Crystallography Open Database

Information card for entry 7705448

Preview

Coordinates	7705448.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C5 H8 Co N2 O7 V2
Calculated formula	C5 H8 Co N2 O7 V2
Title of publication	Inorganic-organic hybrid polyoxovanadates based on [V<sub>4</sub>O<sub>12</sub>]<sup>4-</sup> or [VO<sub>3</sub>]<sub>2</sub><sup>2-</sup> clusters: controllable synthesis, crystal structures and catalytic properties in selective oxidation of sulfides.
Authors of publication	Li, Jikun; Wei, Chuanping; Guo, Daigaojie; Wang, Congcong; Han, Yinfeng; He, Guofang; Zhang, Jianping; Huang, Xianqiang; Hu, Changwen
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	40
Pages of publication	14148 - 14157
a	12.057 ± 0.003 Å
b	5.8528 ± 0.0014 Å
c	15.556 ± 0.004 Å
α	90°
β	98.297 ± 0.004°
γ	90°
Cell volume	1086.3 ± 0.5 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0231
Residual factor for significantly intense reflections	0.02
Weighted residual factors for significantly intense reflections	0.0568
Weighted residual factors for all reflections included in the refinement	0.0586
Goodness-of-fit parameter for all reflections included in the refinement	1.306
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
258848 (current)	2020-11-06	cif/ Updating files of 7705447, 7705448, 7705449 Original log message: Adding full bibliography for 7705447--7705449.cif.	7705448.cif
256488	2020-09-17	cif/ Adding structures of 7705447, 7705448, 7705449 via cif-deposit CGI script.	7705448.cif