#------------------------------------------------------------------------------ #$Date: 2023-01-25 01:31:17 +0200 (Wed, 25 Jan 2023) $ #$Revision: 280561 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/61/7246197.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7246197 loop_ _publ_author_name 'Chakraborty, Madhuparna' 'Chakravarty, Manab' _publ_section_title ; Flanking-donor-controlled diversity in mechanical-force-induced reversible fluorochromism and enhanced emission for carboxylic acid and ester linked solid-state emitters ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D2CE01378A _journal_year 2023 _chemical_formula_moiety 'C31 H24 O4' _chemical_formula_sum 'C31 H24 O4' _chemical_formula_weight 460.50 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _audit_creation_date 2022-11-19 _audit_creation_method ; Olex2 1.5 (compiled 2021.11.18 svn.ra9532c28 for OlexSys, GUI svn.r6427) ; _audit_update_record ; 2022-11-28 deposited with the CCDC. 2023-01-24 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 93.3160(10) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 15.2306(2) _cell_length_b 33.5647(5) _cell_length_c 9.16660(10) _cell_measurement_reflns_used 12169 _cell_measurement_temperature 100 _cell_measurement_theta_max 78.7220 _cell_measurement_theta_min 4.8840 _cell_volume 4678.22(11) _computing_cell_refinement 'CrysAlisPro 1.171.39.20a (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.39.20a (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.20a (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/2 (Sheldrick, 2015)' _computing_structure_solution 'SHELXS (Sheldrick, 2008)' _diffrn_ambient_temperature 100 _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.975 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -72.00 -25.00 0.50 6.15 -- 0.00 -77.00-180.00 94 2 \w -30.00 86.00 0.50 6.15 -- 0.00 77.00 -90.00 232 3 \w -79.00 -54.00 0.50 6.15 -- 0.00 -82.00 -60.00 50 4 \w -19.00 25.00 0.50 6.15 -- 0.00 -77.00-180.00 88 5 \w -11.00 14.00 0.50 6.15 -- 0.00 -82.00 -60.00 50 6 \w 91.00 126.00 0.50 24.58 -- 107.20 -82.00-180.00 70 7 \w 18.00 74.00 0.50 24.58 -- 107.20 -82.00-180.00 112 8 \w 89.00 162.00 0.50 24.58 -- 107.20 61.00 -60.00 146 9 \w 83.00 192.00 0.50 24.58 -- 107.20 61.00 60.00 218 10 \w 44.00 107.00 0.50 24.58 -- 107.20 -82.00-120.00 126 11 \w 98.00 123.00 0.50 24.58 -- 107.20 30.00 120.00 50 12 \w 156.00 182.00 0.50 24.58 -- 107.20 30.00 120.00 52 13 \w 63.00 123.00 0.50 24.58 -- 107.20 -82.00 120.00 120 14 \w 51.00 126.00 0.50 24.58 -- 107.20 -61.00 -30.00 150 15 \w 18.00 131.00 0.50 24.58 -- 107.20 -82.00 150.00 226 16 \w 96.00 191.00 0.50 24.58 -- 107.20 45.00 0.00 190 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Pro: Kappa dual home/near' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0600297000 _diffrn_orient_matrix_UB_12 0.0369268000 _diffrn_orient_matrix_UB_13 0.0120353000 _diffrn_orient_matrix_UB_21 -0.0804852000 _diffrn_orient_matrix_UB_22 0.0271585000 _diffrn_orient_matrix_UB_23 -0.0315139000 _diffrn_orient_matrix_UB_31 -0.0137501000 _diffrn_orient_matrix_UB_32 0.0024526000 _diffrn_orient_matrix_UB_33 0.1648684000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0548 _diffrn_reflns_av_unetI/netI 0.0520 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.975 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_k_max 36 _diffrn_reflns_limit_k_min -42 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 32517 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.975 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 79.730 _diffrn_reflns_theta_min 3.923 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.687 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.48198 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.20a (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear greenish violet' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier greenish _exptl_crystal_colour_primary violet _exptl_crystal_density_diffrn 1.308 _exptl_crystal_description trapezoid _exptl_crystal_F_000 1936 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.677 _refine_diff_density_min -0.270 _refine_diff_density_rms 0.053 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.037 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 643 _refine_ls_number_reflns 9936 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.037 _refine_ls_R_factor_all 0.0710 _refine_ls_R_factor_gt 0.0581 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0649P)^2^+3.4801P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1544 _refine_ls_wR_factor_ref 0.1617 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8151 _reflns_number_total 9936 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d2ce01378a2.cif _cod_data_source_block exp_1001-sgy-1 _cod_database_code 7246197 _shelx_shelxl_version_number 2019/2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.934 _shelx_estimated_absorpt_t_min 0.875 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances O001-H001 0.85 with sigma of 0.02 O002-H002 0.85 with sigma of 0.02 3.a Aromatic/amide H refined with riding coordinates: C00J(H00J), C00L(H00L), C00M(H00M), C00N(H00N), C00R(H00R), C00T(H00T), C00X(H00X), C00Z(H00Z), C010(H010), C012(H012), C013(H013), C014(H014), C015(H015), C016(H016), C017(H017), C018(H018), C019(H019), C01B(H01J), C01C(H01C), C01D(H01D), C01E(H01K), C01F(H01M), C01G(H01N), C01I(H01I), C01J(H01O), C01K(H01P), C01L(H01L), C01N(H01Q), C01O(H01R), C01P(H01S), C01Q(H01T), C01S(H01V), C01T(H01W), C01U(H01U) 3.b Idealised Me refined as rotating group: C01V(H01X,H01Y,H), C01W(H01A,H01B,H01E), C01X(H01Z,HA,HB), C01Y(H01F,H01G,H01H) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL exp_1001-sgy-1_a.res in P2(1)/c exp_1001-sgy-1.res created by SHELXL-2019/2 at 13:05:00 on 19-Nov-2022 REM Old TITL REM SHELXT solution in P2(1)/c REM R1 0.128, Rweak 0.011, Alpha 0.025, Orientation as input REM Formula found by SHELXT: C62 N3 O5 CELL 1.54184 15.2306 33.5647 9.1666 90 93.316 90 ZERR 8 0.0002 0.0005 0.0001 0 0.001 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H O UNIT 248 192 32 DFIX 0.85 O001 H001 DFIX 0.85 O002 H002 L.S. 100 0 0 PLAN 17 SIZE 0.2 0.1 0.2 TEMP -173.15 CONF BOND $H list 4 ABIN fmap 2 53 acta MORE -1 REM REM REM WGHT 0.064900 3.480100 FVAR 0.27710 O001 3 0.898814 0.487687 0.064266 11.00000 0.03018 0.03318 = 0.04112 -0.01063 0.01034 0.00170 O002 3 0.512019 0.490499 0.813744 11.00000 0.02628 0.04239 = 0.04073 -0.00973 0.00721 0.00270 O003 3 0.983353 0.542192 0.096392 11.00000 0.02518 0.03901 = 0.04478 -0.00881 0.01240 -0.00180 O004 3 0.600629 0.478320 1.012710 11.00000 0.03018 0.04585 = 0.03580 -0.01238 0.00766 -0.00089 O005 3 1.278633 0.326206 0.328281 11.00000 0.03275 0.04489 = 0.03780 -0.00431 -0.00149 0.00660 O006 3 1.148166 0.311951 -0.243776 11.00000 0.05049 0.04561 = 0.03091 -0.00551 0.00522 0.00230 O007 3 0.127573 0.652880 1.030677 11.00000 0.03484 0.05691 = 0.04254 -0.00119 0.01502 0.00586 O008 3 0.447446 0.717242 0.893229 11.00000 0.04008 0.03679 = 0.07402 -0.01491 0.00987 -0.00506 C009 1 1.100778 0.391057 0.278193 11.00000 0.02317 0.02466 = 0.02618 -0.00205 0.00119 0.00073 C00A 1 0.384654 0.643530 0.623072 11.00000 0.02374 0.02378 = 0.02821 -0.00110 0.00564 0.00017 C00B 1 0.442785 0.623342 0.529460 11.00000 0.02238 0.02656 = 0.02605 -0.00136 0.00372 -0.00109 C00C 1 1.051298 0.323855 0.331487 11.00000 0.02506 0.02568 = 0.02893 -0.00163 -0.00023 0.00031 C00D 1 0.533852 0.601281 0.742293 11.00000 0.02275 0.02700 = 0.02792 0.00024 0.00524 0.00060 C00E 1 0.403439 0.643233 0.775170 11.00000 0.02446 0.02770 = 0.02881 -0.00177 0.00494 0.00112 C00F 1 0.477520 0.622749 0.835639 11.00000 0.02409 0.02766 = 0.02852 -0.00005 0.00515 0.00079 C00G 1 0.722145 0.572918 0.384736 11.00000 0.02307 0.03026 = 0.02257 -0.00172 0.00088 0.00460 C00H 1 0.846120 0.540502 0.204945 11.00000 0.02341 0.03195 = 0.02467 -0.00317 0.00332 0.00380 C00I 1 0.914011 0.522527 0.116408 11.00000 0.02557 0.03091 = 0.02891 -0.00527 0.00372 0.00138 C00J 1 1.158280 0.417766 0.208225 11.00000 0.02472 0.02964 = 0.02821 0.00016 0.00489 0.00082 AFIX 43 H00J 2 1.199186 0.407356 0.143718 11.00000 -1.20000 AFIX 0 C00K 1 0.516415 0.602266 0.589427 11.00000 0.02381 0.02540 = 0.02763 -0.00264 0.00487 0.00069 C00L 1 0.767432 0.520348 0.225064 11.00000 0.02665 0.02800 = 0.02771 -0.00261 0.00409 0.00156 AFIX 43 H00L 2 0.756156 0.495426 0.178556 11.00000 -1.20000 AFIX 0 C00M 1 0.706000 0.536771 0.312854 11.00000 0.02286 0.02987 = 0.02825 -0.00055 0.00473 0.00100 AFIX 43 H00M 2 0.652045 0.523248 0.324375 11.00000 -1.20000 AFIX 0 C00N 1 0.424850 0.626384 0.374850 11.00000 0.02489 0.02988 = 0.02744 -0.00264 0.00490 0.00110 AFIX 43 H00N 2 0.463637 0.614001 0.311159 11.00000 -1.20000 AFIX 0 C00O 1 1.038568 0.407318 0.374605 11.00000 0.02524 0.02691 = 0.02847 -0.00358 0.00178 0.00049 C00P 1 1.165061 0.333386 0.145501 11.00000 0.02962 0.02213 = 0.03218 -0.00287 0.00755 -0.00054 C00Q 1 1.105239 0.349709 0.255242 11.00000 0.02344 0.02597 = 0.02589 -0.00281 0.00125 0.00220 C00R 1 0.310337 0.664213 0.557031 11.00000 0.02383 0.02948 = 0.03169 -0.00019 0.00597 0.00295 AFIX 43 H00R 2 0.270569 0.677176 0.617523 11.00000 -1.20000 AFIX 0 C00S 1 0.984354 0.381373 0.450555 11.00000 0.02460 0.03020 = 0.02820 -0.00463 0.00413 0.00050 C00T 1 0.606185 0.579627 0.809911 11.00000 0.02448 0.03199 = 0.02892 0.00212 0.00638 0.00368 AFIX 43 H00T 2 0.642665 0.564344 0.750587 11.00000 -1.20000 AFIX 0 C00U 1 0.653189 0.463630 0.780812 11.00000 0.02485 0.02513 = 0.03586 -0.00620 0.00759 -0.00281 C00V 1 0.584438 0.478333 0.876136 11.00000 0.02393 0.02889 = 0.03558 -0.00698 0.00425 -0.00236 C00W 1 0.783688 0.434923 0.604635 11.00000 0.02795 0.02442 = 0.03435 -0.00191 0.00863 0.00018 C00X 1 0.575329 0.582296 0.488844 11.00000 0.02609 0.02843 = 0.02648 -0.00258 0.00317 0.00394 AFIX 43 H00X 2 0.551009 0.562457 0.424570 11.00000 -1.20000 AFIX 0 C00Y 1 0.992861 0.339723 0.434022 11.00000 0.02466 0.02987 = 0.02801 0.00046 0.00264 -0.00064 C00Z 1 0.643412 0.467736 0.629690 11.00000 0.02690 0.02984 = 0.03683 0.00052 0.00643 0.00248 AFIX 43 H00Z 2 0.592597 0.480341 0.586006 11.00000 -1.20000 AFIX 0 C010 1 0.660943 0.590775 0.483945 11.00000 0.02708 0.02997 = 0.02441 -0.00313 0.00231 0.00410 AFIX 43 H010 2 0.684296 0.610171 0.550966 11.00000 -1.20000 AFIX 0 C011 1 0.344198 0.665081 0.872528 11.00000 0.02728 0.03236 = 0.02487 -0.00160 0.00199 0.00661 C012 1 0.499198 0.622734 0.989818 11.00000 0.02846 0.04076 = 0.02585 -0.00121 0.00665 0.00385 AFIX 43 H012 2 0.462972 0.636993 1.052696 11.00000 -1.20000 AFIX 0 C013 1 0.353956 0.646478 0.317061 11.00000 0.02800 0.03561 = 0.02563 0.00047 0.00194 0.00054 AFIX 43 H013 2 0.343229 0.647744 0.214037 11.00000 -1.20000 AFIX 0 C014 1 0.262952 0.648710 0.902744 11.00000 0.02970 0.03371 = 0.02346 0.00001 0.00239 0.00443 AFIX 43 H014 2 0.245691 0.623783 0.861205 11.00000 -1.20000 AFIX 0 C015 1 0.800642 0.593142 0.361382 11.00000 0.02874 0.03088 = 0.03587 -0.00855 0.00423 0.00062 AFIX 43 H015 2 0.812224 0.617966 0.408419 11.00000 -1.20000 AFIX 0 C016 1 0.708150 0.453353 0.542900 11.00000 0.03434 0.03061 = 0.03099 0.00185 0.00909 0.00174 AFIX 43 H016 2 0.700934 0.456097 0.439754 11.00000 -1.20000 AFIX 0 C017 1 0.918504 0.396665 0.549903 11.00000 0.02931 0.03392 = 0.03166 -0.00253 0.00795 -0.00112 AFIX 43 H017 2 0.924964 0.389160 0.649876 11.00000 -1.20000 AFIX 0 C018 1 0.728642 0.445721 0.843909 11.00000 0.02915 0.03179 = 0.03158 -0.00582 0.00501 0.00047 AFIX 43 H018 2 0.735939 0.443141 0.947104 11.00000 -1.20000 AFIX 0 C019 1 0.623991 0.580373 0.956692 11.00000 0.02564 0.03992 = 0.03121 0.00676 0.00359 0.00615 AFIX 43 H019 2 0.672642 0.565799 0.998523 11.00000 -1.20000 AFIX 0 C01A 1 1.252075 0.322287 0.184157 11.00000 0.03116 0.02716 = 0.03387 -0.00296 0.00370 0.00031 C01B 1 1.155666 0.457706 0.232026 11.00000 0.03109 0.02649 = 0.03869 0.00086 0.00702 -0.00356 AFIX 43 H01J 2 1.195128 0.474825 0.185553 11.00000 -1.20000 AFIX 0 C01C 1 0.295639 0.665651 0.409942 11.00000 0.02371 0.03515 = 0.03353 0.00479 0.00321 0.00499 AFIX 43 H01C 2 0.245929 0.679596 0.368639 11.00000 -1.20000 AFIX 0 C01D 1 0.861452 0.577462 0.270836 11.00000 0.02452 0.03527 = 0.03619 -0.00850 0.00524 -0.00256 AFIX 43 H01D 2 0.913553 0.591853 0.253597 11.00000 -1.20000 AFIX 0 C01E 1 1.134636 0.329797 0.000362 11.00000 0.03488 0.02686 = 0.03269 -0.00225 0.00469 0.00096 AFIX 43 H01K 2 1.075964 0.337500 -0.027038 11.00000 -1.20000 AFIX 0 C01F 1 1.037495 0.449623 0.394156 11.00000 0.03005 0.02798 = 0.03920 -0.00794 0.00765 0.00204 AFIX 43 H01M 2 0.996308 0.461015 0.456026 11.00000 -1.20000 AFIX 0 C01G 1 1.052945 0.281686 0.309856 11.00000 0.03447 0.02654 = 0.03665 -0.00157 0.00288 0.00119 AFIX 43 H01N 2 1.089475 0.270852 0.239236 11.00000 -1.20000 AFIX 0 C01H 1 1.187828 0.315204 -0.106207 11.00000 0.04316 0.02814 = 0.03059 -0.00342 0.00829 -0.00161 C01I 1 0.570416 0.602770 1.047933 11.00000 0.03033 0.04588 = 0.02357 0.00348 0.00285 0.00453 AFIX 43 H01I 2 0.584418 0.603813 1.150208 11.00000 -1.20000 AFIX 0 C01J 1 0.851072 0.420133 0.508962 11.00000 0.03169 0.03164 = 0.03158 -0.00367 0.00759 0.00010 AFIX 43 H01O 2 0.845915 0.428046 0.409331 11.00000 -1.20000 AFIX 0 C01K 1 0.793082 0.431661 0.756462 11.00000 0.02935 0.03277 = 0.03491 -0.00548 0.00558 0.00436 AFIX 43 H01P 2 0.844452 0.419614 0.800563 11.00000 -1.20000 AFIX 0 C01L 1 0.232696 0.704885 1.053137 11.00000 0.03963 0.04201 = 0.03048 -0.00231 0.00539 0.01914 AFIX 43 H01L 2 0.194978 0.718406 1.115656 11.00000 -1.20000 AFIX 0 C01M 1 0.207084 0.668511 0.992975 11.00000 0.02852 0.04425 = 0.02413 0.00146 0.00375 0.00787 C01N 1 0.943641 0.312244 0.515588 11.00000 0.03066 0.03742 = 0.03474 0.00169 0.00705 -0.00346 AFIX 43 H01Q 2 0.905863 0.322150 0.586107 11.00000 -1.20000 AFIX 0 C01O 1 0.949461 0.272254 0.494901 11.00000 0.03683 0.03422 = 0.03860 0.00630 0.00137 -0.00797 AFIX 43 H01R 2 0.917091 0.254629 0.552557 11.00000 -1.20000 AFIX 0 C01P 1 1.093828 0.473923 0.326563 11.00000 0.03538 0.02444 = 0.04599 -0.00511 0.00717 -0.00036 AFIX 43 H01S 2 1.091955 0.501872 0.342448 11.00000 -1.20000 AFIX 0 C01Q 1 1.306093 0.308781 0.076626 11.00000 0.02910 0.03199 = 0.04850 -0.00450 0.00873 0.00288 AFIX 43 H01T 2 1.365471 0.301868 0.102313 11.00000 -1.20000 AFIX 0 C01R 1 0.368479 0.702004 0.931189 11.00000 0.03174 0.03504 = 0.03792 -0.00578 0.00396 0.00295 C01S 1 1.003373 0.256754 0.388146 11.00000 0.03896 0.02626 = 0.04409 0.00186 0.00066 -0.00196 AFIX 43 H01V 2 1.004992 0.228856 0.371032 11.00000 -1.20000 AFIX 0 C01T 1 1.273924 0.305381 -0.066881 11.00000 0.04033 0.03491 = 0.03719 -0.00511 0.01283 -0.00058 AFIX 43 H01W 2 1.311403 0.296203 -0.139081 11.00000 -1.20000 AFIX 0 C01U 1 0.312596 0.721706 1.023107 11.00000 0.04696 0.03261 = 0.03932 -0.00983 0.00234 0.00699 AFIX 43 H01U 2 0.329486 0.746645 1.064946 11.00000 -1.20000 AFIX 0 C01V 1 1.361209 0.308525 0.372305 11.00000 0.03723 0.04069 = 0.04355 0.00017 -0.00370 0.00452 AFIX 137 H01X 2 1.407746 0.320752 0.317901 11.00000 -1.50000 H01Y 2 1.358921 0.279865 0.352018 11.00000 -1.50000 H 2 1.373645 0.312820 0.477215 11.00000 -1.50000 AFIX 0 C01W 1 0.093109 0.620693 0.943524 11.00000 0.03254 0.05294 = 0.04590 0.00748 0.00606 -0.00019 AFIX 137 H01A 2 0.086917 0.629018 0.840973 11.00000 -1.50000 H01B 2 0.035440 0.613022 0.976587 11.00000 -1.50000 H01E 2 0.133277 0.597913 0.953101 11.00000 -1.50000 AFIX 0 C01X 1 1.200054 0.296086 -0.353818 11.00000 0.06492 0.04974 = 0.03322 -0.00634 0.01029 0.00632 AFIX 137 H01Z 2 1.164276 0.294025 -0.445861 11.00000 -1.50000 HA 2 1.221425 0.269585 -0.324244 11.00000 -1.50000 HB 2 1.250259 0.313702 -0.367265 11.00000 -1.50000 AFIX 0 C01Y 1 0.471128 0.755802 0.943513 11.00000 0.04792 0.04960 = 0.13406 -0.03309 0.01230 -0.00951 AFIX 137 H01F 2 0.428105 0.775195 0.903403 11.00000 -1.50000 H01G 2 0.529585 0.762558 0.911512 11.00000 -1.50000 H01H 2 0.472110 0.756384 1.050484 11.00000 -1.50000 AFIX 0 H001 2 0.938288 0.476987 0.012213 11.00000 0.14312 H002 2 0.477758 0.500303 0.876564 11.00000 0.15320 HKLF 4 REM exp_1001-sgy-1_a.res in P2(1)/c REM wR2 = 0.1617, GooF = S = 1.037, Restrained GooF = 1.037 for all data REM R1 = 0.0581 for 8151 Fo > 4sig(Fo) and 0.0710 for all 9936 data REM 643 parameters refined using 2 restraints END WGHT 0.0645 3.4874 REM Highest difference peak 0.677, deepest hole -0.270, 1-sigma level 0.053 Q1 1 0.2208 0.6186 0.8396 11.00000 0.05 0.68 Q2 1 0.3644 0.7473 1.1178 11.00000 0.05 0.46 Q3 1 0.4548 0.7604 1.0818 11.00000 0.05 0.35 Q4 1 0.1270 0.5991 0.8575 11.00000 0.05 0.34 Q5 1 1.0651 0.3393 -0.0577 11.00000 0.05 0.32 Q6 1 1.3764 0.2832 0.1662 11.00000 0.05 0.28 Q7 1 1.4140 0.2827 0.3251 11.00000 0.05 0.23 Q8 1 0.3863 0.6390 0.6976 11.00000 0.05 0.23 Q9 1 0.9910 0.4364 0.3129 11.00000 0.05 0.19 Q10 1 0.8762 0.4018 0.4991 11.00000 0.05 0.19 Q11 1 0.6410 0.4593 0.6974 11.00000 0.05 0.19 Q12 1 1.0234 0.4563 0.3015 11.00000 0.05 0.19 Q13 1 1.2607 0.3224 0.4349 11.00000 0.05 0.19 Q14 1 0.3752 0.6798 0.9434 11.00000 0.05 0.19 Q15 1 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0.0004 0 37 4 -0.0083 -0.0031 0 37 5 -0.2167 -0.0014 0 38 0 0.1352 -0.0030 0 38 1 -0.0591 -0.0007 0 38 2 -0.1257 0.0028 0 38 3 0.0312 -0.0014 0 38 4 0.0828 -0.0002 0 38 5 0.1049 0.0037 0 39 1 -0.1015 0.0004 0 39 2 0.0207 0.0001 0 39 3 0.0085 -0.0016 0 39 4 -0.1013 0.0011 0 40 0 -0.0874 0.0004 0 40 1 -0.0205 0.0031 0 40 2 0.0729 -0.0016 0 40 3 0.0109 -0.0008 0 41 1 0.0562 -0.0002 0 41 2 0.0590 -0.0007 0 41 3 -0.0300 0.0011 1 0 2 0.7838 -0.0019 1 0 4 -0.2496 -0.0069 1 0 6 0.0045 0.0052 1 0 8 0.2106 -0.0032 1 0 10 0.2777 0.0051 1 1 1 -0.1229 -0.0165 1 1 2 0.0589 0.0010 1 1 3 0.0037 0.0263 1 1 4 0.0297 0.0061 1 1 5 0.0294 -0.0168 1 1 6 -0.0906 -0.0083 1 1 7 -0.1040 0.0023 1 1 8 0.1767 -0.0015 1 1 9 0.2547 0.0077 1 1 10 -0.3646 0.0051 1 1 11 -0.3613 -0.0064 1 2 0 0.9296 0.0022 1 2 1 0.7701 -0.0107 1 2 2 -0.5559 -0.0029 1 2 3 -0.2537 -0.0008 1 2 4 0.1924 0.0041 1 2 5 0.0443 0.0085 1 2 6 -0.0287 -0.0014 1 2 7 0.1378 -0.0076 1 2 8 -0.1452 -0.0001 1 2 9 0.0032 0.0058 1 2 10 -0.0915 -0.0032 1 2 11 -0.5404 -0.0020 1 3 0 0.0952 -0.0011 1 3 1 0.2490 0.0125 1 3 2 0.0400 0.0157 1 3 3 0.0027 -0.0151 1 3 4 -0.0100 -0.0195 1 3 5 -0.0445 0.0046 1 3 6 -0.0154 0.0121 1 3 7 0.1293 0.0015 1 3 8 0.1822 0.0036 1 3 9 -0.3354 -0.0019 1 3 10 -0.2964 -0.0091 1 3 11 0.5796 0.0018 1 4 0 -0.0312 -0.0095 1 4 1 -0.9957 0.0052 1 4 2 0.0776 0.0061 1 4 3 0.3109 0.0024 1 4 4 -0.1019 0.0006 1 4 5 -0.0477 -0.0084 1 4 6 0.0929 -0.0045 1 4 7 -0.1659 0.0064 1 4 8 -0.0115 0.0051 1 4 9 0.0541 -0.0053 1 4 10 -0.2242 -0.0011 1 4 11 0.4806 0.0029 1 5 0 0.2558 0.0053 1 5 1 -0.1255 -0.0004 1 5 2 -0.1276 -0.0189 1 5 3 -0.0482 -0.0033 1 5 4 -0.0005 0.0175 1 5 5 0.0152 0.0083 1 5 6 0.0432 -0.0071 1 5 7 0.0817 -0.0037 1 5 8 -0.2996 -0.0036 1 5 9 -0.2127 -0.0044 1 5 10 0.6425 0.0067 1 5 11 0.0116 0.0030 1 6 0 -0.6589 0.0088 1 6 1 0.6206 0.0026 1 6 2 0.2581 -0.0055 1 6 3 -0.2158 -0.0028 1 6 4 0.0979 -0.0037 1 6 5 0.0600 0.0038 1 6 6 -0.1626 0.0077 1 6 7 0.0563 -0.0009 1 6 8 0.1471 -0.0074 1 6 9 -0.0951 0.0007 1 6 10 0.2974 0.0033 1 6 11 0.0207 -0.0008 1 7 0 -0.3531 -0.0032 1 7 1 -0.1368 -0.0087 1 7 2 0.0707 0.0086 1 7 3 0.1129 0.0133 1 7 4 0.0252 -0.0050 1 7 5 -0.0204 -0.0113 1 7 6 0.0353 -0.0008 1 7 7 -0.1821 0.0024 1 7 8 -0.0668 0.0011 1 7 9 0.6277 0.0066 1 7 10 -0.1430 -0.0005 1 7 11 -0.6229 -0.0042 1 8 0 0.7117 -0.0018 1 8 1 -0.0750 -0.0062 1 8 2 -0.2834 0.0022 1 8 3 0.1761 0.0021 1 8 4 -0.1364 0.0033 1 8 5 -0.1649 0.0010 1 8 6 0.1701 -0.0055 1 8 7 0.1110 -0.0041 1 8 8 -0.1445 0.0042 1 8 9 0.0435 0.0034 1 8 10 -0.1337 -0.0012 1 8 11 -0.3552 -0.0011 1 9 0 0.1482 -0.0020 1 9 1 0.2693 0.0080 1 9 2 0.1343 0.0037 1 9 3 -0.0983 -0.0099 1 9 4 -0.0976 -0.0046 1 9 5 0.0368 0.0051 1 9 6 -0.0477 0.0042 1 9 7 0.0112 -0.0001 1 9 8 0.4282 0.0018 1 9 9 -0.3251 -0.0036 1 9 10 -0.5637 -0.0041 1 9 11 0.5054 0.0017 1 10 0 -0.3031 -0.0036 1 10 1 -0.1911 0.0040 1 10 2 0.1793 0.0007 1 10 3 -0.2566 -0.0015 1 10 4 0.0345 -0.0014 1 10 5 0.3220 -0.0019 1 10 6 -0.0552 0.0012 1 10 7 -0.2062 0.0041 1 10 8 0.0086 0.0007 1 10 9 0.0107 -0.0026 1 10 10 0.0093 -0.0019 1 10 11 0.2957 -0.0006 1 11 0 0.1258 0.0044 1 11 1 -0.1107 -0.0005 1 11 2 -0.2965 -0.0076 1 11 3 -0.0634 0.0009 1 11 4 0.1403 0.0047 1 11 5 0.0362 0.0012 1 11 6 -0.0391 -0.0020 1 11 7 0.1559 -0.0003 1 11 8 -0.3317 -0.0024 1 11 9 -0.2927 -0.0012 1 11 10 0.6300 0.0037 1 11 11 0.0883 0.0017 1 12 0 -0.0506 0.0028 1 12 1 0.1238 -0.0001 1 12 2 -0.1812 -0.0012 1 12 3 0.2656 0.0013 1 12 4 0.2541 0.0007 1 12 5 -0.3395 -0.0000 1 12 6 -0.1491 0.0001 1 12 7 0.1578 -0.0007 1 12 8 0.1086 -0.0019 1 12 9 0.0527 -0.0010 1 12 10 -0.0062 0.0013 1 12 11 -0.1302 0.0035 1 13 0 -0.1961 -0.0020 1 13 1 -0.1969 -0.0053 1 13 2 0.2022 0.0030 1 13 3 0.2579 0.0036 1 13 4 -0.0351 0.0005 1 13 5 -0.1475 -0.0017 1 13 6 0.0363 -0.0010 1 13 7 -0.0971 -0.0009 1 13 8 -0.0040 0.0004 1 13 9 0.5001 0.0031 1 13 10 -0.1192 -0.0000 1 13 11 -0.3994 -0.0029 1 14 0 0.0431 0.0012 1 14 1 0.0012 -0.0010 1 14 2 0.2651 0.0004 1 14 3 -0.0307 -0.0012 1 14 4 -0.4807 -0.0018 1 14 5 0.0945 0.0005 1 14 6 0.2927 0.0019 1 14 7 -0.0173 -0.0006 1 14 8 -0.0795 -0.0006 1 14 9 -0.1578 0.0019 1 14 10 -0.0367 0.0019 1 15 0 0.0269 -0.0019 1 15 1 0.3292 0.0045 1 15 2 0.1143 0.0028 1 15 3 -0.2651 -0.0013 1 15 4 -0.1594 -0.0033 1 15 5 0.1090 -0.0017 1 15 6 0.1079 0.0011 1 15 7 -0.0017 0.0016 1 15 8 0.1270 0.0017 1 15 9 -0.2391 -0.0013 1 15 10 -0.2658 -0.0027 1 16 0 0.1824 -0.0029 1 16 1 0.0275 -0.0005 1 16 2 -0.2304 -0.0002 1 16 3 -0.2961 0.0006 1 16 4 0.3607 0.0025 1 16 5 0.2484 0.0016 1 16 6 -0.2377 -0.0028 1 16 7 -0.0939 -0.0015 1 16 8 -0.0373 0.0018 1 16 9 0.1258 0.0003 1 16 10 0.1595 -0.0032 1 17 0 0.1634 0.0030 1 17 1 -0.1301 -0.0001 1 17 2 -0.3532 -0.0034 1 17 3 0.0391 -0.0029 1 17 4 0.2211 0.0012 1 17 5 0.0892 0.0039 1 17 6 -0.1601 0.0010 1 17 7 -0.0828 -0.0010 1 17 8 -0.0373 -0.0018 1 17 9 -0.0007 -0.0014 1 17 10 0.2084 0.0022 1 18 0 -0.3012 0.0011 1 18 1 -0.1498 0.0016 1 18 2 0.0374 0.0007 1 18 3 0.3782 0.0002 1 18 4 0.0322 -0.0013 1 18 5 -0.3677 -0.0033 1 18 6 0.0237 0.0005 1 18 7 0.1071 0.0030 1 18 8 0.0858 -0.0001 1 18 9 0.0334 -0.0017 1 18 10 -0.1868 0.0014 1 19 0 -0.1554 -0.0011 1 19 1 -0.1994 -0.0021 1 19 2 0.2700 -0.0001 1 19 3 0.1937 0.0035 1 19 4 -0.0680 0.0025 1 19 5 -0.1963 -0.0026 1 19 6 -0.0191 -0.0029 1 19 7 0.2006 -0.0003 1 19 8 0.0402 0.0006 1 19 9 -0.0112 0.0020 1 19 10 -0.0166 0.0002 1 20 0 0.1891 0.0008 1 20 1 0.2103 -0.0009 1 20 2 0.1128 -0.0009 1 20 3 -0.1399 -0.0004 1 20 4 -0.2982 -0.0004 1 20 5 0.1622 0.0023 1 20 6 0.1563 0.0020 1 20 7 -0.0545 -0.0015 1 20 8 -0.0351 -0.0014 1 20 9 -0.1184 0.0007 1 20 10 0.0489 -0.0000 1 21 0 -0.0368 -0.0006 1 21 1 0.3170 0.0002 1 21 2 0.0361 0.0025 1 21 3 -0.1996 -0.0004 1 21 4 -0.1013 -0.0037 1 21 5 0.0624 -0.0006 1 21 6 0.2012 0.0027 1 21 7 -0.0968 0.0014 1 21 8 -0.1676 0.0004 1 21 9 0.0570 -0.0006 1 21 10 -0.0068 -0.0016 1 22 0 0.0218 -0.0006 1 22 1 -0.1898 -0.0001 1 22 2 -0.0753 0.0005 1 22 3 -0.1088 -0.0001 1 22 4 0.1932 0.0007 1 22 5 0.1196 -0.0002 1 22 6 -0.1661 -0.0017 1 22 7 -0.0077 -0.0005 1 22 8 0.0025 0.0006 1 22 9 0.0462 0.0002 1 23 0 0.2027 -0.0000 1 23 1 -0.1188 0.0024 1 23 2 -0.2366 -0.0007 1 23 3 0.0213 -0.0023 1 23 4 0.0810 0.0015 1 23 5 0.1149 0.0023 1 23 6 -0.1249 -0.0005 1 23 7 -0.1285 -0.0017 1 23 8 0.1732 -0.0007 1 23 9 0.0245 -0.0006 1 24 0 -0.1723 -0.0007 1 24 1 0.1670 -0.0002 1 24 2 -0.0201 -0.0002 1 24 3 0.0776 0.0005 1 24 4 0.0793 0.0003 1 24 5 -0.1921 -0.0002 1 24 6 0.0513 0.0001 1 24 7 0.0722 0.0003 1 24 8 -0.0430 0.0004 1 24 9 0.0268 0.0007 1 25 0 -0.1797 0.0017 1 25 1 -0.1605 -0.0018 1 25 2 0.1519 -0.0024 1 25 3 0.1038 0.0014 1 25 4 0.0543 0.0010 1 25 5 -0.0820 -0.0010 1 25 6 -0.0887 -0.0013 1 25 7 0.1674 0.0006 1 25 8 -0.0034 0.0008 1 25 9 -0.0975 0.0010 1 26 0 0.2348 0.0009 1 26 1 -0.1441 0.0012 1 26 2 -0.0332 0.0007 1 26 3 0.1307 -0.0002 1 26 4 -0.1638 -0.0008 1 26 5 0.0589 -0.0011 1 26 6 0.0642 -0.0001 1 26 7 -0.1382 0.0007 1 26 8 0.0473 0.0004 1 26 9 0.0320 -0.0011 1 27 0 0.0179 -0.0019 1 27 1 0.2300 -0.0010 1 27 2 0.0722 0.0029 1 27 3 -0.0569 0.0014 1 27 4 -0.0852 -0.0005 1 27 5 -0.0855 -0.0012 1 27 6 0.1271 0.0006 1 27 7 0.0059 0.0011 1 27 8 -0.1114 -0.0001 1 28 0 -0.2497 0.0005 1 28 1 0.0455 -0.0014 1 28 2 0.2067 -0.0016 1 28 3 -0.1955 -0.0005 1 28 4 0.0052 -0.0001 1 28 5 0.0673 0.0013 1 28 6 -0.1263 0.0017 1 28 7 0.1435 -0.0002 1 28 8 0.0765 -0.0011 1 29 0 0.1029 0.0006 1 29 1 -0.0593 0.0026 1 29 2 -0.1738 -0.0003 1 29 3 -0.0527 -0.0020 1 29 4 -0.0183 -0.0021 1 29 5 0.1140 0.0008 1 29 6 0.0306 0.0019 1 29 7 -0.1201 -0.0010 1 29 8 0.0432 -0.0014 1 30 0 0.2191 -0.0019 1 30 1 0.1256 0.0002 1 30 2 -0.2768 0.0019 1 30 3 0.0200 0.0009 1 30 4 0.1516 0.0010 1 30 5 -0.0714 0.0004 1 30 6 0.1423 -0.0021 1 30 8 -0.2223 -0.0003 1 31 0 -0.0823 0.0003 1 31 1 -0.1283 -0.0015 1 31 2 0.0740 -0.0017 1 31 3 0.0811 -0.0003 1 31 4 0.0760 0.0028 1 31 5 0.0380 0.0026 1 31 6 -0.1114 -0.0025 1 31 7 0.0472 -0.0017 1 32 0 -0.1220 0.0019 1 32 1 -0.2462 0.0016 1 32 2 0.1379 -0.0011 1 32 3 0.1821 -0.0009 1 32 4 -0.1306 -0.0007 1 32 5 0.0215 -0.0022 1 32 6 -0.1058 0.0003 1 32 7 -0.1545 0.0016 1 33 0 -0.0077 0.0002 1 33 1 0.1359 -0.0000 1 33 2 0.0826 0.0010 1 33 3 -0.0295 0.0023 1 33 4 0.0085 0.0002 1 33 5 -0.1272 -0.0047 1 33 6 -0.0068 -0.0010 1 33 7 0.0428 0.0038 1 34 0 -0.0124 -0.0000 1 34 1 0.2178 -0.0023 1 34 2 0.0697 -0.0004 1 34 3 -0.2065 0.0009 1 34 4 0.0066 -0.0006 1 34 5 -0.0014 0.0020 1 34 6 0.0182 0.0020 1 34 7 0.2424 0.0000 1 35 0 0.0357 -0.0008 1 35 1 0.0049 0.0002 1 35 2 -0.1313 0.0005 1 35 3 -0.0096 -0.0014 1 35 4 -0.1089 -0.0037 1 35 5 0.0032 0.0022 1 35 6 0.1270 0.0050 1 36 0 0.1068 -0.0023 1 36 1 -0.0829 0.0010 1 36 2 -0.1580 0.0017 1 36 3 0.0871 -0.0007 1 36 4 0.0705 0.0010 1 36 5 0.0081 0.0002 1 36 6 0.0610 -0.0024 1 37 0 0.0256 0.0007 1 37 1 -0.1157 0.0004 1 37 2 0.0555 -0.0006 1 37 3 -0.0003 -0.0011 1 37 4 0.0769 0.0036 1 37 5 0.1797 0.0027 1 38 0 -0.1100 0.0026 1 38 1 -0.0327 0.0015 1 38 2 0.0992 -0.0016 1 38 3 0.0191 0.0001 1 38 4 -0.0639 -0.0002 1 38 5 -0.0186 -0.0019 1 39 0 -0.0826 -0.0004 1 39 1 0.0915 -0.0003 1 39 2 0.0436 -0.0003 1 39 3 0.0194 0.0019 1 40 0 0.0487 -0.0001 1 40 1 0.0501 -0.0028 1 40 2 -0.0023 -0.0000 1 40 3 -0.0342 0.0008 1 41 0 0.0553 0.0007 1 41 1 0.0091 0.0000 1 41 2 -0.0790 0.0006 1 41 3 -0.0160 -0.0007 2 0 0 0.9471 -0.0115 2 0 2 -0.5568 0.0067 2 0 4 0.2186 0.0057 2 0 6 -0.0401 -0.0065 2 0 8 0.0350 0.0025 2 0 10 -0.6291 -0.0037 2 1 0 0.6476 0.0008 2 1 1 0.2117 0.0163 2 1 2 -0.1932 -0.0008 2 1 3 -0.0287 -0.0270 2 1 4 0.0056 -0.0029 2 1 5 -0.0431 0.0147 2 1 6 0.1245 0.0063 2 1 7 0.1515 0.0011 2 1 8 -0.2548 0.0013 2 1 9 -0.2320 -0.0080 2 1 10 0.2806 -0.0056 2 1 11 0.1754 0.0066 2 2 0 -0.6875 0.0001 2 2 1 -0.5095 0.0151 2 2 2 0.4128 0.0018 2 2 3 0.1843 -0.0027 2 2 4 -0.1625 -0.0049 2 2 5 -0.0559 -0.0086 2 2 6 0.0200 0.0031 2 2 7 -0.0228 0.0075 2 2 8 0.0785 0.0009 2 2 9 -0.3270 -0.0055 2 2 10 0.1791 0.0011 2 2 11 0.8232 0.0018 2 3 0 -0.1586 0.0034 2 3 1 -0.4428 -0.0104 2 3 2 0.0151 -0.0154 2 3 3 0.0482 0.0168 2 3 4 -0.0215 0.0169 2 3 5 0.0705 -0.0058 2 3 6 0.0491 -0.0085 2 3 7 -0.2180 -0.0023 2 3 8 -0.1572 -0.0043 2 3 9 0.3260 0.0013 2 3 10 0.1612 0.0089 2 3 11 -0.2846 -0.0009 2 4 0 0.1142 0.0100 2 4 1 0.6894 -0.0087 2 4 2 -0.1133 -0.0082 2 4 3 -0.2279 -0.0008 2 4 4 0.0798 0.0008 2 4 5 0.0356 0.0101 2 4 6 -0.0352 0.0033 2 4 7 0.1361 -0.0067 2 4 8 -0.1826 -0.0050 2 4 9 0.1223 0.0037 2 4 10 0.5470 0.0022 2 4 11 -0.6184 -0.0021 2 5 0 -0.3905 -0.0042 2 5 1 0.2798 -0.0008 2 5 2 0.1520 0.0182 2 5 3 0.0064 0.0011 2 5 4 0.0425 -0.0172 2 5 5 -0.0191 -0.0051 2 5 6 -0.1373 0.0055 2 5 7 -0.0587 0.0025 2 5 8 0.3438 0.0030 2 5 9 0.1426 0.0047 2 5 10 -0.3951 -0.0051 2 5 11 -0.0008 -0.0035 2 6 0 0.3517 -0.0103 2 6 1 -0.5106 -0.0018 2 6 2 -0.1062 0.0081 2 6 3 0.1826 0.0033 2 6 4 -0.0848 0.0035 2 6 5 -0.0212 -0.0058 2 6 6 0.1510 -0.0079 2 6 7 -0.1798 0.0018 2 6 8 -0.0075 0.0063 2 6 9 0.3155 0.0006 2 6 10 -0.5915 -0.0031 2 6 11 -0.2688 0.0005 2 7 0 0.5413 0.0015 2 7 1 0.0994 0.0080 2 7 2 -0.1170 -0.0084 2 7 3 -0.0697 -0.0118 2 7 4 -0.0883 0.0067 2 7 5 -0.0278 0.0091 2 7 6 0.0436 0.0001 2 7 7 0.2708 -0.0021 2 7 8 0.0127 0.0001 2 7 9 -0.5328 -0.0049 2 7 10 0.0468 -0.0008 2 7 11 0.3005 0.0032 2 8 0 -0.4577 0.0025 2 8 1 0.2155 0.0073 2 8 2 0.1786 -0.0032 2 8 3 -0.1959 -0.0031 2 8 4 0.1169 -0.0044 2 8 5 0.1273 -0.0003 2 8 6 -0.2371 0.0068 2 8 7 -0.0096 0.0030 2 8 8 0.2880 -0.0032 2 8 9 -0.3430 -0.0034 2 8 10 0.0058 0.0006 2 8 11 0.7078 0.0007 2 9 0 -0.2323 0.0021 2 9 1 -0.3081 -0.0066 2 9 2 -0.0922 -0.0030 2 9 3 0.0151 0.0094 2 9 4 0.1462 0.0031 2 9 5 0.0669 -0.0048 2 9 6 0.0532 -0.0035 2 9 7 -0.1365 0.0010 2 9 8 -0.4589 -0.0015 2 9 9 0.2879 0.0011 2 9 10 0.4633 0.0032 2 9 11 -0.2224 -0.0003 2 10 0 0.2992 0.0043 2 10 1 -0.0213 -0.0048 2 10 2 -0.2247 -0.0013 2 10 3 0.2609 0.0017 2 10 4 -0.0121 0.0022 2 10 5 -0.2828 0.0027 2 10 6 0.1270 -0.0022 2 10 7 0.2662 -0.0033 2 10 8 -0.2537 -0.0009 2 10 9 -0.0365 0.0019 2 10 10 0.3614 0.0019 2 10 11 -0.3500 0.0006 2 11 0 -0.1674 -0.0033 2 11 1 0.1500 0.0001 2 11 2 0.2243 0.0067 2 11 3 0.1689 -0.0010 2 11 4 -0.1031 -0.0042 2 11 5 -0.1558 -0.0012 2 11 6 -0.0511 0.0023 2 11 7 -0.1189 0.0000 2 11 8 0.4522 0.0005 2 11 9 0.3119 0.0020 2 11 10 -0.5092 -0.0015 2 11 11 -0.1286 -0.0015 2 12 0 -0.1374 -0.0035 2 12 1 -0.0708 -0.0007 2 12 2 0.3122 0.0022 2 12 3 -0.1972 -0.0008 2 12 4 -0.2290 -0.0006 2 12 5 0.2875 -0.0010 2 12 6 0.1091 0.0001 2 12 7 -0.2901 0.0003 2 12 8 -0.0539 0.0013 2 12 9 0.2417 0.0014 2 12 10 -0.1511 -0.0012 2 12 11 -0.1126 -0.0028 2 13 0 0.2564 0.0015 2 13 1 0.1682 0.0047 2 13 2 -0.0878 -0.0023 2 13 3 -0.2876 -0.0036 2 13 4 -0.1059 -0.0008 2 13 5 0.2096 0.0024 2 13 6 0.0759 0.0010 2 13 7 0.1872 -0.0001 2 13 8 -0.0812 0.0009 2 13 9 -0.5899 -0.0020 2 13 10 0.0707 -0.0012 2 14 0 0.1014 -0.0018 2 14 1 0.1559 0.0027 2 14 2 -0.3193 -0.0005 2 14 3 -0.0720 0.0006 2 14 4 0.3774 0.0011 2 14 5 -0.0871 -0.0005 2 14 6 -0.2362 -0.0017 2 14 7 0.0901 0.0008 2 14 8 0.2139 0.0013 2 14 9 -0.0400 -0.0019 2 14 10 -0.1403 -0.0017 2 15 0 -0.0112 0.0016 2 15 1 -0.2709 -0.0039 2 15 2 -0.1932 -0.0032 2 15 3 0.1538 0.0014 2 15 4 0.3066 0.0041 2 15 5 -0.0647 0.0013 2 15 6 -0.1742 -0.0021 2 15 7 -0.1276 -0.0008 2 15 8 -0.1868 -0.0017 2 15 9 0.3579 0.0001 2 15 10 0.3256 0.0022 2 16 0 -0.1228 0.0047 2 16 1 -0.2202 -0.0004 2 16 2 0.1267 -0.0008 2 16 3 0.3400 -0.0005 2 16 4 -0.2501 -0.0020 2 16 5 -0.1386 -0.0009 2 16 6 0.1754 0.0029 2 16 7 0.0508 0.0013 2 16 8 -0.0788 -0.0024 2 16 9 -0.1784 -0.0005 2 16 10 0.0693 0.0028 2 17 0 -0.2337 -0.0026 2 17 1 0.0421 -0.0003 2 17 2 0.3038 0.0040 2 17 3 0.1281 0.0031 2 17 4 -0.2447 -0.0021 2 17 5 -0.2022 -0.0046 2 17 6 0.1570 -0.0002 2 17 7 0.1449 0.0011 2 17 8 0.1868 0.0016 2 17 9 -0.0118 0.0018 2 17 10 -0.3217 -0.0014 2 18 0 0.1125 -0.0026 2 18 1 0.1722 -0.0023 2 18 2 0.1416 0.0002 2 18 3 -0.3362 0.0003 2 18 4 -0.0418 0.0015 2 18 5 0.2019 0.0026 2 18 6 -0.0707 -0.0013 2 18 7 -0.0203 -0.0031 2 18 8 -0.0593 0.0006 2 18 9 0.0981 0.0019 2 18 10 0.1479 -0.0013 2 19 0 0.1872 0.0008 2 19 1 0.2549 0.0028 2 19 2 -0.1225 -0.0003 2 19 3 -0.2490 -0.0042 2 19 4 -0.0369 -0.0023 2 19 5 0.2760 0.0034 2 19 6 0.0684 0.0030 2 19 7 -0.1876 0.0002 2 19 8 -0.1320 -0.0008 2 19 9 -0.0992 -0.0023 2 19 10 0.0800 -0.0003 2 20 0 -0.0855 -0.0009 2 20 1 -0.0433 0.0020 2 20 2 -0.2246 0.0011 2 20 3 0.0790 0.0000 2 20 4 0.2191 -0.0004 2 20 5 -0.1138 -0.0024 2 20 6 0.0308 -0.0009 2 20 7 -0.0052 0.0022 2 20 8 -0.0014 0.0010 2 20 9 0.0746 -0.0010 2 20 10 -0.1421 0.0000 2 21 0 0.0902 0.0013 2 21 1 -0.2984 -0.0011 2 21 2 -0.1372 -0.0027 2 21 3 0.0953 0.0011 2 21 4 0.1951 0.0040 2 21 5 -0.0463 0.0004 2 21 6 -0.2586 -0.0029 2 21 7 0.0729 -0.0019 2 21 8 0.1603 -0.0006 2 21 9 0.0366 0.0014 2 21 10 0.0622 0.0017 2 22 0 0.0735 0.0014 2 22 1 0.0034 0.0000 2 22 2 0.0712 -0.0012 2 22 3 0.1355 -0.0004 2 22 4 -0.1644 0.0000 2 22 5 0.0045 0.0011 2 22 6 0.0053 0.0013 2 22 7 -0.0750 -0.0007 2 22 8 0.0764 -0.0008 2 22 9 -0.0542 0.0003 2 23 0 -0.2984 -0.0010 2 23 1 0.0643 -0.0020 2 23 2 0.2045 0.0017 2 23 3 0.1022 0.0020 2 23 4 -0.0462 -0.0017 2 23 5 -0.1858 -0.0024 2 23 6 0.1623 0.0001 2 23 7 0.1408 0.0018 2 23 8 -0.1618 0.0017 2 23 9 -0.0122 0.0006 2 24 0 -0.0209 0.0005 2 24 1 -0.1201 -0.0007 2 24 2 0.0730 0.0002 2 24 3 -0.1092 0.0005 2 24 4 0.0154 -0.0002 2 24 5 0.0627 -0.0008 2 24 6 -0.0809 -0.0008 2 24 7 0.0965 0.0005 2 24 8 0.0186 0.0006 2 24 9 -0.0530 -0.0006 2 25 0 0.2459 -0.0010 2 25 1 0.1891 0.0023 2 25 2 -0.0646 0.0015 2 25 3 -0.0930 -0.0016 2 25 4 -0.1736 -0.0010 2 25 5 0.1181 0.0007 2 25 6 0.0905 0.0017 2 25 7 -0.2094 0.0002 2 25 8 0.0484 -0.0012 2 25 9 0.0599 -0.0019 2 26 0 -0.1302 -0.0014 2 26 1 0.2205 -0.0007 2 26 2 0.0035 0.0003 2 26 3 -0.0342 -0.0003 2 26 4 0.0587 0.0000 2 26 5 -0.1007 0.0011 2 26 6 0.0851 0.0011 2 26 7 0.0586 -0.0002 2 26 8 -0.1212 -0.0012 2 26 9 0.0063 0.0003 2 27 0 -0.0267 0.0018 2 27 1 -0.2319 0.0002 2 27 2 -0.0826 -0.0027 2 27 3 -0.0677 -0.0009 2 27 4 0.1507 0.0004 2 27 5 0.1253 0.0017 2 27 6 -0.1758 -0.0000 2 27 7 0.0746 -0.0017 2 27 8 0.0800 -0.0007 2 28 0 0.2969 -0.0002 2 28 1 -0.1067 0.0018 2 28 2 -0.1910 0.0006 2 28 3 0.0635 0.0002 2 28 4 -0.0463 0.0004 2 28 5 0.0909 -0.0007 2 28 6 0.0637 -0.0015 2 28 7 -0.2020 -0.0011 2 28 8 0.0057 0.0008 2 29 0 -0.1277 -0.0006 2 29 1 0.0817 -0.0021 2 29 2 0.0926 0.0008 2 29 3 0.1425 0.0018 2 29 4 0.0700 0.0022 2 29 5 -0.1988 -0.0007 2 29 6 0.0390 -0.0028 2 29 7 0.0744 0.0002 2 29 8 -0.1036 0.0021 2 30 0 -0.3108 0.0021 2 30 1 -0.1577 -0.0006 2 30 2 0.2195 -0.0015 2 30 3 0.0454 -0.0006 2 30 4 0.0247 -0.0007 2 30 5 0.0014 -0.0002 2 30 6 -0.2242 0.0007 2 30 7 0.0968 0.0017 2 30 8 0.2131 0.0017 2 31 0 0.1065 -0.0006 2 31 1 0.0700 0.0015 2 31 2 -0.0045 0.0012 2 31 3 -0.0512 0.0001 2 31 4 -0.1867 -0.0027 2 31 5 0.0345 -0.0031 2 31 6 0.0826 0.0025 2 31 7 -0.0990 0.0029 2 32 0 0.1331 -0.0018 2 32 1 0.3048 -0.0014 2 32 2 -0.0292 0.0007 2 32 3 -0.1259 0.0010 2 32 4 -0.0164 0.0008 2 32 5 -0.1175 0.0007 2 32 6 0.1906 0.0004 2 32 7 0.1694 0.0000 2 33 0 -0.0046 0.0002 2 33 1 -0.0811 0.0001 2 33 2 -0.0638 -0.0011 2 33 3 -0.0671 -0.0020 2 33 4 0.0757 -0.0004 2 33 5 0.1105 0.0051 2 33 6 -0.0466 0.0019 2 33 7 0.0590 -0.0038 2 34 0 0.0743 -0.0006 2 34 1 -0.1942 0.0018 2 34 2 -0.1668 0.0010 2 34 3 0.0803 -0.0005 2 34 4 -0.0023 -0.0008 2 34 5 0.1348 -0.0007 2 34 6 0.0124 -0.0004 2 35 0 -0.0230 0.0008 2 35 1 -0.0167 -0.0008 2 35 2 0.0529 -0.0001 2 35 3 0.0819 0.0013 2 35 4 0.0863 0.0038 2 35 5 -0.0556 -0.0019 2 35 6 -0.0299 -0.0057 2 36 0 -0.1332 0.0026 2 36 1 -0.0291 0.0002 2 36 2 0.1732 -0.0016 2 36 3 0.0156 -0.0007 2 36 4 0.0184 0.0003 2 36 5 -0.0357 0.0006 2 37 0 -0.0524 -0.0011 2 37 1 0.0859 0.0005 2 37 2 0.0116 0.0006 2 37 3 -0.0153 0.0009 2 37 4 -0.1082 -0.0035 2 37 5 -0.0906 -0.0033 2 38 0 0.0446 -0.0020 2 38 1 0.1323 -0.0023 2 38 2 -0.0303 0.0002 2 38 3 -0.0539 0.0013 2 38 4 -0.0021 0.0004 2 39 0 0.1167 0.0013 2 39 1 -0.0457 -0.0003 2 39 2 -0.0659 -0.0003 2 39 3 -0.0429 -0.0016 2 39 4 0.0063 0.0002 2 40 0 0.0447 -0.0007 2 40 1 -0.0552 0.0021 2 40 2 -0.0864 0.0017 2 40 3 0.0232 -0.0007 2 41 0 -0.0731 -0.0017 2 41 1 -0.0487 -0.0003 2 41 2 0.0638 0.0004 3 0 0 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-0.3299 -0.0020 3 12 3 0.0943 0.0006 3 12 4 0.1576 0.0002 3 12 5 -0.2143 0.0019 3 12 6 -0.0405 -0.0008 3 12 7 0.4567 -0.0002 3 12 8 -0.0288 0.0005 3 12 9 -0.5378 -0.0015 3 12 10 0.2123 -0.0001 3 13 0 -0.1534 -0.0009 3 13 1 -0.1009 -0.0033 3 13 2 -0.0801 0.0013 3 13 3 0.2590 0.0029 3 13 4 0.1858 0.0009 3 13 5 -0.2277 -0.0023 3 13 6 -0.1524 -0.0010 3 13 7 -0.1831 0.0007 3 13 8 0.1800 -0.0017 3 13 9 0.4366 0.0015 3 13 10 -0.0345 0.0020 3 14 0 -0.2104 0.0024 3 14 1 -0.2349 -0.0032 3 14 2 0.2733 0.0003 3 14 3 0.1174 -0.0005 3 14 4 -0.2091 -0.0003 3 14 5 0.0776 0.0000 3 14 6 0.1845 0.0014 3 14 7 -0.2222 -0.0000 3 14 8 -0.3720 -0.0023 3 14 9 0.2643 0.0007 3 14 10 0.3278 0.0016 3 15 0 -0.0423 -0.0004 3 15 1 0.0873 0.0024 3 15 2 0.2529 0.0032 3 15 3 -0.0282 -0.0010 3 15 4 -0.3595 -0.0042 3 15 5 0.0536 -0.0010 3 15 6 0.1915 0.0026 3 15 7 0.2139 0.0002 3 15 8 0.1248 0.0018 3 15 9 -0.3966 0.0006 3 15 10 -0.1955 -0.0023 3 16 0 0.0530 -0.0057 3 16 1 0.2941 0.0007 3 16 2 -0.0375 0.0013 3 16 3 -0.2634 0.0006 3 16 4 0.1108 0.0014 3 16 5 0.0156 0.0002 3 16 6 -0.1334 -0.0025 3 16 7 -0.0039 -0.0016 3 16 8 0.2806 0.0023 3 16 9 0.2182 0.0011 3 16 10 -0.3150 -0.0017 3 17 0 0.1830 0.0010 3 17 1 0.1163 0.0008 3 17 2 -0.1858 -0.0036 3 17 3 -0.2530 -0.0032 3 17 4 0.2427 0.0024 3 17 5 0.1993 0.0045 3 17 6 -0.1372 -0.0005 3 17 7 -0.1758 -0.0009 3 17 8 -0.2664 -0.0014 3 17 9 0.1166 -0.0022 3 17 10 0.3128 0.0012 3 18 0 0.0455 0.0035 3 18 1 -0.1383 0.0028 3 18 2 -0.1886 -0.0008 3 18 3 0.2188 -0.0006 3 18 4 0.0144 -0.0017 3 18 5 -0.0145 -0.0017 3 18 6 0.1125 0.0017 3 18 7 -0.0090 0.0029 3 18 8 -0.0216 -0.0006 3 18 9 -0.2902 -0.0018 3 18 10 -0.0722 0.0007 3 19 0 -0.0799 -0.0001 3 19 1 -0.2517 -0.0026 3 19 2 -0.0761 0.0003 3 19 3 0.2677 0.0041 3 19 4 0.0664 0.0019 3 19 5 -0.2683 -0.0036 3 19 6 -0.0358 -0.0024 3 19 7 0.1280 -0.0002 3 19 8 0.2182 0.0005 3 19 9 0.1181 0.0027 3 19 10 -0.1823 0.0005 3 20 0 0.0228 0.0009 3 20 1 -0.0674 -0.0030 3 20 2 0.2107 -0.0011 3 20 3 -0.0615 0.0002 3 20 4 -0.0742 0.0010 3 20 5 0.0469 0.0024 3 20 6 -0.1907 -0.0000 3 20 7 0.0294 -0.0026 3 20 8 -0.0040 -0.0008 3 20 9 0.0485 0.0012 3 20 10 0.2528 -0.0001 3 21 0 -0.1449 -0.0013 3 21 1 0.1566 0.0014 3 21 2 0.2402 0.0024 3 21 3 -0.0091 -0.0014 3 21 4 -0.2115 -0.0034 3 21 5 0.0774 -0.0001 3 21 6 0.1813 0.0023 3 21 7 -0.0500 0.0017 3 21 8 -0.1331 0.0012 3 21 9 -0.1276 -0.0015 3 22 0 -0.1760 -0.0024 3 22 1 0.0843 0.0003 3 22 2 -0.0671 0.0017 3 22 3 -0.0535 0.0006 3 22 4 0.1090 -0.0003 3 22 5 -0.1277 -0.0019 3 22 6 0.1536 -0.0011 3 22 7 0.1213 0.0017 3 22 8 -0.0869 0.0012 3 22 9 0.0662 -0.0006 3 23 0 0.2551 0.0013 3 23 1 0.0549 0.0012 3 23 2 -0.1498 -0.0019 3 23 3 -0.1917 -0.0012 3 23 4 0.0418 0.0014 3 23 5 0.1269 0.0017 3 23 6 -0.1489 0.0002 3 23 7 -0.0639 -0.0010 3 23 8 0.1110 -0.0021 3 23 9 0.0239 -0.0010 3 24 0 0.1882 0.0002 3 24 1 0.1025 0.0014 3 24 2 -0.0265 -0.0005 3 24 3 0.0877 -0.0011 3 24 4 -0.1442 -0.0001 3 24 5 0.0879 0.0013 3 24 6 0.0709 0.0016 3 24 7 -0.2194 -0.0008 3 24 8 0.0167 -0.0014 3 24 9 0.0058 0.0004 3 25 0 -0.1780 0.0002 3 25 1 -0.1771 -0.0020 3 25 2 -0.0367 -0.0005 3 25 3 0.1064 0.0011 3 25 4 0.1853 0.0007 3 25 5 -0.0995 0.0001 3 25 6 -0.0094 -0.0011 3 25 7 0.1506 -0.0010 3 25 8 -0.0975 0.0005 3 25 9 -0.0092 0.0024 3 26 0 0.0405 0.0016 3 26 1 -0.2391 -0.0002 3 26 2 -0.0393 -0.0008 3 26 3 -0.1093 0.0007 3 26 4 0.0979 0.0004 3 26 5 0.1149 -0.0006 3 26 6 -0.2046 -0.0016 3 26 7 0.0482 -0.0006 3 26 8 0.1216 0.0014 3 26 9 -0.0152 0.0005 3 27 0 0.0295 -0.0012 3 27 1 0.1554 0.0006 3 27 2 0.0978 0.0017 3 27 3 0.1084 0.0006 3 27 4 -0.1682 0.0002 3 27 5 -0.0860 -0.0018 3 27 6 0.1163 -0.0010 3 27 7 -0.1411 0.0012 3 27 8 0.0086 0.0019 3 28 0 -0.3191 -0.0004 3 28 1 0.1127 -0.0016 3 28 2 0.1343 0.0004 3 28 3 0.1421 -0.0003 3 28 4 0.0695 -0.0003 3 28 5 -0.2452 0.0002 3 28 6 0.0308 0.0007 3 28 7 0.1841 0.0017 3 28 8 -0.0628 0.0000 3 29 0 0.0606 0.0006 3 29 1 -0.0783 0.0012 3 29 2 -0.0285 -0.0008 3 29 3 -0.1685 -0.0011 3 29 4 -0.0466 -0.0022 3 29 5 0.1795 0.0001 3 29 6 -0.0945 0.0029 3 29 8 0.1153 -0.0019 3 30 0 0.3610 -0.0019 3 30 1 0.1670 0.0010 3 30 2 -0.0801 0.0006 3 30 3 -0.1250 0.0006 3 30 4 -0.2243 0.0004 3 30 5 0.1041 -0.0004 3 30 6 0.2396 0.0005 3 30 7 -0.1425 -0.0009 3 30 8 -0.1417 -0.0025 3 31 0 -0.0670 0.0005 3 31 1 0.0231 -0.0013 3 31 2 -0.0272 -0.0007 3 31 3 0.0396 -0.0001 3 31 4 0.1832 0.0022 3 31 5 -0.1000 0.0033 3 31 6 0.0105 -0.0013 3 31 7 0.1000 -0.0034 3 32 0 -0.1280 0.0017 3 32 1 -0.2907 0.0009 3 32 2 -0.1017 -0.0001 3 32 3 0.0246 -0.0009 3 32 4 0.2028 -0.0012 3 32 5 0.1633 0.0009 3 32 6 -0.2540 -0.0004 3 32 7 -0.1239 -0.0017 3 33 0 0.0434 -0.0007 3 33 1 0.0008 -0.0000 3 33 2 0.0074 0.0013 3 33 3 0.0876 0.0015 3 33 4 -0.1210 0.0005 3 33 5 -0.0169 -0.0043 3 33 6 0.0568 -0.0028 3 33 7 -0.1643 0.0023 3 34 0 -0.1187 0.0009 3 34 1 0.1277 -0.0010 3 34 2 0.2139 -0.0012 3 34 3 0.0924 -0.0001 3 34 4 -0.0329 0.0020 3 34 5 -0.2533 -0.0003 3 34 6 0.0099 -0.0015 3 35 0 -0.0430 -0.0002 3 35 1 -0.0054 0.0015 3 35 2 0.0320 -0.0007 3 35 3 -0.0902 -0.0013 3 35 4 -0.0137 -0.0031 3 35 5 0.0489 0.0012 3 35 6 -0.0871 0.0050 3 36 0 0.1337 -0.0025 3 36 1 0.1250 -0.0009 3 36 2 -0.1312 0.0011 3 36 3 -0.1328 0.0018 3 36 4 -0.1009 -0.0014 3 36 5 0.1044 -0.0015 3 37 0 0.0704 0.0015 3 37 1 0.0036 -0.0020 3 37 2 -0.0453 -0.0006 3 37 3 0.0188 0.0001 3 37 4 0.0748 0.0030 3 38 0 0.0343 0.0013 3 38 1 -0.1937 0.0022 3 38 2 -0.0567 0.0009 3 38 3 0.0802 -0.0021 3 38 4 0.0928 -0.0006 3 39 0 -0.0828 -0.0028 3 39 1 -0.0172 0.0011 3 39 2 0.0412 0.0016 3 39 3 0.0402 0.0009 3 39 4 -0.0456 -0.0006 3 40 0 -0.1414 0.0010 3 40 1 0.0399 -0.0011 3 40 2 0.1638 -0.0024 3 40 3 0.0047 0.0004 3 41 0 0.0420 0.0031 3 41 1 0.0475 0.0011 4 0 0 0.1678 -0.0111 4 0 2 -0.1391 0.0121 4 0 4 0.1807 0.0025 4 0 6 -0.2511 -0.0096 4 0 8 0.3987 0.0036 4 0 10 -0.5034 -0.0016 4 1 0 0.4797 -0.0058 4 1 1 0.1291 0.0125 4 1 2 -0.1728 -0.0009 4 1 3 -0.0390 -0.0239 4 1 4 0.1286 0.0023 4 1 5 -0.0017 0.0111 4 1 6 0.0353 0.0042 4 1 7 0.0311 0.0052 4 1 8 -0.0533 -0.0028 4 1 9 0.1385 -0.0065 4 1 10 -0.1408 -0.0025 4 1 11 -0.2948 0.0060 4 2 0 -0.1920 0.0020 4 2 1 -0.0531 0.0154 4 2 2 0.1214 -0.0019 4 2 3 0.0813 -0.0062 4 2 4 -0.1044 -0.0010 4 2 5 -0.1541 -0.0117 4 2 6 0.0908 0.0007 4 2 7 0.2512 0.0111 4 2 8 -0.0878 0.0035 4 2 9 -0.4719 -0.0058 4 2 10 0.1252 -0.0034 4 2 11 0.4063 0.0027 4 3 0 -0.1657 0.0063 4 3 1 -0.2820 -0.0063 4 3 2 0.0774 -0.0119 4 3 3 0.0841 0.0179 4 3 4 -0.0991 0.0107 4 3 5 0.0017 -0.0078 4 3 6 0.0265 -0.0031 4 3 7 -0.0926 -0.0054 4 3 8 0.1367 -0.0027 4 3 9 -0.1623 0.0030 4 3 10 -0.3667 0.0056 4 3 11 0.3986 -0.0014 4 4 0 0.2230 0.0053 4 4 1 0.1300 -0.0107 4 4 2 -0.0881 -0.0068 4 4 3 -0.0886 0.0037 4 4 4 -0.0092 -0.0012 4 4 5 0.0910 0.0095 4 4 6 0.1098 0.0064 4 4 7 -0.0384 -0.0062 4 4 8 -0.3306 -0.0060 4 4 9 0.2104 0.0003 4 4 10 0.4591 0.0042 4 4 11 -0.2302 0.0000 4 5 0 -0.1925 -0.0035 4 5 1 0.2245 -0.0019 4 5 2 0.0127 0.0148 4 5 3 -0.0735 -0.0035 4 5 4 0.0807 -0.0155 4 5 5 0.0165 0.0012 4 5 6 -0.1194 0.0020 4 5 7 0.0964 0.0026 4 5 8 -0.0999 0.0037 4 5 9 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0.0473 -0.0001 4 9 9 -0.1461 -0.0003 4 9 10 -0.3112 0.0025 4 9 11 0.5122 -0.0001 4 10 0 0.2209 0.0009 4 10 1 -0.2114 -0.0029 4 10 2 -0.1610 0.0011 4 10 3 0.0914 0.0015 4 10 4 0.0110 0.0015 4 10 5 -0.1416 0.0036 4 10 6 0.2893 -0.0036 4 10 7 0.3106 -0.0006 4 10 8 -0.5958 0.0005 4 10 9 -0.2076 -0.0014 4 10 10 0.4961 0.0004 4 11 0 0.0309 -0.0009 4 11 1 -0.0062 -0.0000 4 11 2 -0.0428 0.0038 4 11 3 0.2263 -0.0020 4 11 4 -0.0044 -0.0023 4 11 5 -0.2485 0.0001 4 11 6 -0.0835 0.0011 4 11 7 0.1749 0.0008 4 11 8 0.1757 -0.0003 4 11 9 -0.0571 0.0024 4 11 10 0.2746 -0.0005 4 12 0 -0.3201 -0.0008 4 12 1 0.0016 -0.0004 4 12 2 0.2304 0.0008 4 12 3 -0.0031 -0.0011 4 12 4 -0.0844 0.0003 4 12 5 0.1579 -0.0025 4 12 6 -0.0156 0.0014 4 12 7 -0.5715 0.0003 4 12 8 0.0647 -0.0023 4 12 9 0.6559 0.0015 4 12 10 -0.1127 0.0012 4 13 0 -0.0175 0.0007 4 13 1 0.0199 0.0021 4 13 2 0.1916 -0.0005 4 13 3 -0.1838 -0.0023 4 13 4 -0.1859 -0.0006 4 13 5 0.2174 0.0018 4 13 6 0.2093 0.0013 4 13 7 0.0493 -0.0007 4 13 8 -0.2997 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0.0025 4 17 10 -0.2030 -0.0019 4 18 0 -0.0760 -0.0034 4 18 1 0.0577 -0.0026 4 18 2 0.1153 0.0007 4 18 3 -0.0846 0.0004 4 18 4 -0.0042 0.0018 4 18 5 -0.1035 0.0011 4 18 6 -0.1289 -0.0015 4 18 7 -0.0180 -0.0028 4 18 8 0.1352 0.0003 4 18 9 0.4206 0.0020 4 18 10 -0.0150 -0.0002 4 19 0 -0.0662 -0.0008 4 19 1 0.2054 0.0022 4 19 2 0.1954 -0.0001 4 19 3 -0.2410 -0.0039 4 19 4 -0.0006 -0.0014 4 19 5 0.1768 0.0033 4 19 6 -0.0328 0.0015 4 19 7 -0.0802 0.0004 4 19 8 -0.3138 -0.0002 4 19 9 -0.0090 -0.0033 4 19 10 0.3099 -0.0005 4 20 0 -0.0484 -0.0008 4 20 1 0.0774 0.0031 4 20 2 -0.1007 0.0007 4 20 3 0.0641 0.0001 4 20 4 -0.0349 -0.0011 4 20 5 0.0233 -0.0023 4 20 6 0.2481 0.0003 4 20 7 -0.0056 0.0026 4 20 8 0.0179 0.0010 4 20 9 -0.1944 -0.0012 4 21 0 0.1624 0.0012 4 21 1 -0.0124 -0.0012 4 21 2 -0.2868 -0.0020 4 21 3 0.0028 0.0015 4 21 4 0.1260 0.0028 4 21 5 -0.1272 -0.0004 4 21 6 -0.0210 -0.0014 4 21 7 0.0157 -0.0011 4 21 8 0.1550 -0.0018 4 21 9 0.1939 0.0016 4 22 0 0.2319 0.0027 4 22 1 -0.0397 -0.0007 4 22 2 0.0657 -0.0015 4 22 3 -0.0600 -0.0006 4 22 4 -0.0563 -0.0001 4 22 5 0.1650 0.0021 4 22 6 -0.2374 0.0012 4 22 7 -0.1180 -0.0017 4 22 8 0.0355 -0.0015 4 22 9 -0.0462 0.0004 4 23 0 -0.1320 -0.0011 4 23 1 -0.1467 -0.0005 4 23 2 0.1325 0.0018 4 23 3 0.1790 0.0006 4 23 4 -0.0570 -0.0011 4 23 5 0.0367 -0.0007 4 23 6 0.0738 -0.0003 4 23 7 -0.0275 -0.0002 4 23 8 -0.0569 0.0020 4 23 9 -0.1018 0.0015 4 24 0 -0.2324 -0.0008 4 24 1 -0.1110 -0.0014 4 24 2 -0.0882 0.0007 4 24 3 -0.0439 0.0007 4 24 4 0.2284 0.0005 4 24 5 -0.1690 -0.0008 4 24 6 -0.0154 -0.0018 4 24 7 0.2395 0.0003 4 24 8 -0.0384 0.0015 4 24 9 0.0724 0.0002 4 25 0 0.0562 0.0005 4 25 1 0.1508 0.0014 4 25 2 0.0577 -0.0003 4 25 3 -0.1322 -0.0006 4 25 4 -0.0779 -0.0003 4 25 5 0.0106 -0.0007 4 25 6 -0.0933 0.0001 4 25 7 -0.0317 0.0015 4 25 8 0.1006 0.0005 4 26 0 -0.0084 -0.0014 4 26 1 0.1745 0.0009 4 26 2 0.1167 0.0004 4 26 3 0.2381 -0.0006 4 26 4 -0.2151 -0.0001 4 26 5 -0.0974 -0.0001 4 26 6 0.2176 0.0010 4 26 7 -0.1316 0.0010 4 26 8 -0.0508 -0.0006 4 27 0 -0.0353 0.0003 4 27 1 -0.0904 -0.0009 4 27 2 -0.0956 -0.0007 4 27 3 -0.0270 -0.0005 4 27 4 0.1109 -0.0006 4 27 5 0.0085 0.0015 4 27 6 0.0209 0.0018 4 27 7 0.1486 -0.0002 4 27 8 -0.0823 -0.0026 4 28 0 0.2775 0.0008 4 28 1 -0.0479 0.0008 4 28 2 -0.0560 -0.0007 4 28 3 -0.3334 0.0008 4 28 4 -0.0715 -0.0004 4 28 5 0.3128 -0.0003 4 28 6 -0.0969 0.0004 4 28 7 -0.0838 -0.0010 4 28 8 0.0597 -0.0010 4 29 0 0.0390 -0.0004 4 29 1 0.0853 -0.0004 4 29 2 0.0355 0.0005 4 29 3 0.0966 0.0008 4 29 4 -0.0287 0.0021 4 29 5 -0.0685 0.0004 4 29 6 0.0952 -0.0023 4 29 7 -0.1369 -0.0027 4 29 8 -0.0818 0.0011 4 30 0 -0.3138 0.0013 4 30 1 -0.1474 -0.0010 4 30 2 -0.0921 0.0005 4 30 3 0.1972 -0.0010 4 30 4 0.3600 -0.0003 4 30 5 -0.1846 0.0016 4 30 6 -0.1772 -0.0009 4 30 7 0.1161 -0.0006 4 31 0 0.0118 -0.0005 4 31 1 -0.1015 0.0010 4 31 2 -0.0245 0.0007 4 31 3 -0.0463 0.0001 4 31 4 -0.0666 -0.0019 4 31 5 0.1189 -0.0029 4 31 6 -0.1112 -0.0001 4 31 7 -0.0545 0.0032 4 32 0 0.1018 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0.0003 5 12 3 -0.0276 0.0018 5 12 4 0.0430 -0.0007 5 12 5 -0.1218 0.0027 5 12 6 0.0419 -0.0014 5 12 7 0.5395 -0.0005 5 12 8 -0.0277 0.0029 5 12 9 -0.5048 -0.0018 5 12 10 -0.1040 -0.0012 5 13 0 0.1260 -0.0010 5 13 1 0.0337 -0.0020 5 13 2 -0.1948 0.0002 5 13 3 0.0954 0.0022 5 13 4 0.1530 0.0000 5 13 5 -0.2034 -0.0012 5 13 6 -0.2763 -0.0019 5 13 7 0.1608 0.0004 5 13 8 0.4277 0.0000 5 13 9 -0.2384 0.0028 5 13 10 -0.0947 0.0017 5 14 0 -0.1405 0.0028 5 14 1 -0.0692 -0.0008 5 14 2 0.0405 0.0001 5 14 3 0.0785 -0.0015 5 14 4 -0.0022 0.0004 5 14 5 0.0383 -0.0008 5 14 6 0.1443 0.0007 5 14 7 -0.3961 0.0015 5 14 8 -0.4170 -0.0036 5 14 9 0.3092 -0.0004 5 14 10 0.3326 0.0017 5 15 0 -0.0885 0.0008 5 15 1 -0.1677 0.0002 5 15 2 0.1818 0.0035 5 15 3 0.0537 -0.0007 5 15 4 -0.2032 -0.0033 5 15 5 0.0664 -0.0006 5 15 6 0.2504 0.0025 5 15 7 0.2436 0.0009 5 15 8 -0.3615 0.0018 5 15 9 -0.3211 -0.0008 5 15 10 0.3050 -0.0038 5 16 0 0.0179 -0.0040 5 16 1 0.0567 -0.0002 5 16 2 0.0189 0.0003 5 16 3 -0.0518 0.0009 5 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5 25 3 0.1533 0.0006 5 25 4 -0.0733 0.0004 5 25 5 0.1168 0.0008 5 25 6 0.1400 0.0003 5 25 7 -0.0766 -0.0015 5 25 8 -0.0472 -0.0010 5 26 0 0.0139 0.0008 5 26 1 -0.0716 -0.0010 5 26 2 -0.1639 0.0003 5 26 3 -0.2959 0.0001 5 26 4 0.2152 -0.0006 5 26 5 0.0760 0.0007 5 26 6 -0.1190 0.0003 5 26 7 0.1543 -0.0008 5 26 8 -0.0298 -0.0008 5 27 0 0.0430 0.0003 5 27 1 0.1025 0.0008 5 27 2 0.0711 0.0004 5 27 3 -0.1319 0.0007 5 27 4 -0.0065 0.0003 5 27 5 0.0407 -0.0013 5 27 6 -0.1534 -0.0018 5 27 7 -0.0866 -0.0004 5 27 8 0.0848 0.0026 5 28 0 -0.1743 -0.0007 5 28 1 -0.0308 0.0001 5 28 2 -0.0124 0.0005 5 28 3 0.4134 -0.0011 5 28 4 0.0730 0.0012 5 28 5 -0.2657 0.0008 5 28 6 0.0892 -0.0014 5 28 7 -0.0467 -0.0007 5 28 8 -0.0104 0.0016 5 29 0 -0.0911 0.0000 5 29 1 -0.1206 0.0002 5 29 2 -0.1166 0.0000 5 29 3 0.0442 -0.0012 5 29 4 0.1032 -0.0018 5 29 5 -0.0593 -0.0001 5 29 6 -0.0360 0.0016 5 29 7 0.1644 0.0029 5 30 0 0.1908 -0.0007 5 30 1 0.0995 0.0007 5 30 2 0.2102 -0.0012 5 30 3 -0.2287 0.0015 5 30 4 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6 2 0.0227 -0.0069 9 6 3 0.0676 0.0025 9 6 4 -0.1494 -0.0007 9 6 5 0.2676 0.0038 9 6 6 0.1535 0.0136 9 6 7 -0.5801 -0.0057 9 6 8 0.0136 -0.0057 9 6 9 0.7441 0.0022 9 7 0 -0.0424 -0.0018 9 7 1 -0.2463 -0.0078 9 7 2 -0.0334 -0.0003 9 7 3 0.0443 0.0086 9 7 4 -0.0293 -0.0053 9 7 5 0.2207 -0.0081 9 7 6 -0.1153 0.0036 9 7 7 -0.3745 0.0016 9 7 8 0.2611 -0.0016 9 7 9 0.4317 -0.0010 9 8 0 -0.0016 -0.0037 9 8 1 -0.0572 -0.0003 9 8 2 0.0061 0.0057 9 8 3 -0.1328 0.0020 9 8 4 0.1984 0.0010 9 8 5 0.0149 0.0029 9 8 6 -0.4183 -0.0110 9 8 7 0.2530 -0.0042 9 8 8 0.4046 0.0042 9 8 9 -0.5002 -0.0006 9 9 0 -0.1645 -0.0015 9 9 1 0.0987 0.0037 9 9 2 0.2214 0.0035 9 9 3 0.0484 -0.0043 9 9 4 0.0068 -0.0016 9 9 5 -0.2160 0.0061 9 9 6 -0.0150 0.0006 9 9 7 0.3589 -0.0010 9 9 8 0.1945 0.0007 9 9 9 -0.3918 0.0035 9 10 0 -0.1047 0.0009 9 10 1 0.0540 0.0012 9 10 2 -0.0404 -0.0016 9 10 3 0.1507 -0.0032 9 10 4 -0.0422 -0.0012 9 10 5 -0.2987 -0.0056 9 10 6 0.2220 0.0027 9 10 7 0.1947 0.0068 9 10 8 -0.3471 0.0004 9 10 9 0.0560 0.0020 9 11 0 0.1657 0.0019 9 11 1 0.1731 -0.0006 9 11 2 -0.1337 -0.0020 9 11 3 -0.1728 -0.0002 9 11 4 -0.1051 0.0026 9 11 5 0.2116 -0.0023 9 11 6 0.0958 -0.0014 9 11 7 -0.1873 -0.0001 9 11 8 -0.3323 0.0004 9 11 9 -0.0509 -0.0035 9 12 0 0.1803 -0.0013 9 12 1 -0.0077 0.0001 9 12 2 0.0385 -0.0006 9 12 3 -0.0631 0.0011 9 12 4 -0.1450 0.0010 9 12 5 0.2372 0.0041 9 12 6 0.1923 0.0031 9 12 7 -0.1963 -0.0026 9 12 8 -0.0533 -0.0015 9 12 9 0.1168 -0.0040 9 13 0 0.0282 -0.0015 9 13 1 -0.2428 0.0001 9 13 2 -0.1090 -0.0010 9 13 3 0.0841 0.0014 9 13 4 0.2267 -0.0009 9 13 5 -0.1333 0.0003 9 13 6 -0.1476 0.0007 9 13 7 0.0978 0.0005 9 13 8 0.1747 -0.0009 9 13 9 0.2866 0.0014 9 14 0 -0.1376 0.0027 9 14 1 -0.0737 -0.0001 9 14 2 -0.0043 -0.0002 9 14 3 -0.0190 0.0009 9 14 4 0.1306 -0.0001 9 14 5 0.0370 -0.0015 9 14 6 -0.2706 -0.0031 9 14 7 -0.2186 -0.0016 9 14 8 0.2082 -0.0014 9 15 0 -0.1722 0.0014 9 15 1 0.0674 -0.0012 9 15 2 0.1887 0.0027 9 15 3 0.1459 0.0003 9 15 4 -0.1804 -0.0004 9 15 5 0.0044 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20 6 -0.0987 0.0004 9 20 7 -0.1777 -0.0020 9 20 8 0.4468 -0.0001 9 21 0 -0.0711 -0.0025 9 21 1 -0.0040 0.0011 9 21 2 0.1996 0.0031 9 21 3 0.1119 -0.0011 9 21 4 -0.1138 -0.0010 9 21 5 -0.0245 -0.0004 9 21 6 -0.1090 -0.0019 9 21 7 -0.1350 0.0003 9 21 8 -0.0842 0.0013 9 22 0 0.0178 -0.0016 9 22 1 0.1367 -0.0004 9 22 2 -0.0205 0.0007 9 22 3 -0.1606 0.0013 9 22 4 0.2906 0.0010 9 22 5 0.0823 -0.0004 9 22 6 -0.1368 -0.0015 9 22 7 0.2548 0.0005 9 22 8 -0.1644 0.0010 9 23 0 0.0212 0.0023 9 23 1 0.1085 0.0009 9 23 2 -0.1044 -0.0024 9 23 3 -0.2053 -0.0011 9 23 4 -0.0160 0.0004 9 23 5 0.0195 -0.0002 9 23 6 0.0926 0.0022 9 23 7 0.0599 0.0009 9 24 0 0.0962 0.0004 9 24 1 -0.0504 0.0007 9 24 2 -0.0986 0.0014 9 24 3 0.2239 -0.0008 9 24 4 -0.0681 -0.0021 9 24 5 -0.3233 -0.0010 9 24 6 0.0979 0.0010 9 24 7 -0.0986 0.0008 9 25 0 0.0680 -0.0017 9 25 1 -0.1305 -0.0012 9 25 2 -0.0124 0.0002 9 25 3 0.1869 0.0013 9 25 4 0.0934 0.0006 9 25 5 0.0525 0.0013 9 25 6 -0.0946 -0.0014 9 25 7 -0.0330 -0.0020 9 26 0 -0.1084 0.0002 9 26 1 -0.0703 0.0010 9 26 2 0.1099 -0.0021 9 26 3 -0.1141 -0.0018 9 26 4 -0.1855 0.0014 9 26 5 0.2679 0.0024 9 26 6 0.1048 0.0006 9 27 0 -0.1092 0.0012 9 27 1 0.0917 0.0005 9 27 2 0.1033 0.0006 9 27 3 -0.1383 0.0001 9 27 4 -0.0970 -0.0006 9 27 5 -0.1103 -0.0021 9 27 6 0.0397 -0.0003 9 28 0 0.0586 0.0009 9 28 1 0.0983 -0.0027 9 28 2 -0.0236 -0.0003 9 28 3 -0.0085 0.0033 9 28 4 0.2286 0.0018 9 28 5 -0.0293 -0.0019 9 28 6 -0.1610 -0.0017 9 29 0 0.0815 -0.0003 9 29 1 -0.0342 -0.0005 9 29 2 -0.1715 0.0003 9 29 3 0.0799 -0.0010 9 29 4 0.0896 -0.0006 9 29 5 0.0996 0.0016 9 29 6 0.0669 0.0022 9 30 0 -0.0219 -0.0031 9 30 1 -0.0446 0.0017 9 30 2 -0.0246 0.0036 9 30 3 0.0228 -0.0009 9 30 4 -0.1279 -0.0041 9 30 5 -0.0971 -0.0008 9 31 0 -0.0340 -0.0014 9 31 1 -0.0212 0.0012 9 31 2 0.2064 -0.0007 9 31 3 0.0128 0.0002 9 31 4 -0.0959 0.0013 9 31 5 -0.0477 0.0002 9 32 0 0.0065 0.0040 9 32 1 0.0101 0.0019 9 32 2 -0.0148 -0.0037 9 32 3 -0.0038 -0.0035 9 32 4 0.0731 0.0026 9 33 0 0.0179 0.0028 9 33 1 0.0807 -0.0007 9 33 2 -0.1821 -0.0006 9 33 3 -0.1248 0.0004 9 33 4 0.0815 -0.0005 9 34 0 0.0171 -0.0017 9 34 1 -0.0274 -0.0047 9 34 2 0.0482 0.0000 9 34 3 0.0504 0.0052 9 34 4 -0.0792 0.0018 9 35 0 -0.0129 -0.0020 9 35 1 -0.1489 -0.0018 9 35 2 0.0882 0.0010 9 35 3 0.1967 0.0007 9 36 0 -0.0419 -0.0024 9 36 1 0.0392 0.0039 9 36 2 -0.0060 0.0039 9 37 0 -0.0407 -0.0014 9 37 1 0.1838 0.0033 10 0 0 -0.0561 -0.0051 10 0 2 0.0986 0.0043 10 0 4 -0.0333 0.0039 10 0 6 -0.3438 -0.0115 10 0 8 0.7179 0.0071 10 1 0 0.2023 -0.0149 10 1 1 0.0851 0.0094 10 1 2 -0.1043 0.0129 10 1 3 -0.1206 -0.0147 10 1 4 0.4117 -0.0072 10 1 5 0.1100 0.0175 10 1 6 -0.3213 -0.0013 10 1 7 0.0867 -0.0019 10 1 8 -0.0728 0.0046 10 1 9 -0.2560 0.0003 10 2 0 -0.0357 0.0012 10 2 1 0.0559 0.0039 10 2 2 -0.0308 -0.0028 10 2 3 -0.0779 -0.0034 10 2 4 -0.0025 -0.0051 10 2 5 -0.0999 -0.0070 10 2 6 0.2956 0.0067 10 2 7 0.2940 0.0099 10 2 8 -0.5492 -0.0049 10 2 9 -0.5237 0.0004 10 3 0 0.0015 0.0144 10 3 1 -0.1082 0.0027 10 3 2 -0.0691 -0.0141 10 3 3 0.2331 0.0017 10 3 4 -0.2146 0.0159 10 3 5 -0.3112 -0.0093 10 3 6 0.3678 -0.0060 10 3 7 -0.0251 0.0045 10 3 8 -0.3393 -0.0036 10 3 9 0.3697 -0.0038 10 4 0 0.1749 0.0026 10 4 1 0.0334 -0.0055 10 4 2 -0.0522 -0.0002 10 4 3 0.0311 0.0018 10 4 4 -0.0051 0.0023 10 4 5 0.2324 0.0097 10 4 6 -0.1035 0.0035 10 4 7 -0.4585 -0.0106 10 4 8 0.1622 0.0003 10 4 9 0.6705 0.0004 10 5 0 -0.1209 -0.0076 10 5 1 -0.0795 -0.0086 10 5 2 0.1426 0.0061 10 5 3 -0.1285 0.0079 10 5 4 -0.0246 -0.0124 10 5 5 0.4075 -0.0019 10 5 6 -0.2367 0.0083 10 5 7 -0.3344 -0.0031 10 5 8 0.4821 -0.0006 10 5 9 0.1138 0.0036 10 6 0 -0.1401 -0.0039 10 6 1 -0.1765 0.0043 10 6 2 -0.0020 0.0029 10 6 3 0.0152 0.0000 10 6 4 0.1504 0.0012 10 6 5 -0.2187 -0.0053 10 6 6 -0.1953 -0.0109 10 6 7 0.3665 0.0041 10 6 8 0.1686 0.0024 10 6 9 -0.4416 -0.0008 10 7 0 0.0061 0.0017 10 7 1 0.2023 0.0070 10 7 2 0.0136 0.0018 10 7 3 -0.0098 -0.0080 10 7 4 0.1423 0.0034 10 7 5 -0.3140 0.0075 10 7 6 -0.0652 -0.0052 10 7 7 0.5136 -0.0004 10 7 8 -0.0609 0.0029 10 7 9 -0.5165 0.0000 10 8 0 -0.0779 0.0035 10 8 1 0.1764 -0.0018 10 8 2 0.1112 -0.0034 10 8 3 0.0918 -0.0016 10 8 4 -0.2416 -0.0025 10 8 5 -0.0483 -0.0018 10 8 6 0.3352 0.0094 10 8 7 -0.0688 0.0033 10 8 8 -0.2269 -0.0011 10 8 9 0.1580 0.0023 10 9 0 0.1435 0.0005 10 9 1 -0.0570 -0.0030 10 9 2 -0.1827 -0.0037 10 9 3 -0.0026 0.0026 10 9 4 -0.1231 0.0023 10 9 5 0.1182 -0.0063 10 9 6 0.2229 0.0004 10 9 7 -0.2626 0.0022 10 9 8 -0.3908 -0.0016 10 9 9 0.3078 -0.0030 10 10 0 0.2698 -0.0029 10 10 1 -0.0131 -0.0002 10 10 2 -0.0916 0.0018 10 10 3 -0.2285 0.0020 10 10 4 0.0737 0.0019 10 10 5 0.3098 0.0051 10 10 6 -0.1353 -0.0022 10 10 7 -0.1430 -0.0050 10 10 8 0.0508 -0.0012 10 10 9 -0.0774 -0.0046 10 11 0 -0.0863 -0.0010 10 11 1 -0.1804 0.0008 10 11 2 0.1162 0.0012 10 11 3 0.0947 0.0013 10 11 4 0.0904 -0.0025 10 11 5 -0.0229 0.0026 10 11 6 -0.0984 0.0023 10 11 7 -0.0424 -0.0012 10 11 8 0.3433 -0.0008 10 11 9 0.1766 0.0029 10 12 0 -0.2611 0.0024 10 12 1 -0.1459 0.0010 10 12 2 -0.0440 -0.0000 10 12 3 0.1726 -0.0009 10 12 4 0.1899 -0.0010 10 12 5 -0.2486 -0.0036 10 12 6 -0.1715 -0.0029 10 12 7 0.0411 0.0014 10 12 8 0.1035 0.0007 10 13 0 -0.1100 0.0014 10 13 1 0.2040 -0.0008 10 13 2 0.1008 0.0016 10 13 3 -0.0602 -0.0011 10 13 4 -0.1231 0.0006 10 13 5 0.0712 -0.0002 10 13 6 -0.0368 -0.0022 10 13 7 0.0038 -0.0010 10 13 8 -0.0120 0.0014 10 14 0 0.0776 -0.0016 10 14 1 0.1742 -0.0012 10 14 2 0.1207 -0.0002 10 14 3 0.0234 -0.0007 10 14 4 -0.2246 0.0005 10 14 5 -0.0252 0.0011 10 14 6 0.2040 0.0026 10 14 7 0.2282 0.0019 10 14 8 -0.0346 0.0022 10 15 0 0.1815 -0.0017 10 15 1 -0.0040 0.0016 10 15 2 -0.1685 -0.0022 10 15 3 -0.1229 -0.0009 10 15 4 0.1372 0.0002 10 15 5 -0.0927 -0.0006 10 15 6 -0.0705 0.0009 10 15 7 0.2060 0.0020 10 15 8 -0.0839 -0.0001 10 16 0 0.1246 0.0004 10 16 1 -0.0956 0.0014 10 16 2 -0.0786 -0.0004 10 16 3 -0.1048 0.0011 10 16 4 0.0436 0.0000 10 16 5 0.1227 -0.0004 10 16 6 0.0382 -0.0000 10 16 7 -0.3160 -0.0012 10 16 8 -0.1943 -0.0037 10 17 0 -0.0440 0.0019 10 17 1 -0.1430 -0.0022 10 17 2 -0.0102 0.0008 10 17 3 0.2346 0.0022 10 17 4 -0.0214 0.0002 10 17 5 -0.0107 0.0009 10 17 6 0.2664 0.0005 10 17 7 -0.1852 -0.0016 10 17 8 -0.0892 -0.0012 10 18 0 -0.2124 0.0006 10 18 1 -0.0098 -0.0015 10 18 2 0.0232 0.0001 10 18 3 0.0153 -0.0005 10 18 4 0.0306 -0.0005 10 18 5 0.0398 0.0010 10 18 6 -0.1924 -0.0006 10 18 7 0.1196 -0.0012 10 18 8 0.3556 0.0023 10 19 0 -0.1116 -0.0021 10 19 1 0.0635 0.0020 10 19 2 0.2094 0.0010 10 19 3 -0.1046 -0.0019 10 19 4 -0.1571 -0.0005 10 19 5 0.1001 -0.0009 10 19 6 -0.2641 -0.0016 10 19 7 -0.0581 0.0006 10 19 8 0.1667 0.0015 10 20 0 0.1568 -0.0009 10 20 1 0.0882 0.0007 10 20 2 -0.0163 0.0007 10 20 3 0.0415 0.0005 10 20 4 0.1183 0.0009 10 20 5 -0.1416 -0.0012 10 20 6 0.0704 -0.0009 10 20 7 0.1225 0.0018 10 21 0 0.0964 0.0022 10 21 1 0.1108 -0.0009 10 21 2 -0.1945 -0.0021 10 21 3 -0.1538 0.0008 10 21 4 0.1993 0.0004 10 21 5 -0.0351 0.0002 10 21 6 0.0958 0.0021 10 21 7 0.1893 0.0004 10 22 0 -0.0301 0.0005 10 22 1 -0.1015 0.0003 10 22 2 0.0007 -0.0002 10 22 3 0.0478 -0.0010 10 22 4 -0.2345 -0.0015 10 22 5 -0.0234 0.0000 10 22 6 0.1097 0.0020 10 22 7 -0.1842 -0.0003 10 23 0 0.0488 -0.0021 10 23 1 -0.1620 -0.0003 10 23 2 0.0083 0.0018 10 23 3 0.2855 0.0003 10 23 4 -0.0395 -0.0003 10 23 5 -0.0838 0.0007 10 23 6 -0.0165 -0.0018 10 23 7 -0.1064 -0.0012 10 24 0 -0.0606 -0.0001 10 24 1 0.0410 0.0000 10 24 2 0.0503 -0.0014 10 24 3 -0.1424 0.0004 10 24 4 0.1087 0.0019 10 24 5 0.2455 0.0017 10 24 6 -0.0959 -0.0012 10 24 7 0.1075 -0.0009 10 25 0 -0.1493 0.0018 10 25 1 0.0655 0.0008 10 25 2 0.1342 -0.0009 10 25 3 -0.2029 -0.0009 10 25 4 -0.1549 0.0003 10 25 5 0.0658 -0.0012 10 25 6 0.0801 0.0007 10 26 0 0.0725 0.0006 10 26 1 0.0351 -0.0018 10 26 2 -0.0690 0.0018 10 26 3 0.1016 0.0018 10 26 4 0.1168 -0.0007 10 26 5 -0.2438 -0.0028 10 26 6 -0.0486 -0.0006 10 27 0 0.1236 -0.0012 10 27 1 0.0329 -0.0011 10 27 2 -0.1360 0.0001 10 27 3 0.0484 0.0010 10 27 4 0.1993 -0.0000 10 27 5 0.0761 0.0009 10 27 6 -0.0968 0.0006 10 28 0 -0.0544 -0.0022 10 28 1 -0.0555 0.0028 10 28 2 0.0238 0.0008 10 28 3 0.0053 -0.0028 10 28 4 -0.1946 -0.0021 10 28 5 0.0595 0.0019 10 28 6 0.1102 0.0020 10 29 0 -0.0428 -0.0004 10 29 1 -0.0399 0.0014 10 29 2 0.0895 0.0007 10 29 3 0.0288 -0.0005 10 29 4 -0.1106 -0.0006 10 29 5 -0.1568 -0.0004 10 30 0 0.0560 0.0036 10 30 1 0.0309 -0.0008 10 30 2 0.0193 -0.0037 10 30 3 -0.0465 0.0002 10 30 4 0.1142 0.0039 10 30 5 0.0717 0.0009 10 31 0 0.0046 0.0028 10 31 1 0.0108 -0.0007 10 31 2 -0.0945 -0.0015 10 31 3 -0.0410 -0.0007 10 31 4 0.0319 0.0008 10 32 0 -0.0526 -0.0029 10 32 1 -0.0239 -0.0027 10 32 2 -0.0144 0.0029 10 32 3 0.0265 0.0038 10 32 4 -0.0343 -0.0021 10 33 0 -0.0174 -0.0037 10 33 1 -0.0360 -0.0017 10 33 2 0.1192 0.0013 10 33 3 0.0746 0.0022 10 34 0 0.0059 0.0002 10 34 1 0.0369 0.0041 10 34 2 0.0035 0.0011 10 34 3 -0.0225 -0.0045 10 35 0 0.0161 0.0009 10 35 1 0.1102 0.0041 10 36 0 0.0461 0.0024 10 36 1 -0.0187 -0.0019 11 0 0 0.1006 -0.0003 11 0 2 -0.1068 0.0020 11 0 4 0.0950 -0.0062 11 0 6 0.2528 0.0085 11 0 8 -0.6549 -0.0038 11 1 0 -0.1300 0.0125 11 1 1 -0.0399 -0.0110 11 1 2 0.0946 -0.0113 11 1 3 0.0952 0.0119 11 1 4 -0.4117 0.0064 11 1 5 -0.1123 -0.0125 11 1 6 0.4038 0.0023 11 1 7 0.0052 -0.0007 11 1 8 -0.2096 -0.0052 11 2 0 0.0328 0.0010 11 2 1 -0.0849 0.0011 11 2 2 0.0112 -0.0009 11 2 3 0.1039 0.0000 11 2 4 -0.0508 0.0080 11 2 5 0.0625 0.0051 11 2 6 -0.1621 -0.0047 11 2 7 -0.3065 -0.0072 11 2 8 0.3951 0.0011 11 3 0 0.0562 -0.0140 11 3 1 0.0588 -0.0004 11 3 2 0.0012 0.0135 11 3 3 -0.2256 -0.0005 11 3 4 0.2580 -0.0128 11 3 5 0.3488 0.0071 11 3 6 -0.3943 0.0029 11 3 7 -0.1583 -0.0037 11 3 8 0.3489 0.0052 11 4 0 -0.2226 -0.0005 11 4 1 -0.0531 0.0011 11 4 2 0.1011 -0.0010 11 4 3 -0.0449 0.0030 11 4 4 0.0204 -0.0035 11 4 5 -0.1133 -0.0089 11 4 6 -0.0286 -0.0027 11 4 7 0.3058 0.0059 11 4 8 0.0611 0.0003 11 5 0 -0.0099 0.0091 11 5 1 0.0119 0.0077 11 5 2 -0.0766 -0.0064 11 5 3 0.2103 -0.0079 11 5 4 0.0165 0.0096 11 5 5 -0.4907 0.0012 11 5 6 0.1724 -0.0063 11 5 7 0.4350 0.0041 11 5 8 -0.2707 -0.0011 11 6 0 0.1469 0.0013 11 6 1 0.2599 -0.0036 11 6 2 -0.0042 0.0010 11 6 3 -0.0376 -0.0027 11 6 4 -0.1076 -0.0022 11 6 5 0.0746 0.0057 11 6 6 0.1523 0.0080 11 6 7 -0.0693 -0.0011 11 6 8 -0.1900 0.0007 11 7 0 0.0295 -0.0031 11 7 1 -0.0592 -0.0078 11 7 2 0.0427 -0.0018 11 7 3 -0.0729 0.0075 11 7 4 -0.2457 -0.0019 11 7 5 0.3514 -0.0062 11 7 6 0.1861 0.0050 11 7 7 -0.4602 -0.0006 11 7 8 -0.0967 -0.0018 11 8 0 0.1603 -0.0034 11 8 1 -0.2249 0.0035 11 8 2 -0.1835 0.0007 11 8 3 -0.0636 0.0010 11 8 4 0.1804 0.0041 11 8 5 0.0772 0.0009 11 8 6 -0.1163 -0.0067 11 8 7 -0.0787 -0.0028 11 8 8 -0.0448 -0.0024 11 9 0 -0.0260 -0.0008 11 9 1 -0.0044 0.0039 11 9 2 0.0449 0.0043 11 9 3 -0.0484 -0.0016 11 9 4 0.2468 -0.0029 11 9 5 -0.0270 0.0057 11 9 6 -0.2987 -0.0005 11 9 7 0.1389 -0.0019 11 9 8 0.3526 0.0012 11 10 0 -0.3568 0.0047 11 10 1 -0.0508 -0.0007 11 10 2 0.1670 -0.0016 11 10 3 0.2443 -0.0002 11 10 4 -0.0562 -0.0025 11 10 5 -0.2050 -0.0042 11 10 6 -0.0122 0.0013 11 10 7 -0.0139 0.0026 11 10 8 0.2250 0.0024 11 11 0 -0.0682 0.0022 11 11 1 0.0980 -0.0007 11 11 2 -0.0563 -0.0015 11 11 3 0.0525 -0.0024 11 11 4 -0.0788 0.0025 11 11 5 -0.1247 -0.0022 11 11 6 0.0593 -0.0028 11 11 7 0.1150 0.0009 11 11 8 -0.2207 0.0006 11 12 0 0.2467 -0.0033 11 12 1 0.2555 -0.0018 11 12 2 0.0635 0.0008 11 12 3 -0.2207 0.0001 11 12 4 -0.1731 0.0007 11 12 5 0.1619 0.0030 11 12 6 0.0855 0.0023 11 12 7 0.1854 0.0002 11 12 8 -0.0935 0.0001 11 13 0 0.1612 -0.0018 11 13 1 -0.0777 0.0001 11 13 2 -0.0256 -0.0019 11 13 3 -0.0115 0.0016 11 13 4 -0.0127 -0.0001 11 13 5 -0.0192 -0.0005 11 13 6 0.1432 0.0027 11 13 7 0.0102 0.0017 11 13 8 -0.0437 -0.0005 11 14 0 0.0144 0.0005 11 14 1 -0.2000 0.0022 11 14 2 -0.2132 0.0002 11 14 3 -0.0231 0.0004 11 14 4 0.2373 -0.0004 11 14 5 -0.0080 -0.0008 11 14 6 -0.0380 -0.0016 11 14 7 -0.2246 -0.0018 11 14 8 -0.1676 -0.0028 11 15 0 -0.1082 0.0011 11 15 1 -0.0455 -0.0012 11 15 2 0.0631 0.0023 11 15 3 0.0538 0.0012 11 15 4 -0.0445 -0.0007 11 15 5 0.1624 0.0011 11 15 6 0.0041 -0.0005 11 15 7 -0.2601 -0.0027 11 15 8 0.0701 -0.0010 11 16 0 -0.1746 0.0013 11 16 1 0.0246 -0.0013 11 16 2 0.1167 -0.0004 11 16 3 0.1941 -0.0009 11 16 4 -0.0828 0.0004 11 16 5 -0.0608 0.0006 11 16 6 -0.0524 -0.0003 11 16 7 0.1203 0.0006 11 17 0 -0.0681 -0.0012 11 17 1 0.0984 0.0021 11 17 2 0.0389 -0.0006 11 17 3 -0.1358 -0.0023 11 17 4 0.0561 -0.0001 11 17 5 -0.0567 -0.0007 11 17 6 -0.2780 -0.0014 11 17 7 0.2330 0.0015 11 17 8 0.0977 0.0018 11 18 0 0.1732 -0.0012 11 18 1 0.0578 0.0004 11 18 2 0.0585 0.0002 11 18 3 -0.1152 0.0009 11 18 4 -0.0538 0.0003 11 18 5 -0.0108 -0.0015 11 18 6 0.0712 0.0003 11 18 7 0.0005 0.0013 11 19 0 0.1718 0.0020 11 19 1 0.0151 -0.0018 11 19 2 -0.1672 -0.0010 11 19 3 0.0824 0.0014 11 19 4 0.0909 0.0007 11 19 5 -0.1224 0.0003 11 19 6 0.2958 0.0019 11 19 7 0.0252 0.0001 11 20 0 -0.1121 0.0001 11 20 1 -0.0298 0.0001 11 20 2 -0.0952 -0.0002 11 20 3 -0.0503 -0.0007 11 20 4 0.0008 -0.0013 11 20 5 0.0711 0.0012 11 20 6 -0.0053 0.0015 11 20 7 -0.0633 -0.0013 11 21 0 -0.0773 -0.0025 11 21 1 -0.1637 0.0007 11 21 2 0.1359 0.0014 11 21 3 0.1271 -0.0004 11 21 4 -0.2078 -0.0005 11 21 5 0.0880 0.0001 11 21 6 -0.0895 -0.0016 11 21 7 -0.1702 -0.0009 11 22 0 0.0702 0.0007 11 22 1 0.0036 -0.0001 11 22 2 0.0113 -0.0003 11 22 3 0.0758 0.0005 11 22 4 0.1203 0.0017 11 22 5 0.0023 0.0006 11 22 6 -0.0575 -0.0022 11 22 7 0.0860 -0.0002 11 23 0 -0.1067 0.0020 11 23 1 0.1583 0.0002 11 23 2 0.0482 -0.0011 11 23 3 -0.2774 -0.0001 11 23 4 0.0892 0.0004 11 23 5 0.0935 -0.0006 11 23 6 -0.0160 0.0010 11 24 0 -0.0388 -0.0003 11 24 1 -0.0249 -0.0008 11 24 2 0.0408 0.0011 11 24 3 0.0218 0.0001 11 24 4 -0.1111 -0.0010 11 24 5 -0.1293 -0.0023 11 24 6 0.0486 0.0009 11 25 0 0.1813 -0.0012 11 25 1 -0.0066 -0.0007 11 25 2 -0.1839 0.0009 11 25 3 0.2006 0.0007 11 25 4 0.1542 -0.0006 11 25 5 -0.1293 0.0004 11 25 6 -0.0637 -0.0002 11 26 0 -0.0124 -0.0014 11 26 1 0.0468 0.0022 11 26 2 -0.0129 -0.0009 11 26 3 -0.0752 -0.0011 11 26 4 -0.0190 -0.0005 11 26 5 0.1571 0.0024 11 26 6 0.0069 0.0011 11 27 0 -0.1041 0.0003 11 27 1 -0.1079 0.0012 11 27 2 0.1476 -0.0001 11 27 3 -0.0020 -0.0014 11 27 4 -0.2475 -0.0002 11 27 5 -0.0358 0.0002 11 28 0 0.0777 0.0031 11 28 1 -0.0289 -0.0021 11 28 2 -0.0232 -0.0009 11 28 3 0.0294 0.0010 11 28 4 0.1082 0.0021 11 28 5 -0.0692 -0.0008 11 29 0 0.0076 0.0014 11 29 1 0.0822 -0.0013 11 29 2 -0.0398 -0.0015 11 29 3 -0.1057 0.0008 11 29 4 0.1317 0.0016 11 30 0 -0.1149 -0.0033 11 30 1 -0.0179 -0.0001 11 30 2 0.0165 0.0023 11 30 3 0.0290 0.0008 11 30 4 -0.0839 -0.0023 11 31 0 0.0029 -0.0033 11 31 1 -0.0083 -0.0005 11 31 2 0.0080 0.0024 11 31 3 0.0829 0.0016 11 31 4 0.0087 -0.0020 11 32 0 0.0844 0.0014 11 32 1 0.0562 0.0024 11 32 2 0.0149 -0.0010 11 32 3 -0.0338 -0.0027 11 33 0 0.0303 0.0030 11 33 1 0.0104 0.0034 11 33 2 -0.0426 -0.0009 11 34 0 -0.0032 0.0009 11 34 1 -0.0503 -0.0021 11 34 2 -0.0377 -0.0015 11 35 0 -0.0173 0.0007 12 0 0 -0.0639 0.0030 12 0 2 0.0919 -0.0062 12 0 4 -0.1549 0.0081 12 0 6 -0.0819 -0.0062 12 0 8 0.3676 0.0013 12 1 0 0.0621 -0.0081 12 1 1 -0.0062 0.0135 12 1 2 -0.0842 0.0081 12 1 3 -0.0612 -0.0094 12 1 4 0.3587 -0.0050 12 1 5 0.1026 0.0074 12 1 6 -0.4024 -0.0019 12 1 7 -0.0882 0.0024 12 1 8 0.3786 0.0040 12 2 0 -0.0398 -0.0023 12 2 1 0.0560 -0.0034 12 2 2 -0.0146 0.0038 12 2 3 -0.1046 0.0029 12 2 4 0.1232 -0.0094 12 2 5 -0.0050 -0.0047 12 2 6 -0.0067 0.0020 12 2 7 0.1822 0.0057 12 2 8 -0.1627 0.0021 12 3 0 -0.1247 0.0139 12 3 1 -0.0181 -0.0035 12 3 2 0.0741 -0.0124 12 3 3 0.1932 0.0005 12 3 4 -0.2583 0.0091 12 3 5 -0.3207 -0.0044 12 3 6 0.3225 -0.0010 12 3 7 0.2662 0.0016 12 3 8 -0.2562 -0.0050 12 4 0 0.1729 0.0003 12 4 1 0.0702 0.0015 12 4 2 -0.0769 0.0011 12 4 3 0.0857 -0.0069 12 4 4 -0.0672 0.0036 12 4 5 -0.0442 0.0080 12 4 6 0.1179 0.0032 12 4 7 -0.0600 -0.0018 12 4 8 -0.1321 -0.0014 12 5 0 0.1351 -0.0122 12 5 1 0.0820 -0.0061 12 5 2 0.0039 0.0074 12 5 3 -0.2647 0.0067 12 5 4 0.0012 -0.0067 12 5 5 0.4500 -0.0010 12 5 6 -0.0894 0.0039 12 5 7 -0.3679 -0.0028 12 5 8 0.0504 0.0029 12 6 0 -0.0760 -0.0010 12 6 1 -0.2360 0.0021 12 6 2 -0.0024 -0.0034 12 6 3 -0.0235 0.0051 12 6 4 0.0439 0.0034 12 6 5 0.1014 -0.0052 12 6 6 -0.0457 -0.0058 12 6 7 -0.1720 -0.0020 12 6 8 0.0595 -0.0022 12 7 0 -0.0269 0.0052 12 7 1 -0.1010 0.0090 12 7 2 -0.1093 0.0008 12 7 3 0.1508 -0.0066 12 7 4 0.2758 0.0007 12 7 5 -0.3095 0.0048 12 7 6 -0.1766 -0.0034 12 7 7 0.2750 0.0008 12 7 8 0.1231 -0.0009 12 8 0 -0.1867 0.0036 12 8 1 0.1749 -0.0032 12 8 2 0.1574 0.0020 12 8 3 0.0687 -0.0007 12 8 4 -0.0379 -0.0057 12 8 5 -0.0949 -0.0006 12 8 6 -0.1217 0.0041 12 8 7 0.1243 0.0029 12 8 8 0.2663 0.0047 12 9 0 -0.1264 0.0016 12 9 1 0.0395 -0.0055 12 9 2 0.1152 -0.0045 12 9 3 0.0809 0.0012 12 9 4 -0.3044 0.0031 12 9 5 -0.0085 -0.0045 12 9 6 0.2111 -0.0003 12 9 7 -0.0642 0.0007 12 9 8 -0.1498 0.0004 12 10 0 0.3060 -0.0047 12 10 1 0.0869 0.0010 12 10 2 -0.1367 0.0004 12 10 3 -0.1810 -0.0018 12 10 4 -0.0141 0.0033 12 10 5 0.0455 0.0037 12 10 6 0.1374 -0.0004 12 10 7 0.1774 -0.0010 12 10 8 -0.3470 -0.0034 12 11 0 0.1992 -0.0042 12 11 1 0.0362 0.0006 12 11 2 -0.0064 0.0021 12 11 3 -0.1889 0.0029 12 11 4 0.0752 -0.0024 12 11 5 0.1533 0.0012 12 11 6 -0.0042 0.0031 12 11 7 -0.0173 0.0006 12 11 8 0.0614 -0.0002 12 12 0 -0.1558 0.0028 12 12 1 -0.2462 0.0016 12 12 2 -0.0758 -0.0012 12 12 3 0.1657 0.0015 12 12 4 0.1119 -0.0003 12 12 5 -0.0264 -0.0028 12 12 6 0.0196 -0.0017 12 12 7 -0.3402 -0.0013 12 12 8 0.0456 0.0000 12 13 0 -0.1394 0.0025 12 13 1 -0.0618 0.0010 12 13 2 -0.0827 0.0018 12 13 3 0.0924 -0.0020 12 13 4 0.1027 -0.0003 12 13 5 0.0012 0.0014 12 13 6 -0.1233 -0.0023 12 13 7 -0.1103 -0.0027 12 13 8 -0.0057 -0.0010 12 14 0 -0.0629 0.0001 12 14 1 0.1460 -0.0021 12 14 2 0.2122 0.0004 12 14 3 0.0286 -0.0004 12 14 4 -0.1623 -0.0005 12 14 5 0.0430 0.0007 12 14 6 -0.1270 0.0011 12 14 7 0.1894 0.0017 12 15 0 -0.0056 -0.0001 12 15 1 0.0426 0.0005 12 15 2 0.0748 -0.0025 12 15 3 0.0198 -0.0011 12 15 4 -0.0449 0.0014 12 15 5 -0.1655 -0.0014 12 15 6 -0.0270 -0.0005 12 15 7 0.2334 0.0027 12 16 0 0.1302 -0.0017 12 16 1 0.0306 0.0011 12 16 2 -0.0961 0.0003 12 16 3 -0.2022 0.0001 12 16 4 0.0958 -0.0001 12 16 5 -0.0394 -0.0004 12 16 6 0.0645 0.0001 12 16 7 0.0337 -0.0003 12 17 0 0.1339 0.0001 12 17 1 0.0041 -0.0020 12 17 2 -0.0466 0.0005 12 17 3 -0.0025 0.0024 12 17 4 -0.0570 -0.0002 12 17 5 0.0804 0.0001 12 17 6 0.2438 0.0021 12 17 7 -0.1598 -0.0008 12 18 0 -0.0795 0.0014 12 18 1 -0.0509 0.0000 12 18 2 -0.1149 -0.0005 12 18 3 0.1602 -0.0005 12 18 4 0.0248 -0.0001 12 18 5 0.0044 0.0011 12 18 6 0.0425 0.0002 12 18 7 -0.0841 -0.0009 12 19 0 -0.1489 -0.0019 12 19 1 -0.0784 0.0016 12 19 2 0.0598 0.0011 12 19 3 -0.0281 -0.0011 12 19 4 -0.0173 -0.0010 12 19 5 0.1008 0.0005 12 19 6 -0.2415 -0.0017 12 19 7 -0.0156 -0.0008 12 20 0 0.0734 0.0001 12 20 1 -0.0545 -0.0006 12 20 2 0.1598 0.0002 12 20 3 0.0325 0.0005 12 20 4 -0.0700 0.0009 12 20 5 0.0173 -0.0006 12 20 6 -0.0551 -0.0015 12 21 0 0.0348 0.0028 12 21 1 0.1374 -0.0003 12 21 2 -0.0424 -0.0008 12 21 3 -0.0712 -0.0003 12 21 4 0.1503 0.0010 12 21 5 -0.0900 -0.0003 12 21 6 0.0759 0.0006 12 22 0 -0.1376 -0.0013 12 22 1 0.0865 0.0003 12 22 2 -0.0165 0.0004 12 22 3 -0.1494 -0.0002 12 22 4 0.0057 -0.0010 12 22 5 -0.0132 -0.0011 12 22 6 0.0093 0.0017 12 23 0 0.1065 -0.0018 12 23 1 -0.1026 -0.0003 12 23 2 -0.0641 0.0001 12 23 3 0.1997 0.0005 12 23 4 -0.0925 -0.0004 12 23 5 -0.0757 -0.0002 12 23 6 -0.0021 -0.0001 12 24 0 0.1471 0.0009 12 24 1 0.0193 0.0010 12 24 2 -0.1124 -0.0007 12 24 3 0.0926 -0.0001 12 24 4 0.0699 -0.0002 12 24 5 0.0216 0.0021 12 24 6 0.0012 -0.0002 12 25 0 -0.1473 0.0002 12 25 1 -0.0212 0.0004 12 25 2 0.1640 0.0000 12 25 3 -0.1628 -0.0004 12 25 4 -0.1235 -0.0001 12 25 5 0.1226 0.0005 12 26 0 -0.0326 0.0012 12 26 1 -0.1267 -0.0021 12 26 2 0.0915 0.0004 12 26 3 0.0231 -0.0001 12 26 4 -0.0626 0.0014 12 26 5 -0.0504 -0.0013 12 27 0 0.0784 0.0010 12 27 1 0.1150 -0.0005 12 27 2 -0.1364 -0.0003 12 27 3 -0.0183 0.0005 12 27 4 0.2310 0.0009 12 27 5 0.0214 -0.0006 12 28 0 -0.1158 -0.0032 12 28 1 0.1068 0.0016 12 28 2 0.0062 0.0004 12 28 3 -0.0586 0.0008 12 28 4 -0.0022 -0.0014 12 29 0 -0.0086 -0.0020 12 29 1 -0.0964 0.0001 12 29 2 0.0213 0.0012 12 29 3 0.1413 0.0003 12 30 0 0.1644 0.0028 12 30 1 0.0039 0.0001 12 30 2 -0.0454 -0.0004 12 30 3 0.0162 -0.0013 12 31 0 0.0092 0.0025 12 31 1 0.0266 0.0015 12 31 2 0.0467 -0.0014 12 31 3 -0.1124 -0.0022 12 32 0 -0.0897 -0.0005 12 32 1 -0.0780 -0.0010 12 32 2 0.0048 -0.0005 12 33 1 -0.0053 -0.0034 13 0 0 -0.0069 -0.0020 13 0 2 -0.0634 0.0078 13 0 4 0.1768 -0.0096 13 0 6 -0.0885 0.0048 13 1 0 -0.0370 0.0042 13 1 1 0.0249 -0.0150 13 1 2 0.0783 -0.0048 13 1 3 0.0350 0.0070 13 1 4 -0.2610 0.0033 13 1 5 -0.0774 -0.0034 13 1 6 0.2930 0.0009 13 1 7 0.1064 -0.0027 13 2 0 0.0342 0.0023 13 2 1 0.0024 0.0027 13 2 2 0.0391 -0.0053 13 2 3 0.0745 -0.0052 13 2 4 -0.1749 0.0094 13 2 5 -0.0407 0.0055 13 2 6 0.1379 0.0003 13 2 7 -0.0003 -0.0050 13 3 0 0.1595 -0.0133 13 3 1 0.0122 0.0067 13 3 2 -0.1122 0.0105 13 3 3 -0.1467 -0.0010 13 3 4 0.2011 -0.0056 13 3 5 0.2240 0.0020 13 3 6 -0.1856 0.0004 13 3 7 -0.2257 0.0005 13 4 0 -0.0531 -0.0023 13 4 1 -0.0605 -0.0020 13 4 2 -0.0048 -0.0004 13 4 3 -0.1250 0.0094 13 4 4 0.1255 -0.0025 13 4 5 0.1601 -0.0073 13 4 6 -0.1397 -0.0043 13 4 7 -0.1574 -0.0004 13 5 0 -0.1786 0.0139 13 5 1 -0.1486 0.0042 13 5 2 0.0332 -0.0077 13 5 3 0.2502 -0.0046 13 5 4 -0.0123 0.0041 13 5 5 -0.2926 0.0011 13 5 6 0.0368 -0.0020 13 5 7 0.1753 0.0004 13 6 0 -0.0182 0.0034 13 6 1 0.1125 -0.0003 13 6 2 0.0149 0.0044 13 6 3 0.1324 -0.0067 13 6 4 -0.0012 -0.0049 13 6 5 -0.2267 0.0042 13 6 6 -0.0558 0.0048 13 6 7 0.2723 0.0040 13 7 0 -0.0079 -0.0065 13 7 1 0.1867 -0.0091 13 7 2 0.1462 0.0005 13 7 3 -0.1682 0.0050 13 7 4 -0.2156 -0.0002 13 7 5 0.1987 -0.0037 13 7 6 0.0485 0.0012 13 7 7 -0.0716 -0.0001 13 8 0 0.1284 -0.0041 13 8 1 -0.0606 0.0013 13 8 2 -0.0459 -0.0041 13 8 3 -0.1074 0.0004 13 8 4 -0.1059 0.0070 13 8 5 0.1054 0.0009 13 8 6 0.2580 -0.0024 13 8 7 -0.0863 -0.0033 13 9 0 0.2164 -0.0019 13 9 1 -0.0340 0.0062 13 9 2 -0.2027 0.0036 13 9 3 -0.0845 -0.0009 13 9 4 0.2556 -0.0027 13 9 5 -0.0145 0.0033 13 9 6 -0.0202 0.0016 13 9 7 0.0662 0.0006 13 10 0 -0.1474 0.0030 13 10 1 -0.0654 -0.0005 13 10 2 0.0187 0.0012 13 10 3 0.0787 0.0036 13 10 4 0.1057 -0.0038 13 10 5 0.0729 -0.0037 13 10 6 -0.1842 -0.0003 13 10 7 -0.2495 0.0005 13 11 0 -0.2307 0.0051 13 11 1 -0.1363 -0.0009 13 11 2 0.0352 -0.0019 13 11 3 0.2384 -0.0025 13 11 4 -0.0673 0.0021 13 11 5 -0.0629 -0.0003 13 11 6 -0.0420 -0.0032 13 11 7 -0.1590 -0.0024 13 12 0 0.0543 -0.0009 13 12 1 0.1221 -0.0007 13 12 2 0.0738 0.0012 13 12 3 -0.0374 -0.0032 13 12 4 -0.0553 -0.0004 13 12 5 -0.0802 0.0030 13 12 6 -0.0832 0.0015 13 12 7 0.3470 0.0014 13 13 0 0.0717 -0.0029 13 13 1 0.1328 -0.0011 13 13 2 0.1600 -0.0014 13 13 3 -0.1325 0.0018 13 13 4 -0.1085 0.0003 13 13 5 -0.0239 -0.0020 13 13 6 0.0142 0.0016 13 13 7 0.2173 0.0036 13 14 0 0.0299 -0.0005 13 14 1 -0.0506 0.0012 13 14 2 -0.1195 -0.0014 13 14 3 -0.0504 0.0005 13 14 4 0.0556 0.0018 13 14 5 -0.0564 -0.0009 13 14 6 0.1983 -0.0012 13 14 7 -0.1338 -0.0014 13 15 0 0.0789 0.0000 13 15 1 0.0012 -0.0001 13 15 2 -0.1669 0.0019 13 15 3 -0.0604 0.0009 13 15 4 0.0842 -0.0015 13 15 5 0.1072 0.0016 13 15 6 0.1032 0.0013 13 15 7 -0.1582 -0.0026 13 16 0 -0.0224 0.0011 13 16 1 -0.0308 -0.0010 13 16 2 0.0259 0.0001 13 16 3 0.1481 0.0009 13 16 4 -0.0742 -0.0008 13 16 5 0.1073 -0.0001 13 16 6 -0.0572 0.0006 13 16 7 -0.0833 0.0005 13 17 0 -0.1174 0.0001 13 17 1 -0.0960 0.0012 13 17 2 0.0363 -0.0001 13 17 3 0.1070 -0.0018 13 17 4 0.0240 0.0003 13 17 5 -0.0496 0.0002 13 17 6 -0.1798 -0.0025 13 18 0 0.0002 -0.0012 13 18 1 -0.0095 0.0001 13 18 2 0.1271 0.0009 13 18 3 -0.1416 -0.0005 13 18 4 0.0135 -0.0002 13 18 5 -0.0059 0.0001 13 18 6 -0.0952 -0.0006 13 19 0 0.0756 0.0015 13 19 1 0.0962 -0.0006 13 19 2 0.0471 -0.0009 13 19 3 -0.0386 0.0003 13 19 4 -0.0189 0.0011 13 19 5 -0.0538 -0.0010 13 19 6 0.1381 0.0014 13 20 0 -0.0734 0.0003 13 20 1 0.1191 0.0010 13 20 2 -0.1585 -0.0007 13 20 3 -0.0073 -0.0004 13 20 4 0.0902 0.0002 13 20 5 -0.0752 -0.0004 13 20 6 0.0726 0.0009 13 21 0 -0.0109 -0.0021 13 21 1 -0.0659 -0.0003 13 21 2 -0.0480 -0.0003 13 21 3 0.0327 0.0011 13 21 4 -0.0631 -0.0010 13 21 5 0.0428 0.0001 13 21 6 -0.0572 0.0001 13 22 0 0.1964 0.0013 13 22 1 -0.1259 -0.0009 13 22 2 0.0183 -0.0003 13 22 3 0.1638 0.0006 13 22 4 -0.0963 -0.0003 13 22 5 0.0250 0.0011 13 23 0 -0.0495 0.0011 13 23 1 0.0354 0.0001 13 23 2 0.0650 0.0015 13 23 3 -0.0987 -0.0008 13 23 4 0.0419 -0.0002 13 23 5 0.0513 0.0009 13 24 0 -0.2073 -0.0018 13 24 1 -0.0186 -0.0007 13 24 2 0.1371 0.0009 13 24 3 -0.1676 -0.0007 13 24 4 -0.0162 0.0011 13 24 5 0.0491 -0.0011 13 25 0 0.0815 0.0005 13 25 1 0.0197 0.0006 13 25 2 -0.1141 -0.0013 13 25 3 0.0876 -0.0005 13 25 4 0.0937 0.0013 13 26 0 0.0504 -0.0000 13 26 1 0.1625 0.0021 13 26 2 -0.1436 -0.0007 13 26 3 0.0362 0.0012 13 26 4 0.1070 -0.0013 13 27 0 -0.0706 -0.0015 13 27 1 -0.0827 -0.0010 13 27 2 0.1046 0.0004 13 27 3 0.0388 0.0014 13 27 4 -0.1657 -0.0015 13 28 0 0.1337 0.0024 13 28 1 -0.1517 -0.0019 13 28 2 0.0289 0.0005 13 28 3 0.0706 -0.0016 13 29 0 0.0400 0.0017 13 29 1 0.0960 0.0011 13 29 2 -0.0105 0.0002 13 29 3 -0.1404 -0.0019 13 30 0 -0.1773 -0.0026 13 30 1 0.0216 0.0008 13 30 2 0.0542 -0.0008 13 31 0 -0.0210 -0.0011 14 0 0 0.0467 -0.0008 14 0 2 0.0375 -0.0080 14 0 4 -0.1451 0.0104 14 0 6 0.1776 -0.0038 14 1 0 0.0444 -0.0024 14 1 1 -0.0111 0.0146 14 1 2 -0.0794 0.0024 14 1 3 -0.0313 -0.0051 14 1 4 0.1582 -0.0015 14 1 5 0.0471 0.0012 14 1 6 -0.1201 0.0001 14 1 7 -0.0578 0.0021 14 2 0 -0.0046 -0.0015 14 2 1 -0.0457 -0.0009 14 2 2 -0.0687 0.0056 14 2 3 -0.0265 0.0071 14 2 4 0.1755 -0.0081 14 2 5 0.0504 -0.0066 14 2 6 -0.1810 -0.0019 14 2 7 -0.1304 0.0045 14 3 0 -0.1335 0.0117 14 3 1 -0.0338 -0.0074 14 3 2 0.0930 -0.0082 14 3 3 0.1117 0.0017 14 3 4 -0.1034 0.0029 14 3 5 -0.1029 -0.0007 14 3 6 0.0415 -0.0008 14 3 7 0.0717 -0.0019 14 4 0 -0.0652 0.0047 14 4 1 0.0192 0.0012 14 4 2 0.0936 0.0001 14 4 3 0.1336 -0.0106 14 4 4 -0.1630 0.0006 14 4 5 -0.1808 0.0068 14 4 6 0.1085 0.0052 14 4 7 0.2490 0.0012 14 5 0 0.1302 -0.0124 14 5 1 0.1459 -0.0027 14 5 2 -0.0151 0.0069 14 5 3 -0.1714 0.0023 14 5 4 -0.0044 -0.0025 14 5 5 0.0903 -0.0012 14 5 6 -0.0247 0.0011 14 5 7 0.0403 0.0019 14 6 0 0.0734 -0.0066 14 6 1 0.0419 -0.0009 14 6 2 -0.0266 -0.0047 14 6 3 -0.2202 0.0069 14 6 4 0.0025 0.0062 14 6 5 0.2480 -0.0030 14 6 6 0.0932 -0.0044 14 6 7 -0.2350 -0.0045 14 7 0 0.0316 0.0058 14 7 1 -0.1575 0.0073 14 7 2 -0.1343 -0.0016 14 7 3 0.1041 -0.0031 14 7 4 0.1087 0.0003 14 7 5 -0.0559 0.0030 14 7 6 0.1137 0.0004 14 7 7 -0.0638 -0.0010 14 8 0 -0.0183 0.0051 14 8 1 -0.0535 0.0005 14 8 2 -0.0815 0.0051 14 8 3 0.1553 0.0004 14 8 4 0.1724 -0.0075 14 8 5 -0.1085 -0.0015 14 8 6 -0.2428 0.0016 14 8 7 0.0281 0.0036 14 9 0 -0.1825 0.0012 14 9 1 0.0051 -0.0051 14 9 2 0.1717 -0.0017 14 9 3 0.0753 0.0009 14 9 4 -0.1224 0.0017 14 9 5 0.0526 -0.0025 14 9 6 -0.1688 -0.0027 14 9 7 -0.1089 -0.0011 14 10 0 -0.0247 -0.0014 14 10 1 0.0067 -0.0003 14 10 2 0.1178 -0.0019 14 10 3 0.0004 -0.0049 14 10 4 -0.1683 0.0036 14 10 5 -0.0924 0.0037 14 10 6 0.1473 0.0005 14 10 7 0.2010 -0.0009 14 11 0 0.1576 -0.0037 14 11 1 0.1388 0.0015 14 11 2 -0.0137 0.0010 14 11 3 -0.1866 0.0012 14 11 4 0.0348 -0.0018 14 11 5 -0.0729 0.0000 14 11 6 0.0725 0.0033 14 11 7 0.2905 0.0033 14 12 0 0.0062 -0.0010 14 12 1 0.0375 0.0005 14 12 2 -0.0689 -0.0014 14 12 3 -0.0881 0.0040 14 12 4 0.0384 0.0011 14 12 5 0.1046 -0.0032 14 12 6 0.0794 -0.0014 14 13 0 -0.0191 0.0027 14 13 1 -0.1019 -0.0002 14 13 2 -0.1691 0.0007 14 13 3 0.1055 -0.0009 14 13 4 0.0575 0.0003 14 13 5 0.0729 0.0021 14 13 6 0.0941 -0.0013 14 14 0 0.0489 0.0013 14 14 1 -0.0388 -0.0009 14 14 2 0.0023 0.0018 14 14 3 0.0870 -0.0003 14 14 4 0.0141 -0.0028 14 14 5 0.0445 0.0011 14 14 6 -0.1548 0.0016 14 15 0 -0.0612 -0.0013 14 15 1 -0.0494 0.0004 14 15 2 0.1703 -0.0004 14 15 3 0.0665 -0.0005 14 15 4 -0.0662 0.0006 14 15 5 -0.0378 -0.0018 14 15 6 -0.1673 -0.0014 14 16 0 -0.0785 -0.0011 14 16 1 -0.0029 0.0007 14 16 2 0.0573 0.0001 14 16 3 -0.0881 -0.0019 14 16 4 0.0336 0.0014 14 16 5 -0.1046 0.0007 14 16 6 0.0294 -0.0014 14 17 0 0.0411 0.0008 14 17 1 0.1240 0.0002 14 17 2 -0.0155 -0.0007 14 17 3 -0.1433 0.0004 14 17 4 0.0141 -0.0001 14 17 5 -0.0005 0.0001 14 17 6 0.1161 0.0023 14 18 0 0.0319 0.0011 14 18 1 0.0770 0.0005 14 18 2 -0.1159 -0.0016 14 18 3 0.0885 0.0012 14 18 4 -0.0218 0.0005 14 18 5 -0.0005 -0.0014 14 19 0 -0.0121 -0.0006 14 19 1 -0.0710 -0.0011 14 19 2 -0.1063 0.0001 14 19 3 0.0917 0.0011 14 19 4 0.0193 -0.0007 14 19 5 0.0069 0.0006 14 20 0 0.0903 -0.0003 14 20 1 -0.1436 -0.0019 14 20 2 0.1213 0.0010 14 20 3 -0.0001 0.0006 14 20 4 -0.0859 -0.0014 14 20 5 0.0836 0.0014 14 21 0 0.0226 0.0002 14 21 1 0.0009 0.0007 14 21 2 0.1092 0.0020 14 21 3 -0.0258 -0.0018 14 21 4 -0.0183 0.0002 14 21 5 0.0147 0.0002 14 22 0 -0.2081 -0.0018 14 22 1 0.1247 0.0016 14 22 2 -0.0162 0.0008 14 22 3 -0.1464 -0.0015 14 22 4 0.1278 0.0015 14 23 0 -0.0214 0.0001 14 23 1 0.0117 0.0010 14 23 2 -0.0727 -0.0033 14 23 3 0.0109 0.0005 14 23 4 0.0325 0.0014 14 24 0 0.2063 0.0030 14 24 1 0.0070 0.0006 14 24 2 -0.1293 -0.0018 14 24 3 0.1902 0.0015 14 24 4 -0.0176 -0.0014 14 25 0 -0.0277 -0.0004 14 25 1 -0.0121 -0.0023 14 25 2 0.0677 0.0022 14 25 3 0.0052 0.0019 14 26 0 -0.0600 -0.0013 14 26 1 -0.1494 -0.0028 14 26 2 0.1669 0.0016 14 26 3 -0.0724 -0.0014 14 27 0 0.0772 0.0007 14 27 1 0.0487 0.0023 14 27 2 -0.0561 0.0003 14 28 0 -0.1090 -0.0017 14 28 1 0.1673 0.0030 14 28 2 -0.0645 -0.0010 14 29 0 -0.0707 -0.0007 14 29 1 -0.0843 -0.0015 15 0 0 -0.0293 0.0027 15 0 2 -0.0303 0.0078 15 0 4 0.0835 -0.0102 15 0 6 -0.1633 0.0027 15 1 0 -0.0431 0.0031 15 1 1 -0.0181 -0.0129 15 1 2 0.0873 -0.0011 15 1 3 0.0521 0.0043 15 1 4 -0.0923 -0.0000 15 1 5 -0.0264 -0.0008 15 1 6 -0.0378 -0.0008 15 2 0 -0.0360 0.0005 15 2 1 0.0467 0.0001 15 2 2 0.0872 -0.0051 15 2 3 -0.0096 -0.0085 15 2 4 -0.1275 0.0062 15 2 5 -0.0307 0.0071 15 2 6 0.1381 0.0027 15 3 0 0.0567 -0.0097 15 3 1 0.0555 0.0061 15 3 2 -0.0324 0.0063 15 3 3 -0.1091 -0.0027 15 3 4 0.0041 -0.0014 15 3 5 0.0137 0.0005 15 3 6 0.0605 0.0017 15 4 0 0.1213 -0.0053 15 4 1 0.0339 -0.0007 15 4 2 -0.1382 -0.0007 15 4 3 -0.1084 0.0106 15 4 4 0.1516 0.0014 15 4 5 0.1162 -0.0058 15 4 6 -0.0542 -0.0051 15 5 0 -0.0420 0.0085 15 5 1 -0.0753 0.0020 15 5 2 -0.0458 -0.0059 15 5 3 0.0736 -0.0003 15 5 4 0.0541 0.0021 15 5 5 0.0689 0.0012 15 5 6 0.0308 -0.0011 15 6 0 -0.0703 0.0079 15 6 1 -0.1470 0.0007 15 6 2 0.0295 0.0052 15 6 3 0.2331 -0.0058 15 6 4 -0.0293 -0.0069 15 6 5 -0.1681 0.0018 15 6 6 -0.0622 0.0038 15 7 0 -0.0082 -0.0032 15 7 1 0.0436 -0.0049 15 7 2 0.0900 0.0022 15 7 3 0.0130 0.0018 15 7 4 -0.0236 -0.0010 15 7 5 -0.0713 -0.0028 15 7 6 -0.2163 -0.0012 15 8 0 -0.0715 -0.0063 15 8 1 0.1172 -0.0005 15 8 2 0.1538 -0.0049 15 8 3 -0.1737 -0.0016 15 8 4 -0.1390 0.0070 15 8 5 0.0915 0.0018 15 8 6 0.1181 -0.0013 15 9 0 0.0444 -0.0003 15 9 1 0.0237 0.0032 15 9 2 -0.0530 0.0002 15 9 3 -0.0796 -0.0013 15 9 4 -0.0261 -0.0008 15 9 5 -0.0575 0.0023 15 9 6 0.2719 0.0033 15 10 0 0.1223 0.0020 15 10 1 0.0393 0.0008 15 10 2 -0.1996 0.0010 15 10 3 -0.0235 0.0053 15 10 4 0.1624 -0.0028 15 10 5 0.0310 -0.0034 15 10 6 -0.0595 -0.0004 15 11 0 -0.0351 0.0011 15 11 1 -0.0524 -0.0015 15 11 2 -0.0489 -0.0002 15 11 3 0.0846 0.0003 15 11 4 0.0277 0.0017 15 11 5 0.1646 -0.0002 15 11 6 -0.0926 -0.0032 15 12 0 -0.0233 0.0015 15 12 1 -0.1408 -0.0017 15 12 2 0.0732 0.0020 15 12 3 0.1445 -0.0034 15 12 4 -0.0517 -0.0015 15 12 5 -0.0479 0.0029 15 12 6 -0.0347 0.0011 15 13 0 0.0153 -0.0016 15 13 1 -0.0011 0.0014 15 13 2 0.1281 0.0001 15 13 3 -0.0255 0.0000 15 13 4 -0.0107 -0.0013 15 13 5 -0.1204 -0.0017 15 13 6 -0.1307 0.0012 15 14 0 -0.0995 -0.0030 15 14 1 0.0947 0.0020 15 14 2 0.0665 -0.0013 15 14 3 -0.1182 -0.0006 15 14 4 -0.0196 0.0028 15 14 5 -0.0282 -0.0011 15 15 0 -0.0263 0.0024 15 15 1 0.0805 -0.0007 15 15 2 -0.1027 -0.0009 15 15 3 -0.0661 -0.0002 15 15 4 0.0202 0.0005 15 15 5 0.0058 0.0018 15 16 0 0.1190 0.0029 15 16 1 0.0198 -0.0003 15 16 2 -0.1147 -0.0016 15 16 3 0.0610 0.0023 15 16 4 -0.0015 -0.0013 15 16 5 0.0518 -0.0008 15 17 0 0.0433 -0.0019 15 17 1 -0.0933 -0.0013 15 17 2 -0.0134 0.0011 15 17 3 0.1289 0.0012 15 17 4 -0.0270 -0.0003 15 17 5 0.0277 -0.0008 15 18 0 -0.0354 -0.0016 15 18 1 -0.1046 -0.0025 15 18 2 0.1107 0.0026 15 18 3 -0.0383 -0.0007 15 18 4 -0.0006 -0.0008 15 18 5 0.0163 0.0020 15 19 0 -0.0143 -0.0003 15 19 1 0.0293 0.0023 15 19 2 0.1193 0.0009 15 19 3 -0.1124 -0.0023 15 19 4 -0.0129 -0.0000 15 20 0 -0.0805 -0.0010 15 20 1 0.1394 0.0038 15 20 2 -0.0875 -0.0005 15 20 3 -0.0171 -0.0015 15 20 4 0.0743 0.0019 15 21 0 -0.0464 0.0017 15 21 1 0.0335 -0.0006 15 21 2 -0.1371 -0.0036 15 21 3 0.0312 0.0020 15 21 4 0.0715 0.0012 15 22 0 0.1667 0.0036 15 22 1 -0.1175 -0.0019 15 22 2 0.0069 -0.0023 15 22 3 0.1227 0.0022 15 23 0 0.0618 -0.0009 15 23 1 -0.0388 -0.0023 15 23 2 0.0860 0.0043 15 23 3 0.0479 0.0004 15 24 0 -0.1739 -0.0041 15 24 1 0.0186 -0.0017 15 24 2 0.1151 0.0032 15 25 0 0.0001 -0.0006 15 25 1 0.0188 0.0037 15 25 2 -0.0330 -0.0021 15 26 0 0.0814 0.0016 15 26 1 0.1127 0.0042 16 0 0 -0.0185 -0.0022 16 0 2 0.0514 -0.0076 16 0 4 -0.0370 0.0087 16 1 0 0.0047 -0.0048 16 1 1 0.0394 0.0113 16 1 2 -0.0967 0.0002 16 1 3 -0.0823 -0.0047 16 1 4 0.0738 0.0011 16 1 5 0.0187 0.0014 16 1 6 0.1247 0.0013 16 2 0 0.0607 -0.0003 16 2 1 -0.0099 -0.0005 16 2 2 -0.0902 0.0046 16 2 3 0.0053 0.0087 16 2 4 0.0618 -0.0040 16 2 5 0.0102 -0.0063 16 2 6 -0.0544 -0.0028 16 3 0 0.0320 0.0085 16 3 1 -0.0558 -0.0045 16 3 2 -0.0315 -0.0055 16 3 3 0.1336 0.0040 16 3 4 0.0589 0.0012 16 3 5 0.0199 -0.0009 16 3 6 -0.1006 -0.0025 16 4 0 -0.1042 0.0038 16 4 1 -0.0727 0.0011 16 4 2 0.1164 0.0015 16 4 3 0.0751 -0.0095 16 4 4 -0.0852 -0.0025 16 4 5 -0.0245 0.0043 16 5 0 -0.0228 -0.0048 16 5 1 -0.0213 -0.0023 16 5 2 0.1136 0.0057 16 5 3 -0.0068 -0.0009 16 5 4 -0.1123 -0.0027 16 5 5 -0.1354 -0.0013 16 6 0 0.0378 -0.0064 16 6 1 0.1634 0.0003 16 6 2 -0.0145 -0.0055 16 6 3 -0.1656 0.0041 16 6 4 0.0393 0.0063 16 6 5 0.0367 -0.0010 16 7 0 -0.0563 -0.0001 16 7 1 0.0837 0.0038 16 7 2 -0.0474 -0.0026 16 7 3 -0.1224 -0.0018 16 7 4 -0.0014 0.0018 16 7 5 0.1427 0.0029 16 8 0 0.0868 0.0069 16 8 1 -0.1188 -0.0012 16 8 2 -0.1472 0.0040 16 8 3 0.1335 0.0024 16 8 4 0.0459 -0.0055 16 8 5 -0.0414 -0.0014 16 9 0 0.1159 0.0011 16 9 1 -0.0432 -0.0017 16 9 2 -0.0757 0.0000 16 9 3 0.1054 0.0022 16 9 4 0.1198 0.0005 16 9 5 0.0207 -0.0022 16 10 0 -0.1204 -0.0045 16 10 1 -0.0396 -0.0006 16 10 2 0.1932 0.0007 16 10 3 0.0076 -0.0047 16 10 4 -0.0837 0.0018 16 10 5 0.0432 0.0024 16 11 0 -0.0727 0.0003 16 11 1 -0.0553 0.0004 16 11 2 0.1240 0.0006 16 11 3 -0.0022 -0.0011 16 11 4 -0.0963 -0.0019 16 11 5 -0.1685 0.0003 16 12 0 0.0279 -0.0002 16 12 1 0.1472 0.0037 16 12 2 -0.0808 -0.0027 16 12 3 -0.1167 0.0020 16 12 4 0.0546 0.0013 16 12 5 -0.0444 -0.0021 16 13 0 -0.0389 -0.0001 16 13 1 0.1137 -0.0008 16 13 2 -0.0852 -0.0006 16 13 3 -0.0630 -0.0001 16 13 4 0.0063 0.0019 16 14 0 0.0774 0.0049 16 14 1 -0.1142 -0.0040 16 14 2 -0.0629 -0.0000 16 14 3 0.1169 0.0015 16 14 4 -0.0153 -0.0019 16 15 0 0.1145 -0.0016 16 15 1 -0.1019 0.0004 16 15 2 0.0189 0.0008 16 15 3 0.0814 0.0012 16 15 4 0.0153 -0.0012 16 16 0 -0.0979 -0.0061 16 16 1 0.0067 -0.0001 16 16 2 0.1266 0.0036 16 16 3 -0.0615 -0.0018 16 16 4 -0.0018 0.0006 16 17 0 -0.0996 0.0015 16 17 1 0.0529 0.0012 16 17 2 0.0504 -0.0002 16 17 3 -0.1011 -0.0021 16 17 4 0.0101 0.0005 16 18 0 0.0455 0.0025 16 18 1 0.0824 0.0050 16 18 2 -0.1169 -0.0033 16 18 3 0.0114 -0.0005 16 19 0 0.0248 0.0007 16 19 1 0.0035 -0.0017 16 19 2 -0.1168 -0.0017 16 19 3 0.0985 0.0026 16 20 0 0.0293 0.0031 16 20 1 -0.1274 -0.0058 16 20 2 0.0719 -0.0006 16 21 0 0.0450 -0.0020 16 21 1 -0.0493 -0.0002 16 21 2 0.1394 0.0038 16 22 0 -0.1025 -0.0061 16 23 0 -0.0611 0.0006 16 23 1 0.0618 0.0029 17 0 0 0.0495 0.0001 17 0 2 -0.0968 0.0068 17 0 4 0.0321 -0.0061 17 1 0 0.0608 0.0057 17 1 1 -0.0399 -0.0104 17 1 2 0.0964 0.0006 17 1 3 0.0972 0.0055 17 1 4 -0.0764 -0.0015 17 1 5 -0.0137 -0.0021 17 2 0 -0.0532 0.0014 17 2 1 -0.0401 0.0011 17 2 2 0.0851 -0.0045 17 2 3 0.0430 -0.0070 17 2 4 -0.0116 0.0023 17 2 5 -0.0095 0.0042 17 3 0 -0.0923 -0.0085 17 3 1 0.0322 0.0039 17 3 2 0.0648 0.0053 17 3 3 -0.1527 -0.0051 17 3 4 -0.0692 -0.0017 17 3 5 -0.0195 0.0009 17 4 0 0.0488 -0.0019 17 4 1 0.0856 -0.0022 17 4 2 -0.0451 -0.0013 17 4 3 -0.0622 0.0074 17 4 4 -0.0125 0.0021 17 5 0 0.0370 0.0035 17 5 1 0.0932 0.0030 17 5 2 -0.1484 -0.0063 17 5 3 -0.0090 0.0012 17 5 4 0.1365 0.0034 17 6 0 -0.0166 0.0033 17 6 1 -0.1099 -0.0004 17 6 2 -0.0228 0.0051 17 6 3 0.0573 -0.0030 17 6 4 -0.0068 -0.0044 17 7 0 0.1192 0.0027 17 7 1 -0.1622 -0.0047 17 7 2 0.0276 0.0028 17 7 3 0.1670 0.0025 17 7 4 -0.0186 -0.0020 17 8 0 -0.0309 -0.0060 17 8 1 0.0780 0.0026 17 8 2 0.0916 -0.0031 17 8 3 -0.0386 -0.0020 17 8 4 0.0423 0.0037 17 9 0 -0.2169 -0.0039 17 9 1 0.0570 0.0016 17 9 2 0.1455 0.0010 17 9 3 -0.1297 -0.0031 17 9 4 -0.1268 -0.0006 17 10 0 0.0578 0.0066 17 10 1 0.0039 -0.0002 17 10 2 -0.1166 -0.0015 17 10 3 0.0056 0.0033 17 10 4 -0.0329 -0.0013 17 11 0 0.1353 0.0008 17 11 1 0.1155 0.0015 17 11 2 -0.1757 -0.0021 17 11 3 -0.0239 0.0011 17 12 0 -0.0432 -0.0019 17 12 1 -0.0832 -0.0046 17 12 2 0.0729 0.0027 17 12 3 0.0394 -0.0008 17 13 0 0.0421 0.0017 17 13 1 -0.1850 -0.0020 17 13 2 0.0719 0.0008 17 13 3 0.1126 0.0011 17 14 0 -0.0030 -0.0055 17 14 1 0.1057 0.0053 17 14 2 0.0171 0.0009 17 14 3 -0.0710 -0.0017 17 15 0 -0.1469 -0.0017 17 15 1 0.1300 0.0006 17 15 2 0.0339 0.0008 17 15 3 -0.1047 -0.0019 17 16 0 0.0529 0.0081 17 16 1 -0.0561 0.0002 17 16 2 -0.0967 -0.0045 17 16 3 0.0593 0.0010 17 17 0 0.1272 0.0007 17 17 1 -0.0441 0.0005 17 17 2 -0.0881 -0.0016 17 18 0 -0.0725 -0.0031 17 18 1 -0.0363 -0.0064 17 18 2 0.1159 0.0033 17 19 0 -0.0540 -0.0003 17 19 1 -0.0197 -0.0009 18 0 0 -0.0407 0.0018 18 0 2 0.1464 -0.0050 18 1 0 -0.1176 -0.0048 18 1 1 0.0211 0.0093 18 1 2 -0.0755 -0.0016 18 1 3 -0.0796 -0.0053 18 2 0 0.0208 -0.0036 18 2 1 0.0783 -0.0003 18 2 2 -0.0804 0.0048 18 2 3 -0.1060 0.0039 18 3 0 0.1076 0.0085 18 3 1 0.0039 -0.0042 18 3 2 -0.0572 -0.0046 18 3 3 0.1325 0.0052 18 4 0 -0.0001 0.0018 18 4 1 -0.0801 0.0031 18 4 2 -0.0344 -0.0006 18 4 3 0.0736 -0.0049 18 5 0 -0.0169 -0.0041 18 5 1 -0.1155 -0.0030 18 5 2 0.1278 0.0065 18 5 3 -0.0109 -0.0012 18 6 0 0.0217 -0.0006 18 6 1 0.0380 -0.0011 18 6 2 0.0720 -0.0033 18 6 3 0.0366 0.0029 18 7 0 -0.1405 -0.0035 18 7 1 0.1701 0.0058 18 7 2 -0.0242 -0.0029 18 7 3 -0.1264 -0.0027 18 8 0 -0.0453 0.0032 18 8 1 -0.0250 -0.0021 18 8 3 -0.0701 0.0004 18 9 0 0.2298 0.0069 18 9 1 -0.0670 -0.0023 18 10 0 0.0071 -0.0060 18 10 1 0.0305 0.0011 18 11 0 -0.1595 -0.0036 18 11 1 -0.1074 -0.0032 18 11 2 0.1771 0.0034 18 12 0 0.0618 0.0032 18 12 1 0.0079 0.0031 18 12 2 -0.0391 -0.0017 18 13 0 -0.0012 -0.0026 18 13 1 0.1988 0.0050 18 13 2 -0.0807 -0.0005 18 14 0 -0.0642 0.0037 18 14 1 -0.0772 -0.0045 18 15 0 0.1189 0.0057 19 1 0 0.1373 0.0024 19 1 1 0.0059 -0.0067 19 2 0 0.0128 0.0058 19 2 1 -0.0915 -0.0017 19 3 0 -0.0883 -0.0068 19 3 1 -0.0389 0.0043 19 4 0 -0.0190 -0.0035 19 4 1 0.0695 -0.0032 19 5 0 -0.0059 0.0046 19 5 1 0.0976 0.0016 19 6 0 -0.0377 -0.0003 19 6 1 0.0079 0.0034 19 7 0 0.1151 0.0026 0 0 0 0.0 0.0 ; _shelx_fab_checksum 56147 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 3.055 _oxdiff_exptl_absorpt_empirical_full_min 0.427 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O001 O 0.89881(10) 0.48769(5) 0.06427(17) 0.0345(3) Uani 1 1 d D . . . . O002 O 0.51202(10) 0.49050(5) 0.81374(18) 0.0363(3) Uani 1 1 d D . . . . O003 O 0.98335(10) 0.54219(5) 0.09639(17) 0.0359(3) Uani 1 1 d . . . . . O004 O 0.60063(10) 0.47832(5) 1.01271(17) 0.0371(4) Uani 1 1 d . . . . . O005 O 1.27863(10) 0.32621(5) 0.32828(17) 0.0386(4) Uani 1 1 d . . . . . O006 O 1.14817(12) 0.31195(5) -0.24378(17) 0.0422(4) Uani 1 1 d . . . . . O007 O 0.12757(11) 0.65288(6) 1.03068(18) 0.0443(4) Uani 1 1 d . . . . . O008 O 0.44745(12) 0.71724(5) 0.8932(2) 0.0500(5) Uani 1 1 d . . . . . C009 C 1.10078(12) 0.39106(6) 0.2782(2) 0.0247(4) Uani 1 1 d . . . . . C00A C 0.38465(12) 0.64353(6) 0.6231(2) 0.0251(4) Uani 1 1 d . . . . . C00B C 0.44278(12) 0.62334(6) 0.5295(2) 0.0249(4) Uani 1 1 d . . . . . C00C C 1.05130(13) 0.32385(6) 0.3315(2) 0.0266(4) Uani 1 1 d . . . . . C00D C 0.53385(12) 0.60128(6) 0.7423(2) 0.0257(4) Uani 1 1 d . . . . . C00E C 0.40344(13) 0.64323(6) 0.7752(2) 0.0269(4) Uani 1 1 d . . . . . C00F C 0.47752(13) 0.62275(6) 0.8356(2) 0.0266(4) Uani 1 1 d . . . . . C00G C 0.72214(12) 0.57292(6) 0.3847(2) 0.0253(4) Uani 1 1 d . . . . . C00H C 0.84612(13) 0.54050(6) 0.2049(2) 0.0266(4) Uani 1 1 d . . . . . C00I C 0.91401(13) 0.52253(6) 0.1164(2) 0.0284(4) Uani 1 1 d . . . . . C00J C 1.15828(13) 0.41777(6) 0.2082(2) 0.0274(4) Uani 1 1 d . . . . . H00J H 1.199186 0.407356 0.143718 0.033 Uiso 1 1 calc R U . . . C00K C 0.51642(12) 0.60227(6) 0.5894(2) 0.0255(4) Uani 1 1 d . . . . . C00L C 0.76743(13) 0.52035(6) 0.2251(2) 0.0274(4) Uani 1 1 d . . . . . H00L H 0.756156 0.495426 0.178556 0.033 Uiso 1 1 calc R U . . . C00M C 0.70600(13) 0.53677(6) 0.3129(2) 0.0269(4) Uani 1 1 d . . . . . H00M H 0.652045 0.523248 0.324375 0.032 Uiso 1 1 calc R U . . . C00N C 0.42485(13) 0.62638(6) 0.3748(2) 0.0273(4) Uani 1 1 d . . . . . H00N H 0.463637 0.614001 0.311159 0.033 Uiso 1 1 calc R U . . . C00O C 1.03857(13) 0.40732(6) 0.3746(2) 0.0269(4) Uani 1 1 d . . . . . C00P C 1.16506(13) 0.33339(6) 0.1455(2) 0.0278(4) Uani 1 1 d . . . . . C00Q C 1.10524(12) 0.34971(6) 0.2552(2) 0.0251(4) Uani 1 1 d . . . . . C00R C 0.31034(13) 0.66421(6) 0.5570(2) 0.0282(4) Uani 1 1 d . . . . . H00R H 0.270569 0.677176 0.617523 0.034 Uiso 1 1 calc R U . . . C00S C 0.98435(13) 0.38137(6) 0.4506(2) 0.0276(4) Uani 1 1 d . . . . . C00T C 0.60619(13) 0.57963(6) 0.8099(2) 0.0283(4) Uani 1 1 d . . . . . H00T H 0.642665 0.564344 0.750587 0.034 Uiso 1 1 calc R U . . . C00U C 0.65319(13) 0.46363(6) 0.7808(2) 0.0284(4) Uani 1 1 d . . . . . C00V C 0.58444(13) 0.47833(6) 0.8761(2) 0.0294(4) Uani 1 1 d . . . . . C00W C 0.78369(13) 0.43492(6) 0.6046(2) 0.0286(4) Uani 1 1 d . . . . . C00X C 0.57533(13) 0.58230(6) 0.4888(2) 0.0269(4) Uani 1 1 d . . . . . H00X H 0.551009 0.562457 0.424570 0.032 Uiso 1 1 calc R U . . . C00Y C 0.99286(13) 0.33972(6) 0.4340(2) 0.0275(4) Uani 1 1 d . . . . . C00Z C 0.64341(14) 0.46774(6) 0.6297(2) 0.0310(4) Uani 1 1 d . . . . . H00Z H 0.592597 0.480341 0.586006 0.037 Uiso 1 1 calc R U . . . C010 C 0.66094(13) 0.59077(6) 0.4839(2) 0.0271(4) Uani 1 1 d . . . . . H010 H 0.684296 0.610171 0.550966 0.033 Uiso 1 1 calc R U . . . C011 C 0.34420(13) 0.66508(6) 0.8725(2) 0.0282(4) Uani 1 1 d . . . . . C012 C 0.49920(14) 0.62273(7) 0.9898(2) 0.0315(4) Uani 1 1 d . . . . . H012 H 0.462972 0.636993 1.052696 0.038 Uiso 1 1 calc R U . . . C013 C 0.35396(13) 0.64648(6) 0.3171(2) 0.0297(4) Uani 1 1 d . . . . . H013 H 0.343229 0.647744 0.214037 0.036 Uiso 1 1 calc R U . . . C014 C 0.26295(13) 0.64871(6) 0.9027(2) 0.0289(4) Uani 1 1 d . . . . . H014 H 0.245691 0.623783 0.861205 0.035 Uiso 1 1 calc R U . . . C015 C 0.80064(14) 0.59314(6) 0.3614(2) 0.0317(4) Uani 1 1 d . . . . . H015 H 0.812224 0.617966 0.408419 0.038 Uiso 1 1 calc R U . . . C016 C 0.70815(14) 0.45335(6) 0.5429(2) 0.0317(4) Uani 1 1 d . . . . . H016 H 0.700934 0.456097 0.439754 0.038 Uiso 1 1 calc R U . . . C017 C 0.91850(14) 0.39667(6) 0.5499(2) 0.0314(4) Uani 1 1 d . . . . . H017 H 0.924964 0.389160 0.649876 0.038 Uiso 1 1 calc R U . . . C018 C 0.72864(14) 0.44572(6) 0.8439(2) 0.0307(4) Uani 1 1 d . . . . . H018 H 0.735939 0.443141 0.947104 0.037 Uiso 1 1 calc R U . . . C019 C 0.62399(14) 0.58037(7) 0.9567(2) 0.0322(4) Uani 1 1 d . . . . . H019 H 0.672642 0.565799 0.998523 0.039 Uiso 1 1 calc R U . . . C01A C 1.25207(14) 0.32229(6) 0.1842(2) 0.0307(4) Uani 1 1 d . . . . . C01B C 1.15567(14) 0.45771(6) 0.2320(2) 0.0319(4) Uani 1 1 d . . . . . H01J H 1.195128 0.474825 0.185553 0.038 Uiso 1 1 calc R U . . . C01C C 0.29564(13) 0.66565(6) 0.4099(2) 0.0307(4) Uani 1 1 d . . . . . H01C H 0.245929 0.679596 0.368639 0.037 Uiso 1 1 calc R U . . . C01D C 0.86145(13) 0.57746(7) 0.2708(2) 0.0319(4) Uani 1 1 d . . . . . H01D H 0.913553 0.591853 0.253597 0.038 Uiso 1 1 calc R U . . . C01E C 1.13464(15) 0.32980(6) 0.0004(2) 0.0314(4) Uani 1 1 d . . . . . H01K H 1.075964 0.337500 -0.027038 0.038 Uiso 1 1 calc R U . . . C01F C 1.03749(14) 0.44962(6) 0.3942(2) 0.0322(4) Uani 1 1 d . . . . . H01M H 0.996308 0.461015 0.456026 0.039 Uiso 1 1 calc R U . . . C01G C 1.05294(14) 0.28169(6) 0.3099(2) 0.0325(4) Uani 1 1 d . . . . . H01N H 1.089475 0.270852 0.239236 0.039 Uiso 1 1 calc R U . . . C01H C 1.18783(15) 0.31520(6) -0.1062(2) 0.0337(5) Uani 1 1 d . . . . . C01I C 0.57042(14) 0.60277(7) 1.0479(2) 0.0332(5) Uani 1 1 d . . . . . H01I H 0.584418 0.603813 1.150208 0.040 Uiso 1 1 calc R U . . . C01J C 0.85107(14) 0.42013(6) 0.5090(2) 0.0314(4) Uani 1 1 d . . . . . H01O H 0.845915 0.428046 0.409331 0.038 Uiso 1 1 calc R U . . . C01K C 0.79308(14) 0.43166(6) 0.7565(2) 0.0322(4) Uani 1 1 d . . . . . H01P H 0.844452 0.419614 0.800563 0.039 Uiso 1 1 calc R U . . . C01L C 0.23270(15) 0.70489(7) 1.0531(2) 0.0372(5) Uani 1 1 d . . . . . H01L H 0.194978 0.718406 1.115656 0.045 Uiso 1 1 calc R U . . . C01M C 0.20708(14) 0.66851(7) 0.9930(2) 0.0322(4) Uani 1 1 d . . . . . C01N C 0.94364(14) 0.31224(7) 0.5156(2) 0.0341(5) Uani 1 1 d . . . . . H01Q H 0.905863 0.322150 0.586107 0.041 Uiso 1 1 calc R U . . . C01O C 0.94946(15) 0.27225(7) 0.4949(2) 0.0366(5) Uani 1 1 d . . . . . H01R H 0.917091 0.254629 0.552557 0.044 Uiso 1 1 calc R U . . . C01P C 1.09383(15) 0.47392(6) 0.3266(3) 0.0351(5) Uani 1 1 d . . . . . H01S H 1.091955 0.501872 0.342448 0.042 Uiso 1 1 calc R U . . . C01Q C 1.30609(15) 0.30878(7) 0.0766(3) 0.0363(5) Uani 1 1 d . . . . . H01T H 1.365471 0.301868 0.102313 0.044 Uiso 1 1 calc R U . . . C01R C 0.36848(14) 0.70200(7) 0.9312(2) 0.0348(5) Uani 1 1 d . . . . . C01S C 1.00337(15) 0.25675(7) 0.3881(3) 0.0365(5) Uani 1 1 d . . . . . H01V H 1.004992 0.228856 0.371032 0.044 Uiso 1 1 calc R U . . . C01T C 1.27392(15) 0.30538(7) -0.0669(2) 0.0371(5) Uani 1 1 d . . . . . H01W H 1.311403 0.296203 -0.139081 0.044 Uiso 1 1 calc R U . . . C01U C 0.31260(16) 0.72171(7) 1.0231(3) 0.0396(5) Uani 1 1 d . . . . . H01U H 0.329486 0.746645 1.064946 0.048 Uiso 1 1 calc R U . . . C01V C 1.36121(16) 0.30852(7) 0.3723(3) 0.0407(5) Uani 1 1 d . . . . . H01X H 1.407746 0.320752 0.317901 0.061 Uiso 1 1 calc R U . . . H01Y H 1.358921 0.279865 0.352018 0.061 Uiso 1 1 calc R U . . . H H 1.373645 0.312820 0.477215 0.061 Uiso 1 1 calc R U . . . C01W C 0.09311(16) 0.62069(8) 0.9435(3) 0.0436(6) Uani 1 1 d . . . . . H01A H 0.086917 0.629018 0.840973 0.065 Uiso 1 1 calc R U . . . H01B H 0.035440 0.613022 0.976587 0.065 Uiso 1 1 calc R U . . . H01E H 0.133277 0.597913 0.953101 0.065 Uiso 1 1 calc R U . . . C01X C 1.2001(2) 0.29609(8) -0.3538(3) 0.0490(6) Uani 1 1 d . . . . . H01Z H 1.164276 0.294025 -0.445861 0.074 Uiso 1 1 calc R U . . . HA H 1.221425 0.269585 -0.324244 0.074 Uiso 1 1 calc R U . . . HB H 1.250259 0.313702 -0.367265 0.074 Uiso 1 1 calc R U . . . C01Y C 0.4711(2) 0.75580(10) 0.9435(5) 0.0769(11) Uani 1 1 d . . . . . H01F H 0.428105 0.775195 0.903403 0.115 Uiso 1 1 calc R U . . . H01G H 0.529585 0.762558 0.911512 0.115 Uiso 1 1 calc R U . . . H01H H 0.472110 0.756384 1.050484 0.115 Uiso 1 1 calc R U . . . H001 H 0.938(3) 0.4770(15) 0.012(5) 0.14(2) Uiso 1 1 d D . . . . H002 H 0.478(3) 0.5003(16) 0.877(5) 0.15(2) Uiso 1 1 d D . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.0302(8) 0.0332(8) 0.0411(8) -0.0106(6) 0.0103(6) 0.0017(6) O002 0.0263(7) 0.0424(9) 0.0407(8) -0.0097(7) 0.0072(6) 0.0027(6) O003 0.0252(7) 0.0390(9) 0.0448(9) -0.0088(7) 0.0124(6) -0.0018(6) O004 0.0302(8) 0.0458(9) 0.0358(8) -0.0124(7) 0.0077(6) -0.0009(6) O005 0.0328(8) 0.0449(9) 0.0378(8) -0.0043(7) -0.0015(6) 0.0066(7) O006 0.0505(10) 0.0456(10) 0.0309(8) -0.0055(7) 0.0052(7) 0.0023(8) O007 0.0348(9) 0.0569(11) 0.0425(9) -0.0012(8) 0.0150(7) 0.0059(7) O008 0.0401(9) 0.0368(9) 0.0740(12) -0.0149(8) 0.0099(9) -0.0051(7) C009 0.0232(9) 0.0247(9) 0.0262(9) -0.0020(7) 0.0012(7) 0.0007(7) C00A 0.0237(9) 0.0238(9) 0.0282(9) -0.0011(7) 0.0056(7) 0.0002(7) C00B 0.0224(9) 0.0266(9) 0.0260(9) -0.0014(7) 0.0037(7) -0.0011(7) C00C 0.0251(9) 0.0257(10) 0.0289(10) -0.0016(7) -0.0002(7) 0.0003(7) C00D 0.0228(9) 0.0270(10) 0.0279(9) 0.0002(7) 0.0052(7) 0.0006(7) C00E 0.0245(9) 0.0277(10) 0.0288(10) -0.0018(7) 0.0049(7) 0.0011(7) C00F 0.0241(9) 0.0277(10) 0.0285(10) -0.0001(7) 0.0051(7) 0.0008(7) C00G 0.0231(9) 0.0303(10) 0.0226(9) -0.0017(7) 0.0009(7) 0.0046(7) C00H 0.0234(9) 0.0320(10) 0.0247(9) -0.0032(7) 0.0033(7) 0.0038(7) C00I 0.0256(10) 0.0309(10) 0.0289(10) -0.0053(8) 0.0037(8) 0.0014(8) C00J 0.0247(9) 0.0296(10) 0.0282(10) 0.0002(7) 0.0049(7) 0.0008(7) C00K 0.0238(9) 0.0254(9) 0.0276(9) -0.0026(7) 0.0049(7) 0.0007(7) C00L 0.0267(10) 0.0280(10) 0.0277(10) -0.0026(7) 0.0041(8) 0.0016(8) C00M 0.0229(9) 0.0299(10) 0.0282(10) -0.0006(8) 0.0047(7) 0.0010(7) C00N 0.0249(9) 0.0299(10) 0.0274(10) -0.0026(7) 0.0049(7) 0.0011(7) C00O 0.0252(9) 0.0269(10) 0.0285(9) -0.0036(7) 0.0018(7) 0.0005(7) C00P 0.0296(10) 0.0221(9) 0.0322(10) -0.0029(7) 0.0076(8) -0.0005(7) C00Q 0.0234(9) 0.0260(10) 0.0259(9) -0.0028(7) 0.0013(7) 0.0022(7) C00R 0.0238(9) 0.0295(10) 0.0317(10) -0.0002(8) 0.0060(8) 0.0029(7) C00S 0.0246(9) 0.0302(10) 0.0282(10) -0.0046(8) 0.0041(7) 0.0005(8) C00T 0.0245(9) 0.0320(10) 0.0289(10) 0.0021(8) 0.0064(8) 0.0037(8) C00U 0.0249(9) 0.0251(10) 0.0359(11) -0.0062(8) 0.0076(8) -0.0028(7) C00V 0.0239(10) 0.0289(10) 0.0356(11) -0.0070(8) 0.0042(8) -0.0024(7) C00W 0.0279(10) 0.0244(10) 0.0343(10) -0.0019(8) 0.0086(8) 0.0002(7) C00X 0.0261(9) 0.0284(10) 0.0265(9) -0.0026(7) 0.0032(7) 0.0039(7) C00Y 0.0247(9) 0.0299(10) 0.0280(9) 0.0005(8) 0.0026(7) -0.0006(7) C00Z 0.0269(10) 0.0298(10) 0.0368(11) 0.0005(8) 0.0064(8) 0.0025(8) C010 0.0271(10) 0.0300(10) 0.0244(9) -0.0031(7) 0.0023(7) 0.0041(8) C011 0.0273(10) 0.0324(10) 0.0249(9) -0.0016(8) 0.0020(7) 0.0066(8) C012 0.0285(10) 0.0408(12) 0.0258(10) -0.0012(8) 0.0067(8) 0.0039(8) C013 0.0280(10) 0.0356(11) 0.0256(9) 0.0005(8) 0.0019(8) 0.0005(8) C014 0.0297(10) 0.0337(11) 0.0235(9) 0.0000(8) 0.0024(8) 0.0044(8) C015 0.0287(10) 0.0309(11) 0.0359(11) -0.0085(8) 0.0042(8) 0.0006(8) C016 0.0343(11) 0.0306(11) 0.0310(10) 0.0019(8) 0.0091(8) 0.0017(8) C017 0.0293(10) 0.0339(11) 0.0317(10) -0.0025(8) 0.0079(8) -0.0011(8) C018 0.0291(10) 0.0318(11) 0.0316(10) -0.0058(8) 0.0050(8) 0.0005(8) C019 0.0256(10) 0.0399(12) 0.0312(10) 0.0068(8) 0.0036(8) 0.0061(8) C01A 0.0312(10) 0.0272(10) 0.0339(10) -0.0030(8) 0.0037(8) 0.0003(8) C01B 0.0311(11) 0.0265(10) 0.0387(11) 0.0009(8) 0.0070(8) -0.0036(8) C01C 0.0237(9) 0.0352(11) 0.0335(10) 0.0048(8) 0.0032(8) 0.0050(8) C01D 0.0245(10) 0.0353(11) 0.0362(11) -0.0085(8) 0.0052(8) -0.0026(8) C01E 0.0349(11) 0.0269(10) 0.0327(10) -0.0022(8) 0.0047(8) 0.0010(8) C01F 0.0301(10) 0.0280(10) 0.0392(11) -0.0079(8) 0.0077(9) 0.0020(8) C01G 0.0345(11) 0.0265(10) 0.0366(11) -0.0016(8) 0.0029(9) 0.0012(8) C01H 0.0432(12) 0.0281(10) 0.0306(10) -0.0034(8) 0.0083(9) -0.0016(9) C01I 0.0303(10) 0.0459(13) 0.0236(9) 0.0035(8) 0.0029(8) 0.0045(9) C01J 0.0317(11) 0.0316(11) 0.0316(10) -0.0037(8) 0.0076(8) 0.0001(8) C01K 0.0293(10) 0.0328(11) 0.0349(11) -0.0055(8) 0.0056(8) 0.0044(8) C01L 0.0396(12) 0.0420(13) 0.0305(11) -0.0023(9) 0.0054(9) 0.0191(10) C01M 0.0285(10) 0.0443(12) 0.0241(9) 0.0015(8) 0.0037(8) 0.0079(9) C01N 0.0307(11) 0.0374(12) 0.0347(11) 0.0017(9) 0.0071(8) -0.0035(9) C01O 0.0368(12) 0.0342(12) 0.0386(12) 0.0063(9) 0.0014(9) -0.0080(9) C01P 0.0354(11) 0.0244(10) 0.0460(12) -0.0051(9) 0.0072(9) -0.0004(8) C01Q 0.0291(11) 0.0320(11) 0.0485(13) -0.0045(9) 0.0087(9) 0.0029(8) C01R 0.0317(11) 0.0350(12) 0.0379(11) -0.0058(9) 0.0040(9) 0.0029(9) C01S 0.0390(12) 0.0263(11) 0.0441(12) 0.0019(9) 0.0007(9) -0.0020(9) C01T 0.0403(12) 0.0349(11) 0.0372(11) -0.0051(9) 0.0128(9) -0.0006(9) C01U 0.0470(13) 0.0326(12) 0.0393(12) -0.0098(9) 0.0023(10) 0.0070(10) C01V 0.0372(12) 0.0407(13) 0.0435(13) 0.0002(10) -0.0037(10) 0.0045(10) C01W 0.0325(12) 0.0529(15) 0.0459(13) 0.0075(11) 0.0061(10) -0.0002(10) C01X 0.0649(17) 0.0497(15) 0.0332(12) -0.0063(10) 0.0103(11) 0.0063(13) C01Y 0.0479(17) 0.0496(18) 0.134(3) -0.0331(19) 0.0123(19) -0.0095(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C00I O001 H001 118(4) . . ? C00V O002 H002 111(4) . . ? C01A O005 C01V 116.12(17) . . ? C01H O006 C01X 116.71(19) . . ? C01M O007 C01W 116.56(17) . . ? C01R O008 C01Y 118.0(2) . . ? C00J C009 C00O 118.63(17) . . ? C00Q C009 C00J 121.02(18) . . ? C00Q C009 C00O 120.34(18) . . ? C00E C00A C00B 119.41(17) . . ? C00E C00A C00R 122.20(17) . . ? C00R C00A C00B 118.37(17) . . ? C00K C00B C00A 120.46(17) . . ? C00K C00B C00N 121.58(17) . . ? C00N C00B C00A 117.94(17) . . ? C00Q C00C C00Y 119.90(18) . . ? C00Q C00C C01G 121.73(18) . . ? C01G C00C C00Y 118.37(19) . . ? C00K C00D C00F 119.60(17) . . ? C00K C00D C00T 122.54(18) . . ? C00T C00D C00F 117.85(17) . . ? C00A C00E C00F 120.41(18) . . ? C00A C00E C011 119.48(17) . . ? C00F C00E C011 120.11(17) . . ? C00E C00F C00D 120.15(18) . . ? C00E C00F C012 121.50(18) . . ? C012 C00F C00D 118.35(18) . . ? C00M C00G C010 123.15(18) . . ? C00M C00G C015 118.51(18) . . ? C015 C00G C010 118.34(18) . . ? C00L C00H C00I 120.45(18) . . ? C01D C00H C00I 119.73(18) . . ? C01D C00H C00L 119.81(18) . . ? O001 C00I C00H 117.43(18) . . ? O003 C00I O001 123.78(18) . . ? O003 C00I C00H 118.79(18) . . ? C009 C00J H00J 119.3 . . ? C01B C00J C009 121.44(19) . . ? C01B C00J H00J 119.3 . . ? C00B C00K C00D 119.90(17) . . ? C00B C00K C00X 118.71(17) . . ? C00D C00K C00X 121.38(17) . . ? C00H C00L H00L 120.1 . . ? C00M C00L C00H 119.86(19) . . ? C00M C00L H00L 120.1 . . ? C00G C00M H00M 119.5 . . ? C00L C00M C00G 120.96(18) . . ? C00L C00M H00M 119.5 . . ? C00B C00N H00N 119.2 . . ? C013 C00N C00B 121.66(18) . . ? C013 C00N H00N 119.2 . . ? C00S C00O C009 119.57(18) . . ? C00S C00O C01F 122.62(18) . . ? C01F C00O C009 117.74(18) . . ? C01A C00P C00Q 121.98(18) . . ? C01E C00P C00Q 119.50(18) . . ? C01E C00P C01A 118.50(18) . . ? C009 C00Q C00C 119.96(18) . . ? C009 C00Q C00P 119.84(17) . . ? C00C C00Q C00P 120.16(17) . . ? C00A C00R H00R 119.4 . . ? C01C C00R C00A 121.27(18) . . ? C01C C00R H00R 119.4 . . ? C00O C00S C00Y 119.85(18) . . ? C00O C00S C017 121.64(18) . . ? C00Y C00S C017 118.50(18) . . ? C00D C00T H00T 119.2 . . ? C019 C00T C00D 121.65(19) . . ? C019 C00T H00T 119.2 . . ? C00Z C00U C00V 120.92(19) . . ? C00Z C00U C018 119.63(18) . . ? C018 C00U C00V 119.45(19) . . ? O002 C00V C00U 117.49(18) . . ? O004 C00V O002 123.88(19) . . ? O004 C00V C00U 118.63(18) . . ? C016 C00W C01J 119.58(19) . . ? C01K C00W C016 118.26(18) . . ? C01K C00W C01J 122.16(19) . . ? C00K C00X H00X 118.3 . . ? C010 C00X C00K 123.40(18) . . ? C010 C00X H00X 118.3 . . ? C00S C00Y C00C 120.14(18) . . ? C00S C00Y C01N 121.94(19) . . ? C01N C00Y C00C 117.92(19) . . ? C00U C00Z H00Z 120.1 . . ? C016 C00Z C00U 119.81(19) . . ? C016 C00Z H00Z 120.1 . . ? C00G C010 H010 116.9 . . ? C00X C010 C00G 126.10(18) . . ? C00X C010 H010 116.9 . . ? C014 C011 C00E 119.81(18) . . ? C01R C011 C00E 120.69(19) . . ? C01R C011 C014 119.49(19) . . ? C00F C012 H012 119.3 . . ? C01I C012 C00F 121.38(19) . . ? C01I C012 H012 119.3 . . ? C00N C013 H013 119.9 . . ? C00N C013 C01C 120.22(19) . . ? C01C C013 H013 119.9 . . ? C011 C014 H014 119.7 . . ? C01M C014 C011 120.7(2) . . ? C01M C014 H014 119.7 . . ? C00G C015 H015 119.5 . . ? C01D C015 C00G 120.93(19) . . ? C01D C015 H015 119.5 . . ? C00W C016 H016 119.4 . . ? C00Z C016 C00W 121.1(2) . . ? C00Z C016 H016 119.4 . . ? C00S C017 H017 117.7 . . ? C01J C017 C00S 124.7(2) . . ? C01J C017 H017 117.7 . . ? C00U C018 H018 119.9 . . ? C01K C018 C00U 120.1(2) . . ? C01K C018 H018 119.9 . . ? C00T C019 H019 119.8 . . ? C00T C019 C01I 120.39(19) . . ? C01I C019 H019 119.8 . . ? O005 C01A C00P 116.21(18) . . ? O005 C01A C01Q 124.12(19) . . ? C01Q C01A C00P 119.7(2) . . ? C00J C01B H01J 120.0 . . ? C00J C01B C01P 120.08(19) . . ? C01P C01B H01J 120.0 . . ? C00R C01C C013 120.51(19) . . ? C00R C01C H01C 119.7 . . ? C013 C01C H01C 119.7 . . ? C00H C01D H01D 120.1 . . ? C015 C01D C00H 119.84(19) . . ? C015 C01D H01D 120.1 . . ? C00P C01E H01K 119.1 . . ? C00P C01E C01H 121.8(2) . . ? C01H C01E H01K 119.1 . . ? C00O C01F H01M 119.1 . . ? C01P C01F C00O 121.75(19) . . ? C01P C01F H01M 119.1 . . ? C00C C01G H01N 119.3 . . ? C01S C01G C00C 121.4(2) . . ? C01S C01G H01N 119.3 . . ? O006 C01H C01E 115.5(2) . . ? O006 C01H C01T 125.7(2) . . ? C01T C01H C01E 118.9(2) . . ? C012 C01I C019 120.29(19) . . ? C012 C01I H01I 119.9 . . ? C019 C01I H01I 119.9 . . ? C00W C01J H01O 117.1 . . ? C017 C01J C00W 125.7(2) . . ? C017 C01J H01O 117.1 . . ? C00W C01K H01P 119.5 . . ? C018 C01K C00W 121.0(2) . . ? C018 C01K H01P 119.5 . . ? C01M C01L H01L 119.6 . . ? C01U C01L H01L 119.6 . . ? C01U C01L C01M 120.7(2) . . ? O007 C01M C014 122.9(2) . . ? O007 C01M C01L 117.73(19) . . ? C01L C01M C014 119.3(2) . . ? C00Y C01N H01Q 119.2 . . ? C01O C01N C00Y 121.6(2) . . ? C01O C01N H01Q 119.2 . . ? C01N C01O H01R 119.8 . . ? C01N C01O C01S 120.4(2) . . ? C01S C01O H01R 119.8 . . ? C01B C01P H01S 119.8 . . ? C01F C01P C01B 120.34(19) . . ? C01F C01P H01S 119.8 . . ? C01A C01Q H01T 119.7 . . ? C01T C01Q C01A 120.5(2) . . ? C01T C01Q H01T 119.7 . . ? O008 C01R C011 116.84(19) . . ? O008 C01R C01U 123.4(2) . . ? C011 C01R C01U 119.8(2) . . ? C01G C01S C01O 120.1(2) . . ? C01G C01S H01V 119.9 . . ? C01O C01S H01V 119.9 . . ? C01H C01T C01Q 120.6(2) . . ? C01H C01T H01W 119.7 . . ? C01Q C01T H01W 119.7 . . ? C01L C01U C01R 120.0(2) . . ? C01L C01U H01U 120.0 . . ? C01R C01U H01U 120.0 . . ? O005 C01V H01X 109.5 . . ? O005 C01V H01Y 109.5 . . ? O005 C01V H 109.5 . . ? H01X C01V H01Y 109.5 . . ? H01X C01V H 109.5 . . ? H01Y C01V H 109.5 . . ? O007 C01W H01A 109.5 . . ? O007 C01W H01B 109.5 . . ? O007 C01W H01E 109.5 . . ? H01A C01W H01B 109.5 . . ? H01A C01W H01E 109.5 . . ? H01B C01W H01E 109.5 . . ? O006 C01X H01Z 109.5 . . ? O006 C01X HA 109.5 . . ? O006 C01X HB 109.5 . . ? H01Z C01X HA 109.5 . . ? H01Z C01X HB 109.5 . . ? HA C01X HB 109.5 . . ? O008 C01Y H01F 109.5 . . ? O008 C01Y H01G 109.5 . . ? O008 C01Y H01H 109.5 . . ? H01F C01Y H01G 109.5 . . ? H01F C01Y H01H 109.5 . . ? H01G C01Y H01H 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O001 C00I 1.279(3) . ? O001 H001 0.87(2) . ? O002 C00V 1.280(3) . ? O002 H002 0.86(2) . ? O003 C00I 1.268(2) . ? O004 C00V 1.262(3) . ? O005 C01A 1.365(3) . ? O005 C01V 1.428(3) . ? O006 C01H 1.371(3) . ? O006 C01X 1.421(3) . ? O007 C01M 1.382(3) . ? O007 C01W 1.426(3) . ? O008 C01R 1.370(3) . ? O008 C01Y 1.414(3) . ? C009 C00J 1.431(3) . ? C009 C00O 1.440(3) . ? C009 C00Q 1.406(3) . ? C00A C00B 1.438(3) . ? C00A C00E 1.407(3) . ? C00A C00R 1.432(3) . ? C00B C00K 1.410(3) . ? C00B C00N 1.431(3) . ? C00C C00Q 1.408(3) . ? C00C C00Y 1.434(3) . ? C00C C01G 1.430(3) . ? C00D C00F 1.440(3) . ? C00D C00K 1.411(3) . ? C00D C00T 1.431(3) . ? C00E C00F 1.407(3) . ? C00E C011 1.497(3) . ? C00F C012 1.433(3) . ? C00G C00M 1.396(3) . ? C00G C010 1.467(3) . ? C00G C015 1.402(3) . ? C00H C00I 1.480(3) . ? C00H C00L 1.398(3) . ? C00H C01D 1.394(3) . ? C00J H00J 0.9500 . ? C00J C01B 1.359(3) . ? C00K C00X 1.483(3) . ? C00L H00L 0.9500 . ? C00L C00M 1.383(3) . ? C00M H00M 0.9500 . ? C00N H00N 0.9500 . ? C00N C013 1.355(3) . ? C00O C00S 1.411(3) . ? C00O C01F 1.431(3) . ? C00P C00Q 1.499(3) . ? C00P C01A 1.402(3) . ? C00P C01E 1.389(3) . ? C00R H00R 0.9500 . ? C00R C01C 1.355(3) . ? C00S C00Y 1.413(3) . ? C00S C017 1.485(3) . ? C00T H00T 0.9500 . ? C00T C019 1.357(3) . ? C00U C00V 1.486(3) . ? C00U C00Z 1.392(3) . ? C00U C018 1.393(3) . ? C00W C016 1.397(3) . ? C00W C01J 1.474(3) . ? C00W C01K 1.395(3) . ? C00X H00X 0.9500 . ? C00X C010 1.338(3) . ? C00Y C01N 1.427(3) . ? C00Z H00Z 0.9500 . ? C00Z C016 1.389(3) . ? C010 H010 0.9500 . ? C011 C014 1.396(3) . ? C011 C01R 1.392(3) . ? C012 H012 0.9500 . ? C012 C01I 1.357(3) . ? C013 H013 0.9500 . ? C013 C01C 1.420(3) . ? C014 H014 0.9500 . ? C014 C01M 1.390(3) . ? C015 H015 0.9500 . ? C015 C01D 1.383(3) . ? C016 H016 0.9500 . ? C017 H017 0.9500 . ? C017 C01J 1.331(3) . ? C018 H018 0.9500 . ? C018 C01K 1.385(3) . ? C019 H019 0.9500 . ? C019 C01I 1.418(3) . ? C01A C01Q 1.396(3) . ? C01B H01J 0.9500 . ? C01B C01P 1.424(3) . ? C01C H01C 0.9500 . ? C01D H01D 0.9500 . ? C01E H01K 0.9500 . ? C01E C01H 1.394(3) . ? C01F H01M 0.9500 . ? C01F C01P 1.359(3) . ? C01G H01N 0.9500 . ? C01G C01S 1.359(3) . ? C01H C01T 1.380(3) . ? C01I H01I 0.9500 . ? C01J H01O 0.9500 . ? C01K H01P 0.9500 . ? C01L H01L 0.9500 . ? C01L C01M 1.386(3) . ? C01L C01U 1.384(4) . ? C01N H01Q 0.9500 . ? C01N C01O 1.359(3) . ? C01O H01R 0.9500 . ? C01O C01S 1.413(3) . ? C01P H01S 0.9500 . ? C01Q H01T 0.9500 . ? C01Q C01T 1.382(3) . ? C01R C01U 1.398(3) . ? C01S H01V 0.9500 . ? C01T H01W 0.9500 . ? C01U H01U 0.9500 . ? C01V H01X 0.9800 . ? C01V H01Y 0.9800 . ? C01V H 0.9800 . ? C01W H01A 0.9800 . ? C01W H01B 0.9800 . ? C01W H01E 0.9800 . ? C01X H01Z 0.9800 . ? C01X HA 0.9800 . ? C01X HB 0.9800 . ? C01Y H01F 0.9800 . ? C01Y H01G 0.9800 . ? C01Y H01H 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O005 C01A C01Q C01T 179.5(2) . . . . ? O006 C01H C01T C01Q -178.0(2) . . . . ? O008 C01R C01U C01L 178.2(2) . . . . ? C009 C00J C01B C01P -1.0(3) . . . . ? C009 C00O C00S C00Y 1.4(3) . . . . ? C009 C00O C00S C017 -179.31(18) . . . . ? C009 C00O C01F C01P -1.0(3) . . . . ? C00A C00B C00K C00D -0.7(3) . . . . ? C00A C00B C00K C00X -179.22(17) . . . . ? C00A C00B C00N C013 -2.1(3) . . . . ? C00A C00E C00F C00D -1.2(3) . . . . ? C00A C00E C00F C012 178.58(19) . . . . ? C00A C00E C011 C014 76.4(3) . . . . ? C00A C00E C011 C01R -102.3(2) . . . . ? C00A C00R C01C C013 0.1(3) . . . . ? C00B C00A C00E C00F -1.2(3) . . . . ? C00B C00A C00E C011 178.51(18) . . . . ? C00B C00A C00R C01C -1.4(3) . . . . ? C00B C00K C00X C010 120.4(2) . . . . ? C00B C00N C013 C01C 0.8(3) . . . . ? C00C C00Y C01N C01O -1.8(3) . . . . ? C00C C01G C01S C01O -0.8(3) . . . . ? C00D C00F C012 C01I -0.6(3) . . . . ? C00D C00K C00X C010 -58.1(3) . . . . ? C00D C00T C019 C01I 0.3(3) . . . . ? C00E C00A C00B C00K 2.1(3) . . . . ? C00E C00A C00B C00N -176.07(18) . . . . ? C00E C00A C00R C01C 177.0(2) . . . . ? C00E C00F C012 C01I 179.6(2) . . . . ? C00E C011 C014 C01M 179.93(18) . . . . ? C00E C011 C01R O008 1.2(3) . . . . ? C00E C011 C01R C01U -179.3(2) . . . . ? C00F C00D C00K C00B -1.7(3) . . . . ? C00F C00D C00K C00X 176.84(18) . . . . ? C00F C00D C00T C019 -2.7(3) . . . . ? C00F C00E C011 C014 -103.9(2) . . . . ? C00F C00E C011 C01R 77.4(3) . . . . ? C00F C012 C01I C019 -1.8(3) . . . . ? C00G C015 C01D C00H -1.9(3) . . . . ? C00H C00L C00M C00G -1.4(3) . . . . ? C00I C00H C00L C00M 177.43(18) . . . . ? C00I C00H C01D C015 -175.8(2) . . . . ? C00J C009 C00O C00S -176.76(18) . . . . ? C00J C009 C00O C01F 0.4(3) . . . . ? C00J C009 C00Q C00C 176.52(18) . . . . ? C00J C009 C00Q C00P -5.7(3) . . . . ? C00J C01B C01P C01F 0.4(3) . . . . ? C00K C00B C00N C013 179.72(19) . . . . ? C00K C00D C00F C00E 2.6(3) . . . . ? C00K C00D C00F C012 -177.13(19) . . . . ? C00K C00D C00T C019 177.3(2) . . . . ? C00K C00X C010 C00G -178.31(19) . . . . ? C00L C00H C00I O001 -2.3(3) . . . . ? C00L C00H C00I O003 177.69(19) . . . . ? C00L C00H C01D C015 3.1(3) . . . . ? C00M C00G C010 C00X -19.8(3) . . . . ? C00M C00G C015 C01D -0.9(3) . . . . ? C00N C00B C00K C00D 177.46(18) . . . . ? C00N C00B C00K C00X -1.1(3) . . . . ? C00N C013 C01C C00R 0.3(3) . . . . ? C00O C009 C00J C01B 0.6(3) . . . . ? C00O C009 C00Q C00C -2.7(3) . . . . ? C00O C009 C00Q C00P 175.05(17) . . . . ? C00O C00S C00Y C00C -5.0(3) . . . . ? C00O C00S C00Y C01N 175.87(19) . . . . ? C00O C00S C017 C01J 61.0(3) . . . . ? C00O C01F C01P C01B 0.6(3) . . . . ? C00P C01A C01Q C01T -1.5(3) . . . . ? C00P C01E C01H O006 177.74(19) . . . . ? C00P C01E C01H C01T -2.3(3) . . . . ? C00Q C009 C00J C01B -178.66(19) . . . . ? C00Q C009 C00O C00S 2.5(3) . . . . ? C00Q C009 C00O C01F 179.66(18) . . . . ? C00Q C00C C00Y C00S 4.8(3) . . . . ? C00Q C00C C00Y C01N -176.04(18) . . . . ? C00Q C00C C01G C01S 177.3(2) . . . . ? C00Q C00P C01A O005 1.6(3) . . . . ? C00Q C00P C01A C01Q -177.39(19) . . . . ? C00Q C00P C01E C01H 179.32(19) . . . . ? C00R C00A C00B C00K -179.43(18) . . . . ? C00R C00A C00B C00N 2.4(3) . . . . ? C00R C00A C00E C00F -179.57(19) . . . . ? C00R C00A C00E C011 0.1(3) . . . . ? C00S C00O C01F C01P 176.1(2) . . . . ? C00S C00Y C01N C01O 177.3(2) . . . . ? C00S C017 C01J C00W 178.46(19) . . . . ? C00T C00D C00F C00E -177.48(19) . . . . ? C00T C00D C00F C012 2.8(3) . . . . ? C00T C00D C00K C00B 178.42(19) . . . . ? C00T C00D C00K C00X -3.1(3) . . . . ? C00T C019 C01I C012 2.0(3) . . . . ? C00U C00Z C016 C00W -0.4(3) . . . . ? C00U C018 C01K C00W -0.3(3) . . . . ? C00V C00U C00Z C016 -179.29(19) . . . . ? C00V C00U C018 C01K 179.63(19) . . . . ? C00Y C00C C00Q C009 -0.9(3) . . . . ? C00Y C00C C00Q C00P -178.67(18) . . . . ? C00Y C00C C01G C01S -2.7(3) . . . . ? C00Y C00S C017 C01J -119.7(2) . . . . ? C00Y C01N C01O C01S -1.6(3) . . . . ? C00Z C00U C00V O002 8.0(3) . . . . ? C00Z C00U C00V O004 -171.64(19) . . . . ? C00Z C00U C018 C01K -0.8(3) . . . . ? C010 C00G C00M C00L -177.30(18) . . . . ? C010 C00G C015 C01D 178.99(19) . . . . ? C011 C00E C00F C00D 179.15(18) . . . . ? C011 C00E C00F C012 -1.1(3) . . . . ? C011 C014 C01M O007 -177.47(19) . . . . ? C011 C014 C01M C01L 0.0(3) . . . . ? C011 C01R C01U C01L -1.3(3) . . . . ? C014 C011 C01R O008 -177.6(2) . . . . ? C014 C011 C01R C01U 1.9(3) . . . . ? C015 C00G C00M C00L 2.6(3) . . . . ? C015 C00G C010 C00X 160.4(2) . . . . ? C016 C00W C01J C017 -168.6(2) . . . . ? C016 C00W C01K C018 1.0(3) . . . . ? C017 C00S C00Y C00C 175.66(18) . . . . ? C017 C00S C00Y C01N -3.4(3) . . . . ? C018 C00U C00V O002 -172.36(19) . . . . ? C018 C00U C00V O004 8.0(3) . . . . ? C018 C00U C00Z C016 1.1(3) . . . . ? C01A C00P C00Q C009 91.1(2) . . . . ? C01A C00P C00Q C00C -91.2(2) . . . . ? C01A C00P C01E C01H 0.6(3) . . . . ? C01A C01Q C01T C01H -0.1(3) . . . . ? C01D C00H C00I O001 176.54(19) . . . . ? C01D C00H C00I O003 -3.5(3) . . . . ? C01D C00H C00L C00M -1.4(3) . . . . ? C01E C00P C00Q C009 -87.5(2) . . . . ? C01E C00P C00Q C00C 90.2(2) . . . . ? C01E C00P C01A O005 -179.70(18) . . . . ? C01E C00P C01A C01Q 1.3(3) . . . . ? C01E C01H C01T C01Q 2.0(3) . . . . ? C01F C00O C00S C00Y -175.62(19) . . . . ? C01F C00O C00S C017 3.7(3) . . . . ? C01G C00C C00Q C009 179.14(19) . . . . ? C01G C00C C00Q C00P 1.4(3) . . . . ? C01G C00C C00Y C00S -175.23(19) . . . . ? C01G C00C C00Y C01N 3.9(3) . . . . ? C01J C00W C016 C00Z -179.83(19) . . . . ? C01J C00W C01K C018 -179.8(2) . . . . ? C01K C00W C016 C00Z -0.7(3) . . . . ? C01K C00W C01J C017 12.3(3) . . . . ? C01M C01L C01U C01R 0.0(3) . . . . ? C01N C01O C01S C01G 3.0(3) . . . . ? C01R C011 C014 C01M -1.3(3) . . . . ? C01U C01L C01M O007 178.2(2) . . . . ? C01U C01L C01M C014 0.6(3) . . . . ? C01V O005 C01A C00P 169.35(19) . . . . ? C01V O005 C01A C01Q -11.7(3) . . . . ? C01W O007 C01M C014 -16.5(3) . . . . ? C01W O007 C01M C01L 166.0(2) . . . . ? C01X O006 C01H C01E -178.3(2) . . . . ? C01X O006 C01H C01T 1.7(3) . . . . ? C01Y O008 C01R C011 176.0(3) . . . . ? C01Y O008 C01R C01U -3.5(4) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.444 0.183 0.269 21.3 0.4 ? 2 0.444 0.317 0.769 21.3 0.4 ? 3 0.556 0.683 0.231 21.3 0.4 ? 4 0.556 0.817 0.731 21.3 0.4 ?