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Information card for entry 7156919
Preview
| Coordinates | 7156919.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Formula | C29 H24 O3 |
|---|---|
| Calculated formula | C29 H24 O3 |
| Title of publication | Diastereoselective synthesis of α-dicarbonyl cyclopropanes via a lanthanide amide-catalysed reaction. |
| Authors of publication | Sun, Wenxi; Peng, Cheng; Yao, Zhigang; Xu, Fan |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2019 |
| Journal volume | 17 |
| Journal issue | 27 |
| Pages of publication | 6620 - 6628 |
| a | 7.8923 ± 0.0012 Å |
| b | 10.3082 ± 0.0014 Å |
| c | 14.777 ± 0.002 Å |
| α | 102.912 ± 0.004° |
| β | 98.48 ± 0.004° |
| γ | 104.031 ± 0.004° |
| Cell volume | 1110.7 ± 0.3 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296.15 K |
| Number of distinct elements | 3 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0993 |
| Residual factor for significantly intense reflections | 0.067 |
| Weighted residual factors for significantly intense reflections | 0.1659 |
| Weighted residual factors for all reflections included in the refinement | 0.1852 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.065 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301861 (current) | 2025-08-22 | Add cross-references to PubChem compounds in COD range 7/15/ Each referenced PubChem compound corresponds to the full crystal structure. |
7156919.cif |
| 225068 | 2019-11-08 | cif/ Updating files of 7156917, 7156918, 7156919 Original log message: Adding full bibliography for 7156917--7156919.cif. |
7156919.cif |
| 216044 | 2019-06-18 | cif/ Adding structures of 7156917, 7156918, 7156919 via cif-deposit CGI script. |
7156919.cif |
All data in the COD and the database itself are dedicated to the
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CC0
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.
Users of the data should acknowledge the original authors of the
structural data.