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Information card for entry 7156914
Preview
Coordinates | 7156914.cif |
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Original paper (by DOI) | HTML |
Formula | C20 H22 F2 O |
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Calculated formula | C20 H22 F2 O |
Title of publication | Copper-mediated cascade radical cyclization of olefins with naphthalenyl iododifluoromethyl ketones. |
Authors of publication | Peng, Peng; Huang, Guo-Zhi; Sun, Ying-Xin; Wang, Xing; Wu, Jing-Jing; Wu, Fan-Hong |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2019 |
Journal volume | 17 |
Journal issue | 26 |
Pages of publication | 6426 - 6431 |
a | 10.0026 ± 0.0006 Å |
b | 25.7449 ± 0.0014 Å |
c | 7.0051 ± 0.0004 Å |
α | 90° |
β | 103.519 ± 0.002° |
γ | 90° |
Cell volume | 1753.94 ± 0.17 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1057 |
Residual factor for significantly intense reflections | 0.0747 |
Weighted residual factors for significantly intense reflections | 0.2071 |
Weighted residual factors for all reflections included in the refinement | 0.238 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.033 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
225119 (current) | 2019-11-08 | cif/ Updating files of 7156914 Original log message: Adding full bibliography for 7156914.cif. |
7156914.cif |
215912 | 2019-06-13 | cif/ Adding structures of 7156914 via cif-deposit CGI script. |
7156914.cif |
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Users of the data should acknowledge the original authors of the
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