Crystallography Open Database

Information card for entry 7157040

Preview

Coordinates	7157040.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H38 N2 O6
Calculated formula	C48 H38 N2 O6
Title of publication	Copper-catalyzed synthesis of spiro-indolofurobenzopyrans: tandem reactions of diazoamides and O-propargyl salicylaldehydes.
Authors of publication	Muthusamy, Sengodagounder; Prabu, Ammasi; Suresh, Eringathodi
Journal of publication	Organic & biomolecular chemistry
Year of publication	2019
Journal volume	17
Journal issue	35
Pages of publication	8088 - 8093
a	9.0014 ± 0.0013 Å
b	9.5478 ± 0.0013 Å
c	23.864 ± 0.003 Å
α	91.65 ± 0.002°
β	95.15 ± 0.002°
γ	113.925 ± 0.002°
Cell volume	1862.4 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.052
Residual factor for significantly intense reflections	0.0465
Weighted residual factors for significantly intense reflections	0.1249
Weighted residual factors for all reflections included in the refinement	0.1282
Goodness-of-fit parameter for all reflections included in the refinement	1.099
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
225273 (current)	2019-11-08	cif/ Updating files of 7157040 Original log message: Adding full bibliography for 7157040.cif.	7157040.cif
217579	2019-08-18	cif/ Adding structures of 7157040 via cif-deposit CGI script.	7157040.cif