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Information card for entry 7160494
Preview
| Coordinates | 7160494.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C35 H27 O2 P |
|---|---|
| Calculated formula | C35 H27 O2 P |
| Title of publication | Base-Promoted Regio- and Diastereoselective Synthesis of Tri- and Tetra-substituted Homoallenyl Phosphine Oxides via Alkynyl Enones |
| Authors of publication | Zhou, Shaochan; Zou, Haotian; Huang, Xianqiang; Qi, Jialin; Xu, Zhenghu |
| Journal of publication | Organic & Biomolecular Chemistry |
| Year of publication | 2025 |
| a | 12.821 ± 0.0014 Å |
| b | 8.9 ± 0.0009 Å |
| c | 23.705 ± 0.002 Å |
| α | 90° |
| β | 98.505 ± 0.01° |
| γ | 90° |
| Cell volume | 2675.2 ± 0.5 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.1432 |
| Residual factor for significantly intense reflections | 0.1036 |
| Weighted residual factors for significantly intense reflections | 0.211 |
| Weighted residual factors for all reflections included in the refinement | 0.2275 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.117 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 299248 (current) | 2025-04-10 | cif/ Adding structures of 7160494, 7160495 via cif-deposit CGI script. |
7160494.cif |
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Users of the data should acknowledge the original authors of the
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