Crystallography Open Database

Information card for entry 7157039

Preview

Coordinates	7157039.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H30 O7
Calculated formula	C31 H30 O7
Title of publication	Exploitation of donor-acceptor cyclopropanes and N-sulfonyl 1-azadienes towards the synthesis of spiro-cyclopentane benzofuran derivatives.
Authors of publication	Verma, Kamal; Taily, Irshad Maajid; Banerjee, Prabal
Journal of publication	Organic & biomolecular chemistry
Year of publication	2019
Journal volume	17
Journal issue	35
Pages of publication	8149 - 8152
a	9.539 ± 0.005 Å
b	9.87 ± 0.005 Å
c	15.022 ± 0.005 Å
α	95.665 ± 0.005°
β	97.294 ± 0.005°
γ	99.247 ± 0.005°
Cell volume	1374.4 ± 1.1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1477
Residual factor for significantly intense reflections	0.0806
Weighted residual factors for significantly intense reflections	0.197
Weighted residual factors for all reflections included in the refinement	0.232
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
225275 (current)	2019-11-08	cif/ Updating files of 7157038, 7157039 Original log message: Adding full bibliography for 7157038--7157039.cif.	7157039.cif
217572	2019-08-17	cif/ Adding structures of 7157038, 7157039 via cif-deposit CGI script.	7157039.cif