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Information card for entry 7160830
Preview
| Coordinates | 7160830.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C26 H23 N O3 |
|---|---|
| Calculated formula | C26 H23 N O3 |
| Title of publication | Diastereoselective Construction of Azabicyclo[3.1.0]hexan-2-ones via a Base-Mediated Cascade Annulation of β-oxo-acrylamides with Vinylsulfonium Salts |
| Authors of publication | Wang, Zhaoxue; Wu, Ping; Yan, Rui; Zhao, Zhen-guo; Du, Yuhang; Xiao, Yilei; Wu, Lingang; Xie, Lei |
| Journal of publication | Organic & Biomolecular Chemistry |
| Year of publication | 2025 |
| a | 11.153 ± 0.0003 Å |
| b | 6.2741 ± 0.0002 Å |
| c | 15.0812 ± 0.0004 Å |
| α | 90° |
| β | 100.252 ± 0.001° |
| γ | 90° |
| Cell volume | 1038.46 ± 0.05 Å3 |
| Cell temperature | 300 K |
| Ambient diffraction temperature | 300 K |
| Number of distinct elements | 4 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0354 |
| Residual factor for significantly intense reflections | 0.0316 |
| Weighted residual factors for significantly intense reflections | 0.0793 |
| Weighted residual factors for all reflections included in the refinement | 0.082 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 303059 (current) | 2025-10-28 | cif/ Adding structures of 7160830 via cif-deposit CGI script. |
7160830.cif |
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Users of the data should acknowledge the original authors of the
structural data.