Crystallography Open Database

Information card for entry 7245923

Preview

Coordinates	7245923.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C92 H158.39 Dy8 N18 O52
Calculated formula	C96 H170 Dy8 N16 O52
Title of publication	Double butterfly-shaped octanuclear dysprosium clusters: structure, magnetism and assembly mechanism
Authors of publication	Li, Yun-Lan; Huang, Zhong-Ming; Wang, Hai-Ling; Zhu, Zhong-Hong; Liang, Fu-Pei; Zou, Hua-Hong
Journal of publication	CrystEngComm
Year of publication	2023
Journal volume	25
Journal issue	2
Pages of publication	225 - 232
a	14.1647 ± 0.0004 Å
b	14.3993 ± 0.0003 Å
c	16.7338 ± 0.0004 Å
α	82.531 ± 0.002°
β	75.268 ± 0.002°
γ	82.046 ± 0.002°
Cell volume	3253.05 ± 0.14 Å³
Cell temperature	99.99 ± 0.1 K
Ambient diffraction temperature	99.99 ± 0.1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1075
Residual factor for significantly intense reflections	0.1024
Weighted residual factors for significantly intense reflections	0.2773
Weighted residual factors for all reflections included in the refinement	0.2811
Goodness-of-fit parameter for all reflections included in the refinement	1.098
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
281443 (current)	2023-03-04	cif/ Updating files of 7245922, 7245923 Original log message: Adding full bibliography for 7245922--7245923.cif.	7245923.cif
279615	2022-11-29	cif/ Adding structures of 7245922, 7245923 via cif-deposit CGI script.	7245923.cif