27 308.593 4 -12 1 6 2124.65 152.987 4 -12 -1 6 2068.53 149.690 4 -12 1 5 3758.69 214.156 4 -12 -1 5 4080.49 221.674 4 -12 -1 4 1217.87 119.654 4 -12 -1 3 12437.0 473.445 4 -12 -1 2 55.4323 54.9686 4 -12 -1 1 3467.35 211.809 4 -12 -1 0 671.746 94.8980 4 -12 -1 -1 7310.80 332.061 4 -12 -1 -2 9.04188 56.7700 4 -12 -1 -3 2530.89 172.264 4 -12 1 -4 2361.53 163.286 4 -12 -1 -4 2082.45 154.272 4 -12 1 -5 2191.58 157.645 4 -12 -1 -5 2278.92 156.033 4 -12 1 -6 6707.85 287.071 4 -12 -1 -6 6627.18 287.707 4 -12 1 -7 1699.33 121.779 4 -12 -1 -7 1625.16 118.232 4 -12 2 8 5279.01 230.603 4 -12 -2 8 5703.48 236.788 4 -12 2 7 3848.55 193.122 4 -12 -2 7 3692.22 191.350 4 -12 2 6 1167.57 107.155 4 -12 -2 6 1183.35 108.598 4 12 2 -5 2473.96 142.918 10 -12 -2 5 2426.97 163.141 4 -12 2 4 1729.62 138.315 4 -12 -2 4 2052.72 149.409 4 -12 2 3 24.7154 54.3131 4 -12 -2 3-24.8517 52.0106 4 -12 2 2 4126.78 222.413 4 -12 -2 2 3868.04 219.703 4 -12 2 1 111.178 55.8796 4 -12 -2 1 240.604 67.0501 4 -12 2 0 5214.01 257.975 4 -12 -2 0 4790.85 251.398 4 -12 2 -1 3205.17 194.795 4 -12 -2 -1 3175.99 195.641 4 -12 2 -2 1522.84 130.417 4 -12 -2 -2 1677.43 137.052 4 -12 2 -3 229.480 64.9176 4 -12 -2 -3 246.149 63.6542 4 -12 2 -4 246.421 61.8344 4 -12 -2 -4 292.075 62.9202 4 -12 -2 -5 200.236 53.2234 4 -12 2 -5 296.179 62.6264 4 -12 2 -6 4146.71 201.330 4 -12 -2 -6 4284.73 203.331 4 -12 2 -7 5902.98 241.213 4 -12 -2 -7 6136.67 244.054 4 -12 3 8 1070.56 80.6120 4 -12 -3 8 1188.02 82.6099 4 -12 3 7 2379.15 132.195 4 -12 -3 7 2320.18 133.321 4 -12 3 6 5929.70 248.218 4 -12 -3 6 6208.54 252.820 4 12 3 -5 41.8051 34.0638 10 -12 3 5 30.9644 40.8407 4 -12 -3 5 50.1819 42.3176 4 -12 3 4 2894.92 167.719 4 -12 -3 4 3225.59 175.672 4 12 3 -4 2968.40 165.586 10 -12 3 3 979.496 97.4491 4 -12 -3 3 933.937 97.3969 4 -12 -3 2 1292.85 111.863 4 -12 3 2 1139.05 106.932 4 -12 3 1 7449.75 307.588 4 -12 -3 1 7227.56 309.356 4 -12 3 0 64.6091 53.5272 4 -12 -3 0-7.23851 44.2690 4 -12 3 -1 14704.5 493.468 4 -12 -3 -1 13559.6 486.239 4 -12 3 -2 568.810 82.7610 13 -12 3 -2 567.274 78.2780 4 -12 -3 -2 626.568 82.1127 4 -12 3 -3 10665.1 382.968 4 -12 -3 -3 10094.3 378.519 4 -12 3 -4 36.0599 39.1691 4 -12 -3 -4 36.3115 38.0083 4 -12 3 -5 2195.77 131.416 4 -12 -3 -5 2210.74 130.786 4 -12 3 -6 115.366 38.0824 4 -12 -3 -6 107.069 42.2183 4 -12 4 6 2577.75 116.144 4 12 4 -6 2231.50 112.940 10 -12 4 5 2562.12 126.985 4 -12 -4 5 2582.98 127.299 4 12 4 -5 2486.17 135.441 10 -12 4 4 3741.55 168.111 4 -12 -4 4 3787.66 170.908 4 12 4 -4 4238.31 192.134 10 -12 4 3 673.213 69.5154 4 12 4 -3 655.522 77.3758 10 -12 -4 3 587.893 69.2781 4 -12 4 2 9012.29 318.343 4 -12 -4 2 8525.94 316.772 4 -12 4 1 1512.21 104.652 4 -12 -4 1 1559.28 105.137 4 12 4 -1 1603.81 124.170 10 -12 4 0 5935.61 236.831 4 -12 -4 0 5958.07 238.540 4 -12 4 -1 363.684 66.7152 13 -12 -4 -1 317.418 53.0276 4 -12 4 -1 213.953 47.6943 4 -12 4 -2 3679.83 196.914 13 -12 4 -2 3664.60 165.894 4 -12 -4 -2 3536.75 164.543 4 -12 4 -3 956.573 93.1036 13 -12 4 -3 848.390 71.9667 4 -12 -4 -3 936.087 75.4215 4 -12 4 -4 40.1623 38.6967 13 -12 4 -4 3.58783 29.5279 4 12 4 5 988.624 80.4495 10 12 5 -4 715.330 68.1493 10 12 5 -3 7874.14 292.073 10 12 5 -2 16.5602 38.8501 10 12 5 -1 4866.27 216.432 10 12 5 0 6420.07 261.539 10 -12 5 -1 2488.88 150.203 13 12 5 2 21.0644 39.6223 10 -12 5 -2 17.3929 33.9906 13 -13 0 6-27.6912 37.3577 4 -13 0 5 2386.19 142.737 4 -13 0 4 25.9269 45.1525 4 -13 0 3 11107.4 405.387 4 -13 0 2 55.7116 51.4687 4 -13 0 1 2627.27 164.178 4 -13 0 0-7.04851 45.3750 4 -13 0 -1-6.91009 42.2583 4 -13 0 -2 6.65027 39.5550 4 -13 0 -3 282.010 59.5429 4 -13 0 -4 17.2720 37.9585 4 -13 1 5 404.079 63.7900 4 -13 -1 5 359.612 60.2598 4 -13 1 4 7193.11 281.941 4 -13 -1 4 7205.31 282.424 4 -13 1 3 754.299 87.0846 4 -13 -1 3 731.166 85.4185 4 -13 -1 2 11071.8 401.886 4 -13 1 2 11087.4 402.031 4 -13 1 1 169.385 56.7788 4 -13 -1 1 197.179 53.1591 4 -13 1 0 67.6047 44.5827 4 -13 -1 0 20.3470 42.5970 4 -13 1 -1 861.231 91.9627 4 -13 -1 -1 837.761 90.0724 4 -13 1 -2 1483.58 119.000 4 -13 -1 -2 1800.79 125.696 4 -13 1 -3 8073.90 309.178 4 -13 -1 -3 7981.74 309.703 4 -13 1 -4 240.559 54.1505 4 -13 -1 -4 202.796 51.4123 4 -13 2 5 926.072 78.8666 4 -13 -2 5 832.577 77.8301 4 13 2 -4 3799.61 163.751 10 -13 -2 4 4111.36 190.028 4 13 2 -3 1243.20 90.6719 10 -13 2 3 1256.87 99.9231 4 -13 -2 3 1291.68 101.101 4 -13 2 2 3230.97 168.867 4 -13 -2 2 3135.21 167.285 4 -13 -2 1 2222.83 136.249 4 -13 2 1 1908.46 126.633 4 -13 2 0 106.237 46.3561 4 -13 -2 0-5.94823 39.6820 4 -13 2 -1 3194.22 164.404 4 -13 -2 -1 2962.26 162.323 4 -13 2 -2 5613.35 229.501 4 -13 -2 -2 5076.63 223.855 4 -13 2 -3 12201.2 408.077 4 -13 -2 -3 12410.6 411.394 4 -13 3 3 140.519 37.3055 4 -13 -3 3 118.436 37.2146 4 13 3 -3 121.539 37.3536 10 -13 3 2 303.792 48.8305 4 -13 -3 2 261.255 47.9808 4 13 3 -2 209.230 45.3225 10 -13 3 1 336.231 50.9194 4 -13 -3 1 275.191 51.1014 4 13 3 -1 300.259 53.0021 10 -13 3 0 608.682 64.2966 4 -13 -3 0 646.635 65.4060 4 -13 -3 -1 2719.96 135.553 4 -13 3 -1 2737.64 138.984 4 0 0 0 0.00 0.00 0 TITL wpu23008 in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 11.343625 9.785794 15.682859 90.0000 93.0143 90.0000 ZERR 4.00 0.000179 0.000150 0.000224 0.0000 0.0014 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O P UNIT 80.00 72.00 4.00 16.00 4.00 REM CrysAlisPro recorded range (K): Min=110.0; max=110.0; aver:110.0 TEMP -163 SIZE 0.08 0.15 0.18 TREF HKLF 4 END ; _shelx_hkl_checksum 63245 _olex2_date_sample_data_collection 2023-04-27 _olex2_date_sample_submission 2023-04-19 _olex2_exptl_crystal_mounting_method 'oil on 200 micrometre micromount' _olex2_submission_original_sample_id YZZ0306-R1 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.097 _oxdiff_exptl_absorpt_empirical_full_min 0.932 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.12282(12) 0.77686(14) 0.51208(9) 0.0163(3) Uani 1 1 d . . . . . C2 C 0.14801(12) 0.85762(14) 0.44037(9) 0.0173(3) Uani 1 1 d . . . . . C3 C 0.15461(13) 0.80263(16) 0.35672(9) 0.0214(3) Uani 1 1 d . . . . . H3 H 0.1484(15) 0.7071(19) 0.3496(10) 0.020(4) Uiso 1 1 d . . . . . C4 C 0.17969(15) 0.88596(17) 0.28934(10) 0.0269(3) Uani 1 1 d . . . . . H4 H 0.1853(16) 0.8490(19) 0.2327(12) 0.028(5) Uiso 1 1 d . . . . . C5 C 0.19366(15) 1.02857(16) 0.30186(11) 0.0274(3) Uani 1 1 d . . . . . H5 H 0.2124(16) 1.0849(19) 0.2529(12) 0.026(5) Uiso 1 1 d . . . . . C6 C 0.19170(13) 1.08338(16) 0.38200(10) 0.0228(3) Uani 1 1 d . . . . . H6 H 0.2006(17) 1.178(2) 0.3912(12) 0.033(5) Uiso 1 1 d . . . . . C7 C 0.16581(12) 0.99992(15) 0.45302(10) 0.0187(3) Uani 1 1 d . . . . . C8 C 0.15601(13) 1.05582(15) 0.53579(10) 0.0212(3) Uani 1 1 d . . . . . H8 H 0.1671(16) 1.151(2) 0.5435(11) 0.025(4) Uiso 1 1 d . . . . . C9 C 0.13097(13) 0.97475(15) 0.60277(10) 0.0203(3) Uani 1 1 d . . . . . H9 H 0.1231(17) 1.0110(19) 0.6585(13) 0.028(5) Uiso 1 1 d . . . . . C10 C 0.11280(12) 0.83198(15) 0.59204(9) 0.0178(3) Uani 1 1 d . . . . . C11 C 0.09237(12) 0.74854(15) 0.67025(9) 0.0188(3) Uani 1 1 d . . . . . C12 C -0.00685(13) 0.55264(16) 0.72978(9) 0.0222(3) Uani 1 1 d . . . . . H12A H -0.0185(16) 0.5982(18) 0.7856(12) 0.025(4) Uiso 1 1 d . . . . . H12B H -0.0795(16) 0.5041(17) 0.7139(11) 0.020(4) Uiso 1 1 d . . . . . C13 C 0.09634(14) 0.45241(17) 0.73725(9) 0.0237(3) Uani 1 1 d . . . . . H13A H 0.1614(17) 0.4933(18) 0.7683(12) 0.024(4) Uiso 1 1 d . . . . . H13B H 0.0748(16) 0.374(2) 0.7707(12) 0.029(5) Uiso 1 1 d . . . . . C14 C 0.13580(13) 0.39818(15) 0.65297(9) 0.0206(3) Uani 1 1 d . . . . . H14A H 0.0689(15) 0.3822(17) 0.6118(11) 0.019(4) Uiso 1 1 d . . . . . H14B H 0.1839(16) 0.3139(18) 0.6622(11) 0.022(4) Uiso 1 1 d . . . . . C15 C 0.34647(12) 0.61227(14) 0.50173(9) 0.0183(3) Uani 1 1 d . . . . . C16 C 0.40218(13) 0.58886(16) 0.42613(10) 0.0224(3) Uani 1 1 d . . . . . H16 H 0.3718(17) 0.5171(19) 0.3888(12) 0.030(5) Uiso 1 1 d . . . . . C17 C 0.50162(14) 0.66338(18) 0.40792(11) 0.0302(4) Uani 1 1 d . . . . . H17 H 0.5369(18) 0.647(2) 0.3571(13) 0.034(5) Uiso 1 1 d . . . . . C18 C 0.54502(15) 0.76099(19) 0.46488(13) 0.0358(4) Uani 1 1 d . . . . . H18 H 0.611(2) 0.812(2) 0.4506(13) 0.042(6) Uiso 1 1 d . . . . . C19 C 0.49148(15) 0.78284(19) 0.54120(13) 0.0354(4) Uani 1 1 d . . . . . H19 H 0.520(2) 0.854(2) 0.5785(14) 0.048(6) Uiso 1 1 d . . . . . C20 C 0.39249(14) 0.70880(16) 0.56010(11) 0.0258(3) Uani 1 1 d . . . . . H20 H 0.3523(16) 0.7216(18) 0.6128(12) 0.024(4) Uiso 1 1 d . . . . . N1 N 0.00676(11) 0.65504(13) 0.66366(8) 0.0187(3) Uani 1 1 d . . . . . H1 H -0.0344(16) 0.6461(18) 0.6164(12) 0.021(4) Uiso 1 1 d . . . . . O1 O 0.10785(8) 0.63634(9) 0.49723(6) 0.0162(2) Uani 1 1 d . . . . . O2 O 0.15362(9) 0.76830(12) 0.73634(6) 0.0258(2) Uani 1 1 d . . . . . O3 O 0.21555(8) 0.49809(10) 0.61555(6) 0.0184(2) Uani 1 1 d . . . . . O4 O 0.18481(9) 0.40664(10) 0.46183(6) 0.0196(2) Uani 1 1 d . . . . . P1 P 0.21125(3) 0.52535(3) 0.51713(2) 0.01497(11) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0140(6) 0.0140(6) 0.0206(7) -0.0020(5) -0.0016(5) 0.0009(5) C2 0.0137(6) 0.0169(7) 0.0209(7) -0.0002(6) -0.0015(5) 0.0028(5) C3 0.0248(8) 0.0180(8) 0.0213(7) 0.0005(6) 0.0011(6) 0.0024(6) C4 0.0346(9) 0.0256(8) 0.0205(8) 0.0013(6) 0.0008(6) -0.0018(7) C5 0.0319(8) 0.0222(8) 0.0285(8) 0.0071(7) 0.0062(7) 0.0023(6) C6 0.0216(7) 0.0156(7) 0.0309(8) 0.0022(6) -0.0012(6) -0.0001(6) C7 0.0135(6) 0.0170(7) 0.0254(7) -0.0002(6) -0.0008(5) 0.0015(5) C8 0.0185(7) 0.0161(7) 0.0287(8) -0.0045(6) -0.0007(6) 0.0003(5) C9 0.0186(7) 0.0206(7) 0.0216(7) -0.0072(6) -0.0001(6) 0.0014(6) C10 0.0136(6) 0.0197(7) 0.0200(7) -0.0024(6) -0.0008(5) 0.0005(5) C11 0.0176(7) 0.0208(7) 0.0180(7) -0.0053(6) 0.0017(5) 0.0016(5) C12 0.0222(7) 0.0263(8) 0.0183(7) -0.0008(6) 0.0037(6) -0.0039(6) C13 0.0260(8) 0.0287(8) 0.0161(7) 0.0042(6) -0.0009(6) -0.0017(6) C14 0.0218(7) 0.0198(7) 0.0201(7) 0.0044(6) -0.0007(6) -0.0012(6) C15 0.0182(7) 0.0167(7) 0.0198(7) 0.0015(5) -0.0008(5) 0.0024(5) C16 0.0227(7) 0.0248(8) 0.0195(7) 0.0035(6) 0.0001(6) 0.0052(6) C17 0.0240(8) 0.0376(10) 0.0296(9) 0.0138(7) 0.0075(7) 0.0075(7) C18 0.0200(8) 0.0344(9) 0.0530(11) 0.0115(8) 0.0031(7) -0.0047(7) C19 0.0250(8) 0.0317(9) 0.0492(11) -0.0074(8) -0.0010(7) -0.0066(7) C20 0.0203(7) 0.0266(8) 0.0305(8) -0.0067(7) 0.0003(6) -0.0006(6) N1 0.0176(6) 0.0220(6) 0.0165(6) -0.0015(5) -0.0006(5) -0.0009(5) O1 0.0181(5) 0.0137(5) 0.0165(5) -0.0008(4) -0.0015(4) 0.0004(4) O2 0.0264(5) 0.0339(6) 0.0169(5) -0.0036(4) -0.0018(4) -0.0072(5) O3 0.0181(5) 0.0209(5) 0.0160(5) 0.0015(4) -0.0007(4) -0.0007(4) O4 0.0221(5) 0.0164(5) 0.0199(5) -0.0025(4) -0.0021(4) 0.0008(4) P1 0.01655(18) 0.01420(19) 0.01397(19) -0.00095(13) -0.00098(13) 0.00066(13) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -1 0 1 0.0360 1 0 -1 0.0487 1 1 0 0.0828 -1 -1 0 0.0502 0 0 -1 0.0564 0 0 1 0.0551 0 1 0 0.0712 0 -1 -1 0.0581 0 1 1 0.0756 1 -1 0 0.0698 -1 1 0 0.0867 1 0 1 0.0799 -1 0 -1 0.0927 -1 0 2 0.0264 4 1 -5 0.0457 1 -1 2 0.0619 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C10 C1 C2 122.35(13) . . ? C10 C1 O1 121.37(13) . . ? O1 C1 C2 116.28(12) . . ? C1 C2 C3 122.93(13) . . ? C1 C2 C7 118.01(13) . . ? C7 C2 C3 119.05(13) . . ? C2 C3 H3 118.5(10) . . ? C4 C3 C2 120.44(14) . . ? C4 C3 H3 120.8(10) . . ? C3 C4 H4 120.8(11) . . ? C3 C4 C5 120.21(15) . . ? C5 C4 H4 119.0(11) . . ? C4 C5 H5 118.3(11) . . ? C6 C5 C4 120.43(15) . . ? C6 C5 H5 121.0(11) . . ? C5 C6 H6 121.3(12) . . ? C5 C6 C7 120.51(14) . . ? C7 C6 H6 118.0(12) . . ? C2 C7 C6 119.14(13) . . ? C8 C7 C2 119.26(14) . . ? C8 C7 C6 121.59(14) . . ? C7 C8 H8 118.7(11) . . ? C9 C8 C7 120.81(14) . . ? C9 C8 H8 120.5(11) . . ? C8 C9 H9 121.7(11) . . ? C8 C9 C10 121.17(14) . . ? C10 C9 H9 117.1(11) . . ? C1 C10 C9 118.38(13) . . ? C1 C10 C11 123.73(13) . . ? C9 C10 C11 117.74(13) . . ? N1 C11 C10 116.90(12) . . ? O2 C11 C10 119.82(13) . . ? O2 C11 N1 123.28(14) . . ? H12A C12 H12B 107.1(14) . . ? C13 C12 H12A 110.9(10) . . ? C13 C12 H12B 110.0(10) . . ? N1 C12 H12A 109.9(10) . . ? N1 C12 H12B 105.9(10) . . ? N1 C12 C13 112.78(12) . . ? C12 C13 H13A 109.9(11) . . ? C12 C13 H13B 109.6(11) . . ? H13A C13 H13B 105.5(15) . . ? C14 C13 C12 114.77(12) . . ? C14 C13 H13A 109.7(11) . . ? C14 C13 H13B 106.9(11) . . ? C13 C14 H14A 112.1(10) . . ? C13 C14 H14B 110.4(10) . . ? H14A C14 H14B 111.2(14) . . ? O3 C14 C13 109.32(12) . . ? O3 C14 H14A 108.2(10) . . ? O3 C14 H14B 105.3(10) . . ? C16 C15 C20 119.91(14) . . ? C16 C15 P1 118.02(11) . . ? C20 C15 P1 121.91(12) . . ? C15 C16 H16 118.2(12) . . ? C17 C16 C15 120.01(15) . . ? C17 C16 H16 121.7(12) . . ? C16 C17 H17 118.6(12) . . ? C18 C17 C16 119.81(16) . . ? C18 C17 H17 121.5(12) . . ? C17 C18 H18 118.4(13) . . ? C17 C18 C19 120.50(16) . . ? C19 C18 H18 121.1(13) . . ? C18 C19 H19 119.4(14) . . ? C20 C19 C18 120.13(17) . . ? C20 C19 H19 120.3(14) . . ? C15 C20 H20 117.9(11) . . ? C19 C20 C15 119.60(16) . . ? C19 C20 H20 122.5(11) . . ? C11 N1 C12 121.38(12) . . ? C11 N1 H1 119.8(12) . . ? C12 N1 H1 118.1(12) . . ? C1 O1 P1 123.09(8) . . ? C14 O3 P1 121.17(9) . . ? O1 P1 C15 105.91(6) . . ? O3 P1 C15 103.46(6) . . ? O3 P1 O1 106.84(5) . . ? O4 P1 C15 116.57(6) . . ? O4 P1 O1 107.06(5) . . ? O4 P1 O3 116.22(6) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.416(2) . ? C1 C10 1.375(2) . ? C1 O1 1.4035(16) . ? C2 C3 1.424(2) . ? C2 C7 1.419(2) . ? C3 H3 0.944(18) . ? C3 C4 1.376(2) . ? C4 H4 0.964(19) . ? C4 C5 1.417(2) . ? C5 H5 0.977(19) . ? C5 C6 1.368(2) . ? C6 H6 0.94(2) . ? C6 C7 1.424(2) . ? C7 C8 1.418(2) . ? C8 H8 0.947(19) . ? C8 C9 1.358(2) . ? C9 H9 0.95(2) . ? C9 C10 1.421(2) . ? C10 C11 1.502(2) . ? C11 N1 1.3343(19) . ? C11 O2 1.2322(17) . ? C12 H12A 0.998(19) . ? C12 H12B 0.973(18) . ? C12 C13 1.527(2) . ? C12 N1 1.4561(19) . ? C13 H13A 0.950(19) . ? C13 H13B 0.97(2) . ? C13 C14 1.514(2) . ? C14 H14A 0.983(18) . ? C14 H14B 0.995(18) . ? C14 O3 1.4746(17) . ? C15 C16 1.391(2) . ? C15 C20 1.397(2) . ? C15 P1 1.7815(15) . ? C16 H16 0.97(2) . ? C16 C17 1.386(2) . ? C17 H17 0.92(2) . ? C17 C18 1.381(3) . ? C18 H18 0.93(2) . ? C18 C19 1.387(3) . ? C19 H19 0.95(2) . ? C19 C20 1.382(2) . ? C20 H20 0.973(18) . ? N1 H1 0.860(19) . ? O1 P1 1.6168(10) . ? O3 P1 1.5647(10) . ? O4 P1 1.4712(10) . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag N1 H1 O4 0.860(19) 2.112(19) 2.9172(16) 155.7(16) 3_566 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 C2 C3 C4 -179.85(14) . . . . ? C1 C2 C7 C6 179.77(13) . . . . ? C1 C2 C7 C8 -0.98(19) . . . . ? C1 C10 C11 N1 -48.01(19) . . . . ? C1 C10 C11 O2 131.94(15) . . . . ? C1 O1 P1 C15 -30.75(12) . . . . ? C1 O1 P1 O3 79.07(11) . . . . ? C1 O1 P1 O4 -155.78(10) . . . . ? C2 C1 C10 C9 -1.3(2) . . . . ? C2 C1 C10 C11 -176.73(13) . . . . ? C2 C1 O1 P1 98.56(13) . . . . ? C2 C3 C4 C5 -3.0(2) . . . . ? C2 C7 C8 C9 0.6(2) . . . . ? C3 C2 C7 C6 -1.0(2) . . . . ? C3 C2 C7 C8 178.22(13) . . . . ? C3 C4 C5 C6 5.2(3) . . . . ? C4 C5 C6 C7 -5.3(2) . . . . ? C5 C6 C7 C2 3.2(2) . . . . ? C5 C6 C7 C8 -176.02(14) . . . . ? C6 C7 C8 C9 179.83(14) . . . . ? C7 C2 C3 C4 1.0(2) . . . . ? C7 C8 C9 C10 -0.6(2) . . . . ? C8 C9 C10 C1 0.9(2) . . . . ? C8 C9 C10 C11 176.58(13) . . . . ? C9 C10 C11 N1 136.58(14) . . . . ? C9 C10 C11 O2 -43.47(19) . . . . ? C10 C1 C2 C3 -177.77(13) . . . . ? C10 C1 C2 C7 1.4(2) . . . . ? C10 C1 O1 P1 -81.74(15) . . . . ? C10 C11 N1 C12 168.88(12) . . . . ? C12 C13 C14 O3 82.55(15) . . . . ? C13 C12 N1 C11 -66.10(18) . . . . ? C13 C14 O3 P1 -141.86(10) . . . . ? C14 O3 P1 C15 -164.20(10) . . . . ? C14 O3 P1 O1 84.27(11) . . . . ? C14 O3 P1 O4 -35.11(12) . . . . ? C15 C16 C17 C18 -0.1(2) . . . . ? C16 C15 C20 C19 1.6(2) . . . . ? C16 C15 P1 O1 -101.87(11) . . . . ? C16 C15 P1 O3 145.92(11) . . . . ? C16 C15 P1 O4 17.05(14) . . . . ? C16 C17 C18 C19 1.5(3) . . . . ? C17 C18 C19 C20 -1.3(3) . . . . ? C18 C19 C20 C15 -0.2(3) . . . . ? C20 C15 C16 C17 -1.4(2) . . . . ? C20 C15 P1 O1 73.60(13) . . . . ? C20 C15 P1 O3 -38.60(13) . . . . ? C20 C15 P1 O4 -167.47(11) . . . . ? N1 C12 C13 C14 -45.18(18) . . . . ? O1 C1 C2 C3 1.92(19) . . . . ? O1 C1 C2 C7 -178.92(11) . . . . ? O1 C1 C10 C9 178.97(12) . . . . ? O1 C1 C10 C11 3.6(2) . . . . ? O2 C11 N1 C12 -11.1(2) . . . . ? P1 C15 C16 C17 174.13(11) . . . . ? P1 C15 C20 C19 -173.76(13) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -1.0000 -0.0000 1.0000 -0.0546 0.1434 0.0566 1.0000 0.0000 -1.0000 0.0546 -0.1434 -0.0566 1.0000 1.0000 0.0000 0.0949 -0.1366 0.1247 -1.0000 -1.0000 -0.0000 -0.0949 0.1366 -0.1247 0.0000 0.0000 -1.0000 0.0698 -0.0088 -0.0687 -0.0000 -0.0000 1.0000 -0.0698 0.0088 0.0687 -0.0000 1.0000 0.0000 0.1101 -0.0020 0.1125 0.0000 -1.0000 -1.0000 -0.0403 -0.0068 -0.1812 -0.0000 1.0000 1.0000 0.0403 0.0068 0.1812 1.0000 -1.0000 -0.0000 -0.1254 -0.1326 -0.1004 -1.0000 1.0000 0.0000 0.1254 0.1326 0.1004 1.0000 -0.0000 1.0000 -0.0851 -0.1258 0.0809 -1.0000 0.0000 -1.0000 0.0851 0.1258 -0.0809 -1.0001 -0.0000 2.0000 -0.1244 0.1522 0.1253 4.0002 1.0001 -5.0001 0.3982 -0.5845 -0.1826 1.0000 -1.0000 2.0000 -0.2650 -0.1149 0.0371